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Table5: ConcentrationfPsFOS inRatScirmiSnanqdesEM)12 Study#FACr-TOX-110Fogowingthe0 (D ID m-u 11@ < <-Z nm m !A a Z Cl P 1> Sampling Time (day) 19501 19502 19503 19504 PFOS Concentratio(npg/inL) Rat Numbcir* 19504F 19505 19505F 19506 1950 0 0.112 0.0701 0.0607 0.0514 NS 0.0550 NS 0.309 NS 7 0.397 0.0535 NS 0.0926 NS 0.0514 NS 0119 NS 15 0.0903 0.0690 NS <LLQ[0.04321<(0.05) NS 0.0609 NS 0.1" NS 21 NS NS NS <U.Q[0.0258]<(0.05)0.0845 <LLQ[0.0353]<(O.OS)0.0880 0.0820 0.26 <LLQ = lass dan theLower LimitofQuanticatio(n0.05ug/mL). *Rat Number with"F indicatesfdalsample, NS: No sample, ?Me 13of24 Table 5: (Coatinned)Concestradons ofPFOS InRat.Semm Sampks from Study#FACT-TOX-1 If Fol 0 mglkg Dose rALm )> z m rm ) !A o Z Swnpling Time (day) 0 7 Is 21 19507F 19509 PFOS Concentratio(npir/mL) RatNumber* 19509 19509F 19510 19511 19512 NS 0.0548 <LLQ[0.0483]<(0.05) NS NS <LLQIO.039SM0.05) <LLO[O-04811<@0.05) NS NS <.AeQ[0.0454]<(0.05<):LLQ[0.0459]<(0.05) NS 0.0942 NS -,@LLQ[0.02691<(0.05)0-102 0.0664 0.0619 <LLQ[0.0449] 0.0636 0.250 0.197 0.0614 0.176 0.238 NS NS 0.0833 <LLQ = Lem Om theLower LimitofQuoifitatio(n0.05pg/mL). *RatNumbcr wM OF"indicatefseW mnple. NS: No sample. Pop 14 of24 MAY, 3.2UUU IU:b4AM ENVIRONMENTAL LAD 2 3E 09 NO.1924 P. 4 wt wt wi Oki Go z CY z 04 coo %.-a CY v fA e4 W*l CA ADVAN CEO BICANAJ-YTCAL SERVICES. INC. to VA Z Table 6: Conomtrationsof PFOS inRat Serum S=ples frgm Study#FACr-TOX-110 Followiogthe9.1 m t)>i(-3< <f mro )M !o a Cl P 1> r Sampling Time (day) 19517 19518 PFOS Concentratio(npg/mL) Rat Numbe& 19518F 19519 19519F 19520 19521 19521F 19522 19523 19523F 19524 0 9.07 9.87 NS 9.37 NS 9.73 11.1 NS 9.32 12.8 NS 10.2 7 9.63 10.3 NS 6.83 NS NS 8.92 NS 8.19 9.65 M 10.4 15 11.5 10.7 NS 9.18 NS NS 14.1 NS 9.57 10.9 NS 9.20 21 NS 6.84 12.1 3.93 8.52 NS 4.93 11.2 NS 5.35 10.2 4.11 1 *RatNumber with "F" indicatesfetalsample. NS: No sample. Pftc 16 or2A Table6: (CondavedC)oncentradoonfsPFOS toRatSerumSmplesfromStudy#FACT-TOX-110F, 0.1mglkg Dose (m0LuPu- m 9 --@, < Z,)$ Sampling Time (I z (dg) mim 19524F 19525 0 NS 12.0 p 7 NS 9.62 Is NS 10.0 21 10.3 NS 19526 9.48 11.2 11.7 NS PFOS Concaftirat(ipoWnmL) RatNwnbcr* - 19527 19529 19528F 19529 19529F 19530 19531 19532 12.0 10.0 NS 11.6 NIS 9.48 9.10 10.6 8.79 7.80 NS 10.3 NS 7.65 7.57 10.1 8.78 9.04 NS 7.31 NS 11.9 10.4 9.66 M 6.19 10.8 3.04 10.4 NS NS NS *Rat Number,%itbL"P" indicetesfetalsamplc. NS: No sample. Page17 of 24 Table7: CojecentratoifoPnFsOS inRatSerumSamplesfromStudy#FACT-TOX-110FoRowimgTheSA M-0 m @ ><ZZ 0>0 m@m Y)-iD 20 1> S=ViingTimc (day) I 19533 0 53.9 7 44.3 