Document R27pBYa6Gd5rbp9pKyvEZyJeV

................................................ ......................................................................................................................... i H+l HMUlilIWUUManW I........ .... !!! 1UI.LLL+1 Vista Polymers A Division of Vista Chemical Company C Highway 25 Post Office Box 91 ..................................................................................... 'i immliinalijmiii----------------IriTTtmi ii imN^rtiliii-LLii -1. i-------------1-l-LI-LJ-LJ Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 CERTIFICATE OF ANALYSIS Ueuiti44444iri|||.|<l..;-..! ............ 111-IJI I hi 111 11 11 A Date: January 4, 1993 Fax No. 601-286--9402 ift' Intex Plastics Corp Corinth Division Golding Drive Corinth, MS 38834 Product: 538$ Attention: Quality Control Dept. Railcar No.: VIPX 45782 Ship Date: December 30, 1992 Property Test Order No.: IPC Specification 0019847-003 nnaia* \pBssssss Analysis Inherent Viscosity ABR-10 0.90 - 0.95 0.93 Residual VCM, ppm ABGC-26 8.5 Max. 0.055 Contamination, BLK + BRN ABR-5A 40 Total A CA CB B Total Black + Brown 12 12 10 9 Hard Particles @ 7 Mins ABR-12 15 Max 2 Dry Flow, Seconds ABR-8 15 Max 8.2 Bulk Density, gm/cc ABR--2A 0.510 Min 0.578 Moisture, % ABR-1A 0.30 Max. 0.16 Particle Size Distribution ABR-3 25.0 Thru 140 Mesh 5.0 Max on Pan MESH 40 60 o 00 100 120 140 200 PAN % ON 0.00 0.3 19.5 30.9 26.8 13.7 7.5 1.3 Brabender Dry Time, Mins. ABR-7 6.0 Max. 5.0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E.^BagwelT-^ Laboratory Supervisor (601) 369-3624 Ch^ VAB.0001201050 rm^tini mUJ il II HH44HH++H j.h i*w<" I................ .. LIM IHIMl H MMikH l*i I IH-H-I+I II II III! II Ikkl-H It*- H III I I kl I II l*kl I hi lTn wi I H i i i>|n rnn-^.|*4-| | I h+|+| I -| 1 HTm 1 > rj - . + V* t *i v"-/-*r,p* ^. *7" Vista Polymers 111111111 j 11'''' 11!' 111' 11:' I' 1: 111' 111' 1111:11 wi i mi V-. ^^ Highway 26 ----- ---------------- ----- .............. " 1111.1111111; 11.11111111111 ` 11' I: i 1111 j 11111........ 1 I 111 -1 I I 11 11 ' I I'' I 111............1 " I'''11 -: 111:11111111111111 11 I'II il II-I III I top Aberdeen, MS 39730 .......................................... ........................ ...................111! I * RAILCAR Load Date: / Z-J* - 72- Product 5385 Car Mo. Time Logged Ship Date: 0f*9 Logged In By: Silo(s): Order No: 0^)1 ^Customer: 477 --- .g 6 tie m HIM Compartment 1 ** Sample From A Bottom Moisture % i BL Contamination ... BR Bulk Density BD after Fluff .14- & 7 .S17 Hard Particle 5 7 2. Viscosity to RVCM >oS5~ 40 Mesh/Glassies o 3CS CA Bottom .k, CB 4 Bottom t g ,X?9 ' - i -31. 7 "1 . 0 P B Bottom .7? ___________________ __________________________ Screen Analysis Mesh 40 60 80 100 120 140 200 Pan Weight % 0*0^ O*o .j /*.jt Je.f 24-7 n-7 7-S~ /. 3 Drytime: s: o Static Flow: 0 / j.0Z- Avg. Microns / Color L: /CO 33 a b Technician: mM.*- VAB.0001201051 ! I i I! | i 11 I t . ,-v. I1;! 11 I I F* M!!l!l"!,l""l":i,l;llv!.l'l.'!!,il.'ll|! I- I- i i .:! hi : L-! :I:a ii ; |!*- iC !.'! t I :-l ii!' i jl m -.-ir -I i:; ? ii?- if/-,. .j -i! ,-fiat ! .`i'V.'JL-;.................... ... `rt-l 1 J Jiu:.iA.iJ!Jiv 'Ivj. U in:!)'.; J"U-I lv -I.'./ .M!.:- ...........................................in , -ji^LHomU- Uiil.;-..ill Ilium ........................................................... i,V ,-i :nrJ V i;.V -J r*-A\r/ -U iff i' iv T3 F rL :-j I = 3l- I* In.. *vtti***-1' :` >LS%-||. -T-I: . =!!-: T-.-Bx -I ! tcs' tlri.-i m. / = RtK| !.rf."-* I.r.I-iJ -I r` I " A ter-sn! V3i.di^;-al: tE-bO-'-f `sm itm fe '^Ll i t 'J'.i. : t IT i ' uvfc \-\ ... t .!; Hu'I I'Vil' * .> i ft-', '-Vr iu.j +>-' ;s i:rr-r .'KlV-'J ir shipment order to divert/re-ship/return RAILCAR DATE: S1^ Gil. i?Stii|i* BHi: sfci! . r. 'iflSBW 3F^-| ft-rr i.&Vt rl; ! Yii: ill id-'L-' il ~u. ^i ;i ii.'-U: v W-` .vjij .1 JFI-J:V- ! RAILCAR NUMBER: ORIGINAL SHIP DATE ORIGINAL ORIGIN PLANT: pNIi: mlit-* Ji/ ORIGINAL PRODUCT WEIGHT: St1(L^ c?fa:?ci CWS.HH win} Lsitti ifi> PRODUCT NAME A CODE: ORIGINAL CUSTOMER: [nl tm i ORIGINAL CUSTOMER LOCATION ORIGINAL ORDER NUMBER: t> l *!r y 7-# % NEW CUSTOMER: NEW LOCATION: h-!: NEW ORDER NUMBER: QQ YOII IMFPn MAII I !AH (Yfifi/NG) REASON FOR CHANGE: (EG. off-spec, etc.) *-afi - -i=! r.- :ij | [ii- CAR RELEASED (YES/NO): rowmAcrs K ISSUM BU. Of IA0B 0 OB T> V TO M< aSW. OTHER COMMENTS: CUSTOMER SERVICE REPRESENTATIVE - T^i^f 4MMNP mhhh ...... PAIL OHUftA 001201052 ' ' rr-L ^--Hb mmmmP Notebook No. Signed Date Signed Date Vista Polymers A Division of Vista Chemical Company ClETMhb*i Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 IFICATE OR ANALYSIS b Date: December 18, 1992 Fax No. 601-286-9402 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 VISTAProduct: 5385 Attention: Quality Control Dept Railcar No.: ACFX 41169 Ship Date: December 17, 1992 Order No. 0019847-001 Property Test Method IPC Specification Analysis Inherent Viscosity ABR-10 0.90 0.95 0.93 Residual VCM, ppm ABGC-26 8.5 Max. 0.104 Contamination, BLK + BRN ABR-5A 40 Total Total Black + Brown Hard Particles 8 7 Mins Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH % ON 15 Max. 3 15 Max. 8.1 0.510 Min. 0.579 0.30 Max. 0.12 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins. ABR-7 6.0 Max. 5.0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E. Bagwe^r Laboratory Supervisor (601) 369-3624 VAB.0001201054 Viata Polymers Highway 25 A Aberdeen, MS 3973Q RVC RAX LCAR ANALYSIS Load Date: Time Logged In: /Ccc Ship Date: Product: Logged In Bv: Order No: Car No.: siio(s): Customer: Compartment Sample From Moisture % ottom Bottom Bottom Bottom Contamination Bulk Density BD after Fluff Hard Particle Viscosity RVCM Meish/Glassies *m *1 w Screen Analysis Mesh 40 Weight % 0*0 /& .^1 nsv m22m 60 .77 AJT 80 / J,r2. 2.7.0 100 1 jr.ff 2f.c 120 J6.7+ 2 /, * 140 L.Za 200 S-iC 7. 3 Pan i.i3 2.* Drytime: sr-o Static Flow: 0 / f. O Avg. 1 icron6: ist.c Color L: foo* 6 0 a b <?:*? Technician: VAB.0001201055 *>* 4* >; * *<; I -k . * . ,- i-juXwy.st=^'^\ j_ * *--'- tmm - r riMU MM *- Vista Polymers Highway 26 NM.L Aberdeen, MS 397SO *> Load Date: 12-M> Time Logged In:____ Ship Date:. \z[ nfa HAX LCAR ANALYSIS yipf- Product: 5385 Logged In By: Car No. (///? mlL Silo(s): 6>8^ Order Not Customer: Compartment A Sample From Bottom 4* 0Uj ____ .__ _______-- _ J- Moisture % BL Contamination BR _ Bulk Density BD after Fluff '$*7 Hard Particle 5 (3 7 2- Viscosity RVCM JOtf 40 Mesh/Glassies Screen Analysis Mesh 40 Weight CA Bottom CB Bottom B Bottom i. * t . 140 rs. ? 200 _*f-3 (s> Pan / *3 O Drytime: Static Flow: P / 3/ Avg. Microns: Color L: /0&w a O'f? b /-7 / Technician: HM yfrf * M VAB.0001201056 I I '! i *1 ... * DATE: RAILCAR NUMBER: ORIGINAL SHIP DATE: ORIGINAL ORIGIN PLAN I: ORIGINAL PRODUCT WEIGHT: PRODUCT NAME & CODE ORIGINAL CUSTOMER: UHIGINAL CUSTOMER LOCATION: ORIGINAL ORDER NUMBER: NEW CUSTOMER: NEW LOCATION: NEW ORDER NUMBER: DO YOU NEED RAILCAR RE-WEIGHED? (YES/NO) REASON FOR CHANGE: <eg. off-spec, etc.) CAR RELEASED (YES/NO); v, BILUNG INSTRUCTIONS MUST BE COMMUNICATED TO RAIL hHbK3H I A CONTRACTS FOR ISSUING BILL OF LADING ON OR BEFORE THE DAY THE CAR IS RELEASED. OTHER COMMENTS: * c* CUSTOMER SERVICE REPRESENTATIVE: \ \ WJBUTION: PfANT, HQU&IQN - RAIL rROGf/TA CONTRACTS, HOUSTON - RAIL v\s \ - % OPERATIONS ' 'X - Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS Date: December 29r 1992 Fax No. 601-286-9402 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 Product: 5385 Attention: Quality Control Dept Railcar No.: VIPX 45791 Ship Date: December 28, 1992 Order No.: 0019847-002 Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A Total Black + Brown 0.90 - 0.95 8.5 Max. 40 Total A CA 15 16 Analysis 0.93 0.043 CB B 17 18 Hard Particlesi 7 Mins. ABR-12 15 Max. 5 00 \ Dry Flow, Seconds ABR-8 15 Max. Bulk Density, gm/cc ABR-2A 0.510 Min. 0.585 Moisture, % ABR-1A 0.30 Max. 0.15 Particle Size Distribution ABR-3 25.0 Thru 140 Mesh 5.0 Max on Pan MESH 40 60 80 100 120 140 200 PAN % ON 0.00 1.5 20.5 31.0 25.1 13.4 7.1 1.4 Brabender Dry Time, Mins. ABR-7 6.0 Max 5.1 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy Bagwell Laboratory Supervisor (601) 369-3624 VAB.0001201058 g -t >: Vista Polymers * - * - yr.iy.r^i^i-*t.<rUiri- > Highway 26 Aberdeen, MS 39730 A Load Date: f 2~ Tine Logged In: Ship Date : \l\-7jl RAILCAR ANALYSIS Product: 5385 Logged In By: Order Ho: ^ Car Ho. Silo(s) Customer: Compartment Sample From Moisture % Contamination <P Bottom Bottom ./s Bottom CD Bottom Bulk Density BD after Fluff .5^6 Hard Particle -584- Viscosity RVCM Lo4s 40 Mesh/Glassies Screen Analysis Mesh 40 Weiffht G.Q0 X 0.6/O 60 80 O. 75 A5 3D-S 100 /S<7 31.9 120 25. f 140 U*i Alt 200 3.sy 5/ Pan 0.7f /m4~ Drytime: &t Static Flow: 0 ,f.4Avst. Microns: Color L: /0O.SI 6>J3 h / 7Z 5&./ Technician: VAB.0001201059  * Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 CERTIFICATE OF ANALYSIS Date: December 29, 1992 Fax No. 601-286-9402 Customer: Intex Plastics Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: December 28, 1992 Product: 5415 Railcar No.: VIPX 45910 Order No.: 0019845-001 Property Test Method Specification Analysis Inherent Viscosity ABR-10 1.00 - 1.04 1.02 Residual VCM, ppm ABGC-26 8.5 PPM Max. 0.023 Contamination, BLK + BRN ABR-5A 20 Total Max. A CA CB B Total Black + Brown 10 9 8 5 Hard Particles @ 7 mins. ABR-12 5 Max. 1 Dry Flow, Seconds ABR-8 15 Sec. Max. 8.8 Bulk Density, gm/cc ABR-2B 0.460 Min. 0.506 Moisture, % ABR-1A 0.30 Max. 0.15 Particle Size Distribution ABR-3 25.0 Thru 140 Mesh Max. 5.0 On Pan Max. 40 60 80 100 120 140 200 PAN % ON 0.00 0.3 28.5 34.2 21.3 8.2 5.8 1.7 Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 5.0 A Laboratory Supervisor (601) 369-3624 VAB.0001201060 Vista PolyBiers Highway 25 Aberdeen, MS 39730 Load Date: PVC IRA. I LOAF? ANALYSIS i_______ Product: j 5415 | Car No. : . vW C^0 Tine Logged In; P7*e Logged In Bv: Ship Date:_ 1 _____ Order No: Qfo /*<1 Sllo(s): / Customer: ifl A Screen Analysis Mesh Height 40 AM _ % Afi Drytime: . 60 At, ,2 80 Z4-.lt, 4k 100 ji,/0 S* i- 120 Static Flow: _ 0 / /./ 140 200 ,/# -2.// / 1. r r/ Avg. Microns: Pan - fJT 112.2_ - Color L: 72+ a - ZS~ b METS: /0553 / /gO. ^ Technician: .____ VAB.0001201061 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A Date: December 18, 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: December 17, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A Fax No. 601- 6-. Product: 5325 Railcar No.: VIPX 45804 Order No.: 0019846-000 Specification Analysis 0.78 - 0.82 0.79 8.5 PPM Max. 0.262 Not Yet Determined Total Black + Brown Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2A Moisture, % ABR-1A Particle Size Distribution ABR-3 15 Sec. Max 0.480 Min. 0.30 Max. 5.0 Max. on Pan 11.2 0.498 0.14 % ON Polyvinyl Chloride, Virgin Resin, Not Reprocessed. \SL Laboratory Supervisor (601) 369-3624 VAB.0001201062 Vista Polymers Highway 25 Aberdeen, MS 39730 A RAILCAR ANALYSIS Load Date: /A/7-?2~ Product: Car No.: Time Logged In: /S&V Ship Date: Logged In By: M <1 Order No: iMG -cvz? Silo(s): Customer : UutZ*/ Compartment Sample From Moisture Bottom Bottom Bottom Bottom Contamination Bulk Density BD w/antistat Viscosity RVCM 713 .713 .712 Screen Analysis Mesh Weight % 40 0*0^. oo CPA: & Color L: 60 80 100 120 140 200 Pan .13 c/.gi? 9. so 12.79 5.31 3 n,o 39-^ <?S.5~ 10.7 /.y % : Glassies !%) Avg. Microns: a .7] b Static Flow: W /IfJL Technician: VAB.0001201063 Vista Polymers Highway 25 Aberdeen, MS 39730 - S /Vvv\^ ^ Ft A X LCAR ANALYS X S A Load Date: Time Logged In: Ship Date: Product: Logged In By: Order No: Car No . : /* m Silo(s) : Customer: Compartment A Sample From Bottom Moisture BL Contamination BR Bulk Density BD w/antistat Viscosity CA Bottom CB Bottom o~/ B Bottom Screen Analysis Mesh 40 Weight % CPA: Color L: 60 80 100 120 140 200 Pan % Glassies: ab Avg. Microns: Static Flow: / Technician: VAB.0001201064 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS Date: December 17, 1992 Fax No. 601-286-9402 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, NS 38834 Product: 5385 Attention: Quality Control Dept Railcar No.: VXPX 45714 Ship Date: December 16, 1992 Order No.: 0019847-000 Inherent Viscosity Test Mftfchflfl ABR-10 I PC 0.90 - 0.95 Analysis 0.93 Residual VCM, ppm ABGC-26 8.5 Max. 0.195 Contamination, BLK + BRN ABR-5A 40 Total A CA CB B Total Black + Brown 10 8 11 11 Hard Particles @ 7 Mins. ABR- 12 15 Max. 7 Dry Flow, Seconds ABR- 8 15 Max. 7.0 Bulk Density, gm/cc ABR-2A 0.510 Min. 0.586 Moisture, % ABR- 1A 0.30 Max. 0.16 Particle Size Distribution ABR-3 MESH 40 60 |I 80 25.0 Thru 140 Mesh 5.0 Max on Pan 100 120 140 200 PAN % ON 0.00 1.0 1-2---0--.-0 29.5 1----- 25.5 13.9 8.0 2.1 Brabender Dry Time, Mins. ABR-7 6.0 Max. 5.0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. \ Amy E. Bagwell Laboratory Supervisor (601) 369-3624 VAB.0001201065 o Vista Polymers Highway 26 Aberdeen, MS 39730 A 0A A'l A U X L- , Load Date: Time Logged In: 6(S0 b Ship Date:. Product: Logged In By: Car Ho.: Silo(g): >S Order Ho: OOO Customer: Screen Analysis Mesh We iaht X 40 0*0 60 Jjfr k 80 100 120 140 200 Pan ?< f IV ?r p.73 o o)s A3.-? <3.1 Drytime: 5,0 0 vstStatic Flow: /// A . Microns: m-&Color L: a -0*1 b /..7* iS?,\ Technician: VAB.0001201066 Vista Polymers A Division of Vista Chomkai Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aberdeen, Mississippi 39730 Phone (601) 369-8111 Date: December 18, 1992 Fax NO. 601--286--9402 Customer: Intex Plastics Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: December 16, 1992 Product: 5415 Railcar No.: UTCX 46550 Order No.: 0019845-000 Property est Method Analysis Inherent Viscosity ABR-10 1.00 - 1.04 1.02 Residual VCM, ppm ABGC-26 8.5 PPM Max. 0.192 Contamination, BLK + BRN ABR-5A 20 Total Max. A CA CB B Total Black + Brown 10 13 9 9 Hard Particles 7 mins. ABR-*12 5 Max. 2 Dry Flow, Seconds ABR--8 15 Sec. Max. 8.2 Bulk Density, gm/cc ABR--2B 0.460 Min. 0.505 Moisture, % ABR-1A 0.30 Max. 0.16 Particle Size Distribution ABR--3 25.0 Thru 140 Mesh Max. 5.0 On Pan Max. 40 60 80 100 120 1 140 200 PAN % ON 0.00 1.5 41.1 27.8 14.4 8.4 5.0 1.8 Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 5.0 A Laboratory Supervisor (601) 369-3624 VAB.0001201067 b# . s P * " r ! . S- wt . V- AiSf -* ^i"-"% * --'t. -_ _b ^ _ iu . m *. taijA1 H , _ A. -J -,-* h Vista Polymers Highway 25 v^V-v* ^r -:' '.J^r-vs; n I .T * '***" J A Aberdeen. MS 39730 RAILCAR ANALYSIS Load Date: Time Logged In >l3t> Ship Date: l7J lb Product: Logged In By: Order No: Car No.: Silo(s) SJlO-ttyl Customer: Conpartnent A Sample From Bottom Top Moisture % BL Contamination BR Bulk Density ,u 4 3 7 5 Hard Particle 7 Viscosity RVCM * <? 2^ CA Bottom Top , if - i r\03 CB Bottom Top B Bottom Top ,/{ 2_ 7 3 7 rtf)-? .' ' | y Screen Analysis Mesh 40 Height % 0. 0 60 * 7~ 80 47, / 100 rt$o 7?7.f 120 7. So /44 140 f,2o /V 200 Sl<0 Pan , 7o /,f Drytime: Static Flow: 0 / f. Avg. Microns: 172., 8 Color L: /oo. ^/ a b /n METS: l03&2> / I~l7-j X Technician VAB.0001201068 * 0 Vista Polymen A Division of Vista Chomical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aberdeen, Mississippi 39730 Phone (601) 369-8111 Date: December 18, 1992 Fax No. 601-286-9402 Customer: Intex Plastics Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: December 15, 1992 Product: 5415 Railcar No.: ACFX 41152 Order No.: 0019844-000 Property Inherent Viscosity Test Method ABR-10 Specification 1.00 1.04 1.03 VCM ppm ABGC PPM 0.061 Contamination, BLK + BRN ABR-5A 20 Total Max. A CA | CB B Total Black + Brown 99 8 5 Hard Particles $ 7 mins ABR-12 5 Max. 2 Dry Flow, Seconds ABR-8 15 Sec. Max 8.1 Bulk Density, gm/cc ABR-2B 0.460 Min. 0.505 Moisture, % ABR-1A 0.30 Max. 0.15 Distribution ABR-3 25.0 Thru 140 Mesh Max 5.0 On Pan Max. 40 60 80 100 120 140 200 pan| 00 % ON 0.00 2.0 40.4 28.5 15.7 6.9 Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 5.0 A U Amy Yr. Bagwel(j/ Laboratory Supervisor (601) 369-3624 VAB.0001201069 SiTi V il ._ ... "I. .<-.P-- - -**# p**-- H Jj I M *-)'> J- - J u| . Vista Polymers Highway 25 ' li1- Aberdeen, MS 39730 4 Load Date: Ship Date: Compartment Sample From Moisture % RAILCAR ANALYSIS MjwL 0130 Product: 5415 Car Mo. Logged In By: AdM&44~co& Customer l/uhf og 'hdZ A's Bottom Top BottomI Top Bottom Top Bottom Top Contamination Bulk Density Hard Particle <oo ier' Viscosity RVCM lotg .ou>[ Screen Analysis Mesh 40 Weight % Q^Oo 0i <P 60 Loo Z.Q 80 2o^z~ 40,4 100 JL&,S 120 7,ry^ /r.7 140 3.^ 200 2rZt 4J Pan Z_2 Drytime: r.e> Static Flow: *>/?! Avg. Microns: n4.o Color L: JW-17 a , og b / MKTS: lOC-fS~~/ rZ-ST.S"'% Technician: mA VAB.0001201070 Vista Pblymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS December 2, 1992 Customer: Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: November 30, 1992 Fax No. 601--286--9402 VK1AProduct: 5415 Railcar No.: UTCX 46512 Order No.: 0018812-001 Test Method IPC Specification Analysis Inherent Viscosity ABR-10 1.00 1.04 1.03 Residual VCM, ppm ABGC-26 8.5 PPM Max. 0.061 Contamination, BLK + BRN ABR-5A 20 Total Max A CA CB B Total Black + Brown 8474 Hard Particles @ 7 mins ABR-12 5 Max. 1 Dry Flow, Seconds ABR-8 15 Sec. Max 9.4 Bulk Density, gm/cc ABR-2B 0.460 Min. 0.486 Moisture, % ABR-1A 0.30 Max. 0.14 Distribution ABR-3 40 60 25.0 Thru 140 Mesh Max 5.0 On Pan Max. 80 1 100 120 140 200 PAN % ON 0.00 3.1 39.9 29.2 15.3 6.7 4.3 1.5 Dry Mins. ABR-7 6.0 Mins. Max. 4.8 Amy EV Bagwell Laboratory Supervisor (601) 369-3624 VAB.0001201071 w Vista Polymers Highway 25 Aberdeen, MS 39730 \ PVC RAILCAR ANALYSTS Load Date: //-3f-?Z Product: Car No.: Time Logged In: Ship Date ! H(soft Logged In By: Order No: "2^00/ Silo(s): Customer: orvo /YYYc^OkJL Compartment A Sample From Bottom Top Moisture % BL Contarnination BR .If R 4 Bulk Density 5 Hard Particle 7 nit a 3 Viscosity RVCM !.0S&> Ml CA Bottom Top i 13 7 CB Bottom Top 34 V B Bottom Top M <2 <5. **0 * O i 0 Screen Analysis Mesh Weiffht 40 &r OO 60 [S 80 /ML m 100 120 22s. IS, 3 140 LI 200 V, 3 Pan '*7(? /rT Drytime: ^tO Static Flow: Avg. Microns: . / 7/. ^ Color L: U-7*> a 1^L_ b 1.3? METS: IDI^S^ / IZ$`I % Technician: VAB.0001201072 Vista Polymers A Division of Vista Chemical Company CER Highway 25 Post Office Box 91 I f= I GATE Date: November 25, 1992 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: November 24, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 ANA 3X3 Fax No. 601-286-9402 4 VISIAProduct: 5385 Railcar No.: ACFX 41160 Order No.: 0018450-004 I PC Specification Analysis 0.90 - 0.95 0.92 8.5 Max. 0.264 40 Total Total Black + Brown Hard Particles 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH % ON 15 Max. 2 15 Max. 8.0 0.510 Min. 0.586 0.30 Max. 0.13 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins ABR-7 6.0 Max. 5.0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor (601) 369-3624 VAB.0001201073 Vieta Polymers Highway 25 A Aberdeen, HS 3973n leVC IRA X LCAR ANALYSIS Load Date: /H Product: Time Logged In: /*?&& Ship Date: __l lM Logged Order No: 4S6-06^ Car No.: SiIo(6): a A aw% A A* jn2p( Mesh Weight X 40 0.00 0-0 60 80 100 120 140 200 Pan .... n to* fl. s.st i I* ,L St. 9 st.s nJ 7.4 2.0 Dry ti me : 5.o Static F low : 0 / to Avg . Microns: Color L: tO0*$f a .o4 b y.rY' Technician: sA____ VAB.0001201074 Vista Polymers A Division of Vista-Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601)369-8111 A CERTIFI Date: November 24, 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: November 23, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A IS Fax No. 601-286- VB1A Product: 5325 Railcar No Order No UTCX 46396 0018452-001 Specification Analvsis 0.78 0.82 0.80 8.5 PPM Max. 0.751 Not Yet Determined Total Black + Brown Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2A Moisture, % ABR-1A Particle Size Distribution ABR-3 15 Sec. Max 0.480 Min. 0.30 Max. 5.0 Max. on Pan 11.1 0.508 0.16 % ON Polyvinyl Chloride, Virgin Resin, Not Reprocessed uj Amy E. Bagwe Laboratory Supervisor (601) 369-3624 VAB.0001201075 Vista Polymers Highway 25 Aberdeen. MS 39730 A Ft AX LCAR ANALYSIS Load Date: Time Logged In: 04^ Ship Date: If Product: Logged In By: Order No: / Sst -oo/ Car No.: Silo{s): Customer : //^ I Compartment A Sample From Bottom Moisture BL Contamination BR X Bulk Density BD w/antistat All Viscosity RVCM .VO-/* ,vtb Screen Analysis Mesh 40 Weight X 0,, O 60 ,3o .0 CA Bottom ,/s~ `f .at. ,%oo ,l4s CB Bottom t /G y -r/ B V Bottom ,// r 7 .1^1 .&>> .JI0 80 4.4* e.i 100 T2A /I* 120 It. 2_ 140 ti.il 200 S'. 3 / /e.i Pan /. CPA: Z.4.T X Glassies: Avg. Microns: 7 ^ r Color L: a J 7 b y.r? Static Flow: * / //,/ Technician: VAB.0001201076 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A Cp I R X O A d K--J T Date: November 24, 1992 Customer: Intex Plastics Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: November 23, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A ANALYS I S Fax No. 601-286-9402 VIS1AProduct: 5415 Railcar No Order No PLCX 47522 0018449-002 I PC Specification 1.00 - 1.04 8.5 PPM Max. 20 Total Max Analysis 1 .03 0.014 Total Black + Brown Hard Particles 7 mi ns Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2B ABR-1A ABR-3 5 Max. 1 15 Sec. Max 8.0 0.460 Min. 0.507 0.30 Max. 0.18 25.0 Thru 140 Mesh Max 5.0 On Pan Max. % ON Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 5.0 dJ Amy E. Bagwe11 Laboratory Supervisor (601) 369-3624 VAB.0001201077 Vista Polymers Highway 25 Aberdeen, HS 3973Q A RAILCAR ANALYSIS Load Date: Time Logged * Ship Date: 1 (9J3Q Product: _ Logged In By: Order Ho: Car No. : Silo(6): Customer: m.jn Compartment A Sample Pro Bottom Top Moisture X BL Contamination BR Bulk Density /c f Co'? S' 7 CA Bottom Top CB Bottom Top // .cot . / r6 ? 4 B Bottom Top $ f? Viscosity RVCM Screen Analysis -* Mesh 40 Weight AJLQ. X ___M. 60 ZJf! S-,f Drytime: C-0 80 ztx +J.S 100 /LtO ZJ.U 120 4.42. /J. 7 140 J.iC 7.7 200 JLfO Pan ,7<T" J. 4T Static P low: /n.i4 / r.o Avg . tticron6: Color L : /0$*72 -*eC b /SO H ETS : lO!} 23 / 133.6 % Technlclan VAB.0001201078 * Vista Polymers A Division of Vista Chemical Company w Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A CE R I R I EE OR ANA YS I 3 Date: November 25, 1992 Fax No. 601-286-9402 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38S34 VISTAProduct: 5385 Attention: Quality Control Dept Railcar No GACX 73383 Ship Date: November 23, 1992 Order No 0018450-003 Property Test Method I PC Specification Analvsis Inherent Viscosity ABR-10 0.90 - 0.95 0.93 Residual VCM, ppm ABGC-26 8.5 Max. 0.101 Contamination, BLK + BRN ABR-5A 40 Total Total Black + Brown Hard Particles 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH % ON 15 Max. 3 15 Max. 8.0 0.510 Min. 0.581 0.30 Max. 0.14 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins. ABR-7 6.0 Max. 4.7 Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E. Bagwe11 Laboratory Supervisor (601) 369-3624 * mm r VAB.0001201079 Viata Polymore Highway 25 A Aberdeen, MS 39730 E^VC JR AX LCAR ANALYSIS Load Date: Product: Time Logged In: lcL3V Logged In By: Ship Date:__(_[ Order No:. I ytfefr-oos Car No. SI lo ( 6 ) : Customer: pi/b Compartment Sample From Bottom] Moisture % .61 Hrbl] Contamination BR !1 A Bulk Density t rlA BD after Fluf:f Hard Particle 5| Jo j Bottom L// J /JL ~~ Lry* Bottom Botto 5~St VIscosity RVCM Mesh/Glassies / Screen Analysis Mesh 40 Weight >> % 60 Drytime: J# 7 80 100 120 /*3g 13/1 LL-31 140 /Sj-H 200 Pan &IL t>-T1 in _ fJL Static Flow: 0/ Avg. Microns: Color L: 3*07 b /. 