Document QvDvmj3bZwo873p3LNxawm5k
MN0 IK&titWetlONS: BATCH UNIT
N35217
fPMENT:
pag e 2 ce 46 c o d e YT868mD
......;............ ......................
DV >P Stir 10 rain or Ions er to wet
es t . w o t . 2253
l bs.
USE N LBS. f1""C.Oy D E
ACCT LBS.
5 iCL. Ad.1 DV to 37* (128116) at 2(K22f ... ;7, ,, s
7,
'
Cont,"< A
A2A*
-Sfcrttonf Stir 30 Record:
ln`1rr 12-15 ditn min at 28-32F maintaining Time Start"^o"W 7 CR
+
.... QH'i, + Kl for
--f+y' Kr
S 27 ""-^.
18x330
52rA' sm
J.1 >/i.w. ,, 925-A "W"*
-----57^T
(+
7 * NOi t?
74
(1) If CR-, KI-, add 20# '`as Is* increments ' Assume 32%
-- S .
Record] CR ^
{+.), KlS
(T)
t: *
C2) If CR+, KI, add 20# "as Is* increments
Record? CR v (+). KN\
(+)
Assume 33% V---- 725-A' ;
IT*"? 25 During S 24 stir weigh:in drums for S31 M
Weigh in Buggy for S 41
7-. 7 H
,
%
Wf /^30-D.
m mm
w
DV .Whn S 24 st1r complete, dump in
_______ .7
15 113-A is
/
0A 0
*r3k
Jump, stir NUIt:
in__...,____ _____________________________________________ 30 min at 28-32MF maintaining +CR, +0 far S 34
,
Ifl
777 ^a 10 57^A
1
CD If CR-, add 20# *as is* increments
Record? CR I (+) Kl
(+) -
Assume 32%
28-D . /.I. ;
rh .
(2) If CR+, KI-, add 20# "as is* Increments
Assume 33%
-..... Record: CR 7
f+). KIv;,
(*) [ 77 ' ' ~
"T25CT
>36' During 5 29 stir, run 10* C970S) water into V-^ /0 k> &
. ^S
install temp chart ..
!;
;
our in N-7-D from S25 _ Adi ta 30* 129286) at fifi.70^F
1- t ^3 Close stack damper
____________________ _
".7. 7
\ . . . . ^7
*
DV When S 29 stir complete, test DV & Record:
!'" 9
Record? CR "T**
f+1. tBDs\ 3 0 (28-32aFl
NOTE:
'' .
(1) If CR-, Kir add 20# "as is* increments
Assume 32%
--
Record: CR
f+). KI ^ (+}
12) If CR+, KI- add 20# "as is* increments
Assume 33%
^X35-
Pump
Record-; CR
1(V),
DV thru clarif press into
KI V*
^ (+) 17 77 A y .f* maintaining
Temp at 28-32c,F Record? time start
Total min 9a
-An 2x330
H
DV
iaK37 1 Dissolve in 20 gal water In drum for S59____ ____ :___ ,___ 1 ^~eT~
:
^ >38
Dumb in from S2 Note: Break u p lumps
Lot ./<$>
/
. .'
#100% %G>0
4CST ..........
%
9Jif
~mz"'
........ ..........................
-
// S7-ft
~57^r 28-A
' ':V >--7
KUwV>
725 A
57-A
"**' " .... ";VHi 79-D ~rr
ysguir7
'fJtLS - ...j
^39 Stir 10 min to dissolve
__x____
a >^0
Open stack damper Run in N-30-D from S26 undersurface In 20-25 min
A? Stir 5 min & Record; pH &,] (5.8-6.3)
,I
L^43
If necessary, ad.1 to pH 5.8-6.3 & Record: d H
Assume &u% As$UWg___772L
7
\
s%4
When S17 stir complete, run in V-303 on surface AFAP t'
"-7
T<
------ ------------- ------------ ----------- ------- --------------- ----- ---- ------ - ^
. ' 1
-
J-
.*
: "~l' \
"
'
v >
'i
/.iJ1
7^0-.-^----41
30-D
. v7-
- '1
J- V' '' ' '!