15 47.3 21 20A 19533F NS NS NS 42.5 19534 46.9 50.0 56.1 20-5 19534F NS NS NS 41.4 PFOS Concentrat(iPognhnL) RatNumbcr* 19535 19536 19536F 19537 19538 19539 19540 19541 50.1 38.6 56.6 36.6 48.2 43.3 NS 16.2 NS 56.6 46.5 45.2 42.9 44.4 NS 58.4 49.1 44.6 45.8 NS NS 50.7 53.5 37-2 48.6 NS 32.2 NS NS NS NS NS *R.atNumber with 'F"indicatesfetalsunple. M: No saniple. Pap 18 of24- Table 7: (Continued)ConcentrationsofPFOS inRat Serum Samples from Study OFACT-TOX-110 FOB, 0.4mgfkg Dose WM> m0 :0 -< < 10; 5m>rZn PFOS ConcCatFafiO(nPg/ML) Smnpling Tivne RatNumber* (day) 19542 19543 19543F 19544 19545 19546 19546F 19547 19548 20 0 45.3 46-3 NS 45.8 47.9 43.5 NS 42.2 57.6 1> 7 40.6 46.1 NS 42.8 NS 46.5 NS 42.2 60.0 15 44.0 43.9 NS 49.1 NS 47.3 NS 43.3 59.0 21 NS 23.0 34.1 NS M 35.8 48.4 NS 65.7 *RatNuinbeWrith*F"indicatfeestaslunple. NS: No smnple. -Pap 19 of24 Table 8: Conceohadons ofPFOS inRat Serum Samples from Study #FACT-TOX-110 FoHowing the1.6 m ,m F, t'1)>f) m@m 1> SamplingTime (day) 0 7 is 21 19549 19550 166 200 NS 216 NS 160 NS NS 19551 PFOS Concentration-(p&Lt@D Rat Number 19552 19553 19554 19555 19556 19557 19538 19559 184 165 t82 203 166 199 198 196 171 NS NS 160 189 195 186 NS 171 160 NS NS 135 176 225 202 NS 164 192 NS NS NS NS NS 251 NS NS 237 NS: No sample. PW 20 of24 Table 9: (Cmdnued) Concm&ntions ofPFOS inRat Serum Samples from Study #FACT-TOX-110 Fe 1.6mg/kg Dose < 0 mqm !D-11) Sampling Time (d 1956OF 0 NS 7 NS is NS 21 131 19561 193 181 219 NS PFOS Concenkadon (pg/ML) RatNumber* - 19562 19562F 19563 185 NS 163 179 NS 168 142 NS 183 63.7 102 NS *RatNumbcr with"F'indicatefsdd suvie. NS: No sample, 19564 195 169 159 NS Page 21 of 24 99 Table 9: Concentrationsof PFOS inRat Serum Samples from Study #FACT-TOX-11(i Followingthe 3.2 MLO-M0 ]]V <Z ; 01>n m@m 9):Ja 0 p )> Swnpling Timc (day) 19565 19566 0 370 337 7 392 280 15 345 311 21 NS NS 1 *Rat Number with "r indicates fetal NS: No sample. 19567 366 327 294 NS sample. PFOS Concentratio(ntigImL) Rat Number* 19569 19568F 19569 19569F 19570 19571 19571F 195 339 NS 334 NS 351 348 NS 351 340 NS 323 NS 337 371 NS 305 336 NS 3t4 NS 269 308 NS 3 l) 241 228 142 176 NS 165 166 123 Pap 22 of U MM> m -0 mim P-0 20 Table 9: - (Continued)ConcentrationsofPFOS inRat Serum Samples from Study NFACT-TOX-110 Fol 3.2mgtkg Doze SamplingTime (day) 19573 19574 19S75 PFOS Concentratio(nag@EL RatNwnber* 19576 19577 19577F 19579 19579 19579F 19.' 0 364 365 413 393 417 NS 373 387 NS 3 7 343 393 387 NS 395 NS NS 399 NS 3 15 317 299 284 NS 361 NS NS 396 NS 3 21 NS NS NS NS 221 226 NS 186 181 -- I *RatNumber with"F" indicatefsetaslanple, NS: No sample. Par 23 of24