1 c) Technician : VAB.0001201080 ..Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A CER X R X EE OR ANALYSIS Date: November 23, 1992 Customer: Intex Plastics Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: November 20, 1992 Fax No. 601-286-9402 VISTAProduct: 5415 Railcar No Order No ACFX 41178 0018812-000 Property Inherent Viscosity Residual VCM, ppm Test Method ABR-10 ABGC-26 I PC Specification 1.00 - 1.04 8.5 PPM Max. Analvsis 1 .03 0.021 Contamination, BLK + BRN ABR-5A 20 Total Max Total Black + Brown Hard Particles 7 mins Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2B ABR-1A ABR-3 5 Max. 3 15 Sec. Max 11.2 0.460 Min. 0.510 0.30 Max. 0.18 25.0 Thru 140 Mesh Max 5.0 On Pan Max. % ON Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 5.0 Amy BU Bagwe Laboratory Supervisor (601) 369-3624 VAB.0001201081 Vista Polymers Highway 25 Aberdeen, MS 3973q A RADCILCAR ANALYSIS Load Date: U Product: Time Logged In: /g 3ft Logged In By: Ship Date: Kli*' . Order Ho: n%YV-'OQO Car Ho Silo(s): (o 90 Customer: ttonefoL- Compartment * Sample From A Bottom Top Hoisture % BL Contamination BR IP- Y 6 Bulk Density .To1- 5 Hard Particle > * ? 9 CA Bottom Top ./* 4' Y Y CB Bottom Top 9Y s~ ? B Bottom 7 'o Viscosity RVCM I. otS .02,1 Screen Analysis \ ***** - * ** - Mesh 40 Height % 0,00 6,0 60 (,t 80 100 120 la.*# Drytime: Static Flow: 0 Color L : jQO t*7 *7 b METS: 1035B ,12(7.1 x 140 200 Pan Lt- 17MAvg. Microns Technician VAB.0001201082 Vista Polymers A Division of } Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730*0091 Phone (601) 369-8111 CERTIFICATE OR ANALYSIS Date: November 23, 1992 Fax No. 601-286-9402 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 Product: 5385 Attention: Quality Control Dept Railcar No.: VIPX 45760 Ship Date: November 20, 1992 Order No.: 0018450-002 Property Inherent Viscosity Test Method ABR-10 I PC Specification 0.90 - 0.95 Analysis 0.93 Residual VCM, ppm ABGC-26 8.5 Max. 0.133 Contamination, BLK + BRN ABR-5A 40 Total A Total Black + Brown Hard Particles 8 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH % ON 15 Max. 6 15 Max. 11 .5 0.510 Min. 0. 575 0.30 Max. 0. 15 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins. ABR-7 6.0 Max 4.9 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor (601) 369-3624 4 VAB.0001201083 Viat-a Polymere Highway 25 A Aberdeen, MS 3973q PVC RAILCAR ANALYSIS Load Date: Time Logged In: Q630 Ship Date: lO Product: 5385 Logged In By: Order No: Car No. 4^? <P S i lo (6) : >7C&. Ct/77 Customer: //u/jfcy* Screen Analysis Mesh 40 Height X 0.0 60 80 100 120 140 200 Pan SL <3.10 7V/ 119c? Ml 7>Vr /.Jr Su 11.1 3S.t- itia Drytime: Static Flow: LIS'/ Avg Microns: ^ Color L : i00.39 UZ b is? Tech nician : r \J>^ VAB.0001201084 Vista Polymers A Division of Vista Chemical Company w Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone {601} 369-8111 A C EE R I R I OR ANALYSIS Date: November 23, 1992 Customer: Intex Plastics Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: November 18, 1992 Fax No. 601-286-9402 VISIAProduct: 5415 Railcar No Order No PLWX 44449 0018449-001 Property Test Method I PC Specification Analvsis Inherent Viscosity ABR-10 1.00 - 1.04 1 .03 Residual VCM, ppm ABGC-26 8.5 PPM Max. 1 .007 Contamination, BLK + BRN ABR-5A 20 Total Max Total Black + Brown Hard Particles 7 mins Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2B ABR-1A ABR-3 5 Max. 2 15 Sec. Max. 8.2 0.460 Min. 0.504 0.30 Max. 0. 16 25.0 Thru 140 Mesh Max 5.0 On Pan Max. % ON Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 4.9 is*m. Amy Bagwel1 Laboratory Supervisor (601) 369-3624 VAB.0001201085 Vieta Polyme re Load Date:__If h Time Logged n : Ship Date: 7^ Highway 25 Aberdeen, MS 397 3 0 A RAILCAR ANALYSTS Product: Logged In By: r Ho: CO/&*? Car No. Silo(6 ) : Cu6tome Compartment Sample From Moisture Bottom] Top Bottom Top Bottom I Top Bott om Contamination Bulk Density Hard Particl -rds Viscosity RVCM LMp l.ool Screen Analysis Mesh Height X 40 o-o 0,0 60 /.? Drytime: 80 100 3S.1 s/.r Static Flow: Color L /co -ft. a 120 ,*r /A? 140 7./ 200 U7 +.3 Pan . 30 Avg. Microns: U9.S b 'technician ntTS *144r rz X VAB.0001201086 Vista Polymers A Division of Vista Chemical Company Highwoy 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601} 369-8111 CERTIFICATE OR ANALYSIS Date: November 20, 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 36834 Attention: Quality Control Dept. Ship Date: November 16, 1992 Fax No. 601-286-9402 XV/IICoTlAA Product: 5325 Railcar No.: VIPX 45251 Order No.: 0018452-000 ProDertv Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A Total Black + Brown Soecification Analysis 0.78 - 0.82 0.80 8.5 PPM Max. 0.172 Not Yet Determined A I CA I CB I B I 14 I 12 I 15 I 13 1 Dry Flow, Seconds ABR-8 15 Sec. Max. 12.7 Bulk Density, gm/cc ABR-2A 0.480 Min. 0.493 Moisture, % ABR-1A 0.30 Max. 0.15 Particle Size Distribution ABR-3 5.0 Max. on Pan 1 40 1 60 1 80 1I 100I 120I 140I 200I pan! SIS ON 1 o.ol 0.3I 6.11Il6.6l34.ll27.7li4.4l 0.8l Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy Et Bagwei1 Laboratory Supervisor (601) 369-3624 VAB.0001201087 Vista Polymers Highway 25 A Aberdeen, MS 3973q IRA X LCAR ANALYSIS Load Date: __ /A/7- Time Logged In: fCoo l( I f7 Ship Date Product: Car No. ?33 9? Logged In By: Order No: 0 C>l%4&2-1X)`Z' Silo(6 ) : Customer: jxJ *2. Compartment A Sample From Bottom Moisture % BL Contamination BR . )U 4 1 Bulk Density .CM BD after Fluff .01 Hard Particle 5 7 Viscosity RVCM dll 40 Mesh/Glassies * ^* * *4 Screen Analysis Mesh 40 Weight % 0.00 0*0 60 _ ,U /.l CA Bottom n t 0f >'7? CB Bottom . 3 7 4'72- B Bottom J3 + . 7 I L 80 % So /%* 100 2t.& 120 >3.19 It. 3 140 zrr jS. 1 200 4./0 Pan TO J.C, Drytirae: -* Static Flow: 0 Avg . Mic rons: Color L: /0O. &0 -OS' b /.77 Technician: >*1^/ VAB.0001201088 4 Vta Polymen A Division of Villa Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aberdeen, Mississippi 39730 Phone (601) 369-8111 : November 17, 1992 Fax No. 601--286--9402 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 VIS1AProduct: 5385 Attention: Quality Control Dept Railcar No.: PLWX 44276 Ship Date: November 13, 1992 Order No.: 0018450-000 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A Total Black + Brown 0.90 0.95 8.5 Max. 40 Total A CA 14 15 0.94 0.586 CB B 21 32 Hard Particles 7 Mins. ABR-12 15 Max. 2 Dry Flow, Seconds ABR-8 15 Max. 7.9 Bulk Density, gm/cc ABR-2A 0.510 Min. 0.579 Moisture, % ABR-1A 0.30 Max. 0.10 Particle Size Distribution ABR-3 25.0 Thru 140 Mesh 5.0 Max on Pan MESH 40 | 60 | 80 100 120 140 200 % ON 0.00 0.9|l7.9 |25.5 28.4 16.1 9.1 PAN 2.1 Brabender Dry Time, Mins. ABR-7 6.0 Max 4.8 Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E Bagwe Laboratory Supervisor (601) 369-3624 VAB.0001201089 Vieta Polymers Highway 25 A Aberdeen, MS 3973q Load Date: PVC RAILCAR ANALYS X S 9A Product: Car No pLtofl Time Logged In:.. Ship Date: Logged In By: Co Silo(6): L2jL??MT D D (3 4-So'to> Custome r: /ncJ*P Compartment Sample From A Bottom Moisture % BL Contamination BR ,o4 _Y_ Bulk Density BD after Fluff .sv Hard Particle 5 7 Viscosity RVCM * X 40 Mesh/Glassies * f *4 * -r * 4* i Screen Analysis Mesh 40 Weight .0 % 0< o 1 60 CA Bottom i o3> 3 IZ , SIS' CB Bottom .OS' -T., 5--T-f->-*-- B Bottom . Ip f n m rn 1* f # _z______ fr 80 173 100 120 -f1-O2J.--7f--s--' fS.93 a s r . 2LAi 140 K.( - 200 7S3 Pan Lai Drytime: Static Flow : o /7'9 Avg . 1tl ic rons : ifr* Color L: tt>. / 7 a b LT7 Technician VAB.0001201090 t*mih/ Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE 07 ANALYSIS Aberdeen, Mississippi 39730 Phone |601) 369-8111 A : November 17, 1992 Fax NO. 601--286--9402 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 VISIAProduct: 5365 Attention: Quality Control Dept Railcar No.: VIPX 45873 Ship Date: November 16, 1992 Order No.: 0018450-001 Property TestMethod IPC Specification Analysis Inherent Viscosity ABR-10 0.90 0.95 0.93 Residual VCM, ppm ABGC-26 8.5 Max. 0.097 Contamination, BLK + BRN ABR-5A 40 Total A CA CB B Total Black + Brown 19 17 21 14 Hard Particles @ 7 Mins. ABR-12 15 Max. 4 Dry Flow, Seconds ABR-8 15 Max. 9.5 Bulk Density, gm/cc ABR-2A 0.510 Min. 0.584 Moisture, % ABR-1A 0.30 Max. 0.17 Particle Size Distribution ABR-3 25.0 Thru 140 Mesh 5.0 Max on Pan MESH 40 60 80 100 120 140 200 PAN % ON 0.00 0.5 10.8 12.2 40.5 19.5 13.9 2.6 Brabender Dry Time, Mins. ABR-7 6.0 Max. 5.0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor (601) 369-3624 VAB.0001201091 Viata Polymers Highway 25 A Aberdeen, MS 39730 Load Date: Tk RAILCAR ANALYSIS \hH Product Car No Time Logged In: 1150. Logged In By: Ship Date: nfif* Order No: Qoii^Sb-ta( SiIo(6): Customer: A!b~htej*t.-- Compartment From Moisture % Bottom Botto Bottom Botto Contamination Bulk Density BD after Fluff Hard Particle Viscosity RVCM Mesh/Glassies / Screen Analysis Mesh Weight % 40 0^00 0.0 60 o.&fr 80 & M&- 100 fe.lZL 120 im. 140 200 17C. ags 17s 07 Pan L3I Drytime : Static Flow: & /%^ Avg. Hicro n s pM. Color L: lPC t r<> b JJA Technician : fer+HM VAB.0001201092 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone 1601)369-8111 h CERTI Date: November 17, 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: November 16, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A ANALYSIS Fax No. 601-286-9402 VISTA Product: 5325 Railcar No Order No VIPX 45844 0018177-002 Specification Analvsis 0.78 - 0.82 0.80 8.5 PPM Max. 0.474 Not Yet Determined Total Black + Brown Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2A Moisture, % ABR-1A Particle Size Distribution ABR-3 15 Sec. Max 0.480 Min. 0.30 Max. 5.0 Max. on Pan 13.8 0.495 0.24 % ON Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy EL BagweTl Laboratory Supervisor (601) 369-3624 VAB.0001201093 Vista Polymers Highway 25 Aberdeen, MS 39730 toS Load Date: // -it- Time Logged In: Ship Date : /III t> Product: Logged In By: Order No:. i<&rt 7-001' Car No Silo( s) : : Itftuj Customer Compartment A Sample From Bottom Moisture BL Contamination BR Bulk Density 3 7 BD w/antistat Viscosity RVCM J5o4. .M Screen Analysis Mesh 40 Weight % Q.O 60 -i CA CB -------------------------------------------------------------------------------------- 1 Bottom Bottom . 19 Z .? 'Zo 1 099 . B Bottom s <r .SIS y M 4 80 Ayf s.o 100 LHl* 120 /?.37 39.0 140 lS.3f 30.7 200 10.21 Q0.U Pan .99/.? CPA: X.O % Glassies: Z' !% Avg. Microns: J10. ^ Color L: $9.89'* b JSO Stat:ic Flow: O / Technician: .................... _ ... - C& -- W I , r/1 sr*- - -- immm ,, -- A VAB.0001201094 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A O EE R I R I E OR ANA 3X5 Date: November 13, 1992 Customer: Intex Plastics Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: November 11, 1992 Fax No. 601-286-9402 VISTAProduct: 5415 Railcar No Order No PLCX 47624 0018449-000 Property Test Method IPC Specification Analysis Inherent Viscosity ABR-10 1.00 - 1.04 1 .03 Residual VCM, ppm ABGC-26 8.5 PPM Max. 0.098 Contamination, BLK + BRN ABR-5A 20 Total Max Total Black + Brown Hard Particles 7 mins Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2B ABR-1A ABR-3 5 Max. 1 15 Sec. Max 11.5 0.460 Min. 0.507 0.30 Max. 0.18 25.0 Thru 140 Mesh Max 5.0 On Pan Max. % ON Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 4.9 Amy E. Bagwe VI Laboratory Supervisor (601) 369-3624 VAB.0001201095 O Vista Polymers Highway 25 Aberdeen, MS 39?3 HArLCAR analysis Load Date: Time Logged Ship Date: 1/- 7~<?2- Product: Car No noo Logged In By: Silo(6): Order Ho: OP I 449-ftOA Custom or * Compartment Sample From Moisture X Contamination Bulk Density Botto Top Bottom Top Bottom Top Botto Top /A? Hard Particle Viscosity RVCM 03Z^ Screen Analysis Mesh Height 40 &&O X 60 O./o 0-A Drytime: *1 80 ?9S !l>-o 100 3 ho 120 U.<7 140 IS ^ 200 Lis Sr 3 Static Flow: O Avg. Microns: Pan A If 2.4 I Color L: /GO,8 fX b I >30 METS: Technician: JuLX^ VAB.0001201096 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OR ANALYSIS Date: November 11, 1992 Fax No. 601-286-9402 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 Product: 5385 Attention: Quality Control Dept Railcar No.: GACX 73389 Ship Date: November 6, 1992 Order No.: 0017372-003 Property Test Method I PC Specification Analvsis Inherent Viscosity ABR-10 0.90 - 0.95 0.93 Residual VCM, ppm ABGC-26 8.5 Max. 0.465 Contamination, BLK + BRN ABR-5A 40 Total Total Black + Brown Hard Particles 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH % ON 15 Max. 4 15 Max. 8.0 0.510 Min. 0.580 0.30 Max. 0.07 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins. ABR-7 6.0 Max 4.7 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor (601) 369-3624 m r m mmmmmmmi VAB.0001201097 Vxeta Polymers Highway 25 Aberdeen, MS 39730 RAILCAR ANALYSIS Load Date *___ //- Time Logged In: Ship Date:. k| Product: ?3O Logged In By: Order Car No. rrt ,7 if.;h Silo(e) : Customer: /V1> j*e.+CL f Compartment A * Sample From Bottom CA Bottom CB Bottom B ---------------------- Bottom Moisture % BL Contamination BR 4 Bulk Density . O 2-- 7 BD after Fluff Hard Particle 5 7 Viscosity RVCM * u 4D Mesh/Glassies f . - ** * n m /o y pt&fclEj . -44 lc>3 whites .O J n .581 -07 r i 56/ ____________________________________________________ Screen Analysis * 1 Mesh Weight 40 >'0 0.0 60 80 100 120 140 200 <5*7/ I2.-Z3, +/ #f 1.sY5 f.ff? jT.A 6 r !>**? / 7. % //-3 Pan * Dry ti roe : sn. Static F low : 0/2*0 Avg. Microns: JJ&L Color L- fco .3 / a ~0oS b ft 67 Technician: 4- VAB.0001201098 Vista Polymers A Division of Vista Chemical Company r Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730*0091 Phone (601) 369-8111 A CERTX F^I Date: November 10, 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: November 9, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A Fax No. 601-286- 9A Product: 5325 Rail car No Order No UTCX 46414 0018177-001 Specification Analysi 0.78 - 0.82 0.81 8.5 PPM Max. 0.130 Not Yet Determined Total Black + Brown Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2A Moisture, % ABR-1A Particle Size Distribution ABR-3 15 Sec. Max 0.480 Min. 0.30 Max. 5.0 Max. on Pan 8.5 0.500 0.22 % ON Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E. Bagwe11 Laboratory Supervisor (601) 369-3624 VAB.0001201099 Vista Polymers Highway 25 Aberdeen, MS 39730 k Load Date: Time Logged Ship Date: M 11 H RAX LCAR U Product: Car No Logged In By: Order No: Q0ll\7>06 ! Silo(s) Customer: In&4 VUQ Compartment A CA Sample From Bottom Bottom Moisture ./f BL Contamination BR JL_ 7 Bulk Density 3 <. BD w/antistat Viscosity RVCM 2>[h . OP! L-------------- 150 * <2fc CB Bottom o? * MT$ M .oat B Bottom .J>2. ? .Bon Screen Analysis Mesh 40 Weight x Q 0.0 ( 60 JO .3 80 100 120 140 200 Pan IMd. UM um -sjf /.x 39,3. CPA: % Glassies: //% !2iJAvg. Microns: Color L: a J1 b hrs Static Flow: 0 / Technician: VAB.0001201100 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 4 C EE R X R X CAT Date: November 5, 1992 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38S34 Attention: Quality Control Dept Ship Date: November 2, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A X3 Fax No. 601-286-9402 VISTAProduct: 5385 Railcar No UTCX 46452 Order No 0017771-001 I PC Specification Analysis 0.90 - 0.95 0.93 8.5 Max. 0.100 40 Total Total Black + Brown Hard Particles 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH % ON 15 Max. 2 15 Max. 12.9 0.510 Min. 0.583 0.30 Max. 0.16 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins ABR-7 6.0 Max. 4.8 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor (601) 369-3624 VAB.0001201101 Vieta Polymera Highway 25 Aberdeen, MS 3973Q ^VC R A ILCAR ANALYSIS Load Date: _ to Product: Time Logged In: 2~<foO Logged In By: Ship Date: m2- Order No: 0'C> 1*1 Car No. : Silo( 6 ) : Customer: AW Compartment A Sample From Bottom Moisture % BL Contamination BR c? s Bulk Density .SI 7 BD after Fluff Hard Particle 5 7 3 A, Viscosity RVCM Mesh/Glassies *f Screen Analysis Mesh 40 Weight % 0.0 60 Drytime: v.f CA Bottom 3 7 l St7 CB Bottom ,S7S B Bottom 3 X 4 JL ______________________,__________________________ 80 7 .to )U 100 13.>4 7 3 Cl 120 P.90 26.7- 140 /4,r 200 -sr.sr ll./ Pan UL 2.3 Static 1j'low: ^ / /?^ Ave. Microns: -- 3(.Color L: /*o. a .17 b J;L3 Technician: VAB.0001201102 Vista Polymers A Division of Vista Chemical Company I* Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730>0091 Phone (601) 369-8111 Date: November 6y 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 3S834 Attention: Quality Control Dept Ship Date: November 4, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A Fax No. 601- m\ Product: 5325 Railcar No Order No ACFX 41157 0018177-000 Specification Analvsis 0.78 - 0.82 0.81 8.5 PPM Max. 0.025 Not Yet Determined Total Black + Brown Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2A Moisture, % ABR-1A Particle Size Distribution ABR-3 15 Sec. Max 0.480 Min. 0.30 Max. 5.0 Max. on Pan 12.4 0.487 0.16 X ON Polyvinyl Chloride, Virgin Resin, Not Reprocessed Laboratory Supervisor (601) 369-3624 VAB.0001201103 J4 Vista Polymers Highway 25 A Aberdeen, MS 39730 Ft A X LCAR ANALY S X S Load Date: Product: 5325 Time Logged In: Logged In By: Ship Date: miOrder No: OO/S/^T Car No. : Silo(s): Customer *7 Compartment A Sample From Bottom Moisture ./J BL Contamination BR 3 Bulk Density BD w/antistat .<fti Viscosity RVCM CA Bottom + sr CB Bottom * 3 S B Bottom ./{ Screen Analysis Mesh 40 Weight A.QO % 0+ O CPA: an 60 2L 80 &.t /J.7 100 -M..A * Zi. iT 120 n.ot* j*. 1 140 200 +r Pan /./* 3. 1 % Glassies: < /fl. Avg. Microns: 141.7 Color L: ^*7.7^ a * b a/2- Static Flow: <0 / Technician: 7 VAB.0001201104 Vista Polymers A Division of Vista Chemical Company G Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601)369-8111 A C E R IFICATE OR ANA 3X3 Date: November 5, 1992 Fax No. 601-286-9402 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 VIS1AProduct: 5385 Attention: Quality Control Dept Railcar No. VIPX 45913 Ship Date: November 2, 1992 Order No. 0017771-002 Property Test Method I PC Specification Analysis Inherent Viscosity ABR-10 0.90 - 0.95 0.93 Residual VCM, ppm ABGC-26 8.5 Max. 0.221 Contamination, BLK + BRN ABR-5A 40 Total Total Black + Brown Hard Particles 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH % ON 15 Max. 2 15 Max. 10.4 0.510 Min. 0.590 0.30 Max. 0.04 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins. ABR-7 6.0 Max. 4.8 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. di Amy E. BagweTl Laboratory Supervisor (601) 369-3624 VAB.0001201105 Viata Polymers KJBoJ vJAreg. Highway 25 K Aberdeen, MS 3973Q IRA. I LCAR ANALYSIS 10 9-9,3, Load Date: Product: Car No.: Time Logged In:.M3Q Logged In By: Silo(s ) : Ship Date: Order No: OC)l ]~>02-- Customer: 1 ttL Compartment A Sample From Bottom Moisture % BL Contamination BR Bulk Density BD after Fluff S21 Hard Particle 5 Jr 7 Viscosity RVCM A* I Mesh/Gla * Screen Analysis Mesh Weight 40 0.0 %P 60 . t.7 CA Bottom jf CB Bottom B Bottom 9 ( i L 80 y/Y 100 tJS~f Into 120 140 *77 200 /AJ Pan Drytime: :M.S Static Flow: ^ //oA Avg. Microns: Color L : /Q&. "? / >'*'> b lAA Technician: Mil VAB.0001201106 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS Date: November 2, 1992 Customer: Intex Plastics Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: October 29, 1992 VIS1AFax No. 601-286-9402 Product: 5415 Railcar No.: UTCX 46523 Order No.: 0017772-001 Inherent Viscosity ABR-10 1.00 1.04 Residual VCM, ppm ABGC-26 8.5 PPM Max. Contamination, BLK + BRN ABR-5A 20 Total Max A CA Total Black + Brown 10 13 1.01 0.057 CB B 19 18 Hard Particles @ 7 mins ABR-12 5 Max. 2 Dry Flow, Seconds ABR-8 15 Sec. Max 8.0 Bulk Density, gm/cc ABR-2B 0.460 Min. 0.515 Moisture, % ABR-1A 0.30 Max. 0.23 Distribution % ON ABR-3 25.0 Thru 140 Mesh Max 5.0 On Pan Max. 40 | 60 80 _' 100 120 140 200 PAN 0.00 1.9 00 0 Is* 64 31.4 20.6 9.9 1 6.5 1.9 Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 4.8 aJJ Amy E Bagwe Laboratory Supervisor (601) 369-3624 VAB.0001201107 Vista Polymer's Highway 25 Aberdeen, MS 3973q * Load Date: Time Logged Ship Date : /0 JOtf R A DC LCAR ANALYSIS UTO/ Product: Logged In By: Orde DC> Car No.: Silo(6): / Customer: AJQ ?7t6hU___ Compartment * Sample From A Bottom Top Moisture % BL Contamination BR .133 Bulk Density .573 5 Hard Particle 7 2 2 HbL_ Viscosity iM RVCM ,057 CA Bottom Top CB Bottom Top >31 B Bottom Top 5 iSL J>7(s> I Screen Analysis *m Mesh 40 Height O 0O % 60 J3_ 80 100 120 140 200 Pan MM . VIS aV7 -fi- Drytime: Static Flo Avg. Microns Color L: ClOS b ilk 10333 /144-Skx METS: Technician: VAB.0001201108 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 * CERT I I OAT EE O Date: November 3, 1992 Customer: Intex Plastics Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: October 27. 1992 Property Test Method Inherent Viscosity ABR-10 Residua1 VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A ANA 3XS Fax No. 601-286-9402 VIS1AProduct: 5416 Railcar No.: PLCX 47628 Order No. :. O017772-000 I PC Specification 1.00 - 1.04 8.5 PPM Max. 20 Total Max Analvsis 1.03 0.003 Total Black + Brown Hard Particles 7 mins Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2B ABR-1A ABR-3 5 Max. 1 15 Sec. Max 8.0 0.460 Min. 0.510 0.30 Max. 0.15 25.0 Thru 140 Mesh Max 5.0 On Pan Max. X ON Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 5.0 Amy E. Bagw Laboratory Supervisor (601) 369-3624 VAB.0001201109 Vista Polymers Highway 25 Aberdeen, MS 3973q Load Date: -J* Time Logged Ship Date: RArLCAK ANALYSIS pud Product: Logged In By: Car No.: Silo(6): Customer: AC W Compartment m_ Sample From A Bottom Top CA Bottom Top CB Bottom Top Moisture % BL Contamination BR . /$ 3 f Bulk Density 5 Hard Particle 7 Viscosity I ,/x r .// 7 r/r" J r RVCM .005 B BottomI Top _r c. i r// Screen Analysis U - Mesh 40 Weight Aoa % 0*0 60 80 100 120 140 200 Pan /t.n. / T1 /> 24' 7* 17.0 n*a ?~0 Dry time -* .0 Static Flou <3 / 1*0 Avg. Microns: *7).? Color L: /^0. f/ -JC -O. 7tf b / 2/ Technician: /o/4s / V/- Q> /kid?