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Region 6 Compliance Assurance and Enforcement Division
INSPECTION REPORT
SUPPLEMENTAL
Inspection Date(s): Media: Regulatory Program(s)
11/13/2017 to 11/16/2017 RCRA Used Oil and Generator Requirements; CEI- Focused Compliance Evaluation Inspection
Company Name: Facility Name: Facility Physical Location:
(city, state, zip code) Mailing address:
(city, state, zip code) County/Parish: Facility Contact:
January Environmental Services Inc.
January Environmental Services Inc. 4300 SW 361h St.
Oklahoma City, OK 73119
2701 S. Prospect
Oklahoma City, OK 73129
Oklahoma Mr. Cris January
I Owner
cris@januaryservices.com
FRS Number: Identification/Permit Number: Media Number: NAICS: SIC:
None OKD42146324 None 48422 None
Personnel participating in inspection:
Debra Pandak
U.S. EPA Region 6
David Robertson
U.S. EPA Region 6
Christina Coffel
Oklahoma Dept. of
Environmental Quality
(ODEQ)
Roarke Blackwell
ODEQ
Tory Smith
ODEQ
Alicia Chen
ODEQ
Cris January
January Environmental
Services
Inspector Inspector Inspector
Inspector Inspector Inspector Owner
214-665-7565 214-665-7363 405-702-5176
405-702-5127 405-702-522 1 405-702-5219
EPA Lead Inspector Signature/Date
Supervisor Signature/Date
6ENFORM-019-R7 {2/15/2017)
~ Debra Pandak
~_J~
Sunita Singhvi
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u
1
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Date
5 I:2./ H?
Date
Section I-INTRODUCTION
January Environmental Service Inc. Supplement to Inspection Report: Inspection Date 11/13/2017- 11/16/2017
PURPOSE OF THE SUPPLEMENTAL REPORT
The purpose of the supplement to the Inspection Report dated January 4, 2018, is to provide the analytical results of sa mples collected during EPA's inspection and analyzed by the EPA Houston Laboratory.
SECTION II SAMPLE RESULTS
The EPA team collected used oil and waste samples on November 14, 2017. Containers sampled and the contents collected are:
Container Tank 15 Tank 19 Tank 21 Tote 6 Drum #10 Roll-off C25276D Roll-off R25036
Contents Used Oil Used Oil/Water Used Oil Waste Ink (according to label) Waste liquid Waste liquid Waste liquid
Analytical results are attached as Appendix 15. Results show detection of 2-butanone, tetrachloroethene and benzene. A summary of organics detected in the used oil tanks, and other units sampled, is shown below.
Unit Sampled 2-butanone Tetrachloroethene
(ppm)
(ppm)
Regulatory limit 200ppm
Regulatory limit 0.70 ppm
Tank 15
13.0
0.60
Tank 19
5.53
ND
Tank 21
10.8
ND
Tote 6
0.128 B
ND
Drum #10
58,000
ND
Roll-off
ND
ND
C25276D
Roll-off
0.66
ND
R25036
B- found in laboratory blank
2
Appendix - 1S
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region 6 Laboratory
Environmental Services Branch 10625 Fallstone Road, Houston, TX 77099 Phone: (281)983-2100 Fax: (281)983-2248
Final Analytical Report
Site Name --------------------Sample Collection Date(s)-Contact------------------------Report Date-------------------Project #----------------------Work Order(s)-----------------
January Environmental Services 11/08/17 - 11/14/17 Debra Pandak (6EN-H2) 03/26/18 18RCRA019
1711006
Analyses included in this report:
Metals ICP (RCRA 8) 6010D Metals Mercury 7470A Metals TCLP ICP 1311/6010D TCLP 1311 Metals Prep VOA 8260C Routine List
Metals Ignitability 1020B Metals TCLP Hg 1311/7470A TCLP 1311 Hg Prep TCLP 1311 VOA/ZHE Prep VOA TCLP 1311/8260C
Report Narrative
Volatiles:
TCLP sample preparation was performed outside recommended holding time in Method 1311. Samples are qualified as HTT. Per customer, the samples are waste and do not have a holding time. However, laboratory policy is to say concentrations should be considered minimum values when prepared past recommended date.
Sample 1711006-08 significantly exceeded the TCLP maximum concentration limit (MCL) for 2-Butanone at 58,700,000 ug/L (limit is 200,000 ug/L). All other samples had concentrations below the TCLP MCL.
In sample 1711006-02, 2-Butanone is qualified as high biased due to high failure of the continuing calibration verification that day of analysis. The result is significantly below the TCLP MCL and is therefore usable.
2-Butanone is qualified as blank related in sample 1711006-07 due to presence of this analyte in the associated analysis blank.
Report Narrative (cont'd)
Batch B8C1304: The surrgate 1,2-Dichloroethane-d4 fails low in the MSD but should not affect the data.
Metals ICP:
Batch B8B2801:
MS1/MSD1 (Sample Source1711006-06): Selenium spike recoveries are outside upper control limits; the sample source results are qualified and are an estimate.
Metals Mercury 7470A
The samples were redigested at reduced initial volume of 0.20 mls instead of 25 mls because of the matrix problems in batch B8C0801 and analyzed with acceptable QC.
Metals Ignitability 1020B:
Samples 1711006-01 and -02 are phasic, each having two layers. Both layers of sample 1711006-01 had no flash @ up to 60C, and that was the result reported for sample 1711006-01. The top layer of sample 1711006-02 had insufficient volume to collect an aliquot for analysis. The bottom layer of sample 1711006-02 had no flash @ up to 60C, and that was the result reported for sample 1711006-02.
The only sample that flashed below 60C was sample 1711006-08 which flashed at 28 C.
Standard procedures for quality assurance and quality control were followed in the analysis and reporting of the sample results. The results apply only to the samples tested. This final report should only be reproduced in full.
The reporting limit (sometimes referred to as a quantitation limit) is defined as the lowest concentration at which an analyte can be reliably measured and reported without qualification. Reporting limits are adjusted for sample size, dilution, and matrix interference. Concentrations below the reporting limit are reported as non-detects or <RL. For a list of ISO 17025 accredited methods go to: http://region6a.epa.gov/intranet/6md/lab/labisocertification2018.pdf
Report Approvals:
Richard McMillin Region 6 Laboratory Technical Manager
David W. McQuiddy Region 6 Laboratory Branch Chief
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY Region 6 Environmental Services Branch Laboratory 10625 Fallstone Road Houston, Texas 77099
Sample Receipt and Disposal
Site Name: January Environmental Services Data Management Coordinator: Christy Warren Data Management Coordinator Signature
Project Number: 18RCRA019
/
/
Date
Date Transmitted: _____/_____/_______
Please have the U.S. EPA Project Manager/Officer call the Data Management Coordinator at 3-2137 for any comments or questions.
Please sign and date this form below and return it with any comments to:
Christy Warren Data Management Coordinator Region 6 Laboratory 6MD-HS
__________________________________________________/_____/_______ Received by and Date
Comments:
The laboratory routinely disposes of samples 90 days after all analyses have been completed. If you have a need to hold these samples in custody longer than 90 days, please sign below.
