Document RJgZ3GLyBQ2zQOK6M2qx3DE18
SEVERN TRENT LABORATORIES ANALYTICAL REPORT
JOB NUMBER: 244404
Prepared For:
Weston Solutions, Inc. 1400 Weston Way Building 5-2
West Chester, PA 19380-1499
Project: Confidential Decatur - FC Investigation
Attention: Jai Kesari
Date: 02/28/2006
Signature Name: Richard C. Wright Title: Project Manager E-Mail: rwright@stl-inc.com
Date
STL Chicago 2417 Bond Street UcSveas iia Park, IL 60466
PHONE: (708) 534 5200 FAX..: (708) 534 5211
This Report Contains (_____) Pages
STL Chicago is part of Severn Trent Laboratories, Inc.
SA M P LE IN F O RM A T ION Date: 02/28/2006
Job Number. 244404 Customer... Weston Solutions, Inc. Attn...... Jai Kesari
Project Number....... 20004891 Customer Project ID.... CONFIDENTIAL DECATUR Project Description.... Confidential Decatur - FC Investigation
Laboratory Sample ID
244404-1 244404-2 244404-3 244404-4 244404-5 244404-6 244404-7 244404-8 244404-9 244404-10 244404-11 244404-12 244404-13 244404-14 244404-15
Customer Sample ID DF13-SB-GP04-0-0010 DF13-SB-GP04-0-0020 DF13-SB-GP04-0-0050 DF13-SB-GP04-DB-0050 DF10-SB-GP01-0-0000 DF10-SB-GP01-0-0005 DF10-SB-GP01-0-0010 DF10-SB-GP01-0-0020 DF10-SB-GP01-DB-0020 DF10-SB-GP01-0-0050 DF10-SB-GP02-0-0000 DF10-SB-GP02-0-0005 DF10-SB-GP02-0-0010 DF10-SB-GP02-0-0020 DF10-SB-GP02-0-0050
Sample Matrix Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil Soil
Date Sampled 02/15/2006 02/15/2006 02/15/2006 02/15/2006 02/15/2006 02/15/2006 02/15/2006 02/15/2006 02/15/2006 02/15/2006 02/15/2006 02/15/2006 02/15/2006 02/15/2006 02/15/2006
Time Sampled
10:25 10:30 10:30 10:30 15:40 15:45 15:45 15:46 15:46 15:50 16:20 16:20 16:23 16:25 16:25
Date Received 02/17/2006 02/17/2006 02/17/2006 02/17/2006 02/17/2006 02/17/2006 02/17/2006 02/17/2006 02/17/2006 02/17/2006 02/17/2006 02/17/2006 02/17/2006 02/17/2006 02/17/2006
Time Received
10:10 10:10 10:10 10:10 10:10 10:10 10:10 10:10 10:10 10:10 10:10 10:10 10:10 10:10 10:10
Page 1
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244404
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF13-SB-GP04-0-0010 Date Sampled.....: 02/15/2006 Time Sampled.....: 10:25 Sample Matrix....: Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn !Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID 244404-1 Date Received...... 02/17/2006 Time Received...... 10:10
Date:02/28/2006 ATTN: Jai Kesari
| SAMPLE RESULT |Q 'FLAGS '
I | 2400
ll I II I
MDL 170
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 730 I1
I I mg/Kg
III
I
1173968 I I02/22/06 1854 ils
* In Description = Dry Wgt.
Page 2
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244404
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF13-SB-GP04-0-0020 Date Sampled.....: 02/15/2006 Time Sampled.....: 10:30 Sample Matrix....: Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn !Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID 244404-2 Date Received...... 02/17/2006 Time Received...... 10:10
Date:02/28/2006 ATTN: Jai Kesari
| SAMPLE RESULT |Q 'FLAGS '
I | 2400
ll I II I
MDL 120
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 500 I1
I I mg/Kg
III
I
1173968 I I02/22/06 1908 2 1 s
* In Description = Dry Wgt.
Page 3
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244404
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF13-SB-GP04-0-0050 Date Sampled.....: 02/15/2006 Time Sampled.....: 10:30 Sample Matrix....: Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn !Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID 244404-3 Date Received...... 02/17/2006 Time Received...... 10:10
Date:02/28/2006 ATTN: Jai Kesari
| SAMPLE RESULT |Q 'FLAGS '
I | 1700
ll I II I
MDL 120
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 540 I1
I I mg/Kg
III
I
1173968 I I02/22/06 1934 ils
* In Description = Dry Wgt.