* VAB.0001201110 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A CERTIFICATE OR ANA 3X3 Date: October 29, 1992 Fax No. 601-286-9402 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 VIS1AProduct: 5385 Attention: Quality Control Dept Railcar No.: UTCX 46486 Ship Date: October 28, 1992 Order No.: 0017771-000 Property Test Method IPC Specification Analysis Inherent Viscosity ABR-10 0.90 - 0.95 0.92 Residual VCM, ppm ABGC-26 8.5 Max. 0.064 Contamination, BLK + BRN ABR-5A 40 Total Total Black + Brown Hard Particles 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH % ON 15 Max. 2 15 Max. 0.510 Min. 0.30 Max. 10 .8 .0 580 .0 15 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins. ABR-7 6.0 Max. 5.0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed Z2 ------------XT-------Amy E. Bagwe Laboratory Supervisor (601) 369-3624 VAB.0001201111 Vista Polymers Highway 25 It Aberdeen, MS 3973ri UTqLPVC RAILCAR ANALYSIS Load Date : _/& - Product: Car No. C4FL Time Logged In: Logged In By: Ship Date: lb(2% r?2^ / Order No: OOIll'llI~COD Sllo(s) : C 1L Customer: aw fuaffll-- Compartment A Sample From Bottom Moisture % .07 BL Contamination BR /* Z-3 Bulk Density BD after Fluff Hard Particle 5 y CA Bottom .12- f & CB Bottom d3 B Bottom m: s jZL .370 Viscosity RVCM SH <o& 40 Mesh/Glassies o & / O Screen Analysis Mesh 40 Weight % o 60 6>-0^ 80 O.i /3.Z 100 120 / /// 4f- 7f 27.9 7.7 140 9.30 200 5rr/ /(.o Pan Drytiroe: SO Static Flow: 1Zo7 Color L: too.fZ list/faX Avg. Microns: b 1.70 Technician: VAB.0001201112 Vista Polymers A Division of Vista Chemical Company o Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 h Ccm R I F I E OR ANALYSIS Date: October 29, 1992 Fax No. 601-286-9402 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 VIS1AProduct: 5385 Attention: Quality Control Dept Railcar No PLCX 43923 Ship Date: October 27, 1992 Order No 0017642-000 Property Test Method IPC Specification Analysis Inherent Viscosity ABR-10 0.90 - 0.95 0.92 Residual VCM, ppm ABGC-26 8.5 Max. 0.190 Contamination, BLK + BRN ABR-5A 40 Total Total Black + Brown Hard Particles 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH % ON 15 Max. 2 15 Max. 9.4 0.510 Min. 0.590 0.30 Max. 0.15 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins. ABR-7 6.0 Max. 4.4 Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E. Bagwerl Laboratory Supervisor (601) 369-3624 VAB.0001201113 Vista Polymera Highway 25 A Aberdeen, MS 39730 Load Date: Time Logged In: Ship Date: iDfiXl JR AILCAR ANALYSIS Product: Ca r No.: . Logged In By: Silo(s): Order Wo: ODIOf. 4Z ~Da> Customer: fjv'hiefo Screen Analysis Mesh Weight % 40 4, > > a d> 60 / P 71 80 It 3 P< 100 120 Drytiroe: tf- Static Flow: ^ Color L : ^oK. a ^ ^ 140 200 foM C=>\ Pan &.zg Avg. Microns: KA t ^ Technician: r # VAB.0001201114 Vista Polymers A Division of Vista Chemical Company o Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601)369-8111 * CERTIFICATE OR ANIA SX3 Date: October 29, 1992 Fax No. 601-286-9402 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 VISTAProduct: 5385 Attention: Quality Control Dept Railcar No.: GACX 73383 Ship Date: October 28, 1992 Order No.: 0017372-002 Property IPC Test Method Specification Analysis Inherent Viscosity ABR-10 0.90 0.95 0.93 Residual VCN, ppm ABGC-26 8.5 Max. 0.195 Contamination, BLK + BRN ABR-5A 40 Total Total Black + Brown Hard Particles 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH X ON 15 Max. 2 15 Max. 9.5 0.510 Min. 0.582 0.30 Max. 0.17 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins. ABR-7 6.0 Max. 5.0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E. Bagwel1 Laboratory Supervisor (601) 369-3624 VAB.0001201115 Vista Polymers Highway 25 h) Aberdeen, MS 3973Q IRA X LCAR ANALYSIS Q>kcd Load Date: _ /0*//m Time Logged In: 2300 > I %d slShip Date: Product: Logged In By: Order No: tk> H37 Car No.: 3 S3 SUo(s) : Customer*! Compartment A Sample From Bottom Moisture % .m BL Contamination BR 8 & Bu Ik Den sity BD after Fluff Hard Particle 5 7 2 **&-- Viscosity RVCM 40 Mesh/Glassies 0 CA Bottom 5 fir 0 Screen Analysis Mesh Weight % 40 0.00 00 60 0 33 80 O.f J? 100 CB Bottom 1? u B Bottom 17 <o 120 140 200 Pan 41 Ll 24- Drytime: Static Flow: ~ / ts Color L A If b W/ Avg. Microns: Technician: VAB.0001201116 Visto Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 11 CERTIFICATE OF ANALYSIS October October 26, 1992 Fax No. 601--286--9402 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 V1SIAProduct: 5385 Attention: Quality Control Dept NO.: VIPX 45251 Ship Date: October 23, 1992 i.asja.ajjir i1 vr:\aa.aaiBB!CTBi:,JT7:i;i:mlT:,r,rp ..rrTTrrTr: ".t:t r^aassaa Order No.: 0017372-001 Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A Total Black + Brown 0.90 - 0.95 8.5 Max. 40 Total A | 21 CA 25 Analysis 0.92 0.120 CB B 23 25 Hard Particles 6 7 Mins. ABR"12 15 Max. 5 Dry Flow, Seconds ABR-8 15 Max. 11.8 Bulk Density, gm/cc ABR--2A 0.510 Min. 0.571 Moisture, % ABR-1A 0.30 Max. 0.12 Particle Size Distribution ABR-3 25.0 Thru 140 Mesh 5.0 Max on Pan MESH 40 60 80 100 120 140 200 PAN % ON 0.00 0.4 16.6 32.7 26.5 14.1 8.0 1.7 Brabender Dry Time, Mins. ABR-7 6.0 Max 4.8 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. Bagwell Laboratory Supervisor (601) 369-3624 VAB.0001201117 Vista Polymers Highway 25 h \ Aberdeen, MS 39730*" RVC RAILCAR ANALYSIS Load Date: Time Logged In: Ship Date: Product: Logged In By: 7^ Order No: <9017.^12 Car No.: Silo(6): Customer: AJc r^ebt Compartment Sample From Moisture % Bottom Contamination Bu Ik Den s ity Fluff Hard Bottom Bottom S'?* Bottom Viscosity RVCM 40 Mesh/Glassies Screen Analysis Mesh 40 60 80 100 120 140 Weight d 0& o. "20l /< (34s % 0.0 &4-- 200 to Pan tab J7- Drytime: it 9Static Flow: itix Avg. Microns: Color I./ o.of b LUL Technician: (o\W VAB.0001201118 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFI Date: October 26, 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: October 23, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 h ANALYSIS Fax No. 601-286-9402 VISTA Product: 5325 Railcar No Order No ACFX 41163 0017193-002 Spec1fication Analysis 0.78 - 0.82 0.81 8.5 PPM Max. 0.180 Not Yet Determined Total Black + Brown Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2A Moisture, % ABR-1A Particle Size Distribution ABR-3 15 Sec. Max 0.480 Min. 0.30 Max. 5.0 Max. on Pan 9.1 0.499 0.19 % ON Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E. Bagw Laboratory Supervisor (601) 369-3624 VAB.0001201119 Vista Polymers Highway 25 Aberdeen, MS 39730 A FtA X LCAR ANALYS X S Load Date : /*>' i*~ Time Logged In: 2,10* Ship Date: Product: Logged In By: Order No: I *1 Car No.: 4/M3 /9<J Silo(s): & ! J 072---"Customer: Compartment Sample From Moisture Contamination Bottom , /? Bottom Bottom , /*? Bottom Bulk Density BD w/antistat Viscosity RVCM SJ r 0$ (p .oti tYfe- .12 7 .l%o Screen Analysis Mesh 40 Weight % 0*0 CPA: 9^6 ^ 60 80 . n .79 .3 //.+ 100 13. IV 120 / 7'<J 3S-.9 140 *J2. y/.* 200 s~.* Pan /. 1 % Glassies: Avff. Microns: At*. 2- Color L: 1 a 4^ b Li 2- Static Flow: 0 /_/ Technician: 7 VAB.0001201120 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A Date: October 22, 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Dept* Ship Date: October 19* 1992 Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A Fax No. 601-286-9402 VK1A Product: 5326 Railcar No.: UTCX 46552 Order No.: 0017193-001 Specification 0.78 - 0.82 0.81 8.5 PPM Max. 0.112 Not Yet Determined Total Black + Brown Dry Flow, Seconds ABR-8 Bulk Density, gn/cc ABR-2A Moisture, X ABR-1A Particle Size Distribution ABR-3 15 Sec. Max. 0.480 Min. 0.30 Max. 5.0 Max on Pan 8.7 0.491 0.17 X ON Polyvinyl Chloride, Virgin Resin, Not Reprocessed. _ Laboratory Supervisor (601) 369-3624 VAB.0001201121 > Vista Polymers Highway 25 Aberdeen, MS 39730 Load Date: Product: Time Logged In:. 1730 Logged In By: Ship Date: Order No: OQII Car No.: Silo(s): 00/ Customer: ?m rts ls. M Compartment A Sample From Bottom Moisture / 2^ _ BL Contamination BR y r Bulk Density */ Yf BD w/antistat Viscosity m RVCM Bob JiZ Screen Analysis Mesh Weight %f 40 t*> .c> 60 O-H * CA Bottom _ . / 5^ ^L> MSI MZ CB Bottom n 3 7 . SOI ,g6 'D7b B Bottom , /& Y r '.r<r/?VxL<?# .Sol ,oti 80 /S--L. 100 19. V> 30.-7 120 /L.L7 33-3 140 (?_%/.. i3h 200 Pan JJL... ./.jg- 3.(0 y--o CPA: o- $ % Glassies: Avg. Microns: (SO. Color L: /0^'03 a OSO b A&7 Static Flow: Technician: /rf/ *T & ~hf > VAB.0001201122 G > Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS A Date: October 21, 1992 Fax No. 601--286--9402 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 VIS1AProduct: 5385 Attention: Quality Control Dept Railcar No.: VIPX 45827 Ship Date: October 19, 1992 Order No.: 0017373-000 Test Method IPC Inherent Viscosity ABR--10 0.90 0.95 0.92 Residual VCM, ppm ABGC-26 8.5 Max. 0.303 Contamination, BLK + BRN ABR-5A 40 Total Total Black + Brown Hard Particles @ 7 Mins. ABR-12 15 Max. 2 Dry Flow, Seconds ABR-8 15 Max. 8.3 Bulk Density, gm/cc ABR-2A 0.510 Min. 0.578 Moisture, % ABR-1A 0.30 Max. 0.16 Particle Size Distribution ABR-3 MESH 40 60 25.0 Thru 140 Mesh 5.0 Max on Pan 80 | 100 12o| 140|| 200 | PAN % ON o oo 0.2 14.8 28.1 28.5 15.8 10.3 2.3 Dry Mins. ABR-7 6.0 Max. 5.0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. Bagw&Il Laboratory Supervisor (601) 369-3624 VAB.0001201123 Vista Polymers Highway 25 * v. Aberdeen, MS 39730 RVC RAILCAR ANALYSIS \JtW Load Date: ~ if f Time Logged In: /> <* Ship Date: Product: Car No Logged In By: Silo(s) : Order No : QD IC&I) Customer: Compartment A Sample From Bottom Moisture % BL Contamination BR Bulk Density BD after Fluff . if 6 Znk Hard Particle 5 7 Viscosity RVCM 40 Mesh/Gl Me. <303 CA Bottom L jffo CB Bottom -1 (t> 3 9 / B Bottom 4 Screen Analysis Me6h 40 Weight % 0*00 0,0- 60 . * . 2- 80 7* /*/ 100 ** i 120 J4kS2 140 7. t/ 200 Pan /* y 2.3 Drytime: Static Flow: *-/ S J Avg. Microns Color L: ^ b 21/0 Technician: VAB.0001201124 Vista Polymers A Division of Vista Chemical Company c Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS Date: October 21, 1992 Fax No 601-286-9402 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 Product VIS1A Attention: Quality Control Dept PTLX 41650 Ship Date: October 16, 1992 Order No 0016920-003 I PC Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN ABR-10 ABGC-26 ABR-5A Total Black + Brown 0.90 - 0.95 8.5 Max. 40 Total A CA 8 11 0.91 0.060 CB B /& I 1Z- Hard Particles 7 Mins. Dry Flow, Seconds ABR-12 ABR-8 15 Max. 15 Max. 2 j- 13 4 Bulk Density, gm/cc ABR-2A 0.510 Min. 0. 556 Moisture, % ABR-1A 0.30 Max. 0. 10 Particle Size Distribution ABR-3 25.0 Thru 140 Mesh 5.0 Max on Pan MESH 40 60 80 100 120 140 200 PAN % ON 0.00 0.3 14.6 30.3 27.7 15.3 9.6 2.2 Brabender Dry Time, Mins. ABR-7 6.0 Max. 4.9 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor (601) 369-3624 VAB.0001201125 Vista Polymers Highway 25 A Aberdeen, MS 3973Q RAILCAR ANALYSIS VTUl Load Date lo Product: Car No. Time Logged In: fO^O Logged In By: Silo(6): Ship Date: Order No: f)T) I (/> Z-O ^00 *i> <nrv\rf/oi$L Compartment A Sample From Bottom Moisture % BL Contamination BR j Bulk Density BD after Fluff CA Bottom , n> * CB Bottom ro 8 B Bottom i 10 3 Screen Analysis Mesh Weight % 40 0,00 0.0 60 A3 .2 80 7.3o m. to 100 JSJ 2 Or 3 120 13.11/ 37.7 140 7U 15,2 200 7>(p Drytime: Hil Static Flow: 0 L IM Avg. Microns: Color L: fPo.S f S- b <^H/ Pan Technician: VAB.0001201126 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A ERT I F- XC--^ -iw-- _ M'i" Date: October 16, 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: October 14, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A ANALYSIS Fax No. 601-286-9402 VISTA Product: 5325 Railcar No Order No VIPX 45878 0017193-000 Specification Analysis 0.78 0.82 0.81 8.5 PPM Max. 0.081 Not Yet Determined Total Black + Brown Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2A Moisture, X ABR-1A Particle Size Distribution ABR-3 15 Sec. Max 0.480 Min. 0.30 Max. 5.0 Max. on Pan 10.9 0.499 0.15 X ON Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy Ev Bagwell Laboratory Supervisor (601) 369-3624 VAB.0001201127 Vista Polymers Highway 25 Aberdeen, MS 39730 A Load Date: Time Logged In: io nthShip Date:_ ^ RAX LCAR SIS V//V Product: Car No. 4rj 7 9 Logged In By: /t O Silo(s): Order No: no t'l143-ooti Customer: C &B7e> si* jtf Screen Analysis Mesh 40 Weight % 0<0 CPA: __A4A 60 80 100 120 140 200 Pan ,// i.SJ /H/3 /7./JT f*/P 2.V1 /. /3 - /J. 2. J>/.3 SMC r.o % Glassies : ^/ Avg. Microns: in.1 Color ai.9t a . b f.ti Static Flow: 0 / .? Technician: u.p 7 fo n VAB.0001201128 3<WX RAILCAR SHIPMENT ORDER TO DIVERT/RE-SHIP/RETURN -to'fym y i*, f\& <-o <?t- DATE: A RAILCAR NUMBER: ORIGINAL SHIP DATE: ORIGINAL ORIGIN PLANT: </<gS' 7/ La/13. L ORIGINAL PRODUCT WEIGHT: PRODUCT NAME & CODE: ORIGINAL CUSTOMER: ORIGINAL CUSTOMER LOCATION ORIGINAL ORDER NUMBER: NEW CUSTOMER: NEW LOCATION: ?Q2oC)a PiB p NEW ORDER NUMBER: DO YOU NEED RAILCAR RE-WEIGHED? (YES/NO) REASON FOR CHANGE: (EG. off-spec, etc.) CAR RELEASED (YES7NO): billing instructions must be communicated to rail freight & comSSSi FOfl ,SSU,NG BILL OF ON OR BEFORE THE DAY THE CAR IS RELEASEO. C OTHER COMMENTS: kJM-B- CUSTOMER SERVICE REPRESENTATIVE: jpc<xij^ o *l5FON: PLANT, HOUSTON - RAIL FREIGHT& CONTRACTS, HOUSTON - RAIL OPBRA T/ONS fcs- vmmmmm mrnmmmmmmmmmmi VAB.0001201129 to Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSIS A Date: October 14, 1992 Fax No. 601-286-9402 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 VIS1AProduct: 5385 Attention: Quality Control Dept Railcar No.: UTCX 46571 Ship Date: October 13, 1992 Order No.: 0016920-002 Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A Total Black + Brown 0.90 0.95 8.5 Max. 40 Total A CA 8 11 Analysis 0.92 0.086 CB B 9 11 Hard Particles 6 7 Mins. ABR-12 15 Max. 2 Dry Flow, Seconds ABR-8 15 Max. 10.1 Bulk Density, gm/cc ABR--2A 0.510 Min. 0.581 Moisture, % ABR-1A 0.30 Max. 0.11 Particle Size Distribution ABR-3 MESH % ON 40 60 00 o oo o 25.0 Thru 140 Mesh 5.0 Max on Pan 80 100 120 140 2 001 PAN 20.1 30.2 23.6 13.6 9.2[ 2.5 Brabender Dry Time, Mins. ABR-7 6.0 Max 5.0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E. Bagwell Laboratory Supervisor (601) 369-3624 VAB.0001201130 Vista Polymers Highway 25 A Aberdeen, MS 39730 Load Date: Ship Date: RVC RAX LCAR ANALYSIS -7^ Product: Car No ucrcjL Logged In By: I (5"72-0 Silo(s): Compartment A Sample From Bottom Moisture % BL JContamination BR <r Bulk Density *ilO BD after Fluff Hard Particle CA Bottom 3 CB Bottom .Sfl B Bottom 7 Viscosity RVCM Mesh/Glas6 * * Screen Analysis Mesh 40 Weight % 6* <0 1 L 60 0<Y 80 100 120 140 /3V^ UK t. 1? 1^1 3. Lkk 200 YU Pan L 2J. Drytime: S,<o fStatic Flow: ^ / 1ft/ Avg. Microns: /-^ Z_. Color L: /oo. 4.4 J 1;*# b Technician V1 /P M- VAB.0001201131 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A p* C I FICATE OR AMAL.V'SX S Date: October 13, 1992 Fax No. 601-286-9402 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 VISTAProduct: 5385 Attention: Quality Control Dept Railcar No VIPX 45913 Ship Date: October 9, 1992 Order No 0016920-001 Property IPC Test Method Specification Analysis Inherent Viscosity ABR-10 0.90 0.95 0.93 Residual VCM, ppm ABGC-26 8.5 Max. 0.050 Contamination, BLK + BRN ABR-5A 40 Total Total Black + Brown Hard Particles 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH % ON 15 Max. 2 15 Max. 9.2 0.510 Min. 0.578 0.30 Max. 0.13 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins. ABR-7 6.0 Max. 4.9 Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E. BagweIr Laboratory Supervisor (601) 369-3624 VAB.0001201132 Vista Polymers Highway 25 A Aberdeen, MS 39730 Load Date - _ /O'""?* Time Logged In: Ship Date:_ io h RAILCAR ANALYSIS Product: Car ?r<2/3 Logged In By: Ib^ZO-OOl Order No Silo(s) Customer: Screen Analysis Me6h Weight % 40 Q0 O' O 60 80 100 miMo_ -lh 22L 120 t!W 140 ((It IX v 200 Pan SJf (.03 73 Q.l Drytiroe: Static Flow: 0 -lllr Avg. Microns: rS7. Color L: ilf0> S" a 0( b AU Technician: VAB.0001201133 1 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 A C EE R I R I EE OR ANALYSIS Date: October 9, 1992 Customer: Intex Plastics Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: October 8, 1992 Fax No. 601-286-9402 VIS1AProduct: 5415 Railcar No.: PLCX 47629 Order No.: 0016884-001 Property Test Method I PC Specification Analysis Inherent Viscosity ABR-10 1.00 - 1.04 1.02 Residual VCM, ppm ABGC-26 8.5 PPM Max. 0.002 Contamination, BLK + BRN ABR-5A 20 Total Max Total Black + Brown Hard Particles 0 7 mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2B ABR-1A ABR-3 5 Max. 1 15 Sec. Max. 9.0 0.460 Min. 0.520 0.30 Max. 0.16 25.0 Thru 140 Mesh Max. 5.0 On Pan Max. % ON Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 4.8 Amy E. Bag Laboratory Supervisor (601) 369-3624 VAB.0001201134 Vista Polymers Highway 25 Aberdeen, MS 3973q Load Date: ! & Time Logged In: Ship Date RAILCAR ANALYSIS Product: >>> Logged In By: Order No: I (o Car No.: Silo(s): a I Customer: Compartment A Sample From Bottom Top Moisture % ./V BL Contamination BR Bulk Density 5 Hard Particle 7 .519 H S Viscosity RVCM -Q6>2 CA CB Bottom Top . Bottom Top j4 <3 2 <R 1 *? e // -5/7 B Bottom Top J<e 3 7 Z lo ,<&i Screen Analysis Mesh Weight % 40 0 .op o. o Drytiroe: 60 /`Mr 80 a.r. 37.x 100 im / 3*k 120 140 lb^^_ S<f tT 200 *>.ay H.s- Pan ,19 j.u Static Flow: 0 /9,o 4 LAvg. Microns: Color L: /C/-Z C" a 0-02. b /-2Z- HETS: 10 ite Technician: d? VAB.0001201135 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 A OER I RIO A E OR ANALYSTS Date: October 9, 1992 Fax No. 601-286-9402 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 36834 VIS1AProduct: 5385 Attention: Quality Control Dept Railcar No ACFX 41153 Ship Date: October 7, 1992 Order No 0016920-000 Property I PC Test Method Specification Analvsis Inherent Viscosity ABR-10 0.90 0.95 0.92 Residual VCM, ppm ABGC-26 8.5 Max. 0.083 Contamination, BLK + BRN ABR-5A 40 Total Total Black + Brown Hard Particles 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH % ON 15 Max. 2 15 Max. 8.0 0.510 Min. 0.577 0.30 Max. 0.17 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins. ABR-7 6.0 Max. 5.1 Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E ~ Bagviej)l Laboratory Supervisor (601) 369-3624 VAB.0001201136 Vieta Poly il Highway 25 A Aberdeen, MS 3973Q PVC RAILCAR ANALY3 XS Screen Analysis Mesh Weight % 40 o-oo Q> o 60 /.j* 2.7 80 ICS4- J/./ 100 2.2 120 ?.*/ //*? 140 T./S SO. 3 200 3.)4 .3 Pan s:fDrytime: Static Flow: & / * *0 Avg. Microns: jU-7 r.toColor L: tad. ? / a . ZZ- . b Technician: MA VAB.0001201137 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 A CERT X ICA OE ANA 3X3 Date: October 6, 1992 Customer: Intex Plastics Corinth Division Golding Drive Corinth, MS 36834 Attention: Quality Control Dept Ship Date: October 5, 1992 Fax No. 601 -`286-9402 VISTAProduct: 5415 Railcar No Order No VIPX 45801 0016884-000 Property Test Method I PC Specification Analvsis Inherent Viscosity ABR-10 1.00 - 1.04 1 .03 Residual VCM, ppm ABGC-26 8.5 PPM Max. 0.016 Contamination, BLK + BRN ABR-5A 20 Total Max Total Black + Brown Hard Particles 7 mins Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2B ABR-1A ABR-3 5 Max. 1 15 Sec. Max 9.6 0.460 Min. 0.522 0.30 Max. 0.16 25.0 Thru 140 Mesh Max 5.0 On Pan Max. % ON Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 4.9 Amy E. Bagwell Laboratory Supervisor (601) 369-3624 VAB.0001201138 Vista Polymers Highway 25 Aberdeen, MS 3973q RVC RAILCAR ANALYSIS Load Date: Time Logged Ship Date: 'lcOO Product: Car No.: Logged In By: /n KoW^'OOC) Silo(s): Customer: /po /7?eh U, Compartment A Sample From Bottom Top Moisture X j4 Contamination Bulk Density 5 Hard Particle 7 3 I Viscosity RVCM Ml *0/ (& CA Bottom Top dU .S/0 CB Bottom Top . /s B Bottom Top z. 3 .2,3 * Screen Analysis ^* ** * * Mesh 40 Weieht 0 % O .O 60 /. 03 <3. 1 80 not 341 100 120 /*'S? &-?o 312^ 17.1 140 3. qf 8.0 200 5.2 Pan AO !*(? Drytime: Static Flow : 0 /?.(, A* vg. Microns: _ Color L: a Onc3 b }.3t. METS: *9?#? / ft % Technician: VAB.0001201139 c & Vista Polymers Highway 25 A Division of Post Office Box 91 Vista Chemical Company Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 A C EE R X R X CAT EE OR ANA SX3 Date: October 6, 1992 Customer: Intex Plastics Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: September 30, 1992 Fax No. 601-286-9402 VISIAProduct: 5415 Railcar No Order No UTCX 46472 0016358-002 Property Test Method I PC Specification Analysis Inherent Viscosity ABR-10 1.00 - 1.04 1.03 Residual VCM, ppm ABGC-26 8.5 PPM Max. 0.027 Contamination, BLK + BRN ABR-5A 20 Total Max Total Black + Brown Hard Particles 7 mi ns Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2B ABR-1A ABR-3 5 Max. 1 15 Sec. Max 9.2 0.460 Min. 0.508 0.30 Max. 0.22 25.0 Thru 140 Mesh Max 5.0 On Pan Max. % ON Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 5.0 Amy t. BagWei 1 Laboratory Supervisor (601) 369-3624 VAB.0001201140 Vista Polymers Alt> T>jt> Highway 25 Aberdee n Ms 39730 A Load Date: f Time Logged I n: Pi# 0 Ship Date: RAILCAR ANALYSIS Product: Car No.: Logged In By:_ Af-4 Silo(s): it*, if/ a\o*mm Compartment A Sample From Bottom Top Moisture % Contamination (0e 1*fS m Bulk Density BL BR JZ .</o 5 Hard Particle 7 3 CA Bottom Top 4* SiO CB Bottom Top .570 B Bottom Top / Viscosity RVCM U&l m 1 Screen Analysis Mesh Weight % 40 0. &0 60 X! 80 Pg> 4nfi 100 !irg(e> 3V7 120 74t 140 3&[ 200 Pan o.t(o Drytime: Static Flow: 0 \% Avg. Microns: Color L: /* 78 b USo METS: 9l*L Z % Technician: VAB.0001201141 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 ^ Date: 10/2/92 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept. Ship Date: 10/1/92 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A Fax No. 601-286-9402 VEIAProduct: 5385 Railcar No.: PLCX 47613 Order No.: 0016821-000 IPC Specification Analysis 0.90 - 0.95 0.94 8.5 Max. 0.046 40 Total Total Black + Brown Hard Particles 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH % ON 15 Max. 5 15 Max. 9.1 0.510 Min. 0.580 0.30 Max. 0.12 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins. ABR-7 6.0 Max. 4.8 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. H. D. Lucas Laboratory Supervisor (601) 369-3624 VAB.0001201142 > Vista Polymers Highway 25 A Aberdeen, MS 3973(1 RVC Load Date: 3//7A& Time Logged Ship Date: /&/( <D&CO RAX LCAH ANALYSIS Product: Car No. Logged In By: Silo(s): QO ! %/LI^0&O Cue tome r: /flesh. Compartment Sample From Bottom Moisture Bottom Bottom Bottom Contamination Bulk Density BD after Fluff -57-S Hard Viscosity RVCM MeSh/Glassies Screen Analysis Mesh Weight % 40 0. O Q-0 60 pb 80 UL3. 100 7' */ 120 - 140 200 sP /13 3*^7 Lk^L 1L2. Pan 3.0 Drytime: Static Flow: O l9rl Avg. Microns: Color L: /(PO'^/S * b /il? Technician: <+ tfS VAB.0001201143 TRANSMISSION CONFIRMATION REPORT No.=000549 X fc DPTE/TIME OCT ;2, 1992 ^ l -r - -1-Pr- 11:47PM DLJRPTIGN TRANSMITTER CFROM5 r ,3 . - . UISTP 601 3i M N J wmn 4 Ml 4 'laitaFiubi A RECE1UER CTO) PPGES XMITTED PPGES ERRORED RESULT COMM. MODE RESOLUTION 4*1* I PI I . f. k. ---------------------------------------------------------------------i 4 i- 4- A-l las . . J J. 601 286 9402 01 i| -i . hJ OK G3 NORMPl I - --m aiim -Ih Vphil ILJi _ VAB.0001201144 55-0000349 Vista Polymers A Division of Vista Chemical Company c Highway 25 Post Office Box 91 Date: October 1, 1992992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: September 29, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A Aberdeen, Mississippi 39730*0091 Phone (601) 369-81 1 1 A X3 Fax No. 601-286-9402 VISIA Product: 5325 RaiIcar No Order No PLWX 44410 0016594-000 Specification Analysis 0.78 - 0.82 0.80 8.5 PPM Max. 0.100 Not Yet Determined Total Black + Brown Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2A Moisture, % ABR-1A Particle Size Distribution ABR-3 15 Sec. Max 0.480 Min. 0.30 Max. 5.0 Max. on Pan 10.9 0.489 0.15 % ON Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E. Bagwell Laboratory Supervisor (601) 369-3624 VAB.0001201145 - Visha Polymers P' Highway 25 Aberdeen. MS 39730 A Load Date: Time Logged In: Ship Date:_ ^(V) /[/ & syf Fi A I L CAR ANALYSIS Product: Car No.: Logged In By: AtJd Order No:, /> S*?C-ooo Silo(s): Customer itr Screen Analysis Mesh Weight 40 0.0 XP >,Q 60 .