____________________________________________ Signature
Please provide a reason for holding:
___________________ Date
Station ID C25276D R25036 Tank 15 Tank 19 Tank B Tank 21 Tote 6 Drum 10 Tote A Sta A
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
ANALYTICAL REPORT FOR SAMPLES
Laboratory ID 1711006-01 1711006-02 1711006-03 1711006-04 1711006-05 1711006-06 1711006-07 1711006-08 1711006-09 1711006-10
Sample Type Liquid Liquid Liquid Liquid Liquid Liquid Liquid Liquid Liquid Liquid
Date Collected 11/14/17 14:51 11/14/17 15:13 11/14/17 15:43 11/14/17 15:51 11/14/17 15:57 11/14/17 16:01 11/14/17 16:28 11/14/17 16:45 11/14/17 16:28 11/8/17 10:30
Date Received 11/16/17 11:55 11/16/17 11:55 11/16/17 11:55 11/16/17 11:55 11/16/17 11:55 11/16/17 11:55 11/16/17 11:55 11/16/17 11:55 11/16/17 11:55 11/16/17 11:55
Project #: 18RCRA019
Report Name: Page 1 of 58
Project #: 18RCRA019
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
QC SUMMARY REPORT
Metals ICP (RCRA 8) 6010D
B8B2801
Samples: 8
Liquid
ReExts: 0
LAB NUMBER
B8B2801-BLK1 B8B2801-BS1 B8B2801-MS1 B8B2801-MSD1
SOURCE
1711006-06 1711006-06
Metals Ignitability 1020B
B8A0501
Samples: 9
Liquid
ReExts: 0
LAB NUMBER
B8A0501-DUP1
SOURCE
1711006-06
Metals Mercury 7470A
B8C0501
Samples: 8
Liquid
ReExts: 0
LAB NUMBER
B8C0501-BLK1 B8C0501-BS1 B8C0501-BS2 B8C0501-BS3 B8C0501-BS4 B8C0501-BS5 B8C0501-BS6 B8C0501-BS7 B8C0501-MS1 B8C0501-MSD1
SOURCE
1711006-06 1711006-06
B8C0801
Samples: 0
Liquid
ReExts: 8
LAB NUMBER
B8C0801-BLK1 B8C0801-BS1 B8C0801-BS2 B8C0801-BS3 B8C0801-BS4 B8C0801-BS5 B8C0801-BS6 B8C0801-BS7 B8C0801-MS1 B8C0801-MSD1
SOURCE
1711006-06RE1 1711006-06RE1
Report Name: Page 2 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
TCLP 1311 VOA/ZHE Prep
B8B1504
Samples: 9
Liquid
ReExts: 0
LAB NUMBER
B8B1504-BLK1 B8B1504-BLK2
SOURCE
VOA 8260C Routine List
B8C1303
Samples: 1
Liquid
ReExts: 0
LAB NUMBER
B8C1303-BLK1 B8C1303-BS1
SOURCE
VOA TCLP 1311/8260C
B8C1304
Samples: 9
Liquid
ReExts: 0
LAB NUMBER
B8C1304-BLK1 B8C1304-BLK2 B8C1304-BLK3 B8C1304-BLK4 B8C1304-BS1 B8C1304-BS2 B8C1304-BS3 B8C1304-BS4 B8C1304-MS1 B8C1304-MSD1
SOURCE
1711006-06 1711006-06
Project #: 18RCRA019
Report Name: Page 3 of 58
Lab ID: 1711006-01
Batch: B8B2801 Sample Type: Liquid
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Metals by EPA Method 6010D - ICP
Date Collected: 11/14/17 Sample Vol: 50ml
Station ID: C25276D
Sample Qualifiers:
Analyte (CAS Number)
Arsenic (7440-38-2) Barium (7440-39-3) Cadmium (7440-43-9) Chromium (7440-47-3) Lead (7439-92-1) Selenium (7782-49-2) Silver (7440-22-4)
Result g/L
U 781 7.0 19.3 86.9 U U
Targets
Analyte Qualifiers
Reporting Limit
120 12.0 6.0 12.0 36.0 120 12.0
Dilution
1 " " " " " "
Prepared
02/28/18 " " " " " "
Analyzed 03/07/18
" " " " " "
Project #: 18RCRA019
Report Name: Page 4 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
TCLP Volatiles by EPA Method 1311/8260C - GC/MS
Lab ID: 1711006-01
Batch: B8C1304 Sample Type: Liquid Batch Matrix: Liquid
Date Collected: 11/14/17 Sample Vol: 5ml
TCLP Prepared: 2/21/18
Station ID: C25276D
Sample Qualifiers: HTT
Analyte
1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene
Analyte (CAS Number)
Vinyl chloride (75-01-4) 1,1-Dichloroethene (75-35-4) 2-Butanone (78-93-3) Chloroform (67-66-3) 1,2-Dichloroethane (107-06-2) Carbon tetrachloride (56-23-5) Benzene (71-43-2) Trichloroethene (79-01-6) Tetrachloroethene (127-18-4) Chlorobenzene (108-90-7) 1,4-Dichlorobenzene (106-46-7)
Surrogates
Result g/L
Analyte Qualifiers %Recovery
%Recovery Limits
46.9
93.9
46.3
92.6
46.5
92.9
Targets
86-117 85-113 73-115
Result g/L
U U U U U U U U U U U
Analyte Qualifiers
Reporting Limit
20.0 20.0 50.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0
Dilution
10 " " " " " " " " " "
Prepared Analyzed
03/02/18 " "
03/02/18 " "
Prepared 03/02/18
" " " " " " " " " "
Analyzed 03/02/18
" " " " " " " " " "
Project #: 18RCRA019
Report Name: Page 5 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Metals by EPA Method 7470A/7471B - CVAAS
Lab ID: 1711006-01RE1
Batch: B8C0801 Sample Type: Liquid
Date Collected: 11/14/17 Sample Vol: 0.2ml
Station ID: C25276D
Sample Qualifiers: HTS
Analyte (CAS Number)
Mercury (7439-97-6)
Result g/L
U
Targets
Analyte Qualifiers
Reporting Limit
25.0
Dilution 1
Prepared Analyzed 03/08/18 03/08/18
Project #: 18RCRA019
Report Name: Page 6 of 58
Lab ID: 1711006-02
Batch: B8B2801 Sample Type: Liquid
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Metals by EPA Method 6010D - ICP
Date Collected: 11/14/17 Sample Vol: 50ml
Station ID: R25036
Sample Qualifiers:
Analyte (CAS Number)
Arsenic (7440-38-2) Barium (7440-39-3) Cadmium (7440-43-9) Chromium (7440-47-3) Lead (7439-92-1) Selenium (7782-49-2) Silver (7440-22-4)
Result g/L
U 573 38.7 52.4 308 737 U
Targets
Analyte Qualifiers
Reporting Limit
120 12.0 6.0 12.0 36.0 120 12.0
Dilution
1 " " " " " "
Prepared
02/28/18 " " " " " "
Analyzed
03/07/18 " " " " " "
Project #: 18RCRA019
Report Name: Page 7 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
TCLP Volatiles by EPA Method 1311/8260C - GC/MS
Lab ID: 1711006-02
Batch: B8C1304 Sample Type: Liquid Batch Matrix: Liquid
Date Collected: 11/14/17 Sample Vol: 5ml
TCLP Prepared: 2/21/18
Station ID: R25036
Sample Qualifiers: HTT
Analyte
1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene
Analyte (CAS Number)
Vinyl chloride (75-01-4) 1,1-Dichloroethene (75-35-4) 2-Butanone (78-93-3) Chloroform (67-66-3) 1,2-Dichloroethane (107-06-2) Carbon tetrachloride (56-23-5) Benzene (71-43-2) Trichloroethene (79-01-6) Tetrachloroethene (127-18-4) Chlorobenzene (108-90-7) 1,4-Dichlorobenzene (106-46-7)
Surrogates
Result g/L
Analyte Qualifiers %Recovery
%Recovery Limits
48.6
97.2
47.2
94.4
48.5
96.9
Targets
86-117 85-113 73-115
Result g/L
U U 667 U U U 56.2 U U U U
Analyte Qualifiers
K
Reporting Limit
40.0 40.0 100 40.0 40.0 40.0 40.0 40.0 40.0 40.0 40.0
Dilution
20 " " " " " " " " " "
Prepared Analyzed
03/02/18 " "
03/02/18 " "
Prepared 03/02/18
" " " " " " " " " "
Analyzed 03/02/18
" " " " " " " " " "
Project #: 18RCRA019
Report Name: Page 8 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Metals by EPA Method 7470A/7471B - CVAAS
Lab ID: 1711006-02RE1
Batch: B8C0801 Sample Type: Liquid
Date Collected: 11/14/17 Sample Vol: 0.2ml
Station ID: R25036
Sample Qualifiers: HTS
Analyte (CAS Number)
Mercury (7439-97-6)
Result g/L
U
Targets
Analyte Qualifiers
Reporting Limit
25.0
Dilution 1
Prepared Analyzed 03/08/18 03/08/18
Project #: 18RCRA019
Report Name: Page 9 of 58
Lab ID: 1711006-03
Batch: B8B2801 Sample Type: Liquid
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Metals by EPA Method 6010D - ICP
