Document RjwENyNg0MD7xREdBj3RpermB

INDUSTRIES APR 1 Qtrie, ,, 1S62 QfOcc PPG INDUSTRIES. INC. INDUSTRIAL CHEMICAL DIVISION P. 0. BOX 1000 April 13, 1982 LAKE CHARLES. LA. 70602 Mr. Richard Goudeau Department of Natural Resources Office of Environmental Affairs Water Pollution Control Division P.0. Box 3047 Lake Charles, LA 70602 Dear Mr. Goudeau: Re: PPG's State Inspection of 4/6-7/82 NPDES Permit No. LA0000761 Listed below, per your request, are the recorded flows of the outfalls sampled during the State Inspection of April 6-7, 1982. Also, you will find attached a copy of the strip chart indicating pH at Outfall 001 for the same period. Outfall 010 Outfal1 Oil Outfall 111 Outfall 017 Outfall 018 Outfal1 118 Outfal1 019 497 gpm 205 490 356 3824 203 56 Should you have any further questions, contact me at 491-4420 or Jim Wyche at 491-4830. Very truly yours. PATRICE M. McFARLAIN Environmental Control Assistant PMM:ap Attachment cc: W. J. Peard/J. E. Wyche/File #306.2.05 3ai9 0^ sample .option r r (S' ^ forts___tewnvyj CtTT m mduitit maim and location OBSERVATIONS REMARKS FOR PERIOO BE6INNIN6Ar. ON ll .!Ja OUTFALL NO.:__ _g/_g_________ ___ SAMPLE NO.: SHIFT SUPERVISOR: SIGN TOUR ENARKS!'.! YSLPUO Stvt>w> .^(WiVi___ UtuvW OivArO --____r*AaJLh.\Q fr<uuwJ) 't&Jfi*?________________ __ (9^krA r\>&& X U>Q ft 3-yx^.-~ CH__.?>, S~ ^ i pop ~ ~C2________i-.x/opd-- ^___A7 - enr- ScoAsl X\vm=> 32TTO JS-fTZyp v.wJtJ. o&c ^ X JOGft f) io o o >___*Lx___ /op t=______ 1*0cH> LfaOO /rfi&~ J?*Sy/e0* ~ ye*# AAt_ o * - n r a VM-T2 SL 023280 DATE: <* STaUbUmFliHA 2OUTFALL NO Ji l --- 7.7y 'mCNnO'i'OunwMPTUiNaO SAMPLE NO.: A. *.0090 7<ft CREW A CREW a CREW C ^/A's/g, klKVj fZ? AkmiHo#/*. &t// SjfX&Oj foiX-k /4C.W/*i^tT 4///^ *r4.A'Mf( f r -------------------------------------------------------A L / 0 U 0 T S----------------------------- -- -------------------------------------------: FIELD DATA PRESERVATIVES t 3 4 5 6 7 8 9 10 If 12 TIME (hours) f l OW TEMPERATURE____ f>H DISSOLVED 0a mg/|. OOOQQOO OQQfrQOQ QQQQQQQ OOOOOOO 0000000 QMS' /tt? tM? *1080 I(0QJ ioad oo i*a_ is>39 0&o9 44)00 t/COO 3&o 00 -- co -- Na a RESIDUAL CHLORINE SAMPLES aon -SOi mS^COLOH-TUHRttlTY SULFATE - FLUORIDE-CHLORIDE OIL ond GREASE - Ono (rob tomnle otr iMI COD TOO METALS COLIFORM - One grob tomple ptr shift PHENOL SULFIDE CYANIOE NUTRIENTS-nitrogen and phosphorus PESTICIOES BIO ASSAY-Initial tost tamplg , BIOASSAY-Full sits sompM MASS SPEC. SAMPLE SUPERVISOR -imtlol soch block 0000000 r\ r\ r\ r\ r\ r\ r\ U U UUUUU SAMPLE ON WET ICE End. concentrated HpSOo par titor ond ploco on ico 2ml. coocontrotod H*S0U par liter * 2 ml. concontrotsd par litsr H'C.L 5ml. concentrated HNO> par litsr Rsturn to lob. In proporod containor on too 1.0 prom. CuSOs par litsr HaPOe to pH 40 B ico 2 ml ono molar ZnAc par tttsr NoOH to pH 10 (opproi. 