</> 80 & i (&' (j? 100 3/j> 120 _3P 3 140 1^2 200 L21 34 Pan Zi3i 2.7 CPA: <2^. f % Glassies: efo Avg. Microns: Color L: l^9's <f0 a b /. <// Static Flow: O / /O' ? Technician: a?* * fL * VAB.0001201146 Visfa Polymers A Division of Vista Chemical Company Highway 25 Post Office -Box 91 Aberdeen, Mississippi 39730*0091 Phone (601) 369*81 1 1 X FICATE OF XS A Date: io/ih Customer: Intex Plastics Corp Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK/BRN ABR-5A Hard Particles Q 7 Mins ABR-12A Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2A Moisture, % ABR-1A Particle Size Distribution ABR-3 MESH % ON VIS1AProduct: 5325 Lot No. : 04*? II Truck No.: "7^ 7 Order No. : OOiLLZ^-OOQ VISTA Specification 0.78 - 0.82 Analvsis 6.So 8.5 PPM Max 35/100 Max. C?DC9*7 3M No Spec. 15 Sec. Max Not 1.1 0.480 Min. 0.30 Max. 5.0 Max. on Pan PAN hi Polyvinyl Chloride, Virgin Resin, Not Reprocessed. (601 ) 369-3624 isor/Lead VAB.0001201147 0 Regulars or Bags Pago of pagas \ \ fs IS Vinyl Sample Log Data Product Typa Altmofld 24 St / VAB.d8t)1201148 Vista Polymers A Division of Vista Chemical Company i'm0t Highway 25 Post Office Box 91 CERTIFICATE Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 ANALYSIS A Date: /o/i Nz- Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: 2^ m Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK/BRN ABR-5A Hard Particles @ 7 Mins ABR-12A Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2A Moisture, % ABR-1A Particle Size Distribution ABR-3 MESH % ON VIS1AProduct: 5325 Lot No. owe& Truck No. :~P~r7D%& Order No. :06OQQ VISTA Specification Analysis 0.78 0.82 8.5 PPM Max 35/100 Max 6.9 Q p.ono 3h No Spec 15 Sec. Max. 7.4 0.480 Min. 0.30 Max. o.n 5.0 Max. on Pan Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor/Lead (601) 369-3624 VAB.0001201149 t RESIN BAG BLEND BLEND HO: 04 * PRODUCT: DATE: '7~J- Avg. Nicrons, 5225/5325/5415: MS' E BLACK/ PARTICLE SIZE DISTRIBUTION 5/7 X BROTH )"".....j----i 11 h BULK HIN. DRY STATIC HOIST CONT. 40 60 80 100 I120 140 m PAN DENS H/P TIKE PLOT !| TIME/TESTED BY: /3'& e> / COLOR LAB itz7cro VABX)0012(J1150 4 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 A A^ f A^ ^M Customer: Intex Plastics Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: September 28, 1992 VISTAProduct: 5415 Railcar No.: UTCX 46406 Order No.: 0016358-001 Property Test Method Inherent Viscosity ABR-10 l.oo - 1.04 Residual VCM, ppm ABGC-26 8.5 PPM Max. Contamination, BLK + BRN ABR-5A 20 Total Max A CA Total Black + Brown 9 10 Analysis 1.01 0.024 CB B 96 Hard Particles @ 7 mins. ABR-12 5 Max. 1 Dry Flow, Seconds ABR-8 15 Sec. Max. 8.0 Bulk Density, gm/cc ABR-2B 0.460 Min. 0.508 Moisture, % ________ ^m __ m Particle Size Distribution ABR-1A ABR-3 0.30 Max. 0.17 25.0 Thru 140 Mesh Max. 5.0 On Pan Max. 40 60 80 100 120 140 200 PAN % ON 0.00 3.9 40.9 29.1 14.4 6.1 4.1 1.5 Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 4.9 Laboratory Supervisor (601) 369-3624 VAB.0001201151 Vista Polymers Highway 25 Aberdeen, MS 3973q A R AILCAR ANALYSIS Load Date: P*7 ^ Time Logged In: Ship Date: ZgArZ- Product: Car No.: Logged In By: //?. 7 Sllofs): Order No. 0 o(USfS%'oo! Customer: A* Jfeat Compartment A Sample From Bottom Top Moisture X BL Contamination BR r/3 Bulk Density 5 Hard Particle 7 . ST>\ Je. Viscosity RVCM .014* CA Bo t tom Top ./ 3 r// 5 CB Bottom Top 17 s . <7/0 B Bottom Top ju L Screen Analysis * ^ mm Mesh 40 Weight % 0*o 60 __/ ^ 3.1 80 100 120 140 200 /fcir 7./r 3.0(e 2?- / /4.4 i.! Pan /i^ Drytime: Static Flow: 0 / P-O Avg. Microns Color L: METS: b / /? / Technician: VAB.0001201152 Vista Polymers A Oivision of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE OF ANALYSIS Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: September 28, 1992 Customer: Intex Plastics Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: September 25, 1992 VIS1AProduct: 5415 ilcar No.: GACX 73408 Order No.: 0016358-000 Property Test Method IPC Specification Analysis Inherent Viscosity ABR-10 1.00 - 1.04 1.02 Residual VCM, ppm ABGC-26 8.5 PPM Max. 0.024 Contamination, BLK + BRN ABR-5A 20 Total Max. A CA | CB B Total Black + Brown 3 2 15 3 Hard Particles 7 mins. ABR-12 5 Max. 1 Dry Flow, Seconds ABR--8 15 Sec. Max. 8.1 Bulk Density, gm/cc ABR--2B 0.460 Min. 0.510 Moisture, % ABR-1A 0.30 Max. 0.15 Particle Size Distribution ABR--3 25.0 Thru 140 Mesh Max. 5.0 On Pan Max. 40 60 80 100 120 14o| 200 PAN % ON 2<2I0.00 3.2 36.4 28.9 16.7 8.1 4.5 Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 4.9 Laboratory Supervisor (601) 369-3624 VAB.0001201153 Vista Polymers Highway 25 Aberdeen, MS 3973q A RVC RAILCAR ANALYSIS Load Date: 7-g/-fg Time Logged In: 03* Product: Logged In By: Ship Date: Order No: Car No -: Sllof s I : too Customer: Compartment A Sample From Bottom! Top Moisture % BL Contamination BR Bulk Density ,/J 2. 1 ds 5 Hard Particle 7 7 / TS Viscosity I.OZf RVCM /Oztf CA Bottom Top *_zr / / S"Jc \ CB Bottom Top /2. it- J - B Bottom Top /0 / r/ Screen Analysis Mesh Weight % 40 A 04 . 0.0 60 /.*; 80 it.it 36.4 100 120 Mif H.7 140 *07 9./ 200 +.S- Pan /0s ND Drytime: Static Flow: * .ij.t Avg . Microns: _ 171.1 Color L: '/ ^ b / METS: / figs', g % Technician: HA VAB.0001201154 t Vista Polymers A Division of Vista Chemical Company Highway 25 Rost Office Box 91 CERTIFICATE OF ANALYSIS Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: September 24, 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: September 18, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A Total Black + Brown VIS1A Product: 5305 Railcar No.: UTCX 46456 Order No.: 0015940-001 IPC Analysis 0.71 0.76 0.73 8.5 PPM Max. 0.010 60 Total A CA CB B 23 21 17 19 H 00 Dry Flow, Seconds ABR--8 15 Sec. Max. Bulk Density, gm/cc ABR--2A 0.510 Min. 0.532 Moisture, % ABR--1A 0.30 Max. 0.21 Particle Size Distribution ABR--3 30.0 Thru 140 Mesh 5.0 Max on Pan 40 60 80 100 120 140 200 PAN % ON 0.00 0.6 12.9 23.2 31.7 20.8 8.2 2.6 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy ET. Bagwell Laboratory Supervisor (601) 369-3624 VAB.0001201155 Vista Polymers Highway-25 Aberdeen, MS 39730 Load Date: Time Logged Ship Date: urc4JriAILCAR ANALYSIS Product: Car No. Logged In By: Order No: 0O 00 / Silo(s): : /P<2- Customer tbtn^nL- Compartment A Sample From Bottom Moisture BL Contamination BR Bulk Density JO /-3 BD w/antistat Viscosity RVCM ,72# ,616 CA Bottom IS ? u .ntf <yzf} Tappi Test Contamination Composite Screen Analysis Mesh Weight % 40 0 CL O .06 or less 60 oil &,,(c> 80 .07 100 CB Bottom (p // V B Bottom 3i it 8 SVCo .72-7 037 .15 .dZ-tf .20 .60 120 15^3 31.7 140 f6H> 200 Pan Avg. Microns: 1 T Color L: a b % Glassies: Static Flow: a / <f/ Technician: VAB.0001201156 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 cE|RTIFICATE of Aberdeen, Mississippi 39730-0091 Phone (601) 369*8111 analysis Date: September 22, 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Dept. Ship Date: September 15, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A VK1A Product: 5325 Railcar No.: GACX 73384 Order No.: 0016012-000 Specification Analysis 0.78 - 0.82 0.80 8.5 PPM Max. 0.135 Not Yet Determined Total Black + Brown Dry Flow, Seconds ABR-- 8 Bulk Density, gm/cc ABR-2A Moisture, % ABR-1A Particle Size Distribution ABR-3 15 Sec. Max 0.480 Min. 0.30 Max. 5.0 Max. on Pan 9.3 0.516 0.30 % ON Polyvinyl Chloride, Virgin Resin, Not Reprocessed <icjdtH 'Amy E. agwel O Labora ory Supervisor (601) 369-3624 VAB.0001201157 P * Vista Polymers Highway 25 Aberdeen, MS 39730 h Load Date: Time Logged In: / Ship Date:. `Thin*- Product: 5 Logged In By: Order No: O Ql (oO\% Car No.: Silo(s): Customer: I P&* alehteftL-- Compartment A Sample From Bottom Moisture % (/ BL Contamination BB 3 C9 Bulk Density ,>o(* BD w/antistat Viscosity RVCM nf4 _ pfe CA Bottom ,3o 10 ,SJ0 m sr .DlO d CB Bottom QjS 7 ,6oe> r?io .istr B Bottom ,3o 3-- 7 .71 (o .OOl i 0 CO * 1 1 1 1 1 o <N Tappi Test Contamination Composite .06 or less i .07---------.15 Screen Analysis Mesh Weight % 100 120 140 {3.f* {<*80 J,6>o 27r0 33./ 77 2 200 3.T9- 5T^ Pan f.jg 2. J Static Flow: Avg. Microns: !4^i (jiASSy \ LlColor L: /K>-^/ a -tf b (Zfft S5TS Technician: VAB.0001201158 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: September 22, 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Dept. Ship Date: September 16, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A VIS1A Product: 5325 Railcar No.: UTCX 46519 Order No.: 0016097-000 Specification Analysis 0.78 - 0.82 0.80 8.5 PPM Max. 0.080 Not Yet Determined Total Black + Brown Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2A Moisture, % ABR-1A Particle Size Distribution ABR-3 15 Sec. Max. 0.480 Min. 0.30 Max. 5,0 Max. on Pan 9.8 0.501 0.30 % ON Polyvinyl Chloride, Virgin Resin, Not Reprocessed. (X tU Amy E. Bagwe1 F3 Laboratory Supervisor (601) 369-3624 VAB.0001201159 * i. Vista Polymers Highway 25 Aberdeen, MS 39730 Load Date: 9"/4^ *9 ^ Time Logged In: fii2Q -Jhk Ship Date Product: Logged In By: Order No: Car No.: *4r/? Silo(s): 4/r Customer .jKz aJo faate l.-- Compartment A Sample From Bottom Moisture .31? BL Contamination BR Bulk Density BD w/antistat Viscosity RVCM .79e> Lnf%IJ t) Screen Analysis Mesh weight * 40 C)~0 0,00 60 0-/2. O.z CA Bottom .& 4- CB Bottom * 23 B Bottom .7 45" .171% .>03' .99*/ .091 80 f-22. Jb.+ 100 /. so 1 (o 120 32. S' 140 "7. M3 200 4.2> Pan /3 3 .7 % Glassies Color L: fep.SS a o.!V~- b /.gfr Avg. Microns Static Flow: Technician: fc VAB.0001201160 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANA IS A Date: September 15, 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: September 11, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A VIS1A Product: 5305 Railcar No. VIPX 45719 Order No.: I PC Specification 0015940-000 mmaamm Analvsis 0.71 - 0.76 0.73 8.5 PPM Max 0.043 60 Total Total Black + Brown Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2A Moisture, % ABR-1A Particle Size Distribution ABR-3 15 Sec. Max 7.7 0.510 Min. 0.527 0.30 Max. 0.06 30.0 Thru 140 Mesh 5.0Max on Pan % ON Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E yBagwe rK Laboratory Supervisor (601) 369-3624 VAB.0001201161 Vista Polymers Highway 25 Aberdeen) MS 39730 Load Date Time Logged In: -MShip Date n Product: /&Q0 Logged In Bv: V' Order No: I*5^9-FZ>> Car No.: Silo(s): <j>%0/68 Customer /pt / Compartment A Sample From Bottom Moisture BL Contamination BR Bulk Density BD w/antistat . oV 3 ....V/ s _ S&3 Viscosity RVCM .otfa CA Bottom O/ 3 3 5<2e> .iz^ .oS"7 CB Bottom * ocT Y jr .S?o n*y\ .OS'S B Bottom O h 3 7 S3? 11$ 02*37 Tappi Test Contamination Composite Screen Analysis Mesh 40 Weight %P 0.0 .06 or less V? 60 ./? *3 80 f2 /<? <f .07-----------.15 .20----------- .60 100 120 3h$ 140 f.^O /?.< 200 /</ 93 Pan /* P'grF>*~ Avg. Microns: / <-! 7. Color L: tf^-37 a 0'37 b /$' Static Flow: ^ / 7> 7 Technician VAB.0001201162 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERT I 1= X CATE Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 ANA L_VS I 3 A Date: September 10, 1992 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept. Ship Date: September 8, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A Product: 5385 Railcar No.: GACX 73398 Order No.: 0015697-000 I PC Specification Analysis 0.90 - 0.95 0.93 8.5 Max. 0.015 40 Total Total Black + Brown Hard Particles 0 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH % ON 15 Max. 2 15 Max. 7.9 0.510 Min. 0.580 0.30 Max. 0.15 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins. ABR-7 6.0 Max. 5.0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor (601) 369-3624 VAB.0001201163 Vista Polymers Highway 25 Aberdeen, MS 39730 }PVO LCARJR AX ANALY S X S Load Date: Time Logged In: Ship Date: Product: Car No.: 7'33IX Logged In By: Order No /6&>f7- nad SIlo(e) : Customer: ft* Compartment Sample From A Bottom Moisture % BL Contamination BR m /JL . Bulk Density BD after Fluff Hard Particle 5 7 Viscosity RVCM k- /2~ 2 XJ 40 Mesh/Glassies V . , * -* * % ,,. CA Bottom AT vT 2/ .r/-2. ,- Screen Analysis Mesh Weight % 40 0-00 . 00 60 -L2X s-c 80 K.l $0.0 100 12.31 zsr.4 CB Bottom B Bottom /<9 . . r?<r # / --L _______________________________________________ 120 ?.2- //</ 140 s.7 /l.'4 200 4.42 1.0 Pan J.4S 2.1 Drytime: ` Co + Static Flow: / Z 9 Avg. Microns: Color L : /iS a - // T b / 7f Technician: VAB.0001201164 Vista Polymers A Division of Vista Chemical Company r~ --* O Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 I R ICAT EE OR ANA SIS * Date September 10, 1992 Customer: 4* Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: September 8, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A VIS1AProduct: 5385 Railcar No.: VIPX 45704 Order No.: 0015061-003 I PC Specification Analvsis 0.90 - 0.95 0.92 8.5 Max. 0.058 40 Total Total Black + Brown Hard Particles a 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH % ON 15 Max. 3 15 Max. 8.1 0.510 Min. 0.581 0.30 Max. 0.15 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins. ABR-7 6.0 Max. 5.0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed uJ Bagwei1 Laboratory Supervisor (601) 369-3624 VAB.0001201165 Vieta Polymers Highway 25 h Aberdeen, MS 39730 RVC RAILCAR ANALYSIS Load Date: > Time Logged In: -jll Ship Date: Product: Car No.: Logged In By: Order No: /*>>& (-003 Silo(6 ) : Customer: Compartment A Sample From Bottom Moisture % BL Contamination BR Bulk Density . 13 d\ BD after Fluff Hard Particle 5 7 n- Viscosity RVCM AVb ose> 40 Mesh/Glassies +4 Screen Analysis Mesh Weight % 40 A *o 0.0 60 CA Bottom * .AT I l^ .S'7? CB Bottom ._n=L 3 . rri B Bottom 5 o / 4 L 1 80 J3.Z7 z.US' 100 is.oi 120 17.7 140 i.21 Jl-t, 200 Pan **. 1/ 9.S -?.7 Drytime: Static Flow: 6 / f.l Avg. Microns: Color L: /00. IS a 7 b 2; w Technician: VAB.0001201166 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTX F X CAT E OF Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 AMA LYSXS Date: September 4, 1992 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept. Ship Date: September 1, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A VISIAProduct: 5385 Railcar No.: ACFX 41174 Order No.: 0014855-003 I PC Specification Analvsis 0.90 - 0.95 0.93 8.5 Max. 0.029 40 Total Total Black + Brown Hard Particles 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH % ON 15 Max. 3 15 Max. 8.2 0.510 Min. 0.580 0.30 Max. 0.15 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins. ABR-7 6.0 Max. 5.0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor (601) 369-3624 VAB.0001201167 Vista Polymers Highway 25 * Aberdeen, MS 39730 FVC RAILCAR ANALYSIS Load Date: Time Logged In: -IkShip Date: Product: Logged In By: Order No: LML JM Compartment A Sample From * Moisture % Bottom 'J4 BL Contamination BR t i Bulk Density BD after Fluff Hard Particle 5 7 jL_ J HA Viscosity RVCM ** - .0'lej 40+- t Mmem st hf /G^lass+ ies ' # ,. Screen Analysis Mesh Weight % 40 0*6 0 0.0 60 2. *7 CA Bottom 3 \ XSo - 80 /r.ri 31.0 100 a.iu Car No.: Silo( Customer: v. CB Bottom < ST?* B Bottom ,)~ C 2- --T77 / -------7A ------ _/______ 4 120 t.tt /7.: / 140 s*. f* /orr 200 V.2/ /:* Pan AS? **7 Drytiroe: &0 Static Flow: Color L: /0. a a o / r.z. JAUAvg. Microns: n. o? b /. 7f Technician: . v-/fw VAB.0001201168 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERT I E X CAT EE OR Aberdeen, Mississippi 39730*0091 Phone (601) 369-81 1 1 ANA LYSIS Date: September 4, 1992 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: September 3, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A Product: 5385 Railcar No.: ACFX 41141 Order No.: 0014855-004 I PC Specification Analvsis 0.90-0.95 0.92 8.5 Max. 0.065 40 Total Total Black + Brown Hard Particles 9 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH % ON 15 Max. 3 15 Max. 9.4 0.510 Min. 0.584 0.30 Max. 0.11 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins. ABR-7 6.0 Max 4.7 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. Bagwell Laboratory Supervisor (601) 369-3624 VAB.0001201169 Vista Polymers Highway 25 Aberdeen, MS 3973Q It A X LCAR ANALYSIS Load Date Time Logged In: /V&Q Ship Date: Product: 5385 Car No.: Logged In By: Order No / s^-oo < Silo(s): Customer: Compartment A Sample From Bottom Moisture % o.r BL Contamination BR 3 r Bulk Density BD after Fluff S*f Hard Particle 5 a. 73 Viscosity till RVCM .Ob^T Mesh/Glassies Screen Analysis Mesh Weight XP 40 OO OO 60 1Z LI CA Bottom .oY u CB Bottom lS z. B Bottom .03 U .SSY A / 80 100 93 /Jb? Z3^ 57 120 140 200 /3l2_ `f.L Pan /.<// 2A 4<7Drytime: 0 /^YStatic Flow: Avg. Microns: X$^-C Color L: /S0 2 / . ojy b t9l Technician: VAB.0001201170 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERT" I FICATE OR Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 IS A Date: September 2, 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 38S34 Attention: Quality Control Dept Ship Date: August 28, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A VB1A Product: 5305 Railcar No UTCX 46436 Order No 0014852-002 I PC Specification Analysis 0.71 - 0.76 0.73 8.5 PPM Max 0.016 60 Total Total Black + Brown Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2A Moisture, % ABR-1A Particle Size Distribution ABR-3 15 Sec. Max. 8.5 0.510 Min. 0.521 0.30 Max. 0.15 30.0 Thru 140 Mesh 5.0Max on Pan % ON Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E.^BagweTU Laboratory Supervisor (601) 369-3624 VAB.0001201171 Vista Polymers Highway 25 Aberdeen, MS 39730 A Ft AX LCAR Load Date: Product: 5305 Car No. Time Logged In: Q-S'O^ mTLogged In By: Silo(s): Ship Date Order No:. /4ftC2~6o Customer Le^~! Compartment A Sample From Bottom Moisture . * 'V . ` 1 '"is BL Contamination BR Bulk Density ,/i /< $ BD w/antistat Viscosity RVCM .734 CA Bottom // z ,754 06> / Tappi Contamination Composite Screen Analysis Mesh Weight % 40 0.50 06 or less v: 60 .J 80 .07 100 torn- 2 J. 4 CB Bottom /r B Bottom Jo Z, 73 d, 0^0 .15 .73/ i<2 .20 .60 120 n.-n 32.4 140 U. 72- 13.4 200 r.77 Pan 2 Avg. Microns: Color L: 77/2- a . % Glassies: b /^ Static Flow: !% / fj Technician: VAB.0001201172 /* V % Vista Polymers Highway 25 Aberdeen, MS 39730 A X LCAR ANALYSIS OB' Load Date:_______ Time Logged In: Ship Date:_______ Product 53of Logged In By Order No: Car No. Silo(s): Customer: COMPARTMENT A Moisture % Contamination / Bulk Density Color "L" Color "a" Color "bH Static Flow / Viscosity TsiP RVCM * Screen Analysis Mesh Weight 40 0-0 0 60 o*>2- % 6.0 CA CB 4 ,B // / / Top / Top / T.qp E^ .. - ............................................................... 80 2.o% 100 MA.i. 120 MX 140 W.Jo 2f.O 200 /(.If 23A Pan ! A'.o Weight CA % & .iS?Q 0J01? 0.2. Weight CB % G-C& Q-O O.o3 Q-{ Weight % O.ol 0,1 Technician: tZA 332 7A /2.3 b 23.7 /(,.of> 3o.7 te_ 15.53 3(.( y.l/L (e /3.02^ USo 2&>o !3.(o fMS~ (3.3 b \i. fZ 4Ul 1.2. n> 32,3 (3.2\ 5?3 Z<?.3 -U4- VAB.0001201173 mm to Vista Polymers A Division of Vista Chemical Company CER Highway 25 Post Office Box 91 X E X OAT EE OR Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 ANA SIS \ A Date: September 2, 1992 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: August 31, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A VISTAProduct: 5385 Railcar No.: VIPX 45772 Order No. 0015061-002 I PC Specification Analvsis 0.90 - 0.95 0.92 8.5 Max. 0.145 40 Total Total Black + Brown Hard Particles 8 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH % ON 15 Max. 3 15 Max. 8.1 0.510 Min. 0.581 0.30 Max. 0.15 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins. ABR-7 6.0 Max. 5.0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E, Bagwel1 Laboratory Supervisor (601) 369-3624 VAB.0001201174 Vista Poly ere Highway 25 A Aberdeen, MS 39730 PVC RAILCAR ANALYSIS Load Date: -30 - Product: Car No Time Logged In: J b 0 2 Logged In By: Ship Date: S Order No: t."" 00*2^ Silo(6): - tfL. Screen Analysis Mesh 40 Weight % 0,00 0,0 60 -.7# 80 fZ-iZ zr.z 100 14.10 it.4 120 16.70 zt.C 140 .24 /?. S' 200 4.Z<* t. 7 Pan /. /2. Z2 Drytime: Static Flow: / f, f Avg. Microns: i5"7.7 Color L: /^ a $2 t b /"7Z-- Technician: VAB.0001201175 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIEX Date: September 2, 1992 Customer: Intex Plastics Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: August 31, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 ANA SIS A VIS1AProduct: 5415 Railcar No Order No VIPX 45839 0014854-002 I PC Specification 1.00 - 1.04 8.5 PPM Max. 20 Total Max Analysis 1 .01 0.227 Total Black + Brown Hard Particles 7 mins Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2B ABR-1A ABR-3 5 Max. 15 Sec. Max 1 .8 1 0.460 Min. 0.503 0.30 Max. 0.15 25.0 Thru 140 Mesh Max 5.0 On Pan Max. % ON Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 5.0 Laboratory Supervisor (601) 369-3624 VAB.0001201176 Vista Polymers Highway 25 Aberdeen, MS 3973q FfcAXLCAR ANALYSIS Load Date: a Time Logged In : Ship Date: Product: 5415 / <h o o \ Logged In By: Order No: 24is4-oo2- Car No.: Silo(s): Customer: > Si Compartment Sample From Moisture X Contamination Bottom Top Bottom! Top Bottomj Top . /J Bottom Top Bulk Density Hard Viscosity RVCM / .ofb .tin r*7 Screen Analysis Mesh Weight X 40 0 0.0 60 80 100 120 140 200 Pan /t.iZ. lC.30 -H2/ Z.+o ,7 L /?,i /.r _ Drytime: f-o Static Flow: Color L: J 0i JO O /f.t Avg . Microns: 4* 0U b AS /7 3.3 METS: Technician: VAB.0001201177 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTI R X CAT E OF Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 AN A L. VS I S Date: August 31, 1992 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: August 26, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A Product: 5385 Railcar No.: GACX 73393 Order No.: 0015061-001 I PC Specification Analvsis 0.90 - 0.95 0.94 8.5 Max. 0.092 40 Total A Total Black + Brown Hard Particles 0 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH % ON 15 Max. 2 15 Max. 7. 7 0.510 Min. 0. 572 0.30 Max. 0. 14 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins. ABR-7 6.0 Max. 5.0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. agw Laboratory S tsl ervisor (601) 369-3624 VAB.0001201178 Vista Polymers Highway 25 Aberdeen, MS 39730 RA X LCAR ANALYSIS Load Date: Time Logged In %[zbl Ship Date: Product 5385 Car No Logged In By: Order No: ______i_i______^_____ Silo(s): Customer: IPC* Compartment * Sample From A Bottom CA Bottom Moisture % BL Contamination BR 4_ Bulk Density BD after Fluff . r7/ -// ? . r?j Hard Particle 5 7 & 3S Viscosity * * .*3? RVCM w .Of* ?