Date Collected: 11/14/17 Sample Vol: 50ml
Station ID: Tank 15
Sample Qualifiers:
Analyte (CAS Number)
Arsenic (7440-38-2) Barium (7440-39-3) Cadmium (7440-43-9) Chromium (7440-47-3) Lead (7439-92-1) Selenium (7782-49-2) Silver (7440-22-4)
Result g/L
U 301 U 1,520 115 551 23.3
Targets
Analyte Qualifiers
Reporting Limit
100 10.0 5.0 10.0 30.0 100 10.0
Dilution
1 " " " " " "
Prepared
02/28/18 " " " " " "
Analyzed
03/07/18 " " " " " "
Project #: 18RCRA019
Report Name: Page 10 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
TCLP Volatiles by EPA Method 1311/8260C - GC/MS
Lab ID: 1711006-03
Batch: B8C1304 Sample Type: Liquid Batch Matrix: Liquid
Date Collected: 11/14/17 Sample Vol: 5ml
TCLP Prepared: 2/21/18
Station ID: Tank 15
Sample Qualifiers: HTT
Analyte
1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene
Analyte (CAS Number)
Vinyl chloride (75-01-4) 1,1-Dichloroethene (75-35-4) 2-Butanone (78-93-3) Chloroform (67-66-3) 1,2-Dichloroethane (107-06-2) Carbon tetrachloride (56-23-5) Benzene (71-43-2) Trichloroethene (79-01-6) Tetrachloroethene (127-18-4) Chlorobenzene (108-90-7) 1,4-Dichlorobenzene (106-46-7)
Surrogates
Result g/L
Analyte Qualifiers %Recovery
%Recovery Limits
44.0
88.0
45.7
91.4
46.1
92.2
Targets
86-117 85-113 73-115
Result g/L
U U 13,100 U U U U U 626 U U
Analyte Qualifiers
Reporting Limit
400 400 1,000 400 400 400 400 400 400 400 400
Dilution
200 " " " " " " " " " "
Prepared Analyzed
03/07/18 " "
03/07/18 " "
Prepared 03/07/18
" " " " " " " " " "
Analyzed 03/07/18
" " " " " " " " " "
Project #: 18RCRA019
Report Name: Page 11 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Metals by EPA Method 7470A/7471B - CVAAS
Lab ID: 1711006-03RE1
Batch: B8C0801 Sample Type: Liquid
Date Collected: 11/14/17 Sample Vol: 0.2ml
Station ID: Tank 15
Sample Qualifiers: HTS
Analyte (CAS Number)
Mercury (7439-97-6)
Result g/L
U
Targets
Analyte Qualifiers
Reporting Limit
25.0
Dilution 1
Prepared Analyzed 03/08/18 03/08/18
Project #: 18RCRA019
Report Name: Page 12 of 58
Lab ID: 1711006-04
Batch: B8B2801 Sample Type: Liquid
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Metals by EPA Method 6010D - ICP
Date Collected: 11/14/17 Sample Vol: 50ml
Station ID: Tank 19
Sample Qualifiers:
Analyte (CAS Number)
Arsenic (7440-38-2) Barium (7440-39-3) Cadmium (7440-43-9) Chromium (7440-47-3) Lead (7439-92-1) Selenium (7782-49-2) Silver (7440-22-4)
Result g/L
U 360 U 1,250 U 772 U
Targets
Analyte Qualifiers
Reporting Limit
100 10.0 5.0 10.0 30.0 100 10.0
Dilution
1 " " " " " "
Prepared 02/28/18
" " " " " "
Analyzed 03/07/18
" " " " " "
Project #: 18RCRA019
Report Name: Page 13 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
TCLP Volatiles by EPA Method 1311/8260C - GC/MS
Lab ID: 1711006-04
Batch: B8C1304 Sample Type: Liquid Batch Matrix: Liquid
Date Collected: 11/14/17 Sample Vol: 5ml
TCLP Prepared: 2/21/18
Station ID: Tank 19
Sample Qualifiers: HTT
Analyte
1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene
Analyte (CAS Number)
Vinyl chloride (75-01-4) 1,1-Dichloroethene (75-35-4) 2-Butanone (78-93-3) Chloroform (67-66-3) 1,2-Dichloroethane (107-06-2) Carbon tetrachloride (56-23-5) Benzene (71-43-2) Trichloroethene (79-01-6) Tetrachloroethene (127-18-4) Chlorobenzene (108-90-7) 1,4-Dichlorobenzene (106-46-7)
Surrogates
Result g/L
Analyte Qualifiers %Recovery
%Recovery Limits
46.4
92.8
46.4
92.8
47.8
95.6
Targets
86-117 85-113 73-115
Result g/L
U U 5,530 U U U U U U U U
Analyte Qualifiers
Reporting Limit
200 200 500 200 200 200 200 200 200 200 200
Dilution
100 " " " " " " " " " "
Prepared Analyzed
03/06/18 " "
03/06/18 " "
Prepared 03/06/18
" " " " " " " " " "
Analyzed 03/06/18
" " " " " " " " " "
Project #: 18RCRA019
Report Name: Page 14 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Metals by EPA Method 7470A/7471B - CVAAS
Lab ID: 1711006-04RE1
Batch: B8C0801 Sample Type: Liquid
Date Collected: 11/14/17 Sample Vol: 0.2ml
Station ID: Tank 19
Sample Qualifiers: HTS
Analyte (CAS Number)
Mercury (7439-97-6)
Result g/L
U
Targets
Analyte Qualifiers
Reporting Limit
25.0
Dilution 1
Prepared Analyzed 03/08/18 03/08/18
Project #: 18RCRA019
Report Name: Page 15 of 58
Lab ID: 1711006-05
Batch: B8B2801 Sample Type: Liquid
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Metals by EPA Method 6010D - ICP
Date Collected: 11/14/17 Sample Vol: 50ml
Station ID: Tank B
Sample Qualifiers:
Analyte (CAS Number)
Arsenic (7440-38-2) Barium (7440-39-3) Cadmium (7440-43-9) Chromium (7440-47-3) Lead (7439-92-1) Selenium (7782-49-2) Silver (7440-22-4)
Result g/L
U 353 U 1,260 U 778 U
Targets
Analyte Qualifiers
Reporting Limit
100 10.0 5.0 10.0 30.0 100 10.0
Dilution
1 " " " " " "
Prepared 02/28/18
" " " " " "
Analyzed 03/07/18
" " " " " "
Project #: 18RCRA019
Report Name: Page 16 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
TCLP Volatiles by EPA Method 1311/8260C - GC/MS
Lab ID: 1711006-05
Batch: B8C1304 Sample Type: Liquid Batch Matrix: Liquid
Date Collected: 11/14/17 Sample Vol: 5ml
TCLP Prepared: 2/21/18
Station ID: Tank B
Sample Qualifiers: HTT
Analyte
1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene
Analyte (CAS Number)
Vinyl chloride (75-01-4) 1,1-Dichloroethene (75-35-4) 2-Butanone (78-93-3) Chloroform (67-66-3) 1,2-Dichloroethane (107-06-2) Carbon tetrachloride (56-23-5) Benzene (71-43-2) Trichloroethene (79-01-6) Tetrachloroethene (127-18-4) Chlorobenzene (108-90-7) 1,4-Dichlorobenzene (106-46-7)
Surrogates
Result g/L
Analyte Qualifiers %Recovery
%Recovery Limits
45.7
91.4
46.8
93.5
48.1
96.2
Targets
86-117 85-113 73-115
Result g/L
U U 5,860 U U U U U U U U
Analyte Qualifiers
Reporting Limit
200 200 500 200 200 200 200 200 200 200 200
Dilution
100 " " " " " " " " " "
Prepared Analyzed
03/06/18 " "
03/06/18 " "
Prepared 03/06/18
" " " " " " " " " "
Analyzed 03/06/18
" " " " " " " " " "
Project #: 18RCRA019
Report Name: Page 17 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Metals by EPA Method 7470A/7471B - CVAAS
Lab ID: 1711006-05RE1
Batch: B8C0801 Sample Type: Liquid
Date Collected: 11/14/17 Sample Vol: 0.2ml
Station ID: Tank B
Sample Qualifiers: HTS
Analyte (CAS Number)
Mercury (7439-97-6)
Result g/L
U
Targets
Analyte Qualifiers
Reporting Limit
25.0
Dilution 1
Prepared Analyzed 03/08/18 03/08/18
Project #: 18RCRA019
Report Name: Page 18 of 58
Lab ID: 1711006-06
Batch: B8B2801 Sample Type: Liquid
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Metals by EPA Method 6010D - ICP
Date Collected: 11/14/17 Sample Vol: 50ml
Station ID: Tank 21
Sample Qualifiers:
Analyte (CAS Number)
