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M INNESOTA POLLUTION CO N TRO L AGEN CY DIVISION O F SO LID AND HAZARDOUS W ASTE In case of Em ergency or S p ill, Im m ediately ca ll 3M For MPCA use only 1935 W EST COUNTY ROM ) 6*2 ROSEVILLE. MN 55113-2785 ATTN: HWIMS (612) 733-6100 Please cri^'or type. (Form rfesiflned for use on elite (12-pitch) typewriter.) Instructions on trad ol form. U N IFO R M H A ZA R D O U S W A STE M A N IFES T 1. Generator's US EPA ID No. A LD-00402316 M anifest 2. Page 1 jDocum arrt No. or 2 .141010 In form ation in shaded area mot rQuird by Fed eral law. M in n e s o ta r o le * re q u ire ite m s H. a n d I. 3.Generator'sName andMailingAddress (01/090) A. State Manifest Document Number 3M STATE DOCKS R D .BLDG.17(F.J.BLACKWELL) DCTR m n 0041010 DECATUR, ALA. 3 5 6 0 2 8. State G en erato r'* ID 4. Generator's Phone ( 205 ) 552-6222 5. Transporter 1 C om pany Nam e 6. 3M P R I V A T E C A R R IA G E h-H-D 7. Transporter 2 Com pany N m * 9 Designated Facility N am e and Site Address 1 10. ______ _____ US EPA ID N um ber 006 1 7308 2 U S EPA ID N um ber U S EPA ID Number ALD004023164 C. State Transporter's ID D. Transporter's Phono E. S late Transporter's ID F. Transporter's Phone G. State Facility's ID 3M Chemolite Bldg. 47 Hwy 61 and County Road 19 H. Facility's Phone |M N D 1) 0- 6- 1 7-Z-9-6 ~9: 6 1 2 - 4 5 8 - 2 1 4 1 11. use OT Description /Including Proper Shipping Name, Harare! Class, and ID Number) HM 12.Conta iners No Type 13. 14. Total Quantity WUUVnoitl a. Hazardous waste liquid,NOS*QRM-E NA9189 X (Cell Product Tars) 50% Fluorine. 2 2 DM 1 4 9 2 1 P Waste No, DO 02 h Waste Flammahle Liquid,NOS*Flammable Liq lid X UN1993 (Acrylate Ketone). Solids in Methyl Isobut 11 -3 DM 1- D 2- (I P D001 iC. Non-Regulated Chemicals (FC Alcohol Bottoms) ^50% Fluorine. 7 DM J J 7-(l P NOMH d. Waste Poisonous Solid NOS{Diphenyl Metha ie X 4,4-Diisocynate) Poison B UN2810. 4 DM 4 & (1 P D003 b. d. 15. Special Handling Instruction* and Additional Information PLACARDS REQUIRED: 48602$ IS. GENERATOR'S CERTIFtCATIOM: I haraby daclamthalttw cont*ntaottW*nalgnnn*nlarahj)ly and aceurawly daacnhad a *w by proper rhipping n*ma n d i n ctauKled, packed, markad, and Lahaled, and are In aM r*apacta In propar condition lor Irampor by highway according to applicable Intoma banal and national goveniTMnt ng ulitloni. Unlaaa I am a amill ouanllty gamrater who hi a bean trampled by atahita dr regulalton Irom tha duty to mace a waste mlnknlullon card'Lea Bon under Section 3M3(b) olRCR A, I alao carilfy that I have program In piact to reduce the volume and loilelfy Of wait* generated ta the degree I hive determined to be aeemomt- catty practteebJe and t hava malactad Via method of traitmant lloraoa. or dllpout currently available ta me which mlnlmlrea the present and future Ihrael to human haetth and the envtronmenL Date Printed/Typed Nam e Signatujrree.