- 40 . M* e- s h* /Gla*ss* ie+ s m ,4 , - L Screen Analysis Mesh 40 Weight % 0.0 60 A t0 3.t> 80 ujz 32.4 100 /y. O zy,3 CB Bottom . /o 5" 1 ,r7i- B Bottom ./0 ip 2- * / --------/7# ------ f _______ r * P " 120 LL-L 140 200 Pan rt 3. +* a jo ?, 7- - JZiR___ Drytime: SlQ Static Flow: 0 /*?? Avg. Microns Color L: /CP* Z 9 a f 0 Technician: VAB.0001201179 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 C E R I R I CA EE OR AM A SIS X * Date: August 31, 1992 Customer: Intex Plastics Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: August 25, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A VIS1AProduct: 5415 Railcar No Order No UTCX 46592 0014854-001 I PC Specification 1.00 - 1.04 8.5 PPM Max. 20 Total Max Analysis 1 .01 0.001 Total Black + Brown Hard Particles 7 mins Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2B ABR-1A ABR-3 5 Max. 1 15 Sec. Max 8.2 0.460 Min. 0.510 0.30 Max. 0.15 25.0 Thru 140 Mesh Max 5.0 On Pan Max. % ON Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 4.9 Amy Ejy Bagw Laboratory Supervisor (601) 369-3624 VAB.0001201180 Vista Polymer's A-O d/t> Highway 25 Aberdeen, MS 3973q h RAILCAR ANALYSIS Load Date: Time Logged I JL0t> Product: Logged In By: Ship Date: Order No: Car No.: 4s?2. Customer: utl f*> J*L Compartment A Sample From Bottom Top Moisture X BL Contamination BR , fZ 1 s ) Bulk Density 5 Hard Particle 7 .Co _ / Viscosity RVCM /.t>IO .DM CA Bottom Top CB Bottom Top ./ /3 bTv7 ,// 92 % s B Bottom Top .JO s * Screen Analysis Mesh Weight % 40 0* 0 P.o 60 80 100 120 140 200 Pan 13-47 ZAl 4. It 3.it A// J6.4 it.f JZ.t f. 2. 2. Drytime: . 9 Static Flow: 0 ft* 2-- Avg. Microns: / 7Z.il Color L: _/gA/V l02 b / NETS: %-lb / >7.1-1 y~ Technician: VAB.0001201181 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 IFI Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 A Date: August 26, 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: August 21, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A VISIA Product: 5305 Railcar No UTCX 46576 Order No 0014852-001 I PC Specification Analysis 0.71 - 0.76 0.72 8.5 PPM Max 0.035 60 Total Total Black + Brown Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2A Moisture, % ABR-1A Particle Size Distribution ABR-3 15 Sec. Max 8. 1 0.510 Min. 0.518 0.30 Max. 0.1 1 30.0 Thru 140 Mesh 5.0 Max on Pan % ON Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy Er Bagwe Laboratory Supervisor (601) 369-3624 VAB.0001201182 Vista Polymers Highway 25 4 Aberdeen, MS 39730 RAILCAR Load Date: L> Product: Car No Time Logged In :J_70O_ Logged In By: Cc3. Silo(s): :Ship Date &\ZI k Order No:. ~ D& / Customer: ce o Compartment A Sample From 4 Moisture Bottom BL Contamination BR 3 5" Bulk Density BD w/antistat ,77 Viscosity RVCM ,7 U CA Bottom .il H :W> .043 CB Bottom .// 7 .72/ .0^ B Bottom .5" - .SfX .1*4 .Cfr( Tappi Test Contamination Composite .06 or less b/ Screen Analysis Mesh Weight % 40 r\,&c> 040 60 0.4 80 475 !3Ji .07 --- .15 -- .20 --------------------------------------------------------------------------------------- .60 100 /i-OZ *** 120 iLU 140 200 Pan s.<% - -3j_ /37 Avg. Microns: % Glasssies: -4 1% Color L: 9^S'^ a <>,/9 b / 3" Static FI ow: 6 / % ( tHt 4AftTechnician: VAB.0001201183 * / f RAILCAR SHIPMENT ORDER TO DIVERT/RE-SHIP/RETURN S'****: DATE: RAILCAR NUMBER: ORIGINAL SHIP DATE: ORIGINAL ORIGIN PLANT: Pt-LO Y -m ------------ / t/o. W II n-*--- > n r || PI FTII Biwngw ORIGINAL PRODUCT WEIGHT: PRODUCT NAME & CODE: ORIGINAL CUSTOMER: ORIGINAL CUSTOMER LOCATION: ORIGINAL ORDER NUMBER: NEW CUSTOMER: # jrr-oo`3- NEW LOCATION: NEW ORDER NUMBER: >! Ti l I H DO YOU NEED RAILCAR RE-WEIGHED? (YES/NO) REASON FOR CHANGE: <eg. off-spec, etc.) CAR RELEASED (YES/NO): BILLING INSTRUCTIONS MUST BE COMMUNICATED TO RAIL FREIGHT & CONTRACTS FOR ISSUING BILL OF LADING ON OR BEFORE THE DAY THE CAR IS RELEASED. / ) OTHER COMMENTS: la 3 0 o l $ t* ~o e> CUSTOMER SERVICE REPRESENTATIVE: 1 DISTRIBUTION: PLANT, HOUSTON - RAIL FREIGHT& CONTRACTS, HOUSTON - RAIL OPERATIONS ;FC492 VAB.0001201184 Ttdd -t* H. mmmmm Aiti lilTnicfTi 609T8St?802,T6:ON Hit? SltOIW3HD tusirvai LI--QT SS.-SI-iDO mm * Vista Polymers A Division of Vista Chemical Company C EE R Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 IRICAT E OR ANA SIS A Date: August 26, 1992 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: August 24, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A VIS1AProduct: 5385 Railcar No.: PLWX 44461 Order No.: 0014855-002 I PC Specification Analysis 0.90 - 0.95 0.93 8.5 Max. 0.052 40 Total Total Black + Brown Hard Particles e 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH % ON 15 Max. 2 15 Max. 8.9 0.510 Min. 0.576 0.30 Max. 0.09 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins. ABR-7 6.0 Max. 5.0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E. Bagwel Laboratory Supervisor (601) 369-3624 VAB.0001201185 Visra Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIRICATE OR Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 ANALYSIS A Date: August 26, 1992 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: August 21, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A Product: 5385 Railcar No.: ACFX 41175 Order No.: 0015061-000 I PC Specification Analysis 0.90 - 0.95 0.93 8.5 Max. 0.057 40 Total Total Black + Brown Hard Particles a 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH % ON 15 Max. 4 15 Max. 8.0 0.510 Min. 0.589 0.30 Max. 0.13 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins. ABR-7 6.0 Max. 4.9 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. agwel Laboratory Supervisor (601) 369-3624 VAB.0001201186 Vista Polymers Highway 25 A Aberdeen, MS 39730 RVC RAILCAR ANALYSIS Screen Analysis Mesh 40 Weight % 0.0 Drytime: 60 LIU 2. 3 80 I3.it zto 100 13* to 2 7.2 120 9.12. 11.1 140 .sr, f 7 //. 7 200 4 23 f.<r Pan A 2-0 2.*/ Static Flow: 0 J /- o Avg. Microns: _ H.LZ- Color L - f00x^0 a b /:ui Technician: VAB.0001201187 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730*0091 Phone (601) 369-81 1 1 CER I E I EE OR AM A SXS A Date: August 20, 1992 Customer: Intex Plastics Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: August 17, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR--5A VIS1AProduct: 5415 Railcar No.: PLWX 44668 Order No.: 0014854-000 I PC Specification 1.00 - 1.04 8.5 PPM Max. 20 Total Max Analvsis 1 .02 0.036 Total Black + Brown Hard Particles G 7 mins Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2B ABR-1A ABR-3 5 Max. 1 15 Sec. Max 9.4 0.460 Min. 0.514 0.30 Max. 0.16 25.0 Thru 140 Mesh Max. 5.0 On Pan Max. % ON Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 4.8 Amy E. Bagw^T1 Laboratory Supervisor (601) 369-3624 VAB.0001201188 Vista Polymers Highway 25 A Aberdeen, MS 39730 Load Dat Time Logged In: Ship Date: RAILCAR ANALYS X S Product: 5415 Logged In By: Order No: Car No - -s Silo(6): Customer: Screen Analysis Mesh Weight % 40 0-0* 60 i&A. 80 jzr? 3?.? 100 . i3.<n (p*/ 120 1.01 -ZiiL 140 7-/ 200 Pan 3 .23 z. HI Drytime: &2- 77/. */Static F low : <>/? Avg. Microns: ** \ Color L: /00'HY a o o'i-- h Ai3 METS: Technician: >*fr> T 7^* //: :XS /a VAB.0001201189 r Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTI 1=1 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 11 X3 A Date: August 20, 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: August 14, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A VIS1A Product: 5305 Railcar No.: ACFX 55814 Order No.: 0014852-000 I PC Specification Analysis 0.71 - 0.76 0.72 8.5 PPM Max 0.015 60 Total Total Black + Brown Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2A Moisture, % ABR-1A Particle Size Distribution ABR-3 15 Sec. Max 7.9 0.510 Min. 0.527 0.30 Max. 0.15 30.0 Thru 140 Mesh 5.0 Max on Pan % ON Polyvinyl Chloride, Virgin Resin, Not Reprocessed ail E. Bagw Laboratory Supervisor (601) 369-3624 VAB.0001201190 Vista Polymers Highway 25 63^S' Aberdeen, MS 39730 ^ Load Date: Time Logged In: Ship Date : Product: Car No.: Logged In By: Order No: / H-<KZ -0 0 > Silo(s): Customer: Compartment A Sample From Bottom Moisture ./J BL Contamination BR Bulk Density 9 A ,, zzf BD w/antistat Viscosity RVCM /tt'l D/S" CA Bottom .// / . Czs" ...7awr , DbI Tappi Test Contamination Composite Screen Analysis Mesh Weight % 40 9*00 P-0 .06 or less 60 80 . a 7,/7 .07 100 jl.lo 27.2- CB Bottom ./r ? A 7/4 .olo . 15 B Bottom }Q A . S" Jc . nsA.0b>\ 20 .60 120 IC.U 140 f.cc /7.1 200 J.ct 7.4 Pan 1*2, 2..C Avg . Microns: /+jrt % Glassi es: c ) *?o Color L: 33*91. a .92, b /. <tl- Static Flow: c / 7.9 Technician: VAB.0001201191 Vista Polymers A Division of Vista Chemical Company C ER Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601)369-8111 IFICATE OR ANA SX3 A Date: August 20, 1992 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: August 19, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A VB1AProduct: 5385 Railcar No.: ACFX 41138 Order No.: 0014855-001 I PC Specification Analvsis 0.90 - 0.95 0.93 8.5 Max. 0.022 40 Total Total Black + Brown Hard Particles e 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH % ON 15 Max. 2 15 Max. 8.8 0.510 Min. 0.588 0.30 Max. 0.17 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins. ABR-7 6.0 Max. 5.0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E: BagweTl Laboratory Supervisor (601) 369-3624 VAB.0001201192 Vieta Polymers Highway 25 A Aberdeen, MS 39730 RAILCAR ANALYSIS Load Date: g -/g -*?2- Product: Time Logged In: Ship Date: jn /*> ? Logged In By: Order No:_ I *-K Car No.: *Z Silo(6): _ Customer: /After Ate 7#*^-- Compartment A Sample From Bottom Moisture % BL Contamination BR Bulk Density IZL S' BD after Fluff Hard Particle 5 7 Viscosity Lt RVCM .Ott* 40 Mesh/Glassies CA Bottom 7 ,88 CB Bottom S / B Bottom J Screen Analysis Mesh 40 Weight QjOQ % 0.0Q 60 80 100 /S so 30-^ 26.1 120 140 200 56/ Pan j?./ Drytime: Static Flow: Avg. Microns: Color L: /*p d & b L8^ Technician: mm VAB.0001201193 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 G ERTIEICATE Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 ANA LVSIS Date: August 20, 1992 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept. Ship Date: August 18, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A VIS1AProduct: 5385 Railcar No.: GACX 73384 Order No.: 0014855-000 I PC Specification Analysis 0.90-0.95 0.93 8.5 Max. 0.142 40 Total Total Black + Brown Hard Particles 8 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH X ON 15 Max. 2 15 Max. 8.8 0.510 Min. 0.587 0.30 Max. 0.17 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins. ABR-7 6.0 Max. 5.0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E; Bagw Laboratory Supervisor (601) 369-3624 VAB.0001201194 Vieta Polymers Highway 25 A Aberdeen, MS 3973Q FVC RAILCAR ANALYSIS Load Date t Time Logged In: Ship Date &1 Product: Car No.: 7 3??V Logged In Bv: 19% ^<"Qc>o Order No: Silo(6) Customer: I ft. No Compartment A Sample From Bottom Moisture % BL Contamination BR . os' 7 Bulk Density BD after Fluff Hard Particle 5 7 Viscosity RVCM 40 Mesh/Glassies 1`iZ' CA Bottom 7^* Screen Analysis Mesh Weight % 40 6. 0D 0,0 60 us 2J3 80 100 s6Tf CB Bottom 17 /o B Bottom 11 s> .S28 N 7 4 L 120 /gff 140 13-'?- 200 1.0 Pan U1 2+ Drytime: Static Flow: ^ / Avg. Microns: mi Color L: o, *7 b ?_ Technician: VAB.0001201195 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 X R I GA ./ OR AIMALYS X S A Date: August 13, 1992 Customer: Intex Plastics Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: August 11, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A VIS1AProduct: 5415 Railcar No Order No GACX 73399 0013894-002 I PC Specification 1.00 - 1.04 8.5 PPM Max 20 Total Max. Analysis 1 .02 0.025 Total Black + Brown Hard Particles @ 7 mins Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2B ABR-1A ABR-3 % ON 5 Max. 2 15 Sec. Max 9.3 0.460 Min. 0.509 0.30 Max. 0.23 25.0 Thru 140 Mesh Max 5.0 On Pan Max. 100 120 1401 2001 PAN 27.8115.51 7.51 5.2 1.8 Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 4.9 Amy E yBagwe Laboratory Supervisor (601 ) 369-3624 VAB.0001201196 Vista Polymers way 25 Aberdeen, MS 39730 E>VC RAXLOAR ANALYSI S Load Date: Mo -92- Time In / SCO Ship Date i4 Product: 5415 Logged In By: Order No: Car No.: Silo(s): Customer: a/p mm-L- Compartment Sample From Moisture % A 1 Bottom Top Contamination BL BR 5 3 Bulk Density ls*\ 3 CA Bottom 1 _j 23 Top 3 (x> *37 CB BottomI Top A3 17 .*3 7 I Bottom 1.22 Top 7 . 13 Hard Viscosity HVCM Screen Analysis Mesh Weight % 40 QjjO 0.0 60 4/ MDrytime: 80 100 2>tJ 2*7.$ 120 77/ 140 J.vs 200 -z Pan e>r?a /.8 Static Flow: o L Avg. Microns: izS3 Color L: a b Aag METS: ?7(Cd ///<? X Technician: VAB.0001201197 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 C t= R X R X OA Date: August 12, 1992 Customer: Intex Plastics Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: August 10, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 ANA LYS X S A VIS1AProduct: 5415 Railcar No Order No ACFX 41161 0013894-001 I PC Specification 1.00 - 1.04 8.5 PPM Max. 20 Total Max. Analysis 1.03 0.01 7 Total Black + Brown Hard Particles 7 mins Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2B ABR-1A ABR-3 5 Max. 1 15 Sec. Max 8.3 0.460 Min. 0.520 0.30 Max. 0.17 25.0 Thru 140 Mesh Max 5.0 On Pan Max. % ON Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 5.0 Amy E. TJagwel Laboratory Supervisor (601) 369-3624 VAB.0001201198 A Vista Polymers Highway 25 Aberdeen, MS 39730 PVC RAILCAR ANALYSIS Load Date: Product: Time Logged In: I yPo Logged In By: /t o fais Ship Date: Order No billet Car No.: Silo(s): Customer: /?o C Compartment A Sample From Bottom Top Moisture % .// BL Contamination BR Bulk Density 3 3" (* 5 Hard Particle 7 7 to Viscosity RVCM 1.03?} .on CA Bottom Top .(1 3 .52/ 7 Screen Analysis Mesh Weight % 40 0*00 o<o 60 ].R5 3.7 80 n.s* 39* L? 100 M.?? 28-1 CB Bottom Top B Bottom Top 2, i V 2. l 7 Sty am- 120 7.57 M.r 140 3.39 .7 200 &.4L 4-<i Pan O.lb Drytime: jr.o Static Flow : o /*3 IZZAvg. Microns: ** /0P.9*>Color L: a 0./ b / 2 METS: Technician:: Q> 114-0 % VAB.0001201199 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 certificate of Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 analysis A Date: August 7, 1992 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: August 6, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A VISHAProduct: 5385 Railcar No.: VIPX 45866 Order No.: 0013892-003 I PC Specification Analysis 0.90 - 0.95 0.92 8.5 Max. 0.063 40 Total Total Black + Brown Hard Particles @ 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-- 2A ABR-1A ABR-3 MESH % ON 15 Max. 3 15 Max. 9.9 0.510 Min. 0.578 0.30 Max. 0.11 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins. ABR-7 6.0 Max. 4.9 Polyvinyl Chloride, Virgin Resin, Not Reprocessed H. D. Lucas Laboratory Supervisor (601) 369-3624 VAB.0001201200 Vista Polymers Highway 25 A Aberdeen, MS 3973q RAILCAR ANALYSIS Load Date Time Logged Ship Date Product: Car No.: Logged In By: n/lh Silo(6) : &> It?. Order No^ ?%*><%3 Customer: He*ynefht___ Compartment A Sample From Bottom Moisture % .>9 BL Contamination BR /? Bulk Density BD after Fluff Hard Particle 5 7 3 ra Viscosity RVCM . 923 .au?> 40 Mesh/Glassies CA Bottom /0 /3 At Screen Analysis Mesh 40 60 80 100 Weight UB % Drytime: f* Static Flow: Color L: /CO. 37 CB Bottom ,// t* 7# B Bottom ./> IA 17 7 4 L * 120 3,9L 140 *^ tog. 200 7A 9.9Z Avg. Microns: Pan (A b /5T Technician: VAB.0001201201 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICAT OF ANALYSIS A Date: August 7, 1992 Customer: Intex Plastics Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: August 6, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A VISIAProduct: 5415 Railcar No.: UTCX 46475 Order No.: 0013689-001 I PC ification 1.00 - 1.04 8.5 PPM Max. 20 Total Max. Analysis 1.03 0.012 Total Black + Brown Hard Particles @ 7 mins Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2B ABR-1A ABR-3 5 Max. 4 15 Sec. Max. 8.7 0.460 Min. 0,496 0.30 Max. 0.15 25.0 Thru 140 Mesh Max 5.0 On Pan Max. % ON Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 5.0 H. D. Lucas Laboratory Supervisor (601) 369-3624 VAB.0001201202 Vista Polymers Highway 25 A Aberdeen, MS 39730 Load Date: Time Logged Ship Date: RVC RA XLCAR ANALYSIS LLTCX JT-9P- Product: Car No. Logged In By: Silo(s): 1outsit Order No: O0(3(o%^ Customer: 6 <h e r to t Compartment A Sample From Bottom Top Moisture % BL Contamination BR jL j 2' Bulk Density 5 Hard Particle 7 A% tv A JS Viscosity / #2f RVCM .012. CA Bottom Top JA 3Y S' Ai d CB Bottom Top dl X j 411 B Bottom Top . 41 3 . S& 7 / 7 Screen Analysis Mesh 40 Weight % a*/7 0~o 60 80 LJJL 1232 .rJ. 31 100 IS. 2^ 3b. { 120 11. / 140 U2 7-2 200 Pan 2 SC Ml Sf u Drytime: J> t> Static Flow: >Z L? Avg. Microns: 02 Color L: a do b /. /f METS: tS*4rL/l3-C % Technician: s VAB.0001201203 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369 8111 A CERTIFICATE OF Date: Customer: Intex Plastics Corp Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Date of Shipment: VISIA Product: 5385 Order No No 7~Yfo $4- Property Inherent Viscosity Residual VCM, ppm Contamination Test Method ABR-10 ABGC-26 ABR-5A Total Black + Brown Hard Particles < 7 Mins. Static Flow, Seconds Bulk Density, gm/cc Moisture, X Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR--1A ABR-3 Analysis . 22 <$><22. 1 (o $.2, /*- 7. ON 40 hO 80 100 o|12 140 oj20 j PAN QJ90 o.tj /f.sj A27 23 7 tf-S //s Brabender Dry Time, Mins. ABR--7 Laboratory Supervisor VAB.0001201204 Regulars or Bags Page of pages &A17<-/ a Vinyl Sample Log Data Product Type VAB.0001201205 Visfa Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 A Date: August 5, 1992 Customer: Intex Plastics Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: August 3, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A VIS1AProduct: 5415 Railcar No.: VIPX 45706 Order No.: 0013894-000 I PC Specification 1.00 - 1.04 8.5 PPM Max. 20 Total Max. Analysis 1.03 0.026 Total Black + Brown Hard Particles 7 mins Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2B ABR-1A ABR-3 % ON 5 Max. 1 15 Sec. Max. 7.9 0.460 Min. 0.510 0.30 Max. 0.15 25.0 Thru 140 Mesh Max. 5.0 On Pan Max. 140 D 2001 PAN 5.11 3.21 1.8 Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 5.0 Amy E. Bagwel Laboratory Supervisor (601) 369-3624 VAB.0001201206 Vista Polymers Highway 25 A Aberdeen! MS 39730 E>VO RAILCAR ANALYSIS Load Date Time Logged In: _/-<6P Ship Date Product Logged In By: Order No 0OO No : 4S7q(q ClSilo(s) Customer: Compartment A Sample From Bottom Top Moisture % BL Contamination BR .> 3 Bulk Density 5 Hard Particle 7 X/J 3 I 6-6 Viscosity \otn RVCM .DUd CA Bottom Top .// f- i 6, 7 CB Bottom Top B Bottom Top ./j .AT' 7 3/ i -for* - . Screen Analysis Mesh Weight 40 & &0 % 60 A l* 80 2.L 73 *tzx 100 /S~./0 30. Z. 120 stxl /2.r 140 S7 S'. / 200 / J. 2. Pan . 10 LJL Drytime H Static Flow: / 7.70 Avg. Microns: _ }?0.1 Color L: /oQ. ~?C a .o<9 b A METS: <>3! / /Z-Z-. I % Technician: VAB.0001201207 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIR X CAT E OR Aberdeen, Mississippi 39730-009) Phone (601) 369-8) 11 ANALYSIS Date: August 5, 1992 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept. Ship Date: August 3, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A VISIAProduct: 5385 Railcar No.: ACFX 41165 Order No. 0013892-002 I PC Specification Analvsis 0.90 - 0.95 0.94 8.5 Max. 0.002 40 Total Total Black + Brown Hard Particles @ 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH % ON 15 Max. 15 15 Max. 8. 1 0.510 Min. 0. 574 0.30 Max. 0. 07 25.0 Thru 140 Mesh 5.0 Max on Pan 120 17.2 Brabender Dry Time, Mins. ABR-7 6.0 Max 5.0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor (601) 369-3624 VAB.0001201208 Vista Polymers Highway 25 * A Aberdeen, MS 3973q RAILCAR ANALYSIS Load Date: Product: Car No. : 4//t. i Time Logged In: Ship Date: l*> 0(p00 Logged In By Order Ho: --002-- Silo(s): Kuntom-r: L'?? 6 /h <7 fir! Compartment Sample From A Bottom Moisture % BL Contamination BR Bulk Density BD after Fluff AM Hard Particle 5 7 - Viscosity RVCM 4 .002, 40 Mesh/Glassies +" Screen Analysis Mesh 40 Weight /? % 0-0 60 I-?! 3-A CA Bottom ,0l 1 ' 80 / 74? 3H,C 100 /V-7F CB Bottom .ol 1 3 B Bottom . 0(p 3 17 AM / */ / --C_______ 120 140 sf.ir 3.<yS' ni- .34-_ 200 Pan J.?<s 032. JLZ- Drytime: 0 Static Flow : Avg. Microns: 111 Color L m<> s 0.63 b IM Technician: KH v- ns VAB.0001201209 Vista tolymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone {601} 369-81 1 1 ft Date: July 30, 1992 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept. Ship Date: July 29, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A VIS1AProduct: 5385 Railcar No.: VIPX 45797 Order No.: 0012628-003 I PC Specification Analysis 0.90 - 0.95 0.93 8.5 Max. 0.086 40 Total Total Black + Brown Hard Particles @ 7 Mins. ABR-12 15 Max. 6 Dry Flow, Seconds ABR-8 15 Max. 9.2 Bulk Density, gm/cc ABR-2A 0.510 Min. 0.575 Moisture, % ABR-1A 0.30 Max. 0.17 Particle Size Distribution ABR-3 25.0 Thru 140 Mesh 5.0 Max on Pan MESH % ON 40 60 O.OOi 4.3 36.6 140 8.8 PAN 2.1 Brabender Dry Time, Mins. ABR-7 6.0 Max. 5.0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Lucas Laboratory Supervisor (601) 369-3624 VAB.0001201210 tf Vista Polymers Highway 25 * Aberdeen, MS 39730 Load Date: 7*^ Time Logged Ship Date: ^VC RAILCAR ANALYSIS ~ ?1 Product Car No.: vtPX "?? 7 Logged In By: /v*<1 Silo(s): I2.U1Order No: <0S> Customer: Compartment Sample From Moisture % A Bottom BL Contamination BR z <o Bulk Density ,S7C= BD after Fluff Hard Particle 5 7 Viscosity (e rvcm Mesh/Gla66 CA Bottom z _r CB Bottom 3 B Bottom jn 3 Screen Analysis Mesh Weight X 40 0i.CK0 0.0 60 Uk 40 Drytime: r.o 80 //.Z<7 C (g 100 <2S< 2- Static Flow: 120 S*oo 140 4.37 !b.Z . <fi<P 200 Pan /,o4> &L Avg. Microns: //S'-e Color L: ^2 <9-o? b J.72" Technician: aa VAB.0001201211 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIEXCAT Aberdeen, Mississippi 39730*0091 Phone (601)369*8111 OF ANALYSIS Date: July 29, 1992 Customer: Intex Plastics Corp Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: July 27, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A V1S1AProduct: 5385 Railcar No.: PTLX 42057 Order No. 0013892-001 I PC Specification Analysis 0.90 - 0.95 0.94 8.5 Max. 0.335 40 Total Total Black + Brown Hard Particles @ 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH % ON 15 Max. 15 Max. 2 8.1 0.510 Min 0.579 0.30 Max. 0.13 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins. ABR-7 6.0 Max. 5.0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. H. D. Lucas Laboratory Supervisor (601) 369-3624 VAB.0001201212 Vista Polymers Highway 25 h Aberdeen, MS 39730 3?VC RAILCAR ANALYSI S f>TL)( Load Date: Product Car No. 4-tpSV Time Logged In: Ship Date: Logged In By: Order No: @0/3 $92. Silo(s) : Customer: lP(L> AO Ai jssJ Compartment A Sample From Bottom Moisture % BL Contamination BR Bulk Density BD after Fluff Hard Particle 5 7 /2- Viscosity RVCM 40 Mesh/Glassies Screen Analysis Mesh 40 Weight O* D # % 0*0 Drytime: 60 .7/ > CA Bottom , >3 A \ CB Bottom . Jo , r?7 B Bottom . // 32L r 7? 7 4 1 80 100 3/. 4 2% Static Flow: 120 140 1.Z1 /f.3 /O' o ** 200 S.ii' 7. 3 Pan /. 0 / // Avg. Microns:: J04 / Color L: 10 b / : t3 Technician: mjs rtf A VAB.0001201213 Vista Polymers A Division of Visto Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 & Date: July, 29, 1992 Customer: Intex Plastics Corp Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Dept. Ship Date: July 27, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A VISIA Product: 5305 Railcar No.: GACX 73382 Order No.: 0013688-002 IPC Specification Analysis 0.71 - 0.76 0.73 8.5 PPM Max. 0.083 60 Total Total Black + Brown Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2A Moisture, % ABR-1A Particle Size Distribution ABR-3 15 Sec. Max. 7.8 0.510 Min. 0.30 Max. 0.532 0.21 30.0 Thru 140 Mesh 5.0 Max on Pan % ON Polyvinyl Chloride, Virgin Resin, Not Reprocessed Laboratory Supervisor (601) 369-3624 VAB.0001201214 Vista Polymers Highway 25 & Aberdeen, MS 39730. FLA X LCAR ANALYS I S Load Date: ~ ^*7 2^ t Time Logged In: /&&* Ship Date: Product: Logged In By: Order Car No. : *733 & Silo( s): Customer go Compartment A Sample From Bottom Moisture BL Contamination BR Bulk Density 7 BD w/antistat .3(fi Viscosity RVCM 724 0S3 CA Bottom ./.s' * .7315 . 