DUP050108179
... r""'v
PAt.i 3 c g 46 c o d e YTi-868-D
es t . v#g t . 2253
LBS.
IM When S35~ complete, "wagft OV Ifnes, ^nip '& press~~TdrTg mio
/'< \
or. to a - CR test on a sample oFtotaT press effluent,
which ever copies first collect washingsin DV ($35)
Stir 5 min necessary,
&adrjectoord2r88~'._T3_2e_m_f_p__mJ_3_<oF__f_dr(2W8-3'2F6) f &;
if
<r g
'4L. Weigh in rubberHducket & wash into
St 1r 5 min & Record: Ki
- (*]
If necessary adjust to - KI & Record; KI
USE LBS,
TT
JJL
CV\ifSL WherT S49 complete, ad.i CV to 38^117586) at 80>S4PF
13 A
ML-:
1^51 Immediately run 1n DV thru.undersurface distributor
80- 84OF. Record: Time Start3,'^gy *,
Total min 10
H
CODE
ACCT LBS.
TH
nr
"59fr /i-
cvv^5 ii^5
When $51 cnnmlete. Stir 10'niiri* " . ~ ' . '
Rer ordT: 01 azo
------t^TBase"T+TpTfU (4.3-3.71
Note*
ID. If Diazo + . Base and pH below 4,3;
fa) ad,l to pH 4,3,4.7______________
Assume 50%
if Dlazo +, Base and pH 4.3 or above?
ID "add 8# 100P-7-D~to~~a 55. G drum___
(b) ad.i with water to # 25 G
TcT add 20# 100% N.-46-C " 7 ; .
.d) stir_ tg dissolve
' YZ
[e) pour into CV ...................
......
(f} stl r to min
/>) Repeat (Tj'.ITU "iMve as fiecessarV to ~ Diazo . + Base
Po l i I lil N fnij
..._
____ .... .
f J-uirip i nN-979-A from $37.. ,
jy j ncul . to 200204&F in 40-45 n n
7..Shyf. off.steam
Record? T1me_
i cf > 5 rnuL & Redord: pH
ts w.m....Jfc&At.z.
TDd4 i.D riveasary, adl to p'H~
*: j&f LRDecord: rp\(H4
___ .... ..
9,2.~,y. Assume 5ti%~~
.... ..... ....A...s.s..u..m. e 321
\t neof^tary. reheat to 200-204F then shut off steam
^^66..jjfr&fe, i| frT n ^]^lfc^.ZlD..,y:CSE!.Sg|[-... JP^rj{.St1.r7ti,me,5^^'
! F icod to 94``"l 91746) & stop agitator t
\
T
"9hs~ its
7*0 Tf
m*
"75 t s ;,
^" TTfV
1
DUP050108180
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DUP050108181
FORM A'
CODE jp DATE n A6.& OPER.
LOT iMSy ' .
_ * -- sd-
h r ij/ 1^3-3
VATS SUPERVISOR
EQUIP, JT, ffiSSX
X^iPbseA all stumps, leave 1 stump identified.
Clean shovel.
yttf. Chute washed & top replaced.
|Jf. Water hose coiled.
........ --
1^5, Steam ejector turned off after finished in vat.
^,J. Scale left clean.
\/f> Added ice to vat only when volume reaches agitator.
|/. Floor cleaned around vats used.
1/9". Hoses coiled or dh rack on diazo press.
Hoses not crossing walkway after finished,
l/fl. Pump shut off after removing hose from intake.
Ice blower shut off after using.
*#3. All spills in area worked clean.
i^3r4. Door on instruments closed.
l^IrS. All empty drums removed from area & discarded.
Ur6. Corrosive.containers' properly covered.
l%f. Top of vats cleaned of color* paper cups, strings, etc,
w8. Vat door closed after finished - hatches,on abbe's.
All tools cleaned & placed in rack or proper places.
2b. Ice house clean - tools on racks. WlTRevolvator cleaned - platform & pit,
ATTACH TO MAKE CARD
DUP050108182
DUP050108183