-*7 / s7 / " Monrn" "ary Year FRANK J. BLACKWELL t 1 7 , Transporter 1 A cknow ledgem ent of Receipt ol Materials P rin ted Typed Nraamii ieb \ 1t (1 1^/ / _____________ _______ _________________________ j_______Pate Signature M onth Day Year _____ | ^ IIS 'j S' ] 11. Transporter 2 A cknow ledgem ent ol Receipt ol M aterials PrirtediTyped Name Signature Month Day Year 19. Discrepancy Indication Space L _ l -- L. - 20. Facility O w n er or O perator: Certification of receipt ol hazardous m aterials covered by this m anilest eccept as noted in Item it . ( Date rrmtodrTyped Nome A , - Month Oay. lV )4M P U \i$X > A riL - 1 M in n eso t* F orm PQ OD371 OHIO 84) Year ProducedPursuant totheMay22, 2007 Settlement AgreementandConsent Orderbetween3MandMPCA Ti*kr n a n v a w w k irn a V7MI Exhibit 2758.0168 Stats o f Mlnnoaxvta v 3M Co.. 2758.0168-0001 C ourt F lo No. 27 CV ID 2MC2 3M M PCA0O014459 on lit |12-ptch) typew riter.} Form A p p ro v e d O M B No 2 0 0 0 0 4 0 4 Empires 7 -3 1 -8 6 ///.tfo u s Snaation Sheet) o ra to r's Name 21. Generator's US E P A 10 No, ALDQ040Z3164 Manifest 22. Page Document No 41010 2 Information in the shaded areas is nol required by Federal law. DCTR 01/090 L . S ta te M a n ife s t D o c u m e n t N u m b e r 3M CO M PAN Y - S T A T E D O C K S R D . BLDG. 1 7 C F .J.B L A C K W E :JJl M N 0 0 4 1 0 1 M . S tate G e n e ra to r's ID DECATUR, ALA. 35602 24. Transporter Company Name 3M PRIVATE CARRIAGE to25. U S ERA N u m b e r I MND006173082 N. State Transporter's ID O. Transporter's Phone 26. Transporter_____Company Name 27. US EPA ID Number P. State T ransporter's ID 20. U S DOT D e scrip tio n (In clud in g P roper S h ip p in g N am e, H a ia rd Class, a n d ID N um b e r) hm ! .... [Q . T ransporter's Phone 29. C o m ainers No. Type 30. T o ta l Q u a n tity 31. U nit W Vol R. Waste No. a. NON REGULATED CHEMICALS. 7 Dt 1955 p NONH b. Hazardous Waste Liquid,NOS*0RM-E NA9189 X DI n 1 .1 -iVichloroethvlenel. 751 Chlorim ,, 1 c. Waste Corrosive Liquid NOS*Corrosive Mat' `rial X UN1760 (Hydrazine,Hydrazine Hydrochloridi Watprl a nrvrmc ima tel1v 7.0% chi nr irie. DM d. N E X R AI OR X Waste Flammable Liquid,Corrosive,NOS*Flaiitniabla. Liquid UN2924 (Acetone,Methanol 6 Potassium HvdrmHdcT. y ' ' 13 DM Waste poisonous liquid NOS (Toluene Diiso :ynat Poison B 8N2SXBX UN2811, 4 ;J)M ------------------------- - ---------------- V ---------------------------- ----------------------------- ~ t. Waste Flammable Liquids NOS*Flammable __ X Liquid UN1993 (Lab Samples). 8 DM 160 p F002 3480 P D002 D001 7802 p D002 692 p D003 2440 P D001 0- Waste Flammable Liquid NOS*Flammable Liq lid X UN1993(Inhibited ethyl acrylate). 2 DM h. Waste Flammable Liquid N0S*Flammable Liq lid 2 X UN1993 (Fluorochemical Solids in Isoprop mol) DM 424 P D001 590 P D001 * S. A d d itio n a l D escriptions fo r M aterials Listed A bove T , H a n d lin g Codes fo r Wastes L is te d A b o ve 32. Special H a n d lin g In stru ctio n s and A d d itio n a l In fo rm a tio n T 3 3, T ra n s p o rte r ___ _ A c k n o w le d g e m e n t o f R e ce ip t o f M a te ria ls a A P rinled/Typed Name , ( Signature N S O 3 4 . T r a n s p o r te r _____A c k n o w le d g e m e n t o f R e ce ip t o f M a te ria ls T Printed/Typed Name f n S ig n a tu re f 35. D iscrepancy Indication Space A C L 1 T Y Form 27193 ^ ProducedPursuanttotheMay22, 2007Settlement AgreementandConsent Orderbetween3MandMPCA 2758.0168-0002 ' D ate M o n t * 09Y In ' 7i s s v n D ate M o n th Day r w ___ 1 1________ _______ 3M MPCAQ0014460