1/3 CB Bottom !& S 7 .JTZf . ZOL* B Bottom .3/ /2 /? .33v tn*$ .oty Tappi Test Contamination .06 or less Composite % __________________________________________ _________________________________________________ Screen Analysis .07 ----- .15 .20------------ .60 Mesh Weight % 40 AO 60 6 / o 80 Sr.x* 100 lS.6>3 120 140 717 200 Pan US : !4g/e Avg. Microns % Glassies: *17* 7T.& Color L: a 6. II b AM Static Flow: 0 / 8.ZL Technician: VAB.0001201215 Vista Polymers A Division of Vista Chemical Company GER Highway 25 Post Office Box 91 I f= I C A Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 AM A l_YS X S Date: July 28, 1992 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: July 24, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A VISIAProduct: 5385 Railcar No.: PLCX 47609 Order No.: 0013690-001 I PC Specification Analvsis 0.90 - 0.95 0.93 8.5 PPM Max. 0.095 40 Total Total Black + Brown Hard Particles @ 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH SIS ON 15 Max. 6 15 Sec. Max 10.6 0.510 Min. 0.569 0.30 Max. 0.13 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max 5.0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E.^Bagweli Laboratory Supervisor (601) 369-3624 VAB.0001201216 Vista Polymers Highway 25 Aberdeen, MS 39730 F>VC RAILCAR ANALYSIS Load Date Z3- 7 Time Logged In: kiShip Date: 2 Product: Logged In By: Car No /j?.r Silo(s): Custome lP{L ?6 /7o Compartment A Sample From Bottom Moisture % BL Contamination BR r 3 6 Bulk Density BD after Fluff .SLf Hard Particle 5 7 3c ^ Co Viscosity ____ _ _ RVCM \ ____ H rDt< 40 Mesh/Glassies Screen Analysis Mesh Weight % 40 Q*QO 0 *0 60 2.13 Drytime: S.o CA Bottom .13 si .srij CB ' Bottom iz. I .Si 9 B Bottom ,sk>9 1 / ,, --------/"/7-- ___________ 80 /S-kS J/-3 100 /J.ofc ;h>. / 120 .97 // 0 ' 140 S~.oC /O. / 200 Pan /. // r Static Flow : 0 //<>< Avg. Microns: Color L: a 0. b -2j// Technician: C U VAB.0001201217 Vista Polymers A Division of Vista Chemical Company G EE R Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 X R I G AX" EE O R ANALYS X3 & Date: July 28, 1992 Customer Intex Plastics Corp Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: July 24, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A VIS1AProduct: 5385 Railcar No.: VIPX 45793 Order No.: 0013892-000 x I PC Specification Analvsis 0.90 - 0.95 0.93 8.5 PPM Max 0.089 40 Total Total Black + Brown Hard Particles e 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH % ON 15 Max. 4 15 Sec. Max. 7.9 0.510 Min. 0.581 0.30 Max. 0.16 25.0 Thru 140 Mesh 5.0 Max on Pan PAN 3.5 Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max 5.1 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. BagwerT Laboratory Supervisor (601) 369-3624 VAB.0001201218 Vista Polymers Highway 25 Aberdeen, MS 39730 RAILCAR ANALYSIS Load Date 7'2S-9Z Product: Time Logged In: //* Logged In By: Ship Date: f 2^ Order No: No 4 S' Sllofe) : 7i.77 a.Customer: ip Si4> Compartment A Sample From Bottom Moisture % BL Contamination BR Bulk Density BD after Fluff i .rn Hard Particle 5 7 lo i-a Viscosity .to RVCM Me6h/Gla6s CA Bottom , /r 3a - STo Screen Analysis Me6h Weight % 40 0* 0. 0 60 U.9o 80 IS.Si> Si 8 . 3o.1 100 /J.*2 o CB Bottom JS tL X21 B Bottom . *7 N \--L J 120 S.7f /(>-9 140 4.9/ ---- 200 ------ liswr---- Pan /.74 Drytime: ' <TJ Static F low: o / Z9 Avg. Microns: /^?*f Color L: 97. ft a b -2 lo</ Technician: VAB.0001201219 Vista Polymers Highway 25 A Division of Post Office Box 91 Vista Chemical Company CERTIFICATE OF Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 ANALYS XS A Date: July 28, 1992 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: July 22, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A VJS1AProduct: 5385 Railcar No.: ACFX 41178 Order No.: 0012^28-002 B I PC Specification Analysis 0.90 - 0.95 0.94 8.5 PPM Max 0.053 40 Total Total Black + Brown Hard Particles @ 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH % ON 15 Max. 4 15 Sec. Max 8.7 0.510 Min. 0.583 0.30 Max. 0.09 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max 4.9 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. Bagwel Laboratory Supervisor (601) 369-3624 VAB.0001201220 V Vista Polymers Highway 25 A Aberdeen, MS 39730 RAILOAR ANALYSIS : 7Load Date 22 Time Logged In: /TOO Ship Date: Product Logged In By: Order No Car No. m: Sllo(s) : &7it(,77.csr Customer Compartment A Sample From Bottom Moisture % BL Contamination BR 3 Bulk Density BD after Fluff Hard Particle 5 7 /* Viscosity RVCM 40 Mesh/Glassies CA Bottom ,o? ? CB Bottom ,>8 10 7 B Bottom o^ 3 T .sif Screen Analysis Mesh Weight 40 &.QO % 60 0.7 Drytime: 80 /7-yo >f.7 100 3.(^7 120 4** 140 200 JU Pan ),>(q L JiZiStatic Flow: a /?<n Avg. Microns: Color L: /oj2^/ a b !*S Technician: VAB.0001201221 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFX CAT Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 A lDate : 'l Z-7 Customer: Intex Plastics Corp Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: Y/z-Z./*? Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK/BRN ABR-5A Hard Particles Q 7 Mins. ABR-12A Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2A Moisture, % ABR-1A Particle Size Distribution ABR-3 MESH % ON VISIAProduct: 5325 Lot No. : 0 Truck No. T'4B00I& Order No.: VISTA Specification 0.78 - 0.82 8.5 PPM Max 35/100 Max Analysis .So .070 . J/7 No Spec. 15 Sec. Max 0.480 Min. 7. t? . S'/ 5" 0.30 Max. .n 5.0 Max. on Pan 2001 PAN Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Labor visor/Lead (601) 369-3624 VAB.0001201222 RESIN BAG BLEND BLEND NO; 04 1 PRODUCT: DATE: 7-J. ' SKID MOIST CONT Aig. Microns, 5225/5325/5415: PARTICLE SIZE DISTRIBUTION /4S^ BULK DENS TINE O. /i.^3 /;.?7 3, IX 111 <5,2> .X h.i i ILX 34^ H-9 . C.2 TIKE/TESTED BY: 13^6 6 / GLASSY VISC RVCM <fZ7<r> VAB.0001201223 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 CERTIFICATE OF ANALYSIS A Date: July 23, 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: July 20, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A VJS1A Product: 5305 Railcar No.: ACFX 41174 Order No.: 0013688-001 I PC Specification Analysis 0.71 - 0.76 0.72 8.5 PPM Max. 0.119 60 Total Total Black + Brown Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2A Moisture, % ABR-1A Particle Size Distribution ABR-3 15 Sec. Max. 7.8 0.510 Min. 0.529 0.30 Max. 0.18 30.0 Thru 140 Mesh 5.0 Max on Pan % ON Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E .^Bagwe' Laboratory Supervisor (601) 369-3624 VAB.0001201224 Vista Polymers Highway 25 _J A Aberdeen, MS 39730 F3 VC Ft A I LCAR ANALYSIS Load Date: Product: Time Logged In: /zc! : 7f^O Ship Date Logged In By: Order No:. Car No. : `f'Z/Tf Silo(s): Customer jiP&him bio "yuetn Compartment A Sample From Bottom Moisture lie BL Contamination BR Bulk Density f 3 BD w/antistat - Viscosity RVCM ' 1U W/4 CA Bottom rr f 1 .mi .CUV . CB Bottom ft 7 >me> .ocS B Bottom ./* f 7 .me. , 0&{ Tappi Test Contamination Composite Screen Analysis Mesh Weight % 40 d, 0.0 .06 or less % 60 OS'Z 80 2.1 M .07 ----- - .15 .20------------ .60 100 (3g(e WJ 120 JikL <2*t/h 140 200 4 Pan 4ZE Avg. Microns: Color L: /<o./6> a 0^3! b % Glassies: /.Z*Static Flow: 0 Technician: VAB.0001201225  Vista Polymers Highway 25 Aberdeen, MS 39730 3? V C HAILGAR ANALYSIS Load Date:________ Time Logged In: Ship Date:________ Product :.-DSBeX Logged In By Order No: Car No. ___ Silo(s):_______ Customer:____________ COMPARTMENT Moisture % A Contamination / Bulk Density Color "L" Color "a" Color "bM Static Flow / Viscosity Top RVCM Screen Analysis Mesh 40 m Weight % o*oo 60 A 22 CA CB // B / // / Top ***** Toe ***** Top ***** . 80 ~"~ioo 120 /&> A/40 33.0 23.2 140 7.^ 200 /23 2S Pan o.bz. A2 Weight G-0@ CA % 040 0.2 /> 7$ /3.iZ />*& ( /J.5 2C,.Z 32,5 t.9o m 3.SA 7-0 A. t( P2- Weight CB % 0. 0*0 0 3& Z.St /SI3 3*& im 9/0 1.3* 2.7 0 Weight % 0.6 0.0 0.2$ <0.5 1.S7 /S7jo m S0.(? A5.3< s/.o /4-o 2.2./ / 20 4'f 2.4- Technician: VAB.0001201226 Vista Polymers Highway 25 Aberdeen, MS 39730 * I Xj ANALYSIS Load Date Time Logged In Ship Date: Product: Logged In By Order No: Car No.:. 4ill4- Silo(s): Customer: COMPARTMENT Moisture % A Contamination / Bulk Density Color "L" Color "a" Color "b" Static Flow / Viscosity Top - RVCM Screen Analysis Mesh Weight % 40 0, OQ 0.0 60 */<? CA CB // B / / Ifil> / Top / Top 80 100 120 Itte & 140 /M 200 2.3(s Pan l.gD Weight % Weight % Weight % Technician: VAB.0001201227 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 Date: July 23, 1992 Customer: Intex Plastics Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept Ship Date: July 20, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A VIS1AProduct: 5415 Railcar No. PLWX 44757 Order No. 0013689-000 IPC Specification 1.00 - 1.04 8.5 PPM Max. 20 Total Max Analysis 1.03 0.010 Total Black + Brown Hard Particles @ 7 mins Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2B ABR-1A ABR-3 5 Max. 1 15 Sec. Max 8.7 0.460 Min. 0.498 0.30 Max. 0.08 25.0 Thru 140 Mesh Max. 5.0 On Pan Max. % ON Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max 4.9 Amy E. Bagwe Laboratory Supervisor/Lead (601) 369-3624 VAB.0001201228 V * Vista Polymers Highway 25 h Aberdeen, MS 39730 Load Date: Time Logged In Ship Date: RAILCAR 9\ Product ANALYSIS Car No (9(gQo Logged In By: tLo :_Jp30 Silo(6) l/hdbfij Customer ~ " --......1 - Compartment ^ A Sample From Bottom Top Moisture % BL Contamination BB O? _2_ Bulk Density 1 Y 5 Hard Particle 7 2^ tK Viscosity 1-07^ RVCM 0!O CA Bottom Top * $ 2L jr . ^>1- 2J <, CB Bottom Top JftJC _ r . B Bottom Top ' z> 3 5" -Vr ?7 Screen Analysis Mesh 40 Weight %p 60 80 7S^ /f-37 \-Y 3t-7 100 /XJ% p.b-% 120 *7. ^ /z.z' 140 f- 200 JS'S Pan , <7*0 h? Drytime: Y- Static Flow: & /?-7 Avg. Microns: Color L: fOO-tl- _ >-/6 b /.tf Technician METS : ZO / / i^+r % VAB.0001201229 Vista Polymers A Division of Highway 25 Post Office Box 91 Vista Chemical Company CERT X WH CATE OF* Aberdeen, Mississippi 39730-0091 Phone (601)369-8111 ANALYSXS Date: July 20, 1992 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept. Ship Date: July 17, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A Product: Railcar No.: UTCX 46419 Order No.: 0013690-001 IPC Specification Analysis 0.90 - 0.95 0.95 8.5 PPM Max. 0.027 40 Total Total Black + Brown Hard Particles 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH % ON 15 Max. 3 15 Sec. Max. 8.1 0.510 Min. 0.582 0.30 Max. 0.12 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 4.9 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor (601) 369-3624 VAB.0001201230 Viot-a Polymers Highway 25 Aberdeen, MS 39730 n: 7-4 -Load Date Time Logged Ship Date: IA 2ia RAILCAR ANALYSIS Product: Logged In By Order No: \ZL96 Car No.: Customer c ?c, c n us: Compartment A Sample From Bottom Moisture % .0L BL Contamination BR 3 Bulk Density S7$ BD after Fluff Hard Particle 5 7 10 IL Viscosity Ml RVCM ,07,1 40 Mesh/Glassies CA Bottom 3 CB Bottom 7 S 7 B Bottom .i V A i Screen Analysis Mesh 40 60 80 100 120 Weicht MlH`07 2- % 0 <0 /.X 33A as.t 140 200 Pan 3,30 J. A? lo - ip Drytime: /S.t ns-<fStatic Flow: v Avg. Microns: -P7Color L: f-OO.T^V a ~~ bh Technician: VAB.0001201231 Vista Pblymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730*0091 Phone (601) 369-8111 CERTIFICATE OF ANALYS Date: July 20, 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Dept. Ship Date: July 17, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A VIS1A Product: 5305 Railcar No.: PLWX 44567 Order No.: 0013688-000 I PC Specification Analysis 0.71 - 0.76 0.73 8.5 PPM Max 0.151 60 Total Total Black + Brown Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2A Moisture, % ABR-1A Particle Size Distribution ABR-3 15 Sec. Max. 7.8 0.510 Min. 0.535 0.30 Max. 0.04 30.0 Thru 140 Mesh 5.0 Max on Pan % ON Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E; Bagwells-J Laboratory Supervisor (601) 369-3624 VAB.0001201232 Vista Polymers Highway 25 A Aberdeen, MS 39730 Ft A. X LCAR ANALYS X S Load Date: S'-1-12. Time Logged In: /OC0 Ship Date: Product: Car No.: Logged In By: /<} Silo( s ): ?7 4tZ Order No:_ g-ooa Customer: Compartment A Sample From Bottom Moisture BL Contamination BR Bulk Density erf z \5 BD w/antistat Viscosity RVCM .72$ r/*57 CA Bottom ,6*f J H .5"S7 .725" CB Bottom <} . 5V7 .w ,5-ST) B Bottom .<>X z V .64/ 72<f * ---TT--- .zm Tappi Test Contamination Composite Screen Analysis Mesh 40 Weight % .06 or less 60 O'b 80 7, a H-t, .07------------ . 15 .20------------ .60 100 13-Zte Zk* s 120 j*/-77 Zl.i, 140 /7 c, 200 v./T 7.4 Pan t.3S z,n Avg. Microns : /yer % Glassies: J Color L: 0 /13La b A# Static Flow: Technician frt & + J-S VAB.0001201233 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 A Date: July 20, 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Dept. Ship Date: July 16, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A VIS1A Product: 5305 Railcar No.: VIPX 45747 Order No.: 0012627-001 I PC Specification Analysis 0.71 - 0.76 0.73 8.5 PPM Max. 0.205 60 Total Total Black + Brown Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2A Moisture, % ABR-1A Particle Size Distribution ABR-3 15 Sec. Max. 8.7 0.510 Min. 0.533 0.30 Max. 0.18 30.0 Thru 140 Mesh 5.0Max on Pan % ON Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy Bagwell Laboratory Supervisor (601) 369-3624 VAB.0001201234 Vista Polymers Highway 2 5 Aberdeen, MS 39730 RAILCAR ANALYSX Load Date: 7 ^^ Time Logged In: Ship Date: Product: Logged In By: Order No: Car No.: Silo( s ) : Customer: 1 Pdap&i Compartment Sample From A Bottom CA Bottom CB Bottom B Bottom - Moisture BL Contamination BR 7 Bulk Density .S3<f BD w/antistat ./& 3 S' ,S3( .(f c* .Si( J7 *f (0 **3 to Viscosity RVCM Tappi Test Contamination Composite ,7 .20^ .1ZI M-z .12& .2.4%. .06 or less 2/ti__________________ .07 ----- .15 .w * </*? .20------------ . 60 Screen Analysis Mesh 40 Weight 0,00 % 60 M .5 80 333 6-7 100 AIL 120 mi 21V 140 200 1213 t-W I 4,9 Pan 2.23 u.s~ Avg. Microns: /a ?. / % Glassies /% Color L : 7S~ a ,z<? b Aw Static Flow: O / ician: (jO ^ Techn VAB.0001201235 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 OF ANALYSIS A Date: July 17, 1992 Customer: Intex Plastics Corp Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept. Ship Date: July 15, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A VIS1AProduct: 5385 Railcar No.: VIPX 45901 Order No.: 0012628-001 I PC Specification Analysis 0.90 - 0.95 0.95 8.5 PPM Max. 0.039 40 Total Total Black + Brown Hard Particles @ 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR--8 ABR-2A ABR-1A ABR-3 MESH % ON 15 Max. 2 15 Sec. Max. 8.7 0.510 Min. 0.577 0.30 Max. 0.04 25.0 Thru 140 Mesh 5.0Max on Pan Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 4.8 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. Bagwell Laboratory Supervisor (601) 369-3624 VAB.0001201236 Vista Polymers Highway 25 A Aberdeen, MS 39730 Load Date: 7-3^9 Time Logged In: Ship Date : |I RAILCAR ANALYSIS Product: Logged In By: Order No: I 7*1# ^ Car No Sll0(6) Customer : IPC^ SI/ & Compartment St ct A Sample From Bottom Moisture % BL Contamination BR Bulk Density 7 BD after Fluff Hard Particle 5 2 CA Bottom A 1 CB Bottom 2i y B Bottom 3 7 Viscosity RVCM 40 Me6h/Glass Screen Analysis Mesh 40 Weight % Drytime: $ 60 80 L00 120 140 200 Pan ot> fTM 7 3U>7 /* 8-8 S'7 LI *V Static Flow: (P / Avg. Microns: / &7 C Color L /#o*sY 6) b /. tf Technician: /n^T 'Jr' VAB.0001201237 Vista Polymers A Division of Vista Chemicol Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 Date: July 15, 1992 Customer: Intex Plastics Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept. Ship Date: July 10, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A ViSlAProduct: 5415 Railcar No.: PLWX 44717 Order No.: 0012626-000 IPC Specification 1.00 - 1.04 8.5 PPM Max. 20 Total Max Analysis 1.02 0.013 Total Black + Brown Hard Particles @ 7 mins Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2B ABR-1A ABR-3 % ON 5 Max. 1 15 Sec. Max 8.5 0.460 Min. 0.495 0.30 Max. 0.16 25.0 Thru 140 Mesh Max. 5.0 On Pan Max. 1001 120 1401 2001 PAN 7.61 6.81 2.5 Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max 4.8 Amy E.c/Bagwell Laboratory Supervisor/Lead (601) 369-3624 VAB.0001201238 Vista Polymers Highway 25 Aberdeen, MS 39730 RAILCAR ANALYSIS -.1Load Date Product: Time Logged In .JROO : *11LoJl Ship Date Logged Order No: In By: Car Ho. : 7/ 7 .AllSilo(s) Customer: J^ Compartment A Sample From Bottom Top Moisture % BL Contamination BR > 12-" z 3~ Bulk Density 7 5 Hard Particle 7 3 flit Viscosity RVCM .015 CA Bottom Top 3 J7 CB Bottom Top if Y L S' B Bottom Top (A J /a y? ? 7 Screen Analysis Mesh 40 Weight 0.0 % /> 0.0 60 /'9J 3.1 Drytime: yr. -2 80 100 } 9.3*2-- /3-&S a/ Static Flow 120 7- 43 //-* / 5> J> 140 200 Pan Avg. Microns: /' Color L: /^/. O ? a LL b METS: %%sn,m % Technician: *,.r +* VAB.0001201239 Vista Polymers Highway 25 A Division of Post Office Box 91 Vista Chemical Company CERTIFICATE OE Aberdeen, Mississippi 39730-0091 Phone (601) 369-811 1 ANALYS X S ^ Date: July 10, 1992 Customer: Intex Plastics Corp* Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept. Ship Date: July 8, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A Total Black + Brown Product: 5385Wj^||^ Railcar No.: GACX 73400 Order No.: 0012628-000 I PC Specification Analysis 0.90 - 0.95 0.93 8.5 PPM Max. 40 Total 0.101 1 8 1 8 1 12 1 9 1 Hard Particles @ 7 Mins. ABR-12 15 Max. 2 Dry Flow, Seconds ABR-8 15 Sec. Max. 8.0 Bulk Density, gm/cc Moisture, % ABR-2A ABR-1A 0.510 Min. 0.30 Max. 0.582 0.18 Particle Size Distribution * ABR-3 25.0 Thru 140 Mesh 5.0 Max on Pan MESH 1 40 I 60 1 80 I lool 1 120 1401 I200 PANI % ON |0.00| 2.2138.2 27.4|l7.o| . I8 4 5.if 1.71 Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 4.9 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor (601) 369-3624 VAB.0001201240 Via^ta Polymers Highway 25 A Aberdeen, MS 39730 ^VC RAILOAH ANALYSIS Load Date: ~^2- Time Logged In >/ di Ship Date Prodact Car No. 71^00 Logged In By: 4L Silo(6): / 74'7 7- *T '2.(o'2<^-0<yd Customer: /fle'/tL /}c Mesh Weight % 40 . 0*0 60 /./g 3.2. Drytime: V.q 80 /?.!/ 3.2. 100 13.7J 23. 120 /7.0 140 4 200 Pan . o-SV /7 Static Flow: Q /f.o Avg. Microns: /7/? Color L: a o.fpjf b /' 77 Co d-Technician: VAB.0001201241 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369*8111 CERTIFICATE OF ANALYSIS * Date: July 10, 1992 Customer: Intex Plastics Corp Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Dept. Ship Date: July 9, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM,V ppm ABGC-26 Contamination, BLK + BRN ABR-5A VISIA Product: 5305 Railcar No UTCX 46510 Order No 0012627-000 IPC Specification Analysis 0.71 - 0.76 0.72 8.5 PPM Max 0.058 60 Total Total Black + Brown Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2A Moisture, % ABR-1A Particle Size Distribution ABR-3 15 Sec. Max 8.6 0.510 Min. 0.527 0.30 Max. 0.15 30.0 Thru 140 Mesh 5.0 Max on Pan % ON Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E. Bagwe Laboratory Supervisor (601) 369-3624 VAB.0001201242 Vista Polymers Highway 25 A Aberdeen, MS 39730 Ft A X LCAR Load Date: r-/o- ? * Time Logged In: >63?O jih Product: Logged In By: Car No.: Silo(s): Customer : [ (. io aJo TyetA-- Compartment Sample From Bottom Moisture Contamination BL BR /< Bulk Density BD w/antistat Viscosity RVCM mi 058 Bottom J ms OCerf Bottom f6 Bottom .021 .SfZ .72A .e>r?~s Tappi Test Contamination Composite .06 or less fa Screen Analysis Mesh Weight % 40 e>.o0 QrQO 60 0.1 80 4.6 ( to Avg. Microns: .07-------------.15 .20------------- .60 100 120 /a+< 31 & 140 M7& 23.4 200 /2.o Pan /At % ies: Glass ^ {*?<> Color L: a *Yt b LM* Static Flow: & / & k Technician: VAB.0001201243 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: July 6, 1992 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Dept. Ship Date: June 30, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A VISTAProduct: 5385 Railcar No.: UTCX 46414 Order No.: 0011894-005 I PC Specification Analysis 0.90 - 0.95 0.93 8.5 PPM Max. 0.012 40 Total Total Black + Brown Hard Particles @ 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH % ON 15 Max. 3 15 Sec. Max. 7.9 0.510 Min. 0.581 0.30 Max. 0.13 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 4.9 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. & Amy E. Laboratory Supervisor (601) 369-3624 VAB.0001201244 Vista Polymers Highway 25 * Aberdeen, MS 39730 RAILCAR ANALYSIS Load Date: Time Logged In; &(&eO Product: Logged In By: Ship Date Order No: IlS^^ Car No.: Silo(6) Customer: -'sf~i Compartment A CA CB B Sample From Bottom Bottom Bottom Bottom Moisture % BL Contamination ___ BR 1 Bulk Density ,r?l BD after Fluff Hard Particle 5 7 2/ Viscosity RVCM * % ,0/7^ 40 Mesh/Glassies - 5 , SW j) 3 i? ,r?o a s V y _______ ./O (f .<7~? 4 Screen Analysis Mesh Weight % 40 P+00 0+0 60 1.7A 2.* Drytime: 4.1 80 JMl 21,o 100 /f.xar 3o. 4T 120 /fl.oc 140 0 2c* L__ / 0+0 200 3.0 7 JL Static Flow: d *9/ *7. Avg. Microns: Pan .t AZ /et.+ iML Color L: / V0 * ^ ^ a of b / 7< Technician ^i^U-rf A VAB.0001201245 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 RTIFIOATE OF Aberdeen, Mississippi 39730 Phone (601) 369-8111 ANALYSX S * Date: June 19, 1992 Customer: Intex Plastics Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: June 15, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A Product: 5415 Railcar No.: PTLX Order No.: 0011898-001 IPC Specification 1.00 - 1.04 8.5 PPM Max. 20 Total Max. 1.01 0.013 Total Black + Brown Hard Particles ! 7 mins Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2B ABR-1A ABR-3 5 Max. 2 15 Sec. Max 9.3 0.460 Min 0.521 0*30 Max. 0.25 25.0 Thru 140 Mesh Max. 5.0 On Pan Max. % ON Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 5.0 Amy E. Bagw Laboratory Supervisor/Lead (601) 369-3624 VAB.0001201246 9 / Vista Polvmere Highway 25 Aberdeen, MS 39730 PVC RAI LC AR ANALYSX S Load Date : /A Time Logged In: ffi foO Product: Logged In By: Car No . : /P7 Silo(e): Ship Date: Order No: / ^ O/ Customer: ^ 0 Compartment Sample From Moisture % Contamination Bulk Density Hard Particle Viscosity RVCM Screen Analysis Mesh Weight % 40 0,* 60 2-Je 4-2, jf-0Drytime: . 80 // i T'iV 100 /4z7 120 /Lf Static F low : c, fs 140 ^L_ 7. (r 200 Par .e 4? U Avg . Microns' /7S'& Co lor L: /<%?. 