2ml. par Dior) 40 mg. HgClj par litsr B Okies on les Rsturn to lob. In prsporod comtolnar on ico Crow A rsturn to lob. on collection Crow C coUset lost hour ond rsturn to lob. Rsturn to isb. in contalnsr provided 000GG05 r\r\r\ r\r\ r\ r\/-\ r\ r\r\ r\ Ann r\r\ r\ r\r\ r\ r^r\r\ AAA AAA r\r\ r> UUU UUU UUU UUU UUU UUU UUU UUU UUU UUU UUU UUU lZnt4) [20*P I3Sm iXd //low: >v*l i% A I35~{ 1 MiV J-^ Ms fHti , )PK, M [H-WIDITI SAMPLE LOCATION^ tr& Z#6. CITY OT MDulTRt MAMC MO LOCATION OBSERVATIONS ft REMARKS FOR PERIOO BEGIN NINOhr*. ON 4*i/` OUTFALL NO.: -JU0._______ SAMPLE NO. +0*0<rt/ SHIFT SUPERVISOR: SION YOUR REMARKS!'! Sinur duixariX^ Sorrrvy v cX&jdr % * 0*3 t /-S- Af.S , #.s J , ,3 ^ se: /6*C'4- /S' - " * ', k i \ SL sample location- T T LT *X/g/ LfrKL ,/ ClTr OR INDUSTRY N*r MHO -OCrfriON PATE: y4> Kj / 6 / 1 g ' STMT SAMPLING V /fJ*. END `tAMPUM* OUTFALL NO.: CIO__________ SAMPLE NO.|_ ^ ftA, its SAMPLING CREW SUPERVISORS SIGNATURES. CREW A CREW B rtf )**l*/$jt/*4f/t'// CREW C ' //+i* s J>/d Ja-v*df ( FIELD DATA PRESERVATIVES ------------------------------------------------------ A L 1 0 U 0 r S-------------------------------------------------------------------------- 9/ e 3 4 3 6 7 8 to // 12 * TIME (hour*) FLO W _ *% , |i temperature #____ 't DISSOLVED Ot mg/i. 0000000 0}[}f OOBQGGQ tb.S fiA 0000000 0000000 0Q-6-Q0QQ /5?jO Us* SIIS ooos o3t>\ Dfo&J /1-5 to 15 11 r?y r \ 1l M RESIDUAL CHLORINE 0060000 samples nUUn unUnUnUnUn BOO -SOLIDS-COLOR-TURBIOITY SULFATE- FLUORIDE-CHLORIOE OIL ond GREASE - Ont grab ,, somole off Shift COD SAMPLE ON WET ICE 2ml. concontrotod HpSOo por litor ond pioco on ico 2ml. concontrotod HiSOj por litor TOC 2 ml. concontrotod Hj S04 por litor METALS Cf((<kim.vw 5ml. concontrotod HNO( por litor COLIFORM-Ont grab sample par thift Return to lob. In proparod container on Ico PHENOL 1.0 gram- CuS04 per liter HsPOo to pH 4.0 B Ico JULFIDE 2 ml onomolor ZnAc per Ntor CYANIDE NoOH to pH K) (appros. 2ml. por Ntor) NUTRIENTS-nltrogan and phosphorus PESTICIDES 40 mg. HgClj por liter BpMco on Ico Return to lob. In prepared container on lee BlOASSAY-lnitiol tost eomplt BIOASSAY-Full silt somplo Crow A return to lob. t-gn collection CrewC collect lost hour and roturn to lob. \ MASS SPEC.SAMPLE Roturn to lob. in container provided '\ 0 QOQQOQSUPERVISOR -initial ooch bMck \- J1 r\r\ r\ r\r\ r\ UUU UUU UUU i 'zpi$ 1.