Arsenic (7440-38-2) Barium (7440-39-3) Cadmium (7440-43-9) Chromium (7440-47-3) Lead (7439-92-1) Selenium (7782-49-2) Silver (7440-22-4)
Result g/L
U 310 U 242 33.0 463 40.0
Targets
Analyte Qualifiers
J
Reporting Limit
100 10.0 5.0 10.0 30.0 100 10.0
Dilution
1 " " " " " "
Prepared
02/28/18 " " " " " "
Analyzed
03/07/18 " " " " " "
Project #: 18RCRA019
Report Name: Page 19 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
TCLP Volatiles by EPA Method 1311/8260C - GC/MS
Lab ID: 1711006-06
Batch: B8C1304 Sample Type: Liquid Batch Matrix: Liquid
Date Collected: 11/14/17 Sample Vol: 5ml
TCLP Prepared: 2/21/18
Station ID: Tank 21
Sample Qualifiers: HTT
Analyte
1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene
Analyte (CAS Number)
Vinyl chloride (75-01-4) 1,1-Dichloroethene (75-35-4) 2-Butanone (78-93-3) Chloroform (67-66-3) 1,2-Dichloroethane (107-06-2) Carbon tetrachloride (56-23-5) Benzene (71-43-2) Trichloroethene (79-01-6) Tetrachloroethene (127-18-4) Chlorobenzene (108-90-7) 1,4-Dichlorobenzene (106-46-7)
Surrogates
Result g/L
Analyte Qualifiers %Recovery
%Recovery Limits
44.9
89.7
46.3
92.6
46.9
93.8
Targets
86-117 85-113 73-115
Result g/L
U U 10,800 U U U U U U U U
Analyte Qualifiers
Reporting Limit
400 400 1,000 400 400 400 400 400 400 400 400
Dilution
200 " " " " " " " " " "
Prepared Analyzed
03/07/18 " "
03/07/18 " "
Prepared 03/07/18
" " " " " " " " " "
Analyzed 03/07/18
" " " " " " " " " "
Project #: 18RCRA019
Report Name: Page 20 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Metals by EPA Method 7470A/7471B - CVAAS
Lab ID: 1711006-06RE1
Batch: B8C0801 Sample Type: Liquid
Date Collected: 11/14/17 Sample Vol: 0.2ml
Station ID: Tank 21
Sample Qualifiers: HTS
Analyte (CAS Number)
Mercury (7439-97-6)
Result g/L
54.0
Targets
Analyte Qualifiers
Reporting Limit
25.0
Dilution 1
Prepared Analyzed 03/08/18 03/08/18
Project #: 18RCRA019
Report Name: Page 21 of 58
Lab ID: 1711006-07
Batch: B8B2801 Sample Type: Liquid
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Metals by EPA Method 6010D - ICP
Date Collected: 11/14/17 Sample Vol: 50ml
Station ID: Tote 6
Sample Qualifiers:
Analyte (CAS Number)
Arsenic (7440-38-2) Barium (7440-39-3) Cadmium (7440-43-9) Chromium (7440-47-3) Lead (7439-92-1) Selenium (7782-49-2) Silver (7440-22-4)
Result g/L
U 36.5
U U U U U
Targets
Analyte Qualifiers
Reporting Limit
100 10.0 5.0 10.0 30.0 100 10.0
Dilution
1 " " " " " "
Prepared 02/28/18
" " " " " "
Analyzed 03/07/18
" " " " " "
Project #: 18RCRA019
Report Name: Page 22 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
TCLP Volatiles by EPA Method 1311/8260C - GC/MS
Lab ID: 1711006-07
Batch: B8C1304 Sample Type: Liquid Batch Matrix: Liquid
Date Collected: 11/14/17 Sample Vol: 5ml
TCLP Prepared: 2/21/18
Station ID: Tote 6
Sample Qualifiers: HTT
Analyte
1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene
Analyte (CAS Number)
Vinyl chloride (75-01-4) 1,1-Dichloroethene (75-35-4) 2-Butanone (78-93-3) Chloroform (67-66-3) 1,2-Dichloroethane (107-06-2) Carbon tetrachloride (56-23-5) Benzene (71-43-2) Trichloroethene (79-01-6) Tetrachloroethene (127-18-4) Chlorobenzene (108-90-7) 1,4-Dichlorobenzene (106-46-7)
Surrogates
Result g/L
Analyte Qualifiers %Recovery
%Recovery Limits
43.8
87.7
45.3
90.5
46.5
92.9
Targets
86-117 85-113 73-115
Result g/L
U U 128 U U U U U U U U
Analyte Qualifiers
B
Reporting Limit
20.0 20.0 50.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0
Dilution
10 " " " " " " " " " "
Prepared Analyzed
03/06/18 " "
03/06/18 " "
Prepared 03/06/18
" " " " " " " " " "
Analyzed 03/06/18
" " " " " " " " " "
Project #: 18RCRA019
Report Name: Page 23 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Metals by EPA Method 7470A/7471B - CVAAS
Lab ID: 1711006-07RE1
Batch: B8C0801 Sample Type: Liquid
Date Collected: 11/14/17 Sample Vol: 0.2ml
Station ID: Tote 6
Sample Qualifiers: HTS
Analyte (CAS Number)
Mercury (7439-97-6)
Result g/L
U
Targets
Analyte Qualifiers
Reporting Limit
25.0
Dilution 1
Prepared Analyzed 03/08/18 03/08/18
Project #: 18RCRA019
Report Name: Page 24 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
TCLP Volatiles by EPA Method 1311/8260C - GC/MS
Lab ID: 1711006-08
Batch: B8C1304 Sample Type: Liquid Batch Matrix: Liquid
Date Collected: 11/14/17 Sample Vol: 5ml
TCLP Prepared: 2/21/18
Station ID: Drum 10
Sample Qualifiers: HTT
Analyte
1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene
Analyte (CAS Number)
Vinyl chloride (75-01-4) 1,1-Dichloroethene (75-35-4) 2-Butanone (78-93-3) Chloroform (67-66-3) 1,2-Dichloroethane (107-06-2) Carbon tetrachloride (56-23-5) Benzene (71-43-2) Trichloroethene (79-01-6) Tetrachloroethene (127-18-4) Chlorobenzene (108-90-7) 1,4-Dichlorobenzene (106-46-7)
Surrogates
Result g/L
Analyte Qualifiers %Recovery
%Recovery Limits
47.3
94.7
48.5
96.9
48.8
97.6
Targets
86-117 85-113 73-115
Result g/L
U U 5.87E7 U U U U U U U U
Analyte Qualifiers
Reporting Limit
100,000 100,000 2.50E6 100,000 100,000 100,000 100,000 100,000 100,000 100,000 100,000
Dilution
50000 "
500000 50000
" " " " " " "
Prepared Analyzed
03/06/18 " "
03/06/18 " "
Prepared 03/06/18
" " " " " " " " " "
Analyzed 03/06/18
" 03/06/18 03/06/18
" " " " " " "
Project #: 18RCRA019
Report Name: Page 25 of 58
Lab ID: 1711006-09
Batch: B8B2801 Sample Type: Liquid
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Metals by EPA Method 6010D - ICP
Date Collected: 11/14/17 Sample Vol: 50ml
Station ID: Tote A
Sample Qualifiers:
Analyte (CAS Number)
Arsenic (7440-38-2) Barium (7440-39-3) Cadmium (7440-43-9) Chromium (7440-47-3) Lead (7439-92-1) Selenium (7782-49-2) Silver (7440-22-4)
Result g/L
U 34.6
U U U U U
Targets
Analyte Qualifiers
Reporting Limit
100 10.0 5.0 10.0 30.0 100 10.0
Dilution
1 " " " " " "
Prepared 02/28/18
" " " " " "
Analyzed 03/07/18
" " " " " "
Project #: 18RCRA019
Report Name: Page 26 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
TCLP Volatiles by EPA Method 1311/8260C - GC/MS
Lab ID: 1711006-09
Batch: B8C1304 Sample Type: Liquid Batch Matrix: Liquid
Date Collected: 11/14/17 Sample Vol: 5ml
TCLP Prepared: 2/21/18
Station ID: Tote A
Sample Qualifiers: HTT
Analyte
1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene
Analyte (CAS Number)
Vinyl chloride (75-01-4) 1,1-Dichloroethene (75-35-4) 2-Butanone (78-93-3) Chloroform (67-66-3) 1,2-Dichloroethane (107-06-2) Carbon tetrachloride (56-23-5) Benzene (71-43-2) Trichloroethene (79-01-6) Tetrachloroethene (127-18-4) Chlorobenzene (108-90-7) 1,4-Dichlorobenzene (106-46-7)
Surrogates
Result g/L
Analyte Qualifiers %Recovery
%Recovery Limits
47.4
94.9
44.5
88.9
47.3
94.5
Targets
86-117 85-113 73-115
Result g/L