1,2 0.V? b /Jo METS 77s7 /i7-^ Z /ft Techniclan VAB.0001201247 Vista Polymers A Division of Visla Chemical Company * Highway 25 Rost Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 Date: June 19, 1992 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: June 15, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A Product: 5385 VISTA Railcar No.: PLWX 44676 Order No.: 0011894-004 IPC Specification Analysis 0.90 - 0.95 0.93 8.5 PPM Max. 0.064 40 Total Total Black + Brown Hard Particles 7 Mins. ABR-12 Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2A Moisture, % ABR-1A Particle Size Distribution ABR-3 MESH % ON 15 Max. 3 15 Sec. Max. 9.6 0.510 Min. 0.581 0.30 Max. 0.18 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 5.0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. . Bagwell Laboratory Supervisor (601) 369-3624 VAB.0001201248 Vista Polymers Highway 25 A Aberdeen, MS 39730 F>VC RAILCAR ANALYSTS Load Date: Time Logged In: Ship Date: Product Car No ^/ Q Logged In By: Order No : ll%q4-o4f~ Silo(s) : :id- Customer ^ Compartment L, Sample From Bottom Moisture % BL Contamination BR \2 /Z Bulk Density STS! BD after Fluff Hard Particle 5 7 Viscosity RVCM 40 Mesh/Glassies S Bottom il /o Bottom IX /S Bottom IS /5 5V(m Screen Analysis Mesh Weight % 40 e>. op ao 60 80 11-3 100 l?3t 120 UM. 140 is! 200 6J>3 M_ Pan f-94 s:o Drytime Static Flow: oL Avg. Microns . /?/ Color L: a b IA Technician: VAB.0001201249 Virtu Polymer* Highway 25 A Division of Post Office Box 91 Vista Chemical Company o ER.TI FI CATE OE Aberdeen, Mississippi 39730 Phone (601) 369-8111 ANALYSIS A Date: June 16, 1992 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: June 12, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A Product: 5385 VIS1A Railcar No.: UTCX 46522 Order No.: 0011894-003 I PC Specification Analysis 0.90 - 0.95 0.93 8.5 PPM Max. 0.362 40 Total Total Black + Brown Hard Particles % 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH % ON 15 Max. 2 15 Sec. Max* 8. 1 0.510 Min. 0. 586 0.30 Max. 0. 15 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 4.9 Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E. vBa)gwe 1 sr Laboratory Supervisor (601) 369-3624 VAB.0001201250 A Vista Polymers Highway 25 Aberdeen, MS 39730 RAILCAR ANALYSIS Load Date // :/330Time Logged In Date: 6/ l~ZShip Product: Car No.: Logged In By: Silo(6): 6&/6fS :lP&Order No: do H SW'-ftsa Customer M J&t Compartment A Sample From Bottom Moisture % BL Contamination BR J/ 2. Bulk Density BD after Fluff .S7f Hard Particle 51 7 /- Z Viscosity ,^3| RVCM 40 Mesh/Glassies CA Bottom ./r . 'Stf' CB Bottom JL- $ ^. fU B Bottom Screen Analysis Mesh 40 Weight % 1*0 60 z.H 4.z* 80 H.SI- 33.0 100 13.13 2 C.3 120 /7,f 140 /0. 2- 200 S.Z7 i.S" Pan A? Drvtime: -f.f Static Flow: o/$.l Avg. Microns: . /7P.f Color L: a o! b f./S Technician: VAB.0001201251 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369*8111 A Date: June 16, 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: June 12, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A VBIAProduct: 5305 Railcar No.: PLCX 43394 Order No.: 0011897-001 IPC Specification Analysis 0.71 - 0.76 0.72 8.5 PPM Max 0.185 60 Total Total Black + Brown Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2A Moisture, % ABR-1A Particle Size Distribution ABR-3 15 Sec. Max 8.4 0.510 Min. 0.529 0.30 Max. 0.17 30.0 Thru 140 Mesh 5.0 Max on Pan % ON Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E V tfagwe Laboratory Supervi VAB.0001201252 k> Vista Polymers Highway 25 Aberdeen, MS 39730 Ft A ILCAR ANALYSIS Load Date: Time Logged In: /7 :JbJj Ship Date Product: Logged In By Order No:_ (l%97-OC>l Car No. : 3 ?4___________ Silo( s ) : L>F// ^7 Customer : l PC fJo TvefaL-- Compartment A Sample From Bottom Moisture Contamination BL BR /> Bulk Density BD w/antistat Viscosity RVCM J25 CA Bottom IX /*> .071 CB Bottom nxi .ns B Bottom .z>&3 Tappi Test Contamination Composite i Screen Analysis .06 or less % Mesh Weight % 40 <9. OO 0,0 60 80 7,4/ .07------------- . 15 20------------- .60 100 P.W7 120 JJtfo 140 200 Pan go %L Avg. Microns Color L: a % Glass ies: b /-</V Static Flow: /8J4- Techn ician: ftP VAB.0001201253 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: June 11, 1992 Customer: Intex Plastics Corp Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: June 8, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A Product: 5385 Railcar No. ACFX Order No.: 0011894-002 I PC Specification 0.90 - 0.95 8.5 PPM Max. 40 Total Analysis 0.93 0.111 Total Black + Brown Hard Particles @ 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 MESH % ON 15 Max. 2 15 Sec. Max. 10 .2 0.510 Min. 0. 580 0.30 Max. 0. 10 25.0 Thru 140 Mesh 5.0 Max on Pan Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 4.9 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. Bagwe Laboratory Supervisor (601) 369-3624 VAB.0001201254 Vista Polymers Highway 25 Aberdeen, MS 39730 A F VC RAILCAR ANALYSIS Load Date: Time Logged In: Ship Date :_J41 Product: Car No.: Logged In By: Sllo(e) . 22fajfl^]-L Order No: !(67^-002-- Customer Compartment Sample From Bottom Moisture % [Q r BL Contamination BR (? Bulk Density ^77 BD after Fluff Hard Particle 5 {p 7 JCo Viscosity te! RVCM m 40 Mesh/Glassies Bottom ip Sg'B _i_ ... /6b) Bottom ./> 3 S' f%>) Bottom M H & ,57o Screen Analysis Mesh 40 Weicht 6'0d % a-d 60 80 100 120 140 200 Pan 43'2.04 JO. aw JJl. ).& /s.2. a/.? as.r i i-H iS.S Drytime: Static Flow: Avg. Microns: I<f0, 2 Color L Jdo.9 a .IZ h // 77 Technician: VAB.0001201255 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALY S A Date: June 8, 1992 Customer: Intex Plastics Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: June 2, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A VIS1AProduct: 5415 Railcar No.: ACFX 41184 Order No.: 0011898-000 IPC Specification 1.00 - 1.04 8.5 PPM Max. 20 Total Max. Analysis 1.01 0.024 Total Black + Brown Hard Particles @ 7 mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2B ABR-1A ABR-3 5 Max. 1 15 Sec. Max. 9.2 0.460 Min. 0.516 0.30 Max. 0.24 25.0 Thru 140 Mesh Max. 5.0 On Pan Max. % ON Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 4.9 Amy ET. Bagwell Laboratory Supervisor/Lead (601) 369-3624 VAB.0001201256 A Vista Polymers Highway 25 Aberdeen, MS 39730 IP VC R A T LCAR ANALYST S Load Date:_ /- 9^ Product: Time Logged In: /2-'-0 Ship Date:_ (oh* Logged In By: Order No: ~od Car No.: *///&</ Silo(e) : Customer: 0<L* t&> TTtofnL-- Compartment A Sample From Bottom Top Moisture % 24 Contamination BL BR S' S Bulk Density .sis Hard Particle 5 7 / } fc Viscosity bolt RVCM <oiA' , CA Bottom Top . 2f S 4 sr/i CB Bottom Top B Bottom Top 6 .s/o A. <8 3f Z2 7z --, ----f- -.. .Sjfa Screen Analysis Mesh Weight % 40 D'& &0 60 /Of 22- 80 100 120 140 200 3! a 03- 41 Pan Drytiroe 4& Static Flow 6 / Avg. Microns Color L: a Qb f~ METS: tyl?Z> / f'Z-P1 x * Technician: VAB.0001201257 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIFICATE Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A Date: June 8, 1992 Customer: Intex Plastics Corp Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: June 2, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A VISIA Product: 5305 Railcar No.: VIPX 45850 Order No.: 0011897-000 I PC Specification Analysis 0.71 - 0.76 0.73 8.5 PPM Max 0.036 60 Total Total Black + Brown Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2A Moisture, % ABR-1A Particle Size Distribution ABR-3 15 Sec. Max. 10.5 0.510 Min. 0.525 0.30 Max. 0.16 30.0 Thru 140 Mesh 5.0 Max on Pan % ON Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E. BagweTl Laboratory Supervisor VAB.0001201258 Vista Polymers Highway 25 Aberdeen, MS 39730 A RAILCAH ANALYSIS Load Date: ~/2 ^^2^ Product: Car No.: Tine Logged In: Ship Date : 6 llh Logged In By: Order No: // *7 QOQ Silo(s) Customer c Compartment A Sample From Bottom Moisture BL Contamination CA Bottom tfeloAd Bottom Mr B Bottom Bulk Density BD w/antistat Viscosity RVCM Tappi Test Contamination Composite Screen Analysis Mesh Weight % 40 0.00 0,0 . 06 or less 60 80 o* SJ4 6./ /J.S .07-------------.15 .20------------- .60 100 11-41 2.2.x 120 l'c>l 39 f 140 /D.13 2/S' 200 SJ?I //.L Pan /33 3l-7 CPA: % Glassies: Avc. Microns: ts : l N Color L: MSS' a b Static Flow: Technician: Cp VAB.0001201259 Vista Polymers Highway 25 J. Aberdeenf MS 39730A Load Date : /2 ~2/b ~91 Product:) 5305 Car No. Time Logged I n: /$& 0 Logged In By: Ship Date: Silo(s) : Customer Contamination Syntron Method Wet Method ft Bulk Density BD w/antistat Viscosity RVCM Blown Film .S27 ,733 .061 17/1 11 .SZiT .121 .bo(<? 11 1 3A fa >jT/J 33d , Ol'Z- y9 .7% .DCF? Tappi Test Contamination Composite Screen Analysis Mesh Weight % *P 40 S> jO >> . 06 or less 60 &* D 0.D 80 f z. .07 - ----------.15 . 20 .60 100 SF3 120 /z.32 //S 140 200 /s- /ji$ 3 o.l Pan Static Flow: & //o-F % Glassies: ^Y *7 <y Avg. Microns: /ff.o Color L: 9f-J^ a O b /F5 CPA: Technician: VAB.0001201260 Viski Pofymen A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (6011 369*8111 CERT X LIGATE OF ANALYSIS A Date: June 8, 1992 Customer: Intex Plastics Corp Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: June 4, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination. BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A Product: 5385 Railcar No.: UTCX 48029 Order No.: 0011894-001 I PC Specification 0.90 - 0.95 8.5 PPM Max 40 Total 0.93 0.169 Total Black + Brown Hard Particles @ 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 15 Max. 2 15 Sec. Max. 8.9 0.510 Min. 0.576 0.30 Max. 0.12 25.0 Thru 140 Mesh 5.0 Max on Pan % ON Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 4.8 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. Bagwe Laboratory Supervi VAB.0001201261 Vista Polymers Highway 25 Aberdeen, MS 39730 A R cia t r,p a -p> AMAT . V T Q Load Date: Product -* Car No. : ?0 ^*9 Time Logged In: O.2J2..0 Logged In By: Silo(s): ^J>2~ Ship Date: kl Order Ho: OC> I ^5<?</~'0O/ _ZCustomer: no^-h#) Compartment A Sample From Bottom Moisture % ,/a BL Contamination BR cl /jL Bulk Density BD after Fluff , SFf Hard Particle 5 7 Viscosity A RVCM . 1 u[ 40 Mesh/Glassies CA Bottom , >n >S' .&7A CB Bottom , /0 </ /Z. i . B Bottom ,a? J *7 . ,.50 Screen Analysis Mesh Weight 40 Q-rz> O-o 60 aa-z o 80 f /3, F 100 i3.> g cL(*. *f- 120 i3.n 140 8.23 MHaWMPMMpAMM 200 Pan fc.S2T hi? <3, / 3-sr Drytime: Static Flow: O /M Avg. Microns: Color hi a O.IX b 11* Technician: i - a fi VAB.0001201262 p Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A RTIFICATE OF ANALYSIS Date: June 8. 1992 Customer: Intex Plastics Corp Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: June 2, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A Product: 5385 Railcar No.: PLCX 43278 Order No.: 0011894-000 I PC Specification 0.90 - 0.95 8.5 PPM Max 40 Total Analysis 0.93 0.040 Total Black + Brown Hard Particles @ 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 15 Max. 3 15 Sec. Max. 9.8 0.510 Min. 0.576 0.30 Max. 0.13 25.0 Thru 140 Mesh 5.0Max on Pan X ON Brabender Dry Time, Mins* ABR-7 6.0 Mins. Max. 4.8 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor VAB.0001201263 * Vista Polymers Highway 25 Aberdeen, MS 39730 Load Date: Time Logged In: Ship Date: RAXLCAR ANALYSTS Product Logged In By: liOrder No: Car No 527T Silo (e ) : y&*' jL !P<Ls AJ? 7 Compartment i Sample From A Bottom Moisture % BL Contamination BR ,u / Bulk Density BD after Fluff ,376 Hard Particle 5 7 // 3 Viscosity RVCM b 40 Mesh/Glassies Screen Analysis Mesh Weight % 40 0 00 O'Q 60 &U i0Q? CA Bottom r/3 3 O ,37* CB Bottom r ,377 1 : . i i . i B Bottom rS o -2. /2~ .S7<f 80 100 "7 ^3 /g./7 l . I 120 /J 33 L1 140 Till ig-JL 200 Pan t.*o Drytime: fig Static Flow: oL Avg. Microns l^-X- Color L: _9fV7J a 'OUl b h $) Technician: / P S I VAB.0001201264 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE O F* ANALYST k Date: June 2, 1992 Customer: Intex Plastics Corp. Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: May 29, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A VIS1AProduct: 5385 Railcar No.: VIPX 45908 Order No.: 0010549-006 I PC Specification 0.90 - 0.95 8.5 PPM Max 40 Total Analysis 0.93 0.136 Total Black + Brown Hard Particles @ 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 15 Max. 2 15 Sec. Max. 9.4 0.510 Min. 0.582 0.30 Max. 0.04 25.0 Thru 140 Mesh 5.0 Max on Pan % ON Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 4.7 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. Bagwell Laboratory Supervisor VAB.0001201265 Viata Polymers Highway 25 Aberdeen, MS 39730 h PVC HAILCAR ANALYSI3 Load Date: S-Q&'fO- Product: Car No.: Time Logged In: /*?&& Ship Date:. Logged In By: Q? Order No:. Ib'o'tf-0o Silo(e) -.67<*-&77-rPK IftL Cubtomer: Compartment A Sample From Bottom Moisture % *of BL Contamination BR f2~ Bulk Density S7<f BD after Fluff Hard Particle 5 7 1 Viscosity ft : RVCM 1% 40 Mesh/Glassies -------- CA Bottom / 2- & CB Bottom o'f w fo 7 S'S"*- B Bottom . >22 /O '8 , Screen Analysis Mesh Weight %P 40 0O 00 60 3<f 7 80 If,2$ jZ2v 120 //-? 140 6>-3? .J2^1 200 Pan A3 2.<- Drytime: Static Flow: Color L: /00-Z2- a O'O^ b Technician sri.T AM VAB.0001201266 mm Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 O ERTIFICATE OF ANALYSIS h Date: June 2, 1992 Customer: Intex Plastics Corinth Division Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: May 27, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A VIS1AProduct: 5415 Railcar No.: UTCX 46497 Order No.: 0010547-*-003 IPC Specification 1.00 1.04 8.5 PPM Max. 20 Total Max* Analysis 1.01 0.000 Total Black + Brown Hard Particles % 7 mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2B ABR-1A ABR-3 5 Max. 1 15 Sec. Max. 9.2 0.460 Min 0.508 0.30 Max. 0.14 25.0 Thru 140 Mesh Max. 5.0 On Pan Max. % ON Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 4.9 Amy E< Bagwe Laboratory Supervisor/Lead (601) 369-3624 VAB.0001201267 Vista Polviners Highway 25 Aberdeen, MS 39730 PVC R AILG AR ANALYSIS Load Date: Time Logged I n ,/M. Ship Date Product: Car No. Logged In By: Silo(s) : '*fo Order No: lo^H 7-ooS Customer: I /* Compartment A Sample From Bottom Top Moisture % BL Contamination BR /3 (? Bulk Density 5 Hard Particle 7 ( ^ Viscosity /. oi 4- RVCM mo CA Bottom Top 73 * -S^>7 - ------------------------------- CB Bottom Top B Bottom Top . f^ 7 ? J5Y2- ---------------f------------------------ ------?T-------- -So f l i \ J Screen Analysis Mesh Weight % 40 ,<s> OP 60 80 100 120 140 200 Pan l- fo g1-^ -7-87- J2.X/ -2-fe 'lo 27 Drytime: Static Flow: ^ Avg. Microns: Color L: /DO. P/ 2- b / 22- Technician METS /?; <s/ z M-Q % VAB.0001201268 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: May 28, 1992 Customer: Intex Plastics Corp Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: May 27, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A 53,1 VISTAProduct: Railcar No.: PLWX 44668 Order No.: 0010549-005 I PC Specification 0.90 - 0.95 8.5 PPM Max. 40 Total Analysis 0.94 0.077 Total Black + Brown Hard Particles @ 7 Mins. ABR-12 Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2A Moisture, % ABR-1A Particle Size Distribution ABR-3 15 Max. 3 15 Sec. Max. 9.4 0.510 Min. 0.581 0.30 Max. 0.17 25.0 Thru 140 Mesh 5.0 Max on Pan % ON Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 4.8 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor VAB.0001201269 Vista Polymers Highway 25 Aberdeen, MS 39790 A PVC HAILCAH ANALYST3 Load Date: Time Logged In: Ship Date: Product: Logged In By: Order No: /"C>6^~ Car No. : Silo(s) : ?&-- ? ?-4ST~ Customer: pc. ^ Compartment A Sample From Moisture % Bottom off BL Contamination BR /o Bulk Density ,&v(* BD after Fluff Hard Particle 5 7 Viscosity RVCM Ml? .mi 40 Mesh/Glassies _________________________________________________________________________________ Screen Analysis Mesh Weight % 40 ^^ e- 60 0. (S' 03 CA Bottom fjL 3 3 CB 1 Bottom /T 7 3 S33l B Bottom .17 5" 9 ,s% - 1 80 7.68 100 m3 120 IZIt 140 /ST 2- 0 200 JT? 11.8 Pan Drytime: _ *3 Static Flow: ^m m-i Avg. Microns: Color L: a^ b /-^/ Technician: VAB.0001201270 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 A Phone (601) 369-8111 CERTXFIOAT OF ANALYSIS Date: May 19, 1992 Customer: Intex Plastics Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: May 15, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A VISIAProduct: 5415 Railcar No.: UTCX 46406 Order No.: 0010547-002 IPC Specification 1.00 - 1.04 8.5 PPM Max. 20 Total Max. Analysis 1.00 0.017 Total Black + Brown Hard Particles 7 mins Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2B ABR-1A ABR-3 5 Max. 2 15 Sec. Max. 8.2 0.460 Min. 0.30 Max. 0.515 0.21 25.0 Thru 140 Mesh Max 5.0On Pan Max. % ON Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 5.0 Amy E. BagWeal Laboratory Supervisor/Lead (601) 369-3624 ******* Hi VAB.0001201271 Vista Polymers Highway 25 Aberdeen, MS 39730 Load Date: 5T- n. Time Logged In: Ship Date:. RAILCAR ANALYSIS Product: Logged In By: Order No: Car No.: /n Silo(s): ^>90^69/ /PL. Custo ner: r wiefrfL- Compartment A Sample From Bottom Top Moi6ture % !& Contamination BL BR X Bulk Density .s/ Hard Particle 5 7 > f- Viscosity RVCM .m .on CA Bottom Top 3 .m 3 CB Bottom Top .2/ 3 / .S7& <6 B Bottom Top V! <2 X 6/^- Screen Analysis Mesh Weight % 40 O. &? 0 60 80 100 120 140 200 (^1 <^/ ^7 js_ Drytime: Static Flow: & /Om^ Avg. Microns: Color L: /e/ gg- *^ b METS: ^ZQ/ 114.P % Technician VAB.0001201272 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OE ANTAL,YS I A Date: May 19, 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: May 15, 1992 Property Inherent Viscosity Residual VCM, ppm Contamination, BLK + BRN Test Method ABR-10 ABGC-26 ABR-5A visiaProduct: 5385 Railcar No.: UTCX 46413 Order No.: 0010549-004 I PC Specification 0.90 - 0.95 8.5 PPM Max. 40 Total Analysis 0.93 0.144 Total Black + Brown Hard Particles G 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 15 Max. 3 15 Sec. Max. 7. 9 0.510 Min. 0. 581 0.30 Max. 0. 12 25.0 Thru 140 Mesh 5.0 Max on Pan % ON Brabender Dry Time, Mins. ABR-7 6.0 Mins. Max. 4.9 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E i' Bagwel Laboratory Supervisor VAB.0001201273 * < Vista Polymers Highway 25 Aberdeen, MS 39730 RAILCAR ANALYSIS Load Date: Time Logged In : (60 Ship Date: I Product: Logged In By: Order No: Car No.: Silo(s): .muCustomer k /*> /h Compartment A Sample From Bottom Moisture % BL Contamination ___ BR ./z 2. Bulk Density /ST/ * BD after Fluff Hard Particle 5 7 If 3huS Viscosity RVCM ./<Af 40 Mesh/Glassies CA Bottom ,/0 . SS3 CB Bottom o o .^)9 r B Bottom Vr - Cr Screen Analysis Mesh Weight 40 t* 0*0 Drytime: 60 80 100 120 140 200 11.7? ll.sl* * 3.70 f.o 31.3 22.7 JILT... 7. s: / Static Flow: 7 9O / Avg. Microns: Color L: l' 13 Pan . fl /.? ltS.5 Technician: VAB.0001201274 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A Date: May 19, 1992 Customer: Intex Plastics Corp Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: May 15, 1992 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination, BLK + BRN ABR-5A VISIA Product: 5305 Railcar No.: UTCX 46403 Order No.: 0010531-002 I PC Specification Analysis 0.71 - 0.76 8.5 PPM Max. 0.72 0.112 60 Total Total Black + Brown Dry Flow, Seconds ABR-8 Bulk Density, gm/cc Moisture, % ABR-- 2A ABR-1A Particle Size Distribution ABR-3 15 Sec. Max. 8.4 0.510 Min. 0.531 0.30 Max. 0.08 30.0 Thru 140 Mesh 5.0Max on Pan % ON Polyvinyl Chloride, Virgin Resin, Not Reprocessed lumirt KJO^JUJ Amy EK Bagwexl Laboratory Supervisor (601) 369-3624 VAB.0001201275 Vista Polymers Highway 25 A Aberdeen, MS 39730 Load Date Time Logged In: h Ship Date RAILCAR, ANALYSIS Product: Logged In By Order No: Car No Silo ( s ) : Ce/?S. / Customer = lAjjjAl DkUy M* Compartment A Sample From Bottom Moisture .OS Contamination BL BR 3 Bulk Density BD w/antistat .3/ Viscosity RVCM to 4 CA Bottom ,<P /S' 723 // { CB Bottom ,0 JL .Sl(r 7^/ .d4z B Bottom ,<o7 ./// Tappi Test Contamination Composite Screen Analysis Mesh Weight % 40 0*00 0*0 06 or less .07 . 15 .20 .60 60 . o% 80 3.is1 100 loyz 20-<? 120 /S CS ^// 140 II. 3.3.JP 200 ksi S3.2. Pan im Avg. Microns: 163.7 % Glassies: Color L: Pft^ a M7 b /*6o Static Flow: O Techn ician: jp ^<dcsJL VAB.0001201276 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OE AlsTA SIS h Date: May 13, 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth) MS 38834 Attention: Quality Control Manager Ship Date: May 12, 1992 VISIAProduct: 5385 Railcar No.; PLWX 44726 Order No.: 0010549-003 Property Inherent Viscosity Residual VCM, ppm Contamination Test Method ABR-10 ABGC-26 ABR-5A Analysis 0.93 0.119 Total Black + Brown Hard Particles % 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 00 m CO 4 0.578 0.13 % ON Brabender Dry Time, Mins. ABR-7 5.0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. H.D. Lucas Laboratory Supervisor (601) 369-3624 VAB.0001201277 * Vista Polymers Highway 26 Aberdeen, MS 39730 h F*A I LCAR ANALYSIS PLOJtf : ALoad Date Time Logged In: /S'E> Ship Date: Product Logged In By: Order No: <09/ Car No. : C mx Silo(e) ; Li7.gr -*>3 : Uctoq Customer >p Compartment Sample From A CA --------------------------------------------------------------------.------------- - ' Bottom ' Bottom Moisture % BL Contamination BF ./j Bulk Density BD after ......................... Fluff . SU Hard Particle 5 7 /(. Viscosity Ml RVCM .//*? 40 Me6h/Glassies .IZ 7 .s* - CB Bottom // b 7 B Bottom ./0 & k . sra Screen Analysis Mesh Weight % 40 0,6 0 0,0 60 J./O 80 /r.ji JO.7 100 n.u 120 //.* 140 s-.fo /o.X 200 3XO *7, o Pan .is 2,o Drytime: Static Flow: 0 fM/ Avji. Microns: n/x Color L 27_ a ... b /. n Technician Wd4- ti ft VAB.0001201278 Vista Polymers I A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A RTIFICAT OF ANALYSIS Date: May 13, 1992 Customer: Intex Plastics Corp Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: May 11, 1992 VIS1AProduct: 5385 Railcar No Order No UTCX 46464 0010549-002 Property Inherent Viscosity Residual VCM, ppm Contamination Test Method ABR-10 ABGC-26 ABR-5A Analysis 0.93 0.057 Total Black + Brown Hard Particles 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 6 8.9 0.583 0.02 % ON Brabender Dry Time, Mins. ABR-7 4.9 Polyvinyl Chloride, Virgin Resin, Not Reprocessed H.D. Lucas Laboratory Supervisor (601) 369-3624 VAB.0001201279 Vista Polymers Highway 25 Aberdeen, MS 39730 A T'VC RAILCAR ANALYSTS OLTQC Load Date: Time Logged In: 24*0 Ship Date: Product: Car No . Logged In By: A)& Silo(e) C?7j LfS Order No: &0/&S49-&>_ Customer: ^7^ Screen Analysis Mesh Weight % 40 >Q iP.O 60 3f <M. 80 /7.fcQ 0>5.Z, 100 'iS' (=> 120 140 200 2. %(c> Si Pan Drytime: 4^ Static Flow: ^ / %'^f Avg. Microns: / 73*7 Color L: /so- ?</ a <9'f( b Z_Z Technician: /usr~<Ptar VAB.0001201280 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 * CERTIFICATE Date: May 11, 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: May 8, 1992 ANALYSXS VISIA Product: 5305 Railcar No.: GACX 73409 Order No.: 0010531-001 Property Inherent Viscosity Residual VCM, ppm Test Method ABR-10 ABGC-2 6 Analysis 0.72 0.051 Contamination ABR-5A Total Black + Brown Dry Flow, Seconds ABR-8 Bulk Density, gm/cc Moisture, % ABR-2A ABR-1A Particle Size Distribution ABR-3 9.2 0.533 0.13 % ON Polyvinyl Chloride, Virgin Resin, Not Reprocessed H.D. Lucas Laboratory Supervisor (601) 369-3624 mmmm VAB.0001201281 Vista Polymers Highway 25 Aberdeen, MS 39730 Load Date:_ Time Logged Ship Date: * Product: Car Logged In By: Order No: > >/63 t-oo/ _ Silo( Customer: Mesh Weight % 40 0 *-/ 60 6-O/Q 0,,o 80 3/o i.i 100 It.l Avg . Microns: Z2.7.7 Color L: ft `3 a .13 b 120 zt.c 140 ix. 200 9, ft.o % Glassies: <:/ Pan 33 fj Static Flow: 0 /.t.r Technician: ____MX*-rf?