^0^ \ SL 023284 \ || r\r\r\ r\r\r\ r\r\r\ r\r\ r\ r\r\ r\ UUU UUU UUU UUU UUU iSSml llOid /`foJ <Ree AT>K n>* rsr\ r\ r\r\r\ UUU UUU r\r\r\ UUU An < ay f S =z: CAMPLE "CATION: $Amru- sf*/J , L M* dJt**/** 4tCCIITTYV OMft IMMMfMISJITT*V MMAMttftt AAMNOfi^lfOifiCAATTMIOMM OBSERVATIONS B REMARKS FOR PERIOD BE8INNIN6>* ON **>/& . tX OUTFALL N0.:_ j2/7L &LnS> 'Stnvr SAMPLE NO.: Strata CXaj^ ^ 2. fp )({? " ' ;<i $?* &t>f* ti.0 /<&>** Jfc. i5T J4L r^&r rye 5vy FT SHIFT SUPERVISOR: SION TOUR REMARKS!'! . JE XT- -- SL 023283 SAMPLE LOCAIION- f / Q- ttm.it* . wr<u A DATE: . - Cl tv OK INDUSTR~Y NAME A*kHOtf LOCXATTION 1/112. /Ff**;Tl. ft 22. * SsTtAaRbtT Ss^luhptliInUsA mo rfimjr rain UUM IMfl " OUTFALL NO.: Q\7 SAMPLE NO.:_______ U//i<f,j **t*0 7*f CREW A CREW B /2**imm ^ uce /^Mfta/? t >***{ 2/t/^y/y/ CREW C &'//S*r*.LO. O/U /fcl A4A^y/ * M L f tt u c/ / > FIELD DATA PRESERVATIVES / 2j 45 7 a 9 to // t2 TIME (hour*) fi-w--2S-- (J ~ OOQQQ&e CFtl'S V3<^o ftp (M OQQQOQQ TEMPERATURE ____ ooeooee 00 33 os<a fit* 6X C.X o6*9 72- H e-oeeooe OlSSOLVEO Oj mg/i. ooeoooo RESIDUAL CHLORINE 0000000 SAMPLE* nunuOuAuAuOuun BOb rSbLib^HtOLdft-tuRBIOITT SULFAT|=Tt!U0RlDE-CHLORIOE OIL ond GREASE - On* grob tompit per ihrft________ ___________ COO SAMPLE ON WET ICE 2ml. concentrated HjSOe p*r liter ond ploc* on c 2 ml. concentrated H*S04 p*r liter TOC 2 ml. concentrated Hj S04 per liter metals J 5ml. concentrated HN0 per liter CONFORM-On* grob Return to lob. In --male!* t!i *wil . EffCflrel- fiaafainsr sa !s* \A\mi mm Mj miitlif HaPOo <0 pH d.0 B Ice SULFIDE 2mL on* molar ZnAe per liter CYANIDE NoOH to pH 10 (approx. 2ml. per liter) NUTRlENTS-nltrogen ond phoepborut 40 mg. HgCI* per Jitll a rtm on lee nUUivUi r\r\ r\ UUU UUU r\r\r\ r\s~\r\ r\s\r\ r\r\ r\ UUU UUU UUU UUU UUU ttoM) T\ /VoU l^lomX I'M /V<W ^2w^ no JL ftQ,ft/ )U~J AAA UUU AAA UUU r\r\r\ UUU 60 ---- PESTICIDES prepared contolnor on Ice BlOASSAY-lniliol t**t tompi* BIOASSAY-Full tin tompN MASS SPEC. SAMPLE SUPERVISOR -- mithat *ocb block on col lection Crew C collect tort hour and return to lob. Return to lab. in contolnor provided 0000000' IS>)La YUA J OK J Vv: t&h ! iMWII m-HFi SL 023285 ______________________-L A- . t j . r. ranMB e f HrSAMPLE LOCATION^ ,-4a. /jbit, CA^dis Lt-oeoe ?l c>tv on Moutrm namc mo lccatkm OBSERVATIONS ft REMARKS FOR PERIOO BEGINNINGhrs. ON _,I9i!