U U 77.4 U U U U U 22.8 U U
Analyte Qualifiers
Reporting Limit
20.0 20.0 50.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0 20.0
Dilution
10 " " " " " " " " " "
Prepared Analyzed
03/05/18 " "
03/05/18 " "
Prepared 03/05/18
" " " " " " " " " "
Analyzed 03/05/18
" " " " " " " " " "
Project #: 18RCRA019
Report Name: Page 27 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Metals by EPA Method 7470A/7471B - CVAAS
Lab ID: 1711006-09RE1
Batch: B8C0801 Sample Type: Liquid
Date Collected: 11/14/17 Sample Vol: 0.2ml
Station ID: Tote A
Sample Qualifiers: HTS
Analyte (CAS Number)
Mercury (7439-97-6)
Result g/L
U
Targets
Analyte Qualifiers
Reporting Limit
25.0
Dilution 1
Prepared Analyzed 03/08/18 03/08/18
Project #: 18RCRA019
Report Name: Page 28 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Lab ID: 1711006-10
Batch: B8C1303 Sample Type: Liquid
Volatiles by EPA Method 8260C - GC/MS
Date Collected: 11/08/17 Sample Vol: 5ml
Station ID: Sta A
Sample Qualifiers: HTS
Analyte
1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene
Analyte (CAS Number)
Dichlorodifluoromethane (75-71-8) Chloromethane (74-87-3) Vinyl chloride (75-01-4) Bromomethane (74-83-9) Chloroethane (75-00-3) Trichlorofluoromethane (75-69-4) 1,1-Dichloroethene (75-35-4) Carbon disulfide (75-15-0) 1,1,2-Trichloro-1,2,2-trifluoroethane (76-13-1) Acetone (67-64-1) Methylene chloride (75-09-2) Methyl acetate (79-20-9) trans-1,2-Dichloroethene (156-60-5) cis-1,2-Dichloroethene (156-59-2) Methyl tert-butyl ether (1634-04-4) 1,1-Dichloroethane (75-34-3) 2-Butanone (78-93-3) Chloroform (67-66-3) 1,2-Dichloroethane (107-06-2) 1,1,1-Trichloroethane (71-55-6) Cyclohexane (110-82-7) Carbon tetrachloride (56-23-5) Benzene (71-43-2) Trichloroethene (79-01-6) Methylcyclohexane (108-87-2) 1,2-Dichloropropane (78-87-5) Bromodichloromethane (75-27-4)
Project #: 18RCRA019
Surrogates
Result g/L
Analyte Qualifiers %Recovery
%Recovery Limits
49.5
99.1
49.5
99.0
49.6
99.2
Targets
86-117 85-113 73-115
Result g/L
U U U U U U U U U U U U U U U U U U U U U U U U U U U
Analyte Qualifiers
Reporting Limit
5.0 5.0 2.0 5.0 2.0 2.0 2.0 2.0 2.0 10.0 2.0 2.0 2.0 2.0 2.0 2.0 5.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0
Dilution
1 " " " " " " " " " " " " " " " " " " " " " " " " " "
Prepared Analyzed
03/02/18 " "
03/02/18 " "
Prepared 03/02/18
" " " " " " " " " " " " " " " " " " " " " " " " " "
Analyzed 03/02/18
" " " " " " " " " " " " " " " " " " " " " " " " " "
Report Name: Page 29 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Lab ID: 1711006-10
Batch: B8C1303 Sample Type: Liquid
Volatiles by EPA Method 8260C - GC/MS
Date Collected: 11/08/17 Sample Vol: 5ml
Station ID: Sta A
Sample Qualifiers: HTS
Targets (Continued)
Analyte (CAS Number)
Result g/L
cis-1,3-Dichloropropene (10061-01-5)
U
trans-1,3-Dichloropropene (10061-02-6)
U
1,1,2-Trichloroethane (79-00-5)
U
Dibromochloromethane (124-48-1)
U
Bromoform (75-25-2)
U
4-Methyl-2-pentanone (108-10-1)
U
Toluene (108-88-3)
U
Tetrachloroethene (127-18-4)
U
2-Hexanone (591-78-6)
U
1,2-Dibromoethane (106-93-4)
U
Chlorobenzene (108-90-7)
U
Ethylbenzene (100-41-4)
U
meta-/para-Xylene (na)
U
ortho-Xylene (95-47-6)
U
Styrene (100-42-5)
U
Isopropylbenzene (98-82-8)
U
1,1,2,2-Tetrachloroethane (79-34-5)
U
1,3-Dichlorobenzene (541-73-1)
U
1,4-Dichlorobenzene (106-46-7)
U
1,2-Dichlorobenzene (95-50-1)
U
1,2-Dibromo-3-chloropropane (96-12-8)
U
1,2,4-Trichlorobenzene (120-82-1)
U
This sample was received at pH 5. If biological activity is present, then aromatics may be biased low.
Analyte Qualifiers
Reporting Limit
2.0 2.0 2.0 2.0 2.0 5.0 2.0 2.0 5.0 2.0 2.0 2.0 4.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 5.0 5.0
Dilution
1 " " " " " " " " " " " " " " " " " " " " "
Prepared 03/02/18
" " " " " " " " " " " " " " " " " " " " "
Analyzed 03/02/18
" " " " " " " " " " " " " " " " " " " " "
Project #: 18RCRA019
Report Name: Page 30 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Batch: B8A0501
Ignitability by EPA Method 1020B
Laboratory ID
1711006-01 1711006-02 1711006-03 1711006-04 1711006-05 1711006-06 1711006-07 1711006-08 1711006-09
Station ID
C25276D R25036 Tank 15 Tank 19 Tank B Tank 21 Tote 6 Drum 10 Tote A
Result
No Flash @ 60 C No Flash @ 60 C No Flash @ 60 C No Flash @ 60 C No Flash @ 60 C No Flash @ 60 C No Flash @ 60 C
Flash @ 28 C No Flash @ 60 C
MJF
Project #: 18RCRA019
Report Name: Page 31 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Volatiles by EPA Method 8260C - GC/MS - Quality Control
Batch: B8C1303
ANALYTE 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene
ANALYTE Dichlorodifluoromethane Chloromethane Vinyl chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Carbon disulfide 1,1,2-Trichloro-1,2,2-trifluoroethane Acetone Methylene chloride Methyl acetate trans-1,2-Dichloroethene cis-1,2-Dichloroethene Methyl tert-butyl ether 1,1-Dichloroethane 2-Butanone Chloroform 1,2-Dichloroethane 1,1,1-Trichloroethane Cyclohexane Carbon tetrachloride Benzene Trichloroethene Methylcyclohexane
Project #: 18RCRA019
Blank (B8C1303-BLK1)
Prepared: 3/2/2018 Analyzed: 3/2/2018
Result g/L
46.9 46.0 46.4
Surrogates
Analyte Qualifier
Spike Level
50.0 50.0 50.0
Result g/L
U U U U U U U U U U U U U U U U U U U U U U U U U
Targets
Analyte Reporting Qualifiers Limit
5.0 5.0 2.0 5.0 2.0 2.0 2.0 2.0 2.0 10.0 2.0 2.0 2.0 2.0 2.0 2.0 5.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0
Sample Type: Liquid
%REC
93.8 92.1 92.9
%REC Limits
86-117 85-113 73-115
Report Name: Page 32 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Volatiles by EPA Method 8260C - GC/MS - Quality Control
Batch: B8C1303
ANALYTE 1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Dibromochloromethane Bromoform 4-Methyl-2-pentanone Toluene Tetrachloroethene 2-Hexanone 1,2-Dibromoethane Chlorobenzene Ethylbenzene meta-/para-Xylene ortho-Xylene Styrene Isopropylbenzene 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene 1,2-Dibromo-3-chloropropane 1,2,4-Trichlorobenzene
Blank (B8C1303-BLK1)
Prepared: 3/2/2018 Analyzed: 3/2/2018
Result g/L
U U U U U U U U U U U U U U U U U U U U U U U U
Targets (Continued)
Analyte Reporting Qualifiers Limit
2.0 2.0 2.0 2.0 2.0 2.0 2.0 5.0 2.0 2.0 5.0 2.0 2.0 2.0 4.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 5.0 5.0
Sample Type: Liquid
Project #: 18RCRA019
Report Name: Page 33 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Volatiles by EPA Method 8260C - GC/MS - Quality Control
Batch: B8C1303
ANALYTE 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene
ANALYTE Dichlorodifluoromethane Chloromethane Vinyl chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Carbon disulfide 1,1,2-Trichloro-1,2,2-trifluoroethane Acetone Methylene chloride Methyl acetate trans-1,2-Dichloroethene cis-1,2-Dichloroethene Methyl tert-butyl ether 1,1-Dichloroethane 2-Butanone Chloroform 1,2-Dichloroethane 1,1,1-Trichloroethane Cyclohexane Carbon tetrachloride Benzene Trichloroethene Methylcyclohexane
Project #: 18RCRA019
LCS (B8C1303-BS1)
Prepared: 3/2/2018 Analyzed: 3/2/2018
Result g/L
49.4 46.7 49.4
Surrogates
Analyte Qualifier
Spike Level
50.0 50.0 50.0
Result g/L
49.7 51.4 49.8 53.8 48.1 47.5 48.7 50.8 47.2 35.1 48.0 50.4 47.1 48.5 50.2 49.8 45.4 47.4 47.3 49.0 50.6 46.0 46.8 45.3 48.6
Targets
Analyte Reporting Spike Qualifiers Limit Level
5.0
50.0
5.0
50.0
2.0
50.0
5.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
10.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
5.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
Sample Type: Liquid
%REC
98.8 93.4 98.8
%REC Limits
86-117 85-113 73-115
%REC %REC Limits
99.5 69-132 103 73-130 99.6 76-130 108 75-129 96.2 75-121 95.0 79-130 97.5 76-127 102 74-122 94.3 79-126 70.1 44-140 96.0 79-122 101 78-118 94.3 78-123 97.1 80-120 100 78-124 99.5 80-122 90.8 71-127 94.7 81-121 94.6 80-121 97.9 80-120 101 77-120 92.0 78-121 93.6 81-119 90.5 80-120 97.2 79-122
Report Name: Page 34 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Volatiles by EPA Method 8260C - GC/MS - Quality Control
Batch: B8C1303
Sample Type: Liquid
LCS (B8C1303-BS1)
Prepared: 3/2/2018 Analyzed: 3/2/2018
ANALYTE
1,2-Dichloropropane Bromodichloromethane cis-1,3-Dichloropropene trans-1,3-Dichloropropene 1,1,2-Trichloroethane Dibromochloromethane Bromoform 4-Methyl-2-pentanone Toluene Tetrachloroethene 2-Hexanone 1,2-Dibromoethane Chlorobenzene Ethylbenzene meta-/para-Xylene ortho-Xylene Styrene Isopropylbenzene 1,1,2,2-Tetrachloroethane 1,3-Dichlorobenzene 1,4-Dichlorobenzene 1,2-Dichlorobenzene 1,2-Dibromo-3-chloropropane 1,2,4-Trichlorobenzene
Result g/L
51.1 49.8 50.8 53.8 50.3 49.5 51.2 52.0 45.3 43.1 54.7 46.8 43.7 45.5 91.3 46.3 47.7 48.8 50.0 45.2 45.0 45.3 49.8 47.0
Targets (Continued)
Analyte Reporting Spike Qualifiers Limit Level
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
5.0
50.0
2.0
50.0
2.0
50.0
5.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
4.0
100
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
5.0
50.0
5.0
50.0
%REC
102 99.7 102 108 101 99.0 102 104 90.6 86.2 109 93.6 87.4 91.0 91.3 92.6 95.4 97.6 99.9 90.4 90.0 90.6 99.7 93.9
%REC Limits
81-121 80-121 79-119 78-119 80-120 80-118 79-119 77-121 81-118 80-120 77-122 81-118 81-118 80-118 81-117 81-118 79-118 74-124 79-119 81-118 80-117 79-119 77-123 78-128
TCLP Volatiles by EPA Method 1311/8260C - GC/MS - Quality Control
Project #: 18RCRA019
Report Name: Page 35 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
TCLP Volatiles by EPA Method 1311/8260C - GC/MS - Quality Control
Batch: B8C1304
ANALYTE 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene
ANALYTE Vinyl chloride 1,1-Dichloroethene 2-Butanone Chloroform 1,2-Dichloroethane Carbon tetrachloride Benzene Trichloroethene Tetrachloroethene Chlorobenzene 1,4-Dichlorobenzene
Blank (B8C1304-BLK1)
Prepared: 3/2/2018 Analyzed: 3/2/2018
Result g/L
47.6 46.3 46.6
Surrogates
Analyte Qualifier
Spike Level
50.0 50.0 50.0
Result g/L
U U U U U U U U U U U
Targets
Analyte Reporting Qualifiers Limit
2.0 2.0 5.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0
Sample Type: Liquid
%REC
95.1 92.7 93.3
%REC Limits
86-117 85-113 73-115
Project #: 18RCRA019
Report Name: Page 36 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
TCLP Volatiles by EPA Method 1311/8260C - GC/MS - Quality Control
Batch: B8C1304
ANALYTE 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene
ANALYTE Vinyl chloride 1,1-Dichloroethene 2-Butanone Chloroform 1,2-Dichloroethane Carbon tetrachloride Benzene Trichloroethene Tetrachloroethene Chlorobenzene 1,4-Dichlorobenzene
Blank (B8C1304-BLK2)
Prepared: 3/5/2018 Analyzed: 3/5/2018
Result g/L
46.4 45.8 46.0
Surrogates
Analyte Qualifier
Spike Level
50.0 50.0 50.0
Result g/L
U U U U U U U U U U U
Targets
Analyte Reporting Qualifiers Limit
2.0 2.0 5.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0
Sample Type: Liquid
%REC
92.8 91.7 92.0
%REC Limits
86-117 85-113 73-115
Project #: 18RCRA019
Report Name: Page 37 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
TCLP Volatiles by EPA Method 1311/8260C - GC/MS - Quality Control
Batch: B8C1304
ANALYTE 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene
ANALYTE Vinyl chloride 1,1-Dichloroethene 2-Butanone Chloroform 1,2-Dichloroethane Carbon tetrachloride Benzene Trichloroethene Tetrachloroethene Chlorobenzene 1,4-Dichlorobenzene
Blank (B8C1304-BLK3)
Prepared: 3/6/2018 Analyzed: 3/6/2018
Result g/L
47.5 48.4 48.8
Surrogates
Analyte Qualifier
Spike Level
50.0 50.0 50.0
Result g/L
U U U U U U U U U U U
Targets
Analyte Reporting Qualifiers Limit
2.0 2.0 5.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0
Sample Type: Liquid
%REC
94.9 96.7 97.6
%REC Limits
86-117 85-113 73-115
Project #: 18RCRA019
Report Name: Page 38 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
TCLP Volatiles by EPA Method 1311/8260C - GC/MS - Quality Control
Batch: B8C1304
ANALYTE 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene
ANALYTE Vinyl chloride 1,1-Dichloroethene 2-Butanone Chloroform 1,2-Dichloroethane Carbon tetrachloride Benzene Trichloroethene Tetrachloroethene Chlorobenzene 1,4-Dichlorobenzene
Blank (B8C1304-BLK4)
Prepared: 3/7/2018 Analyzed: 3/7/2018
Result g/L
45.0 45.7 45.6
Surrogates
Analyte Qualifier
Spike Level
50.0 50.0 50.0
Result g/L
U U U U U U U U U U U
Targets
Analyte Reporting Qualifiers Limit
2.0 2.0 5.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0 2.0
Sample Type: Liquid
%REC
89.9 91.4 91.2
%REC Limits
86-117 85-113 73-115
Project #: 18RCRA019
Report Name: Page 39 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
TCLP Volatiles by EPA Method 1311/8260C - GC/MS - Quality Control
Batch: B8C1304
ANALYTE 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene
ANALYTE Vinyl chloride 1,1-Dichloroethene 2-Butanone Chloroform 1,2-Dichloroethane Carbon tetrachloride Benzene Trichloroethene Tetrachloroethene Chlorobenzene 1,4-Dichlorobenzene
LCS (B8C1304-BS1)
Prepared: 3/2/2018 Analyzed: 3/2/2018
Result g/L
50.1 47.0 49.6
Surrogates
Analyte Qualifier
Spike Level
50.0 50.0 50.0
Result g/L
51.2 49.8 46.2 48.4 48.5 46.2 47.8 45.9 43.7 44.7 45.8
Targets
Analyte Reporting Spike Qualifiers Limit Level
2.0
50.0
2.0
50.0
5.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