Page 4
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244404
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF13-SB-GP04-DB-0050 Date Sampled.....: 02/15/2006 Time Sampled.....: 10:30 Sample Matrix....: Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn !Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID 244404-4 Date Received...... 02/17/2006 Time Received...... 10:10
Date:02/28/2006 ATTN: Jai Kesari
| SAMPLE RESULT |Q 'FLAGS '
I | 1000
ll I II I
MDL 75
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 320 I1
I I mg/Kg
III
I
1173968 I I02/22/06 1952ils
* In Description = Dry Wgt.
Page 5
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244404
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF10-SB-GP01-0-0000 Date Sampled.....: 02/15/2006 Time Sampled.....: 15:40 Sample Matrix....: Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn !Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID 244404-5 Date Received...... 02/17/2006 Time Received...... 10:10
Date:02/28/2006 ATTN: Jai Kesari
| SAMPLE RESULT |Q 'FLAGS '
I | 890
ll I II I
MDL 110
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 460 I1
I I mg/Kg
III
I
1173968 I I02/22/06 2023 5 1 s
* In Description = Dry Wgt.
Page 6
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244404
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF10-SB-GP01-0-0005 Date Sampled.....: 02/15/2006 Time Sampled.....: 15:45 Sample Matrix....: Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn !Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID 244404-6 Date Received...... 02/17/2006 Time Received...... 10:10
Date:02/28/2006 ATTN: Jai Kesari
| SAMPLE RESULT |Q 'FLAGS '
I | 800
ll I II I
MDL 98
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 420 I1
I I mg/Kg
III
I
1173976 I I02/23/06 0822ils
* In Description = Dry Wgt.
Page 7
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244404
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF10-SB-GP01-0-0010 Date Sampled.....: 02/15/2006 Time Sampled.....: 15:45 Sample Matrix....: Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn !Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID 244404-7 Date Received...... 02/17/2006 Time Received...... 10:10
Date:02/28/2006 ATTN: Jai Kesari
| SAMPLE RESULT |Q 'FLAGS '
I | 1000
ll I II I
MDL 99
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 420 I1
I I mg/Kg
III
I
1173976 I I02/23/06 0858Icls
* In Description = Dry Wgt.
Page 8
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244404
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF10-SB-GP01-0-0020 Date Sampled.....: 02/15/2006 Time Sampled.....: 15:46 Sample Matrix....: Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn !Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID 244404-8 Date Received...... 02/17/2006 Time Received...... 10:10
Date:02/28/2006 ATTN: Jai Kesari
| SAMPLE RESULT |Q 'FLAGS '
I | 670
ll I II I
MDL 79
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 340 I1
I I mg/Kg
III
I
117397 6 I I02/23/06 0919ils
* In Description = Dry Wgt.
Page 9
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244404
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF10-SB-GP01-DB-0020 Date Sampled.....: 02/15/2006 Time Sampled.....: 15:46 Sample Matrix....: Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn !Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID 244404-9 Date Received...... 02/17/2006 Time Received...... 10:10
Date:02/28/2006 ATTN: Jai Kesari
| SAMPLE RESULT |Q 'FLAGS '
I | 840
ll I II I
MDL 72
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 310 I1
I I mg/Kg
III
I
117397 6 I I02/23/06 093951s
* In Description = Dry Wgt.
Page 10
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244404
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF10-SB-GP01-0-0050 Date Sampled.....: 02/15/2006 Time Sampled.....: 15:50 Sample Matrix....: Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn !Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID 244404-10 Date Received...... 02/17/2006 Time Received...... 10:10
Date:02/28/2006 ATTN: Jai Kesari
| SAMPLE RESULT |Q 'FLAGS '
I | 990
ll I II I
MDL 78
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 330 I1
I I mg/Kg
III
I
1173976 I I02/23/06 1014 ils
* In Description = Dry Wgt.
Page 11
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244404
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF10-SB-GP02-0-0000 Date Sampled.....: 02/15/2006 Time Sampled.....: 16:20 Sample Matrix....: Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn !Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID 244404-11 Date Received...... 02/17/2006 Time Received...... 10:10
Date:02/28/2006 ATTN: Jai Kesari
| SAMPLE RESULT |Q 'FLAGS '
I | 4700
ll I II I
MDL 120
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 510 I1
I I mg/Kg
III
I
1173976 I I02/23/06 1035ils
* In Description = Dry Wgt.