~ SHIFT SUPERVISOR: SIGN YOUR REMARKS!'! OUTFALL NO.: OIL_________ SAMPLE NO.: Akyv c&aA \n Ugj-___dlxattV vsn. C qQQ - WW. Z*2. pi ..ft\Ae^*A. fljLffe- lo<____ ~ JcvLmx. Srnnvv, 0 ______ [miW. --_______ V, *2^--/2(}____j ^'2.----------- 41 BS /?.......... at iML so < / ?<> loAb.i3 Z2u2. iff zz /y o TCTo /By.1/ Ij aff 7# / ?l 3/3o ^*4-" *:*>----------------- .7<ae>- n x t Hfl-UB SL 023286' jMrtir'i.c LUlMHUr* V / DATE: OUTFALL NO QU IJ____ {_i_v_O__r_H___ agm,-lac. . !~fxi <-*!/>*.{Cl ITT OK IH0U1TWT N*MC /N0 LOcAlOH ^ 4* At CNO ) SAMPLE NO- rt SAMPLING CREW SUPERVISORS SIGNATURES: CREW A CREW B CREW C /{ex,# <f Q*rig/ &,'//rfi.&Q , Ak4 FtELP DATA TIME (hourej fi nw _ %i TEMPERATURE____ FH DISSOLVED 0, oif/l. RESIOUAL CHLORINE SAMPl 5 606 -4aOLIDS>-COLOR-TURBOITY SULFATE- ftllORIOE-CHLORlOE OIL and GREASE - One qrob omol# otr ihtft COO TOC metals) rAcc COLIFORM-On* grab ompt* pit iltlir PHENOL SULFIDE CYANIOE NUTRIENTS-nltro^en and phoaphorut PESTICIDES BlOASSAY-inltlol Nat tempi* BIOASSAY-Full *m templa MASS SPEC. SAMPLE SUPERVISOR -initial aoch block PRESERVATIVES ooooeoe 0000000 QQOOOOQ 0000000 // Cf)i& Wo 31 .So-S" 3 }SS<f 3/,S A pit S3 L / Q UO T S -- l)h5 6 7 JP(p 0 otps W& vr 3(0 8 9 to // 12 >> 00 -- CN -- n CM 0 e 0-00000 cn 0000000 uuynUnUnvUnUnUnUn nUoUnU AA A AA Ak AAA AA AAAA UUU f\AA AAA r\r\r\ r\r\ r\ UUU UUU UUU UUU UUU r\r\r\ UUU UUU UUU utre SAMPLE ON WET ICE Eml. concantratad KjS04 par Mar and plocaon ica n&A iasJ)2*d IKttl Hod IV~S 2ml.ceneantrot*d H*SCu par lilar 2ml. concantratad H.SO4 par lit*r Snl. concantratad HNO. par litar Return to lob. In praporcd container on let hnA /Jod i&d 3\ SA usd \chJP to1.0 prom. C11SO4 par litar HsPOa pH 4.0 B let 2mL onemolor ZnAc par Star NoOH to pH l6 (appro*. 2ml. par Mar) 40* HflClj par litar B etaca an tea Ratum to lab. In praparad container on lea Crew A return to lob. n collection Craw C collect loot hour and raturn to lab Raturn to lab. in ruco\nuntainnuer pnuroAvuidehud Au u9^. 1 WbOii. Uu'./iM pw JRK ri-MtMi v __J____1____ SAMPLE LOCATION: CITY ON IMUT*Y MAMt AND LOCATION OBSERVATIONS A REMARKS FOR PERIOD BEGINNINGArt. ON 1 ,i fa. OUTFALL NO.: 0)9 SAMPLE NO.: Ma^ itiLtrir " wVa < ta-Q s> = rg> 314 a. 1--^7V\ o^. ------------------------------------- -Si HOW r Vd - *______ 3? r V/ jf/-i ^>4 ^___ Lj~p*-\ tLPK SUf*ESvSOR: SIG*N TOOR RCAiARKS'.l! Uwi^ Atl 7N$ CW-MF8 a a r z SL 023288 LOCATION; Sit] DATS: OUTFALL NO.: 0/9 Ia4l tA**ks yffci. > 1WVIIM SAMPLE NO.: ri SAMPLING CREW SUPERVISORS SIGNATURES: CREW A acrew f^/y