Sample Type: Liquid
%REC
100 94.0 99.3
%REC Limits
86-117 85-113 73-115
%REC %REC Limits
102 76-130 99.7 76-127 92.4 71-127 96.7 81-121 97.0 80-121 92.5 78-121 95.6 81-119 91.8 80-120 87.4 80-120 89.3 81-118 91.6 80-117
Project #: 18RCRA019
Report Name: Page 40 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
TCLP Volatiles by EPA Method 1311/8260C - GC/MS - Quality Control
Batch: B8C1304
ANALYTE 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene
ANALYTE Vinyl chloride 1,1-Dichloroethene 2-Butanone Chloroform 1,2-Dichloroethane Carbon tetrachloride Benzene Trichloroethene Tetrachloroethene Chlorobenzene 1,4-Dichlorobenzene
LCS (B8C1304-BS2)
Prepared: 3/5/2018 Analyzed: 3/5/2018
Result g/L
47.9 47.9 47.9
Surrogates
Analyte Qualifier
Spike Level
50.0 50.0 50.0
Result g/L
49.6 48.7 42.5 47.5 46.9 45.5 47.2 46.2 43.0 44.3 45.0
Targets
Analyte Reporting Spike Qualifiers Limit Level
2.0
50.0
2.0
50.0
5.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
Sample Type: Liquid
%REC
95.8 95.8 95.9
%REC Limits
86-117 85-113 73-115
%REC %REC Limits
99.3 76-130 97.4 76-127 85.0 71-127 95.0 81-121 93.8 80-121 91.0 78-121 94.5 81-119 92.5 80-120 86.0 80-120 88.6 81-118 90.0 80-117
Project #: 18RCRA019
Report Name: Page 41 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
TCLP Volatiles by EPA Method 1311/8260C - GC/MS - Quality Control
Batch: B8C1304
ANALYTE 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene
ANALYTE Vinyl chloride 1,1-Dichloroethene 2-Butanone Chloroform 1,2-Dichloroethane Carbon tetrachloride Benzene Trichloroethene Tetrachloroethene Chlorobenzene 1,4-Dichlorobenzene
LCS (B8C1304-BS3)
Prepared: 3/6/2018 Analyzed: 3/6/2018
Result g/L
44.9 46.8 47.0
Surrogates
Analyte Qualifier
Spike Level
50.0 50.0 50.0
Result g/L
50.0 50.9 43.6 49.0 46.9 47.0 49.0 49.9 45.9 46.9 47.9
Targets
Analyte Reporting Spike Qualifiers Limit Level
2.0
50.0
2.0
50.0
5.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
Sample Type: Liquid
%REC
89.8 93.7 94.0
%REC Limits
86-117 85-113 73-115
%REC %REC Limits
100 76-130 102 76-127 87.3 71-127 97.9 81-121 93.8 80-121 94.1 78-121 97.9 81-119 99.8 80-120 91.7 80-120 93.8 81-118 95.8 80-117
Project #: 18RCRA019
Report Name: Page 42 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
TCLP Volatiles by EPA Method 1311/8260C - GC/MS - Quality Control
Batch: B8C1304
ANALYTE 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene
ANALYTE Vinyl chloride 1,1-Dichloroethene 2-Butanone Chloroform 1,2-Dichloroethane Carbon tetrachloride Benzene Trichloroethene Tetrachloroethene Chlorobenzene 1,4-Dichlorobenzene
LCS (B8C1304-BS4)
Prepared: 3/7/2018 Analyzed: 3/7/2018
Result g/L
45.5 47.6 48.0
Surrogates
Analyte Qualifier
Spike Level
50.0 50.0 50.0
Result g/L
50.3 50.9 43.5 48.7 46.6 46.6 48.7 49.1 45.0 46.5 47.5
Targets
Analyte Reporting Spike Qualifiers Limit Level
2.0
50.0
2.0
50.0
5.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
2.0
50.0
Sample Type: Liquid
%REC
91.0 95.1 95.9
%REC Limits
86-117 85-113 73-115
%REC %REC Limits
101 76-130 102 76-127 87.0 71-127 97.4 81-121 93.1 80-121 93.1 78-121 97.5 81-119 98.2 80-120 90.1 80-120 93.1 81-118 95.0 80-117
Project #: 18RCRA019
Report Name: Page 43 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
TCLP Volatiles by EPA Method 1311/8260C - GC/MS - Quality Control
Batch: B8C1304
Source: 1711006-06
ANALYTE 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene
ANALYTE Vinyl chloride 1,1-Dichloroethene 2-Butanone Chloroform 1,2-Dichloroethane Carbon tetrachloride Benzene Trichloroethene Tetrachloroethene Chlorobenzene 1,4-Dichlorobenzene
Sample Type: Liquid
Matrix Spike (B8C1304-MS1)
Prepared: 3/7/2018 Analyzed: 3/7/2018
Result g/L
47.2 48.7 49.2
Surrogates
Analyte Qualifier
Spike Level
50.0 50.0 50.0
%REC
94.4 97.4 98.4
%REC Limits
86-117 85-113 73-115
Result g/L
9,990 10,100 20,700 9,760 9,430 9,450 10,000 10,100 9,120 9,460 9,650
Targets
Analyte Reporting Spike Qualifiers Limit Level
400 400 1,000 400 400 400 400 400 400 400 400
10,000 10,000 10,000 10,000 10,000 10,000 10,000 10,000 10,000 10,000 10,000
Source Result
10,800
106 62.0
%REC
99.9 101 99.3 97.6 94.3 94.5 99.0 101 90.6 94.6 96.5
%REC Limits
75-123 72-134 51-139 75-125 73-126 74-123 79-122 79-126 80-115 82-121 79-116
Project #: 18RCRA019
Report Name: Page 44 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
TCLP Volatiles by EPA Method 1311/8260C - GC/MS - Quality Control
Batch: B8C1304
Sample Type: Liquid
Source: 1711006-06
ANALYTE 1,2-Dichloroethane-d4 Toluene-d8 4-Bromofluorobenzene
Matrix Spike Dup (B8C1304-MSD1)
Prepared: 3/7/2018 Analyzed: 3/7/2018
Result g/L
42.9 44.9 45.1
Surrogates
Analyte Qualifier
Spike Level
50.0 50.0 50.0
%REC
85.8 # 89.9 90.3
%REC Limits
86-117 85-113 73-115
ANALYTE
Vinyl chloride 1,1-Dichloroethene 2-Butanone Chloroform 1,2-Dichloroethane Carbon tetrachloride Benzene Trichloroethene Tetrachloroethene Chlorobenzene 1,4-Dichlorobenzene
Result g/L
9,810 9,960 20,300 9,630 9,210 9,320 9,910 9,960 9,060 9,280 9,510
Targets
Analyte Reporting Spike Qualifiers Limit Level
400 400 1,000 400 400 400 400 400 400 400 400
10,000 10,000 10,000 10,000 10,000 10,000 10,000 10,000 10,000 10,000 10,000
Source Result
10,800
106 62.0
%REC
98.1 99.6 95.6 96.3 92.1 93.2 98.0 99.6 90.0 92.8 95.1
%REC
RPD
Limits RPD Limit
75-123 1.82 16 72-134 1.73 21 51-139 1.80 21 75-125 1.38 13 73-126 2.34 13 74-123 1.32 14 79-122 1.02 16 79-126 1.10 14 80-115 0.68 12 82-121 1.94 10 79-116 1.46 11
Metals by EPA Method 6010D - ICP - Quality Control
Project #: 18RCRA019
Report Name: Page 45 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Metals by EPA Method 6010D - ICP - Quality Control
Batch: B8B2801
ANALYTE Arsenic Barium Cadmium Chromium Lead Selenium Silver
Blank (B8B2801-BLK1)
Prepared: 2/28/2018 Analyzed: 3/7/2018
Result g/L
Targets
Analyte Reporting Qualifiers Limit
U
100
U
10.0
U
5.0
U
10.0
U
30.0
U
100
U
10.0
Sample Type: Liquid
Project #: 18RCRA019
Report Name: Page 46 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Metals by EPA Method 6010D - ICP - Quality Control
Batch: B8B2801
ANALYTE Arsenic Barium Cadmium Chromium Lead Selenium Silver
LCS (B8B2801-BS1)
Prepared: 2/28/2018 Analyzed: 3/7/2018
Result g/L
2,020 2,050 51.2 408 405 1,010 51.3
Targets
Analyte Reporting Spike Qualifiers Limit Level
100
2,000
10.0 2,000
5.0
50.0
10.0
400
30.0
400
100
1,000
10.0
50.0
Sample Type: Liquid
%REC %REC Limits
101 75-125 103 75-125 102 75-125 102 75-125 101 75-125 101 75-125 103 75-125
Project #: 18RCRA019
Report Name: Page 47 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Metals by EPA Method 6010D - ICP - Quality Control