Page 12
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244404
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF10-SB-GP02-0-0005 Date Sampled.....: 02/15/2006 Time Sampled.....: 16:20 Sample Matrix....: Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn !Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID 244404-12 Date Received...... 02/17/2006 Time Received...... 10:10
Date:02/28/2006 ATTN: Jai Kesari
| SAMPLE RESULT |Q 'FLAGS '
I | 1400
ll I II I
MDL 95
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 410 I1
I I mg/Kg
III
I
117397 6 I I02/23/06 n N c l s
* In Description = Dry Wgt.
Page 13
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244404
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF10-SB-GP02-0-0010 Date Sampled.....: 02/15/2006 Time Sampled.....: 16:23 Sample Matrix....: Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn !Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID 244404-13 Date Received...... 02/17/2006 Time Received...... 10:10
Date:02/28/2006 ATTN: Jai Kesari
| SAMPLE RESULT |Q 'FLAGS '
I | 1200
ll I II I
MDL 88
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 380 I1
I I mg/Kg
III
I
1173976 I I02/23/06 1130Cls
* In Description = Dry Wgt.
Page 14
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244404
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF10-SB-GP02-0-0020 Date Sampled.....: 02/15/2006 Time Sampled.....: 16:25 Sample Matrix....: Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn !Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID 244404-14 Date Received...... 02/17/2006 Time Received...... 10:10
Date:02/28/2006 ATTN: Jai Kesari
| SAMPLE RESULT |Q 'FLAGS '
I | 1200
ll I II I
MDL 93
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 400 I1
I I mg/Kg
III
I
1173976 I I02/23/06 1143 Cls
* In Description = Dry Wgt.
Page 15
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244404
CUSTOMER: Weston Solutions , Inc.
Customer Sample ID: DF10-SB-GP02-0-0050 Date Sampled.....: 02/15/2006 Time Sampled.....: 16:25 Sample Matrix....: Soil
TEST METHOD '
PARAMETER/TEST DESCRIPTION
Lloyd Kahn !Total Organic Carbon (Soils) TOC Average Duplicates, Solid
LA B ORA TOR Y TE ST R E SU L T S
PROJECT: CONFIDENTIAL DECATUR
Laboratory Sample ID 244404-15 Date Received...... 02/17/2006 Time Received...... 10:10
Date:02/28/2006 ATTN: Jai Kesari
| SAMPLE RESULT |Q 'FLAGS '
I | 1300
ll I II I
MDL 87
RL IDILUTION I UNITS I BATCH IDT ' DATE/TIME ITECH
I 380 I1
I I mg/Kg
III
I
1173976 I I02/23/06 1157 ils
* In Description = Dry Wgt.
Page 16
STL Chicago is part of Severn Trent Laboratories, Inc.
Job Number: 244404
LA B ORA T O R Y C H R ON IC LE
Date: 02/28/2006
| CUSTOMER: Weston Solutions, Inc.
PROJECT: CONFIDENTIAL DECATUR
ATTN: Jai Kesari
| Lab ID: 244404-1 | METHOD | EDD | Lloyd Kahn
Client ID: DF13-SB-GP04-0-0010 DESCRIPTION Electronic Data Deliverable Total Organic Carbon (Soils)
| Lab ID: 244404-2 Client ID: DF13-SB-GP04-0-0020
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
| Lab ID: 244404-3 Client ID: DF13-SB-GP04-0-0050
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
| Lab ID: 244404-4 Client ID: DF13-SB-GP04-DB-0050
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
| Lab ID: 244404-5 Client ID: DF10-SB-GP01-0-0000
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
| Lab ID: 244404-6 Client ID: DF10-SB-GP01-0-0005
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
| Lab ID: 244404-7 Client ID: DF10-SB-GP01-0-0010
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
| Lab ID: 244404-8 Client ID: DF10-SB-GP01-0-0020
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
| Lab ID: 244404-9 Client ID: DF10-SB-GP01-DB-0020
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
| Lab ID: 244404-10 Client ID: DF10-SB-GP01-0-0050
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
| Lab ID: 244404-11 Client ID: DF10-SB-GP02-0-0000
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
| Lab ID: 244404-12 Client ID: DF10-SB-GP02-0-0005
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