ZW>V Rtttf/f/t'// &//J/frCfg J___ &&A '/a CREW C ALIQUOT $ flCtO DATA TIME (hour*) FLOW temperature____ PH DISSOLVED 0, mg/|. RESIDUAL CHLORINE SAMPLES BOD tSOuBb-COLOR-MtaltiUY SULFATE - FLUORIOC-CHLORIOC OIL ond GREASE - Om grob tamo la ixr ahdt COD TOC METALS COLIFORM-One grob ample par ahitt PHENOL SULFIOE CYANIDE NUTR lENTS-nltragen jnd pho*pitorat PESTICIDES i< 310 AS SAY-initial ttat aompla BIOASSAY-Full tilt temple MASS SPEC SAMPLE SUPERVISOR -initlol eoch blech PRESERVATIVES / E 3 4 5 6 ? a 9 to // 12 Q000000 \OVo 0000000 OQOOOOQ oOooooo 0000000 ISJn 'KeS ai/5 0(o$. fitjo? 0 ?p Hi 3<? Ut HI cn 00 (M CA 1 cm 0 to 6-000300 nununununununu SAMPLE ON WET ICE ZM. concentrated H|SO par litar and plocaon ci 2 ml.concentrated H.SOa par lilar * 2 ml. concentrated M. S04 par liter 5 Ml concantratad HNO* par litar Return to lab. In praporad contalnor on lea 1.0 gram- C0SO4 par Mar HsPOa to pH 4.0 ft lea 2 Ml ana molar ZnAc par Htar NeOH to pH id (appro*. 2ml. per Htar) 40 mg. HgClj par litar A olaca an lea Return to lab. In prepared container on lea Craw A return to lob. an col (action CrawC collect last hour and return to lob. Return to lab. In container provided ooooeeo' Ur\Ur\rU\ Ur\rU\ Ur\ rU\rU\ Ur\ UAUAUA AUUAUA Ur\Ur\Ur\ Ur\rU\ Ur\ UaaUUr\ Ur\rU\/Ua UaaUUr\ rU\sU^Ur\ |Z>& II dJ / .^6aX lldruf ho~t //A H t&u. ieM' ` l AUvU/A U/A _____I____ * v-n I g<mn m u SAMPLE LOCATION TTtr "- ./i ^ : je--itr on iNDwusTtvZnudz*nud lorcc*tiom OUTFALL NO.: /// SAMPLE NO.: LINA < ti Cfa/kfeJ <+0*0*ISa sampling crew supervisors signatures. CREW A CREW B CREW C :I t / Q U 0 T *f ~ " " . ,, ............ Ft4.0 DAT* PRESERVATIVES /t 3 6 7 8 9 to u 12 TIME (hour*) F1--3PTEMPERATURE ____ AH DISSOLVED Ot rn/|. 0000000 iqfl GQQOOOO T3o 5ao e-eeoeoQ t^QOoOOO ;$s? ofif 500 </o 0000000 \Q9$S bJ^7 5^0 I pto <* %----- ~o~ --> RESIDUAL CHLORINE 0000000 SAMPLES fllJb -SOuDS-COLOd-TURBIOITY SULFATE - FLUORIDE-CHLORIDE HWNPH OffOIL and GREASE - On* |rtb Ihlft _______________ COD aUUa auuauauaua SAMPLE ON WET ICE End. cancantratad HgSO* par litar and piaca an ica *2ml.concantrotad H.SO* par lllar * TOC figTALS^ rr>E4EA4y COLIFORM -- On# grab temple par thifl PHENOL SULFIDE CYANIOE 2 ml. concentrated H. S04 par litar 5 ml cancantralad HNOm par lllar Return to lab In prepared contalnoren Ica I.Ogrom- C*S04 par lilar ftHsPO. ta pH 40 let 2 ml ont molar ZnAc par Star Na5napHT5 (approt. 