Document RJo1kx4B7NgDBpLp2jJm061DV

w r GRACE & oo. RESEARCH DIVISION Telephone 3 C' - 531-57 1! HEW POSTAL ADDRESS: 7379 ROUTE 32 COLUMBIA, M A fi Y L A N 2 l 04H CONSOLIDATED MONTHLY REPORT MAY 1973 This Consolidated Monthly Summary contains the technical information for May 1973. Because of the highly confidential nature of its contents, circulation is limited. Those receiving copies are requested to limit access to only those members within their organi zation who have a real need-to-know. GRACE CONFIDENTIAL 15208068 MONTHLY REPORT FOR MAY 1973 CONSOLIDATED EDITION ;'iie 1, NOD iC GO CUTS.IDE U.S. This report contains information on the following activities at the Washington Research Center: PROJECT TITLE PROJECT NO. DAREX Desalting Plant Services - WRC Support Mono-Kote Product Improvement Davison Cracking Catalyst New Construction Products Catalytic Ozonation for NH3 Removal From Waste Water Possible Specific Uses of Fully Delaminated Vermicullte or Biotite Auto Exhaust Catalyst Monolithic Catalyst Support Monolith Cement Air Pollution Control - Alumina Sphere Process 2451 2659 2419 2680 2677 2680 2302 2304 22 64 2212 PAGE 1 2 -2 3 3 4 4a 4c 4c 4d HYPOLTM Type FHP HYPOLTM Type CHC Emulsion Breakers Epoxy Hardeners New Epoxy Resins Printable Water-Based Release Coatings Wet-Strength Agents Floerger Polyacrylamides Polystyrene Bead-Board G irinkage Fire-Resistant Bag Study Intumescent Formulation Study Alrmold Support Golding Brothers Consultation Fire Retardancy - Marco Polyester Resins Disposable Dishes for Microwave and Thermal Ovens 1432 1438 1656 1404 1408 1435 1441 1440 1437 1427 1656 1561 1560 1407 1332 5 6 6 7 7 8 9 9 10 10 10 11 11 11 12 Photopolymer Wear Coating For Resilient Flooring Dry-Film Photoresist Solder Photoresist Offset Lithographic Plate Polyene Development LETTERFLEX - GLASS Project 1343 1372 1387 1373 1340 1385 13 14 14 17 17 17a 15208069 I CONSOL II .0 June 1, 1973 PROJECT TITLE PROJECT NO. PAGE Adapted p.umeri Microbes -- CHRGN-X Dal ry Methane Inhibition nzyrr.atic Treatment of Feedlot Bloat cours preventative Poultry Growth Promoter FDA Consultant 4640 4 647 4649 4650 4634 4661 l8 18 18 19 19 19 19 Foam Studies - Forgipac Support 3427 Phillips Magnapore5' Silica Process Development (Davison) 24l6 Industrial Catalyst Technical Service 2838 20 20 ' 21 Research Division Activity Report Appendix Co M 15208070 l- 2- June 1, 1973 v :-K.:~E PRODUCT IMPROVEMENT (Project ?659) The emphasis of this month's activity has not changed from last month. Characterization of Mono-Kote raw materials, vermiculite end gypcum, from different sources with the view of determining their properties relating to the shrink-crack problem is continu ing. Effort has been made to relate compressive strength, flexural strength, and elasticity of ZOU mortars to shrink-crack. These show little relation to the problem when considered alone. However, the combined responses of flexural strength and elastic moduli as a function of cure time appear to offer some explanation for the cause of crack formation. Two unsatisfactory ZCU's, one from Gypsum, Ohio and other from Maryland, when made up into neat' passes and cured in a similar manner, undergo expansion, shrink age, and expansion again. California and Iowa ZOU's, which are less brittle with relatively little change in flexural strength and elastic moduli, shrink or change little in dimensions with drying and give satisfactory performance. No great differences were found in wet density and set times of mortars prepared with Maryland ZOU mixed with No. 3 Llbty and Kearney vermiculite expanded at Trenton and Muirkirk. Vlcat consistency for Libby ore expanded at Muirkirk was greater than for Trenton. No difference was found for Kearney ore expanded at either plant. Comparison of attrition resistance for Libby and Kearney vermicu lite exfoliated at Trenton and Muirkirk showed that Libby vermi culite is more resistant to attrition than Kearney. Exfoliation at Trenton causes less attrition than Muirkirk. The characterization of ZOU's and vermiculltes along with their interatlon as related to shrink-crack will continue. (Kraus, Kolbe, Legal) DAVISON CRACKING CATALYST (Project 2L19) The objective is to determine if technology developed for sodiumsillcofluorlde sodium-silicate cements can be applied to improve the attrition resistance of Davison's cracking catalyst. Davison completed their physical and chemical testing of spray-dried sam ples submitted to them. Results indicate that attrition resis tance has been improved; however, activity has been sharply re duced. This is probably due to residual sodium which is much higher than usual and also fluorine which normally Is not present. 1820807 1