| Lab ID: 244404-13 Client ID: DF10-SB-GP02-0-0010
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
| Lab ID: 244404-14 Client ID: DF10-SB-GP02-0-0020
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
| Lab ID: 244404-15 Client ID: DF10-SB-GP02-0-0050
| METHOD
DESCRIPTION
| Lloyd Kahn
Total Organic Carbon (Soils)
Date Recvd: 02/17/2006 Sample Date: 02/15/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1
1 173968 173968
02/22/2006 1854
DILUTION
Date Recvd: 02/17/2006 Sample Date: 02/15/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 173968 173968
02/22/2006 1908
DILUTION
Date Recvd: 02/17/2006 Sample Date: 02/15/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 173968 173968
02/22/2006 1934
DILUTION
Date Recvd: 02/17/2006 Sample Date: 02/15/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 173968 173968
02/22/2006 1952
DILUTION
Date Recvd: 02/17/2006 Sample Date: 02/15/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 173968 173968
02/22/2006 2023
DILUTION
Date Recvd: 02/17/2006 Sample Date: 02/15/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 173976 173976
02/23/2006 0822
DILUTION
Date Recvd: 02/17/2006 Sample Date: 02/15/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 173976 173976
02/23/2006 0858
DILUTION
Date Recvd: 02/17/2006 Sample Date: 02/15/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 173976 173976
02/23/2006 0919
DILUTION
Date Recvd: 02/17/2006 Sample Date: 02/15/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 173976 173976
02/23/2006 0939
DILUTION
Date Recvd: 02/17/2006 Sample Date: 02/15/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 173976 173976
02/23/2006 1014
DILUTION
Date Recvd: 02/17/2006 Sample Date: 02/15/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 173976 173976
02/23/2006 1035
DILUTION
Date Recvd: 02/17/2006 Sample Date: 02/15/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 173976 173976
02/23/2006 1116
DILUTION
Date Recvd: 02/17/2006 Sample Date: 02/15/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 173976 173976
02/23/2006 1130
DILUTION
Date Recvd: 02/17/2006 Sample Date: 02/15/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 173976 173976
02/23/2006 1143
DILUTION
Date Recvd: 02/17/2006 Sample Date: 02/15/2006
RUN# BATCH# PREP BT #(S)
DATE/TIME ANALYZED
1 173976 173976
02/23/2006 1157
DILUTION
Page 17
Job Number.: 244404 CUSTOMER: Weston Solutions , Inc.
QUA LITY CON TRO L R ESU LTS PROJECT : CONFIDENTIAL DECATUR
Report Date.: 02/28/2006 ATTN: Jai Kesari
Test Method...... Lloyd Kahn Method Description. Total Organic Carbon (Soils) Parameter........ Organic Carbon, Tot. (TOC)
Batch.......... .: 173968 Equipment Code... .: TOC4
Analyst... cls Test Code. TOC
QC Lab ID
Reagent
Units
CCV 173968-017 I06BSTTC2 MB 173968-003 CCV 173968-017 I06BSTTC2 CCB 173968-018 CCV 173968-017 I06BSTTC2 CCB 173968-018
mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg
QC Result
QC Result
2156.70 29.00
2190.22 29.00
2113.34 29.00
U U U
True Value 2000.00 2000.00 2000.00
Orig. Value
QC Calc. F * Limits
Date Time
108 % 85-115 02/22/2006 1640
02/22/2006 1643
110 % 85-115 02/22/2006 1923 02/22/2006 1926
106 % 85-115 02/22/2006 2107 02/22/2006 2111
Test Method...... : Lloyd Kahn Method Description. Total Organic Carbon (Soils) Parameter........ Organic Carbon, Tot. (TOC)
Batch.......... .: 173976 Equipment Code... .: TOC4
Analyst... cls Test Code. TOC
QC Lab ID
Reagent
Units
ICV 173976-002 I06BSTTC2 MB 173976-003 CCV 173976-017 I06BSTTC2 CCB 173976-018 CCV 173976-017 I06BSTTC2 MB 173976-003
mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg mg/Kg
QC Result
QC Result
2069.04 29.00
2159.69 29.00
2283.61 29.00
U U U
True Value 2000.00 2000.00 2000.00
Orig. Value
QC Calc. F * Limits
Date Time
103 % 85-115 02/23/2006 0749
02/23/2006 0753
108 % 85-115 02/23/2006 1209 02/23/2006 1213
114 % 85-115 02/23/2006 1459 02/23/2006 1503
Test Method...... : Lloyd Kahn Method Description. Total Organic Carbon (Soils) Parameter........ TOC Average Duplicates
Batch.......... .: 173968 Equipment Code... .: TOC4