2ml. par Mar) NUTRIENTS- nitrogen and photphorut PESTICIDES ,. BIOASSAY-Initial tail tempi* J BIOASSAY -Full tut tempt* MASS SPEC. SAMPLE 40*9- H Clj par litar ft etac* an Ica Raturn to lab. In praparad contain* on let Craw A raturn to lab. c_#fl collection Craw collect (act hour and raturn to lob. Raturn to lab. In container provided SUPERVISOR-initial *ocb block 0000000 uAuAuA AUAUAU rU\sU\ Ur\ Ur\rU\Ur\ Ur\sU\Ur\ rU\rU\rU\ Ur\rU\ Ur\ Ur\rU\ Ua Or\rU\ Ua UAAUUA Ur\rU\rU\ UAUAUA 120+J DjJ H IzolIk ) r-- ! lAtt. aM' SBBBMI tftf' M& t r WK m-nntvn 1-------- T J IE C IJ H -w O ^ po & i/D^C 4^7 *?-<//(> izo ^5`C, f/o .iiXnn^ie,.^o,-I it ^7 TYfyS" VJ? XSl<PO HL * 2_ t\s __ (oylivD f T-? * 2.0 =4^~ $J*jCL f7 / T-O ~L X J ^i> SL 023292 SAMPLING CREW SUPERVISORS SIGNATURES: CREW A CREW B 'j-ffl/W1/Hj C^fch--s-*-***"*/, CREW C lX*t>V. ^**y*_________________ FIELD DATA | 1 M E (hours) i> L-Fl.OW % UAiU TEMPERATURE ____ -------------------------------------------------------------- 4 L t Q u0 T S------------------------------------------------------------------------------------- i " | PRESERVATIVES t 3 4 5 6 7 6 9 to // t2 .i ooooooe o?er OQOOOQQ (n~*> 0000000 63 IH01 *17 Cco-U- 033f OtmQO St --------r-------- ti 1 H oeeoooo DISSOLVED Ot mg/t. 0000000 RESIDUAL CHLORINE KAttO^Fg 1 -Jinn -cm Ata-Yiiamnrrv SULFATE- FLUORIDE-CHLORIDE OIL ond GREASE - One groto omoio otr shift COO METALS COL 1 FORM-Ono grob sample psr shift PHENOL SULFIDE CYANIDE NUTRIENTS-nitrogen and phosphorus PESTictOES BlOASSAY-lnitiol tost sompls BIOASSAY-Full silt sample MASS SPEC. SAMPLE oe-eeooe hU Uanununununu SAMPLE ON WET ICE 2ml eoncontrotod H3SO4 por lilor ond ploeo on tea 2 ml. eoncontrotod H*SGL par liter '^ 2 ml. concentrated pw liter Prf ij 5ml. eoncontrotod HNO. por Dior Return to lob. In praporod container on tec 1.0 gram- CuS04 par liter HsPOa to pH 4.0 ft let 2 ml one molor ZnAc por liter NoOH to pH 10 (appros.2ml.per liter) 40 mg. HgCI* per litar ft piece on lee Return to lob. in praporod eontolner on lee Crow A return to lab. on collection C'twC collect loet hour and return to lab. Return to lob. In container provided nnnUUU f\r\ r\ r\r\r\ UUU UUU UAUAAU UUU AUAUAU r\r\ r\ UUU AAA UUU izerf UOaJL llo*t It*M M I7V7vQ \iau*L U9mI UAUrt Urt UrtrUtAU Ur\Ur\rU\ r\r\ t UU< k --SUPERVISOR -initiol ooch bloch '* Mv /M- JDK 1 023293 --m --4 \_________ SAMPLE LOCAHOH- \ DATE: MR J3AMI PLIN0 5OUTFALL NO.: o h \ --WQ-~^ rv or inoustrvnanc AND LOCATION fND SAMA.IN0 SAMPLE NO.: _____ dMMrLHiu ^ \ c_ CREW A CREW B CREW C ^lutiHiuituj ------------------------------------------------------ A L f 0 u 0 t