Batch: B8B2801
Source: 1711006-06
ANALYTE Arsenic Barium Cadmium Chromium Lead Selenium Silver
Sample Type: Liquid
Matrix Spike (B8B2801-MS1)
Prepared: 2/28/2018 Analyzed: 3/7/2018
Result g/L
1,880 2,370 59.7 708 472 2,180 80.5
Targets
Analyte Reporting Spike Qualifiers Limit Level
100
2,000
10.0 2,000
5.0
50.0
10.0
400
30.0
400
100
1,000
10.0
50.0
Source Result
310
242 33.0 463 40.0
%REC %REC Limits
93.8 103 119 116 110 171 # 81.0
75-125 75-125 75-125 75-125 75-125 75-125 75-125
Project #: 18RCRA019
Report Name: Page 48 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Metals by EPA Method 6010D - ICP - Quality Control
Batch: B8B2801
Sample Type: Liquid
Source: 1711006-06
Matrix Spike Dup (B8B2801-MSD1)
Prepared: 2/28/2018 Analyzed: 3/7/2018
ANALYTE
Arsenic Barium Cadmium Chromium Lead Selenium Silver
Result g/L
1,970 2,430 61.5 714 489 2,210 80.4
Targets
Analyte Reporting Spike Qualifiers Limit Level
100
2,000
10.0 2,000
5.0
50.0
10.0
400
30.0
400
100
1,000
10.0
50.0
Source Result
310
242 33.0 463 40.0
%REC
RPD
%REC Limits RPD Limit
98.6 75-125 5.00 20 106 75-125 2.56 20 123 75-125 3.03 20 118 75-125 0.95 20 114 75-125 3.58 20 175 # 75-125 1.52 20 80.8 75-125 0.14 20
Metals by EPA Method 7470A/7471B - CVAAS - Quality Control
Project #: 18RCRA019
Report Name: Page 49 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Metals by EPA Method 7470A/7471B - CVAAS - Quality Control
Batch: B8C0801
ANALYTE Mercury
Blank (B8C0801-BLK1)
Prepared: 3/8/2018 Analyzed: 3/8/2018
Result g/L
Targets
Analyte Reporting Qualifiers Limit
U
0.200
Sample Type: Liquid
Project #: 18RCRA019
Report Name: Page 50 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Metals by EPA Method 7470A/7471B - CVAAS - Quality Control
Batch: B8C0801
ANALYTE Mercury
LCS (B8C0801-BS1)
Prepared: 3/8/2018 Analyzed: 3/8/2018
Result g/L
1.98
Targets
Analyte Reporting Spike Qualifiers Limit Level
0.200 2.00
Sample Type: Liquid
%REC %REC Limits
99.2 85-115
Project #: 18RCRA019
Report Name: Page 51 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Metals by EPA Method 7470A/7471B - CVAAS - Quality Control
Batch: B8C0801 Source: 1711006-06RE1
ANALYTE Mercury
Sample Type: Liquid
Matrix Spike (B8C0801-MS1)
Prepared: 3/8/2018 Analyzed: 3/8/2018
Result g/L
275
Targets
Analyte Reporting Spike Qualifiers Limit Level
25.0
250
Source Result
54.0
%REC 88.2
%REC Limits
75-125
Project #: 18RCRA019
Report Name: Page 52 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Metals by EPA Method 7470A/7471B - CVAAS - Quality Control
Batch: B8C0801
Sample Type: Liquid
Source: 1711006-06RE1
Matrix Spike Dup (B8C0801-MSD1)
Prepared: 3/8/2018 Analyzed: 3/8/2018
ANALYTE Mercury
Result g/L
269
Targets
Analyte Reporting Spike Qualifiers Limit Level
25.0
250
Source Result
54.0
%REC 86.0
%REC Limits
75-125
RPD RPD Limit
2.02 20
Ignitability by EPA Method 1020B - Quality Control
Project #: 18RCRA019
Report Name: Page 53 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Ignitability by EPA Method 1020B - Quality Control
Batch: B8A0501 Source: 1711006-06
ANALYTE No Flash @
Duplicate (B8A0501-DUP1)
Prepared: 1/5/2018 Analyzed: 1/5/2018
Result C
60
Targets
Analyte Reporting Spike Qualifiers Limit Level
Source Result
60
Sample Type: Liquid
RPD RPD Limit
0.00 20
Project #: 18RCRA019
Report Name: Page 54 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
SURROGATE SUMMARY REPORT VOA 8260C Routine List
Liquid
LAB NUMBER 1711006-10
B8C1303-BLK1 B8C1303-BS1
1,2-DCE-d4 99.1 93.8 98.8
1,2-DCE-d4 = 1,2-Dichloroethane-d4
TOL-d8
= Toluene-d8
4-BFB
= 4-Bromofluorobenzene
TOL-d8
99.0 92.1 93.4
QC LIMITS 86 - 117 85 - 113 73 - 115
LAB NUMBER 1711006-01 1711006-02 1711006-03 1711006-04 1711006-05 1711006-06 1711006-07 1711006-08 1711006-09
B8C1304-BLK1 B8C1304-BLK2 B8C1304-BLK3 B8C1304-BLK4 B8C1304-BS1 B8C1304-BS2 B8C1304-BS3 B8C1304-BS4 B8C1304-MS1 B8C1304-MSD1
VOA TCLP 1311/8260C Liquid
1,2-DCE-d4 93.9 97.2 88.0 92.8 91.4 89.7 87.7 94.7 94.9 95.1 92.8 94.9 89.9 100 95.8 89.8 91.0 94.4 85.8 #
TOL-d8 92.6 94.4 91.4 92.8 93.5 92.6 90.5 96.9 88.9 92.7 91.7 96.7 91.4 94.0 95.8 93.7 95.1 97.4 89.9
4-BFB 99.2 92.9 98.8
4-BFB 92.9 96.9 92.2 95.6 96.2 93.8 92.9 97.6 94.5 93.3 92.0 97.6 91.2 99.3 95.9 94.0 95.9 98.4 90.3
Project #: 18RCRA019
Report Name: Page 55 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
SURROGATE SUMMARY REPORT VOA TCLP 1311/8260C
1,2-DCE-d4 = 1,2-Dichloroethane-d4
TOL-d8
= Toluene-d8
4-BFB
= 4-Bromofluorobenzene
QC LIMITS
86 - 117 85 - 113 73 - 115
Project #: 18RCRA019
Report Name: Page 56 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
Notes and Definitions
K
The identification of the analyte is acceptable; the reported value may be biased high. The actual value is
expected to be less than the reported value.
J
The identification of the analyte is acceptable; the reported value is an estimate.
B
Blank Related - The concentration found in the sample was less than 10X the concentration found in the
associated extraction, digestion and/or analysis blank. Presence in the sample is therefore suspect.
A
This sample was extracted at a single acid pH.
HTS
Sample was prepared and/or analyzed past recommended holding time. Concentrations should be
considered minimum values.
ABN
Acid Base Neutrals (Semivolatile Compounds)
AES
Atomic Emission Spectrometer
BS
Blank Spike
CVAA
Cold Vapor Atomic Absorption
DCB
Decachlorobiphenyl
ECD
Electron Capture Detector
GC
Gas Chromatograph
ICP
Inductively Coupled Plasma
ISTD
Internal Standard
LCS
Laboratory Control Sample
MS
Mass Spectrometer
MS/MSD Matrix Spike/Matrix Spike Duplicate
NA
Not Applicable
NPD
Nitrogen Phosphorous Detector
NR
Not Reported
PCB
Polychlorinatedbiphenyl
Project #: 18RCRA019
Report Name: Page 57 of 58
Environmental Protection Agency
Region 6 Laboratory
10625 Fallstone Road, Houston, TX 77099
Phone:(281)983-2100
Fax:(281)983-2248
RL
Reporting Limit
RT
Retention Time
RPD
Relative Percent Difference
TCLP
Toxicity Characteristic Leaching Procedure
TCMX
Tetrachloro-meta-xylene
U
Undetected
VOA
Volatile Organic Analysis
#
Out of QC limits
>LR
The result was greater than the linear range.
Initial pressure in air analyses is the pressure at which the canister was received in psia (pounds per square inch absolute pressure).
The pH reported for Volatile liquid samples was tested using a 0-14 pH indicator strip for the purpose of verifying chemical preservation.
The statistical software used for the reporting of toxicity data is ToxCalc 5.0.32, Environmental Toxicity Data Analysis System 1994-2007 Tidepool Scientific Software.
Project #: 18RCRA019
Report Name: Page 58 of 58