Analyst... cls Test Code. TOCAV2
QC Lab ID
Reagent
Units
LCS 173968-004 I00FSTLK3 mg/Kg MS 244404-4 I06BSTTC2 mg/Kg MSD 244404-4 I06BSTTC2 mg/Kg
QC Result
3924.26 3106.56 2953.78
QC Result 2953.78
True Value
4780.00 2000.00 2000.00
Orig. Value
3106.56 3106.56
QC Calc. F * Limits
Date Time
82 96 107
8.9
% 53-140 02/22/2006 1658 % 53-140 02/22/2006 2009 % 53-140 02/22/2006 2016
Test Method...... : Lloyd Kahn Method Description. Total Organic Carbon (Soils) Parameter........ TCC Average Duplicates
Batch.......... .: 173976 Equipment Code... .: TOC4
Analyst... cls Test Code. TOCAV2
QC Lab ID
Reagent
Units
LCS 173976-004 I00FSTLK3 mg/Kg MS 244404-6 I06BSTTC2 mg/Kg MSD 244404-6 I06BSTTC2 mg/Kg
QC Result
4153.30 2890.75 2946.35
QC Result 2890.75
True Value
4780.00 2000.00 2000.00
Orig. Value
799.82 799.82
QC Calc. F * Limits
Date Time
87 % 53-140 02/23/2006 0802 98 % 53-140 02/23/2006 0839 96 53-140 02/23/2006 0846
2 R 30
Page 18
* %=% REC, R=RPD, A=ABS Diff., D=% Diff.
QUA L ITY A SSU RA N CE M E THO D S
RE FEREN CE S AN D N O TES
Report Date: 02/28/2006
REPORT COMMENTS 1) All pages of this report are integral parts of the analytical data. Therefore, this report should
be reproduced only in its entirety. 2) Soil, sediment and sludge sample results are reported on a "dry weight" basis except when analyzed for
landfill disposal or incineration parameters. All other solid matrix samples are reported on an "as received" basis unless noted differently. 3) Reporting limits are adjusted for sample size used, dilutions and moisture content if applicable. 4) The test results for the noted analytical method(s) meet the requirements of NELAC. Lab Cert. ID# 100201 5) According to 40CER Part 136.3, pH, Chlorine Residual and Dissolved Oxygen analyses are to be performed immediately after aqueous sample collection. When these parameters are not indicated as field (e.g. pH Field) they were not analyzed immediately, but as soon as possible on laboratory receipt.
Glossary of flags, qualifiers and abbreviations (any number of which may appear in the report) Inorganic Qualifiers (Q-Column) U Analyte was not detected at or above the stated limit. < Not detected at or above the reporting limit. J Result is less than the RL, but greater than or equal to the method detection limit. B Result is less than the CRDL/RL, but greater than or equal to the IDL/MDL. S Result was determined by the Method of Standard Additions. F AFCEE: Result is less than the RL, but greater than or equal to the methoddetection limit. Inorganic Flags (Flag Column) A ICV,CCV,ICB,OCB,ISA,ISB,CRI,CRA,MRL: Instrument related QC exceed the upper or lower
control limits. * LCS, LCD, MD: Batch QC exceeds the upper or lower control limits. + MSA correlation coefficient is less than 0.995. 4 MS, MSD: The analyte present in the original sample is 4 times greater
than the matrix spike concentration; therefore, control limits are not applicable. E SD: Serial dilution exceeds the control limits. H MB, EB1, EB2, EB3: Batch QC is greater than reporting limit or had a
negative instrument reading lower than the absolute value of the reporting limit. N MS, MSD: Spike recovery exceeds the upper or lower control limits. Wf AS(GFAA) Post-digestion spike was outside 85-115% control limits. Organic Qualifiers (Q - Column)
Analyte was not detected at or above the stated limit. Compound not detected. Result is an estMiated value below the reporting limit or a tentatively identified compound (TIC). Result was qualitatively confirmed, but not quantified. Pesticide identification was confirmed by GC/MS. The chromatographic response resembles a typical fuel pattern. The chromatographic response does not resemble a typical fuel pattern. Result exceeded calibration range, secondary dilution required. AFCEE:Result is an estMiated value below the reporting limit or a tentatively identified compound (TIC)
B MB: Batch QC is greater than reporting limit. +- LCS, LCD, ELC, ELD, CV, MS, MSD, Surrogate: Batch QC exceeds the upper or lower control limits.