s----------------------------------------------------------------------------- FIELD DATA PRESERVATIVES / z 3 4 5 6 7 8 9 to // 12 TIME (hours) ( i, r\ r\ r\ r\ r\ r\ r\ uuuuuuu \\7>0 *1 fi nw TEMPE RATURE ____ QOOQOQQ QOOOOOO 00K)Q0Q flf/ DISSOLVED 0, mg/i 0-006606 RESIDUAL CHLORINE 0006000 SAMPLES nu nu nununununu BOD -SOLIDS-CbLOR-TURBIDITY SULFATE- FLUORIOE-CHLORIDE OIL ond GREASE - One (rob sowplo per shift___________________ SAMPLE ON WET ICE 2ml. concentrated HgSO* per liter and pioca on ct COO 2 ml. concentrated H*SOu par liter TOC 2 ml. concentrated H2 S04 per liter metals 5ml. concentrated HNO* par liter COLIFORM - On* (rob sample per shift Return to lab. In prepared container an Ice PHENOL I.Ogram- CuS04 per liter HsPOa to pH 4.0 S ice JLFIDE 2ml one molar ZnAe par liter CYANIDE NaOH to pH tO (appro*. 2ml per (ter) NUTRIENTS-nitrogon and phosphorus PESTICIDES ' 40mg HgClg per liter apiece on kte Return to lab. in prepared container on ice BlOASSAY-lnittol fast tornpla BIOASSAV -Full siia sample Crew A return to lab. . on collection CreC collect last hour and return to lob- MASS SPEC. SAMPLE Return to lab. in container provided r\r\r\ UUU /UYU1UA r\r\ r\ UUU r\r\r\ r\r\r\ r\r\r\ r\r\ r\ r\r\ r\ UUU UUU UUU UUU UUU ;i - . , ' I \ t* i j; i ; i1 1 AA A r\r\r\ AAT UUU UUU UUU UUU J: SUPERVISOR-initial aoch block -i 11 A QcndueAw far__________________ _______ tyW<s i, ; tPA-HFSSVT* ot Hold>qz.------------------------------------ sample location^ rre?i CITY OH INOUSTRY NAME 4*0 LOCATtOK DATE:____ STMT UHPLINI END SAMPLIN* OUTFALL NO.i_jQO.SL_ SAMPLE NO.:__________ SAMPLING Crib* SUPtKVtSOHS SIGNA1 UKtS. CREW A CREW B CREW C A L t 0 U0 T 5 FIELD DATA PRESERVATIVES 1 2 J 4 5 6 ? B 9 to n 12 TIME (hour*) f ,, | r\ r\ aaaa r\ UUUUtrtMJ h4q 1h FI OW unil TEMPERATURE 0____ \ QO^OeOG 0000000 0000000 7-If) DISSOLVED Oj mg/1, 0000000 RESIDUAL CHLORINE SAMPLES BOO -&>LIDS-C6L0R-TURBI0ITY SULFATE-FLUORIDE-CHLORIDE OIL ond GREASE - On* 9rob mpl per hifl___________________ COD TOC METALS COL 1 FORM-On* grab tompi* p*r thill PHENOL ULF10E CYANIDE NUTRIENTS-nltrogtn and phosphorus PESTICIDES BtOASSAY-Initial taat tompi* BIOASSAY-Full tilt tempi* MASS SPEC.SAMPLE SUPERVISOR --Initial *ach bkyck 000 0000 nUUnnUnIMnJnUnU AAA uuu SAMPLE ON WET ICE 2mi conc*nlrat*d H]SO par liter ond pioc* on ct 2 ml. concentrated HS04 p*r lit*r 2 ml. concentrated Hj S0 p*r titer 5ml. concantrated HNO. par liter R*turn to lab. In prtporod containar on lc* 1.0 gram- CuS04 p*r titer HsPOe to pH 4.0 ft lc* 2 ml. on* molar ZnAc par lltar NaOH to pH K) (appro*. 