- VAB.0001201282 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 * CERT X Date: May 11, 1992 Customer: Intex Plastics Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: May 8, 1992 Product: 5415 Railcar No.: VIPX 45735 Order No.: 0010547-001 Property Test Method Inherent Viscosity ABR--10 Residual VCM, ppm ABGC-26 Contamination ABR-5A Total Black + Brown Hard Particles % 7 mins. ABR-12 Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2B Moisture, % ABR-1A Particle Size Distribution ABR-3 Analysis 1.02 0.020 11.8 0.507 0.13 % ON Brabender Dry Time, Mins ABR-7 5.0 H.D. Lucas Laboratory Supervisor/Lead (601) 369-3624 / VAB.0001201283 / / r i- Vista Polymers Highway 25 Aberdeen, MS 39730 r Load Date: Time Logged Ship Date: I? V C RAX L.C AR ANALYST S im Product: ^S73S~ Car No.: DC, <K7 Logged In By: Co Silo( s ) : *>0-61/ //dm;OQ(a&7~)G/Order No: Customer: Compartment A Sample From Bottom Moisture % Contamination BL BR JZ 3 Top J2 Bulk Density , So $ Hard Particle 5 7 3 .! XT Viscosity /02o RVCM _- . .- .020 ' 1 CA Bottom Top .a 2 9 .Sol / 7 CB Bottom Top ./-* 3 B Bottom Top ,O? 2 L Screen Analysis Mesh Weight % 40 {?*#/? i 60 0*^1 Ao 80 it* XJ 33./ 100 tsJ? 3/3 120 9./9 Af.4 140 U- 200 233 Pan O.JPo /^ Dry time: <*>*0 Static Flow: 0 ///.% Avg. Microns: Color L: 2S* a 0*0 7 b / METS: 4" / / ^4-1 % Technician: Co <P VAB.0001201284 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Adendeen, Mississippi 39730-0091 Phone (601) 369-8111 CERT I FT OATH! OF Xr j jl td -,-4u- Date: May 8, 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: May 5, 1992 vm Product: 5385 Railcar No.: PLWX 44265 Order No.: 0010549-001 Property Inherent Viscosity Residual VCM, ppm Contamination Test Method ABR-10 ABGC-26 ABR-5A Analysis 0.93 0.026 Total Black + Brown Hard Particles @ 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-- 2A ABR-1A ABR-3 2 7.7 0.573 0.08 % ON Brabender Dry Time, Mins. ABR-7 5.0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed H.D. Lucas Laboratory Supervisor VAB.0001201285 Vista PolymerB Highway 25 Aberdeen, MS 39730 E*A I LCAR ANALYSIS ?loj)( Load Date Time Logged Ship Date:_^ Product: Logged In By: Order No: Compartment Sample From Bot Moisture % BL Contamination BR 63 * _5 Bulk Density BD after Fluff ,s~7/ Hard Particle 5 7 Viscosity RVCM 92U> 40 Mesh/Glassies Bottom ~ 0 (t? I 7 . Car No. Silo(6) : / Customer: i W7 Bottom W Bottom &7 43 ,'12- Screen Analysis Mesh 40 Weight % fl,&Q 0.0 60 2S4) 80 /2~0o Z.0 100 M.S! ZJ.O 120 i.si u.4 140 L.^0 IS. 9 200 i-io Drytime: StO Static Flow: jJ~Z0 Avg. Microns: - Color L: /0*~6/ a b Ate Pan 2.Ji Technician: /*M* trs VAB.0001201286 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 CERTIFICATE OF ANALYSX S ^ Date: May 6, 1992 Customer: Intex Plastics Corp Corinth Div. Golding Drive Corinth. MS 38834 Attention: Quality Control Manager Ship Date: May 4, 1992 Product: 5385 Railcar No.: VIPX 45750 Order No.: 0010549-000 Property Inherent Viscosity Residual VCM, ppm Contamination Test Method ABR-10 ABGC-26 ABR-5A Analysis 0.92 0.048 Total Black + Brown Hard Particles @ 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 3 8. 5 0. 591 0. 15 % ON Brabender Dry Time, Mins. ABR-7 5.0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed Laboratory Supervisor (601) 369-3624 VAB.0001201287 i iu Vista Polymers Highway 25 Aberdeen, MS 39730 Load Date: Time Logged In: Ship Date: <k_ 92- Product: Car No. : *4 % 7 & & Logged In By: Co Silo(6): : Order No IQ&fa 6CO Customer: frio TTlettl____ Compartment A Sample From Bottom Moisture % 07 Contamination 'Bulk Density BL 4 BR 1 /o .53? BD after Fluff Hard Particle 5 7 Viscosity RVCM . 40 Mesh/Glassies CA Bottom 13 Z 7 .sn CB Bottom fc /5T (x? 5 SfeL B Bottom IS* .S9S ' i Screen Analysis Mesh 40 Weight % &-0 60 6.8 80 100 120 140 12ZL 2Jk6: gX/7_ !2<0 200 6.38 !*.l Pan Drytime: Static Flow: ^ Color L: /^- a ^#7 b Avg. Microns: Technician: nMMHMMWHIMMM m VAB.0001201288 M*< Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A Date: May 6, 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: May 1, 1992 VISIA Product: 5305 Railcar No.: VIPX 45833 Order No.: 0010531-000 Property Inherent Viscosity Residual VCM, ppm Test Method ABR-10 ABGC-26 Analysis 0.72 0.077 Contamination ABR-5A Total Black + Brown Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2A Moisture, % ABR-1A Particle Size Distribution ABR-3 9.2 0.516 0.13 % ON Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E.^Bagwell Laboratory Supervisor (601) 369-3624 VAB.0001201289 \* ' Vista Polymers Highway 25 Aberdeen, MS 39730 A Ft A X LCAR ANALYS X S Load Date: Time Logged In: 0/00 Product: Logged In By: Ship Date Order No : i Car No.: Silofs \ :&7-H>88 Customer: _J /T- Compartment A Sample From Bottom Moisture Contamination BL BR Bulk Density BD w/antistat .n jr u .c ic Viscosity .753 RVCM ,017 CA Bottom _y /A .753. CB Bottom 3 .s'/2nA on B Bottom - /0 /O .s/g .123 -on Tappi Test Contamination Composite Screen Analysis Mesh 40 Weight % .06 or less .07-------------.15 ________________________ 60 80 100 120 .20------------- .60 140 200 Pan Avg. Microns: Color L: ?9- *2 a ^2 b /* % Glassies: </ p Static Flow: Technician: VAB.0001201290 Jljn s<, Vista Polymers Highway 25 Aberdeen, MS ANALYST S OKKORADK Load Date : 92- Time Logged In: 0/& <? Product: Logged In By: Ship Date: Order No: Car No.: Silo(6): Customer: COMPARTMENT A Moisture % Contamination / Bulk Density Color "L" Color "a" Color *'b" Static Flow / Viscosity Top RVCM ysis io'ffcC, Mesh Weight 40 Ct<XyO % 60 .Ole 0<t CA CB // B / // / Toe Balia* Top Balia* Top Balia* 80 /o-c 100 120 /i.o>r i^.iS AC-/ 32-3 140 200 H.so Pan l.ro 3.o Weight % A. 0 0 0*0 . 0 Z0* O S~.fi ft. A 12.71 /r.^9 3/o A tf.x /.S'/ Weight % 0-0 0' / /8.A l&<2? M.io 3m Ar2.< L>. ZU 13.1 3.17 & 1/4 Weight 0. 00 i.72 % 0.0 0.0 U.'/ Technician: #A- A?.ir A<*. ? tf.U S9 4 1.11 n.i, 4ns 9<5~ i.it VAB.0001201291 mrnmrnmmm Vista Polymers A Division of Vista Chemical Company 0 Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: May 6, 1992 Customer: Intex Plastics Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: May 1, 1992 Product: 5415 Railcar No.: VIPX 45720 Order No.: 0010547-000 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination ABR-5A Total Black + Brown Hard Particles 7 mins. ABR-12 Dry Flow, Seconds ABR-8 Bulk Density, gm/cc Moisture, % ABR-2B ABR-1A Particle Size Distribution ABR-3 1.02 0.032 8.8 0.501 0.11 % ON Brabender Dry Time, Mins ABR-7 4.7 Amy ET Bagwe1 Laboratory Supervisor/Lead (601) 369-3624 VAB.0001201292 Vista Polymers Highway 25 Aberdeen, MS 39730 RAILCAR ANALYSIS Load Date: Time Logged Ship Date: l: /fee *s\\ Product: Car No.: Logged In By: J05O1 noi> Customer ft/ & Compartment A Sample From Bottom Top Moisture % * Contamination BL BR if Bulk Density Hard Particle 5 7 Viscosity % bc.l. RVCM CA Bottom Top CB Bottom Top o? c? 8 S' / B Bottom Top L So I e Screen Analysis Mesh Weight %r 40 0.0 >jO 60 ,S2 /, 2- 80 37'% 100 JtM- 3*-j 120 / >'S 140 (s' (*> 200 >2- od> Pan 70 SL -M& Drytime: ^7 Static Flow: (0 / $*% Avg. Microns: /*7\ *f Color L: /QO.S& a ^~ ^ b /* 9^S METS: 9051, 17,1.6, % Technician: VAB.0001201293 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: May 6, 1992 Customer: Intex Plastics Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: April 30, 1992 Product: 5415 Railcar No.: VIPX 45783 Order No.: 0010058-002 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination ABR-5A Total Black + Brown Hard Particles 7 mins. ABR-12 Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2B Moisture, X ABR-1A Particle Size Distribution ABR-3 Analysis 1.02 0.030 1 11.5 0.503 0.18 X ON Brabender Dry Time, Mins ABR-7 5.0 Amy EBagwe 1 Laboratory Supervisor/Lead (601) 369-3624 VAB.0001201294 s * Vista Polymers Highway 25 Aberdeen, MS 39730 RVC RAILCAR ANALYSIS Load Date *-27- 92- Time Ship Logged Date: In: Zi?** if 1^0 Product: Car No.: *r?f3 Logged In By: /* Silo(s): if/ I OOfSZ" OCO- P<L; No Compartment A Sample From Bottom Top Moisture % BL Contamination BR 'IS /21 CA Bottom Top 17 Bulk Density Hard Particle 5 7 Viscosity RVCM m. ! htPt" .D#b .020 1 Screen Analysis Mesh Weight % 40 & e>G 0.0 60 <9.6?) ).p~ 80 19M tfOjQ 100 yo.t CB Bottom Top .17 3 6? B Bottom Top 3 4> 120 &oih 140 3jfij 70 200 3>H Pan Q-7/ JJL Drytime: Static Flow: Oz Avg. Microns: 172.*+- Color L: !(.*/ Om b METS: Technician Xxtati-pi*' / MS ' Ck VAB.0001201295 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A Date: May 1, 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: April 29, 1992 Product: 5305 Railcar No.: UTCX 46474 Order No.: 0010423-000 Property Inherent Viscosity Residual VCM, ppm Test Method ABR-10 ABGC-26 Analysis 0.72 0.000 Contamination ABR-5A Total Black + Brown Dry Flow, Seconds ABR-8 Bulk Density, gm/cc Moisture, % ABR-2A ABR-1A Particle Size Distribution ABR-3 8.8 0.530 0.06 % ON Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy EL7 Bagwe Laboratory Supervisor (601) 369-3624 VAB.0001201296 t Vista Polymers t Highway 25 Aberdeen, MS 39730 A flM Ft A X LCAR ANALYSIS Load Date: <A /A 2_ Product: Car No.: Time Logged In : & C? O & Logged In By: /W :_4[Z2 Ship Date : l0^Z3'6OO Order No Silo(s): Customer yy" -6#!? /9f Compartment A Sample From Bottom Moisture Contamination BL BR O& Bulk Density BD w/antistat ZS Viscosity RVCM m. CA Bottom O 5 in CB Bottom <9 f 7 zX JUS B Bottom 7 mu Tappi Test Contamination Composite Screen Analysis Mesh Weight %r 40 ao OO 06 or less z 60 80 1.3 .07 .15 .20 100 212 120 2H 140 //3J 200 n.o . 60 Pan Avg. Microns: / 33 % Glassies: f 7j Color L: a 0-2(, b /r C& Static Flow: O / %'P Technician: t'H tT <P jLH VAB.0001201297 Vista Polymers Highway 25 Aberdeen, MS 39730 Load Date:_______ Time Logged In Ship Date: Ft A X LCAR JK IsTA -4 YS X S Product: Logged In By Order No: Car No.: ___ Silo(s):________ Customer:______________ % 0 o0 0-1 Z7 22.0 2>!, o 22./ M3 Avg. Microns: % Glassies Color L: ab Static Flow: / Techn lcian: \ -- VAB.0001201298 Vista Polymers Highway 25 Aberdeen, MS 39730 RAILCAR ANALYSIS Time Logged In: Ship Date: Products--MBOX-- Logged In By: Order No: Car No.: Silo(s): Customer: COMPARTMENT Moisture % Contamination Bulk Density Color "LM Color "a < Color "b" Static Flow Viscosity RVCM Screen Analysis Mesh 40 60 80 100 120 140 200 Pan Weight % > 37/7 src= f0 l Weight % 6 36J3 JST Weight % 0 7-8 37.8 13 Weight % *)/ 3&> Z.CJ7 Its 8 ML Technician: VAB.0001201299 Vista Polymers A Division of Vista Chemical Company CERT I Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 O AT OF ANALYSX S Date: May 1, 1992 Customer: Intex Plastics Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: April 28, 1992 VISIA Product: 5415 Railcar No.: ACFX 41166 Order No.: 0010058-001 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination ABR-5A Total Black + Brown Hard Particles @ 7 mins. ABR-12 Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2B Moisture, % ABR-1A Particle Size Distribution ABR-3 Analysis 1.01 0.025 8.8 0.521 0.25 X ON Brabender Dry Time, Mins ABR-7 4.7 Laboratory Supervisor/Lead (601) 369-3624 VAB.0001201300 A Vista Polymers Highway 25 Aberdeen, MS 39730 RAILCAR ANALYSIS Load Date: Product: Car No 4//L C> Time Logged In:. /&oo Logged In By: Silo(s) : b 9& Ship Date: Order No ) 0&D%~CO I Customer : lPlL. 9/ tlointt* Compartment A Sample From Bottom Top Moisture % BL Contamination BR Bulk Density 7 3 5 Hard Particle CA Bottom Top 3 Z S3-& CB Bottom Top <23 4 3 B Bottom Top .2/ 3 Viscosity RVCM Lom Screen Analysis Mesh Weight % 40 J>D n/>0 60 A/S 2-3 80 22/( 100 120 H. 140 ss? 200 34Q 6*0 Pan 2*/ Drytime: zStatic Flow: A) At Avg. Microns: 17^~ Color L: M 21 0_Oj~ b METS: %C0 Z % Technician: VAB.0001201301 /* tX Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601J 369-8111 CERTIFICATE OF ANALYSIS A Date: May 1, 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: April 28, 1992 Product: 5305 Railcar No.: GACX 73412 Order No.: 0009579-002 Property Inherent Viscosity Residual VCM, ppm Test Method ABR-10 ABGC-26 Analysis 0.72 0.145 Contamination ABR-5A Total Black + Brown 1 A 1 CA 1 CB |Bj 11 10 1 10 | 10 I 10 I Dry Flow, Seconds Bulk Density, gm/cc Moisture, % ABR-8 ABR-2A ABR-1A 9.3 0.530 0.12 Particle Size Distribution ABR-3 % ON 1 40 1 60 I 80 I 1001[ 1201 1401 2001 PAN 1 lo.ool O.ll 5.7116.91I29.0l26.2li7.6l 4.5| Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Laboratory Supervisor (601) 369-3624 if 1: VAB.0001201302 Vista Polymers Highway 25 Aberdeen, MS 39730 A RAILCAR ANALYSIS it mf4- 2-Load Date: Time Logged In : /4* Ship Date : Product: 5305 Car No.: 7jy/2- Logged In By: Order No: *0 Silo(s): .mlCustomer A/* Tlfetnl-- Compartment Sample From A l Bottom Moisture .IZL Contamination BL BR ~7 3 Bulk Density BD w/antistat Viscosity RVCM .mo ./4b" CA Bottom .0(0 S S 1 1 1 .72?f CB Bottom of * b J-si -/4Z. B Bottom jS 3 7 .nub .C&4 Tappi Test Contamination Composite Screen Analysis Mesh Weight % 40 a a# 0. o 06 or less 9/* .07 60 a of' A/ 80 100 P-S S.Y7 {<~?i .15 .20 120 140 /`fr-5'8 /3. 200 .60 Pan :Avg. Microns l&fr .97Color L: a 4* b UQ>7 % Glassies: <l*7& Static Flow:. a/ Technician: t .0001201303 V Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 A Date: May 1, 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth) MS 38834 Attention: Quality Control Manager Ship Date: April 29, 1992 VIS1AProduct: 5385 Railcar No.: UTCX 46491 Order No.: 0010424-000 Property Inherent Viscosity Residual VCM, ppm Contamination Test Method ABR-10 ABGC-26 ABR-5A Analysis 0.93 0.064 Total Black + Brown Hard Particles @ 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-- 2A ABR-1A ABR-3 4 11.7 0.565 0.12 % ON Brabender Dry Time, Mins. ABR-7 4.8 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E/ BagweXT Laboratory Supervisor (601) 369-3624 VAB.0001201304 Vista Polymers Highway 25 Aberdeen. MS 39730 A Load Date: Time Logged In: / Ship Date RAILCAR ANALYSIS Product: Car No.: Logged In By: Sllo(s) : tp7C?H</77 Order No: l O^S^cnso omer: iP(^ aSD Compartment Sample From Bottom Moisture % .V BL Contamination BR t* Bulk Density *SV7 BD after Fluff Hard Particle 5 7 /$ Viscosity RVCM 40 Mesh/Glassies /6aJ) Bottom Of /& /o Si ^ CB Bottom ,7*Z~ 8 B Bottom , 1 'L . 1 Screen Analysis Mesh 40 Weight %r 60 2. & 80 Mo 100 /3-7b 2 7.^, 120 /0-2-1 JLJ.O 140 S.b </ /A? 200 ^-O a S-o Pan /, dS 2/ Drytime: 2 Static Flow: & / //r 7 Avg. Microns Color L: /a b /-63 / Technician J+ VAB.0001201305 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aderdeen, Mississippi 39730-0091 Phone (601) 369-8111 Date: April 27, 1992 Customer: Intex Plastics Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: April 24, 1992 Product: 5415 Railcar No.: ACFX 53666 Order No.: 0010058-000 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination ABR-5A Total Black + Brown Hard Particles @ 7 mins. ABR-12 Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2B Moisture, % ABR-1A Particle Size Distribution ABR-3 Analysis 1.01 0.024 10.2 0.516 0.18 X ON Brabender Dry Time, Mins. ABR-7 5.0 to Amy E. Bafewell__/ Laboratory Supervisor/Lead (601) 369-3624 VAB.0001201306 Vista Polymers Highway 25 Aberdeen. MS 39730 RAILCAR ANALYSIS Load Date: Time Logged In: 00^3^0 Ship Date: Product: Logged In By: Order No: t Car No. Silo(s) : `"OQO Customer Compartment A Sample From Bottom Top Moisture % .13 BL Contamination BR 2 2, Bulk Density 5 3 Hard Particle 5 7 CA Bottom Top JO 37 2- CB Bottom Top ll 2 J ./n 3 B Bottom Top I .JL (r 3 Screen Analysis Mesh 40 Weight % 0,0 60 80 2.X qt 100 13.(0 120 C.37 12L 140 7.12 S.</ Drytime: ,o Static Flow: 0 /Avg. 200 /.?r 3.9 Pan .12. IM HU Color L: METS ab 9*fc7, tSL^x Technician: VAB.0001201307 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 CERTIRIGAT R OR Aberdeen, Mississippi 39730 Phone (601) 369-8111 ANALYSIS Date: April 23, 1992 Customer: Intex Plastics Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: April 21, 1992 VISIAProduct: Rai1 car No.: UTCX 46483 Order No.: 0009577-001 Property Test Method Inherent Viscosity ABR-10 Residual VCM, ppm ABGC-26 Contamination ABR-5A Total Black + Brown Hard Particles 7 mins. ABR-12 Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2B Moisture, % ABR-1A Particle Size Distribution ABR-3 Analysis 1 .00 0.017 1 11.7 0.514 0.14 % ON Brabender Dry Time, Mins. ABR-7 4.9 Amy E. Bagwe Laboratory Supervisor/Lead (601) 369-3624 VAB.0001201308 Vista Polymers Highway 25 A Aberdeen, MS 39730 Load Date: Time Logged In -Jhd Ship Date RAILCAR ANALYSIS Product: Logged In By: Order No Car No. Silofsh if*. Hi Customer ltCs Screen Analysis Mesh Weight % 40 q,qd 0.0 Drytime: 60 1.03 7,\ 80 100 3/.7/ 13, (C ^3S OJm.3 120 1.33 13L% 140 ML 6.7 200 Pan 3,33 _ . &r MJ-_ JJL /ILLStatic Flow: o UJL Avg. Microns: Color L: 1 OP- % .o b Ml METS: / iTsD.bx Technician: VAB.0001201309 Vista Polymers A Division of Vista Chemical Company Crdz". ii--x> Highway 25 Post Office Bax 91 I R I CA Aberdeen, Mississippi 39730 Phone (601) 369-8111 AM A L_ YS X S Date April 23, 1992 Customer: Intex Plastics Corp Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: April 21, 1992 Product: 5385 Railcar No.: UTCX 46553 Order No.: 0009578-003 Property Inherent Viscosity Residual VCM, ppm Contamination Test Method ABR-10 ABGC-26 ABR-5A Analysis 0.92 0.080 Total Black + Brown Hard Particles 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 % ON 2 9.4 0.581 0.15 2001 PAN 4.9 1.6 Brabender Dry Time, Mins. ABR-7 5.0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy E. B agwe Laborato ry Supervisor (601 ) 369-3624 VAB.0001201310 Vista Polymers Highway 25 A Aberdeen, MS 39730 rvc railcar analysis Load Date: 7^ Product: Time Logged In: Ship Date: 4tu Logged In By: Order No: 9$7% -cos Car No.: S ilo ( b ): Customer u* w*** t Screen Analysis Mesh Weight % 40 O. 0.0 Drytime: 60 fz3 80 If*7 100 120 73& 140 sn rp Co 200 Static Flow: l 9.<h Avg. Microns Color L : / a_ __-_o__p_(a ,b Pan 430 it* : Af&ftfrTechnician VAB.0001201311 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi Phone (601) 369-8111 a Date: April 23, 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: April 20, 1992 Product: Railcar No.: UTCX 46422 Order No.: 0009579-001 Property Inherent Viscosity Residual VCM, ppm Test Method ABR-10 ABGC-26 Analvsis 0.72 0.055 Contamination ABR-5A Total Black + Brown Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2A Moisture, % ABR-1A Particle Size Distribution ABR-3 A CA 11 CB 1 B 86 11 12 11 12 1 13 9.4 0.530 0.18 % ON Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E. Bagwell__J Laboratory Supervisor (601) 369-3624 VAB.0001201312 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 Date: April 20, 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: April 16, 1992 Product: 5385 Railcar No.: GACX 73389 Order No.: 0009578-002 Property Inherent Viscosity Residual VCM, ppm Contamination Test Method ABR-10 ABGC-26 ABR-5A Analysis 0.92 0.063 Total Black + Brown V Hard Particles @ 7 Mins. ABR-12 Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2A Moisture, % ABR-1A Particle Size Distribution ABR-3 2 8. 3 .0 591 .0 02 % ON Brabender Dry Time, Mins. ABR-7 4.8 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. \ s Amy E. Bagwe Laboratory Supervisor (601) 369-3624 VAB.0001201313 Vista Polymers Highway 25 Aberdeen. MS 39730 * FVC RAILCAR ANALYSIS Load Bate Time Logged In: WaShip Bate:. Product: Logged In By: Order No:. Car No.: n338*7 Silo(s): teT? \9<LCustomer : syS P /yf Compartment c*-*$ Sample From Bottom Moisture % BL Contamination BR Bulk Bensity DI C BB after Fluff Hard Particle Bottom of 7 13 Bottom 3 f V Bottom >0 I /rtf ? * o 8$ Viscosity RVCM 40 Mesh/Glass Screen Analysis Mesh Weight %r 40 <s> > o 60 3. SO '7. Cp 80 Zt-*> 100 7-3 f 120 7.5V /S.S 140 7-7 200 -f y Pan J&L n Dry time: 4 T? Static Flow: 0_L kstg. Microns: m- y Color L: /60 ^ a ^ b /~ Technician: f VAB.0001201314 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 CERTIRIGAT E OR ANALYSTS Date: April 16, 1992 Customer: Intex Plastics Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: April 15, 1992 VISIAProduct: 5415 Railcar No Order No mass UTCX 46520 0009577-000 Property Test Method Analvsis Inherent Viscosity ABR-10 1 .00 Residual VCM, ppm Contamination ABGC-26 ABR-5A 0.0/0 Total Black + Brown Hard Particles @ 7 mins. ABR-12 2 Dry Flow, Seconds ABR-8 8.5 Bulk Density, gm/cc ABR-2B 0.520 Moisture, % ABR-1A 0.20 Particle Size Distribution ABR-3 % ON Brabender Dry Time, Mins. ABR-7 4.9 gwe Laboratory Supervisor/Lead (601) 369-3624 VAB.0001201315 Vista Polymers Highway 25 Aberdeen, MS 39730 F>Va A I LCAR ANALYSIS Load Date : 4'~?~ Time Logged In: Ship Date: *t| IS~ Product: Car No. ^ -iT.2, Q Logged In By: WLfSL Order No: ^T? too Silo(s): 69o, i9l )P<L-Customer: Screen Analysis Mesh Weight 40 0-9)0 % 0.0 60 1A3 XI 80 3X, 13 mi 100 13, 211 120 Jos' WL 140 .US' ts,3 200 Pan q.3 JN3 Drytime: __Static Flow: 0 / C* ^ Avg. Microns: /7 7* - Color L: |QQ a * OV b Ic$3 METS: 4/ m-o x Technician: VAB.0001201316 Vista Polymers A Division of Vista Chemical Company CER ~fo Highway 25 Post Office Box 91 X R I G A EE OR -}hJULcLtrrv^ > / L* )t(*Aberdeen, Mississippi 39730 Phone (601) 369-8111 ANALYSIS 9 h Date: April 16, 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: April 14, 1992 VIS1AProduct: 538 Railcar No. VIPX 45760 Order No.: 0009578-001 Property Inherent Viscosity Residual VCM, ppm Contamination Test Method ABR-10 ABGC-26 ABR-5A Analysis 0.92 0.057 Total Black + Brown Hard Particles 3 7 Mins. Dry Flow, Seconds Bulk Density, gm/cc Moisture, % Particle Size Distribution ABR-12 ABR-8 ABR-2A ABR-1A ABR-3 516 ON 5 9.6 0.575 0.03 2001 PAN 5.01 3.0 Brabender Dry Time, Mins. ABR-7 5.0 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. my E. Bagwell Laboratory Supervisor (601) 369-3624 VAB.0001201317 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730 Phone (601) 369-8111 A Date: April 15, 1992 Customer: Intex Plastics Corp. Corinth Div. Golding Drive Corinth, MS 38834 Attention: Quality Control Manager Ship Date: April 10 , 1992 Property Inherent Viscosity Residual VCM, ppm Test Method ABR-10 ABGC-26 Contamination ABR-5A Total Black + Brown Dry Flow, Seconds ABR-8 Bulk Density, gm/cc ABR-2A Moisture, % ABR-1A Particle Size Distribution ABR-3 yisiA Product: 530 Railcar No.: ACFX 41135 Order No.: 0009579-000 Analysis 0.73 0.006 7.6 0.542 0.20 % ON Polyvinyl Chloride, Virgin Resin, Not Reprocessed Amy E. Bagwell Laboratory Supervisor (601) 369-3624 VAB.0001201318 Vista Polymers A Division of Vista Chemical Company Highway 25 Post Office Box 91 Aberdeen, Mississippi 39730-0091 Phone (601) 369-81 1 1 A IFI Date: February 4, 1992 Customer: Marley Mouldings, Inc P. 0. Box 610 Marion, VA 24354 Attention: Brenda Sauls Ship Date: January 29, 1992 ANA V S I s VIS1A FAX No. 703-783-8169 Products 5305 Railcar No.: ACFX 41135 Order No.: 0006278-003 Property Moisture, 7. Bulk Density, GM/CC Particle Size, 7. on Test Method ABR-1A ABR-2A ABR-3 14.8 Analysis .20 .543 140 200 PAN 19.4 8.8| 1.8 Residual VCM, ppm Inherent Viscosity Static Flow, Seconds ABGC-26 ABR-10 ABR-8 .006 7.6 Polyvinyl Chloride, Virgin Resin, Not Reprocessed. Amy EX/Bagwel Laboratory Supervisor Phone (601) 369-8111 VAB.0001201319