EB1, EB2, EB3, M E : Batch QC is greater than reporting Limit A Concentration exceeds the instrument calibration range a Concentration is below the method Reporting Limit (RL) B Compound was found in the blank and sample. D Surrogate or matrix spike recoveries were not
obtained because the extract was diluted for analysis; also compounds analyzed at a dilution will be flagged with a D. H Alternate peak selection upon analytical review I Indicates the presence of an interfence, recovery is not calculated. M Manually integrated compound. P The lower of the two values is reported when the % difference between the results of two GC columns is
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greater than 25%.
Abbreviations
AS Post Digestion Spike (GFAA Samples - See Note 1 below)
Batch Designation given to identify a specific extraction, digestion, preparation set, or analysis set
CAP Capillary Column CCB Continuing Calibration Blank
CCV Continuing Calibration Verification
CF Confirmation analysis of original
C1 Confirmation analysis of A1 or D1
C2 Confirmation analysis of A2 or D2
C3 Confirmation analysis of A3 or D3
CRA Low Level Standard Check - GFAA; Mercury
CRI Low Level Standard Check - ICP
CV Calilbration Verification Standard
Dil Fac Dilution Factor - Secondary dilution analysis
D1 Dilution 1
D2 Dilution 2
D3 Dilution 3
DLFac Detection Limit Factor
DSH Distilled Standard - High Level
DSL Distilled Standard - Low Level
DSM Distilled Standard - Medium Level
EB1 Extraction Blank 1
EB2 Extraction Blank 2
EB3 DI Blank
ELC Method Extracted LCS
ELD Method Extracted LCD
ICAL
Initial calibration
ICB Initial Calibration Blank
ICV Initial Calibration Verification
IDL Instrument Detection Limit
ISA Interference Check Sample A - ICAP
ISB Interference Check Sample B - ICAP
Job No. The first six digits of the sample ID which refers to a specific client, project and sample group
Lab ID An 8 number unique laboratory identification
LCD Laboratory Control Standard Duplicate
LCS Laboratory Control Standard with reagent grade water or a matrix free from the analyte of interest
MB Method Blank or (PB) Preparation Blank
MD Method Duplicate
MDL Method Detection Limit
MLE Medium Level Extraction Blank
MRL Method Reporting Limit Standard
MSA Method of Standard Additions
MS Matrix Spike
MSD Matrix Spike Duplicate
ND Not Detected
PREPF Preparation factor used by the Laboratory's Information Management System (LIMS)
PDS Post Digestion Spike (ICAP)
RA Re-analysis of original
A1 Re-analysis of D1
A2 Re-analysis of D2
A3 Re-analysis of D3
RD Re-extraction of dilution
RE Re-extraction of original
RC Re-extraction Confirmation
RL Reporting Limit
RPD Relative Percent Difference of duplicate (unrounded) analyses
RRF Relative Response Factor
RT Retention Time
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RTW Retention Time Window Sample ID A 9 digit number unique for each sample, the first six digits are referred as the job number
SCB Seeded Control Blank SD Serial Dilution (Calculated when sample concentration exceeds 50 times the MDL) UCB Unseeded Control Blank SSV Second Source Verification Standard SLCS Solid Laboratory Control Standard(LCS) PHC pH Calibration Check LCSP pH Laboratory Control Sample LCDP pH Laboratory Control Sample Duplicate MDPH pH Sample Duplicate MDFP Flashpoint Sample Duplicate LCFP Flashpoint LCS G1 Gelex Check Standard Range 0-1 G2 Gelex Check Standard Range 1-10 G3 Gelex Check Standard Range 10-100 G4 Gelex Check Standard Range 100-1000 Note 1: The Post Spike Designation on Batch QC for GFAA is designated with an "S" added to the current abbreviation used. EX. LCS S=LCS Post Spike (GFAA); MSS=MS Post Spike (GFAA) Note 2: The MD calculates an absolute difference (A) when the sample concentration is less than 5 times the reporting limit. The control limit is represented as +/- the RL.
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