2 ml. pr Hter) 40 mg. HgClj par titer a Mac* on lc* Return to tab. in prepared containar on lc* Craw A return to tab. an cel lection CrtwC collect lact hour and return to lob. Return to lob. In container provided 0 W&&00' LSIL r\r\ r\ r\r\ r\ UUU UUU r\r\r\ r\f\r\ r\r\r\ r\r\ r\ r\r\ r\ UUU UUU UUU UUU UUU \ tmAti -- r\r\r\ r\r\r\ s\r\r\ r\r\ rUUU UUU UUU UUl % 1j 1 EPfc-MFS Vlllt 0 " 023295 ** SAMPLE LOCAIIUN CITY Oir IMOUSTMr NAME AND LOCATION DA7. ^^PTHhpunI END SAMM.INO OUTFALL NO.: QO ^ SAMPLE NO.:__________ 7 dHMrLHiu <*t\ u " JW Ln*ijyr> j wnLJ. 0V4L ^-cnvJLj a erar u &f t 3 FIELD DATA PRESERVATIVES / 2 3 4 5 6 7 8 9 to // 12 TIME (hour*) t ,, , OOOOOQQ ---- Ft nw initB TEMPERATURE JbC QQQQQOQ eeo-eoee ee-oeooe 34.^ DISSOLVED 0t mg/i. 0000000 RESIOUAL CHLORINE SAMPLES BOD -OHO-66l6A -TURBID IT Y SULFATE - FLUORIDE-CHLORIDE OIL ond GREASE - On* grab tamale Mr shift COD TOC METALS COLIFORM-On* grab *ample per shift PNENOL ULFIDE CYANIDE NUTRIENTS-nitrogen and phoiphorti* PESTICIDES BIOASSAY-Initial t**t (ompi* BIOASSAY-Full til* tompl* MASS SPEC.SAMPLE SUPER* ISOR -initial. each block 860-0000 nUUnnUnUnUnUnU SAMPLE ON WET ICE 2ml concentrated HXS04 par liter and pioc* on ice 2 ml. conc*ntrat*d H*S0U per liter * 2 ml. concentrated H, SO, per liter 5 ml concentrated HNO> per liter Return to lab. In prepared container on Ice 1.0 gram. CuSO, per titer HsPOe to bH 4.0 B Ic* 2 ml on* molar ZnAc per liter NoOH to pH tO (appro*. 2ml. per Htor) 40 mg. HgCIi per liter B piece on Ice Return to lob. In prepored container on Ice Crew A return to lab. on collection CrewC collect loct hour and return to lob. Return to lab. in container provided 560e00o~ AUPUIUA UUU r\r\ r\ UUU r\r\r\ r\r\r\ r\r\r\ r\r\ a UUU UUU UUU UUU ' AAA UUU UAAUUA UAAUAU UAUAUA aoautr % 1J 'TA.Y*AtJ_C_i_c_________ ELl _ 0 *ri COMPLIANCE MONITORING ed: April 6 and 7, 1982Date Received: April 7, 1982 Company PPG, lake Charles, Louisiana_____________________________ ;__________ 1 r E ANALYZED 1 R VALUE ANALYST DATE/TIME METHOD -93 x -127 -93 ^ -127 *'' =89 ^ -92/ -95 ^ -94 ^ -128 ' -91 ' =87 ^ -88 ' -90 " 1.0 *0.6 22,0 240.0 2.0 4.0 16.0 **9.4 455.0 **0.54 0.0080 1.89 2,05 ESS 11 MSH H 11 II II II II ESS/FSM it FSM II 4/7/82 1 PM w Membrane Electrode II 4/7/82 1 tM Gravimetric n II 11 II W " _____________________ 11 " J Astro Ecology Auto Analyzer II II A/7/82 4/12/82 4/13/82 II ' * -V A. A. Graphite Furnace II -------------- fft/ t/l l(" 1 'L-'V'j*"r- A. A. Graphite Furnace II * . ecreas( Interference.