Document QkeN5je5gqmRaoYXNvnD5Bjv5
CLIENT ID:
sakmp* Drn"*: Blank Data FS.name: Cd. VW. Dota Flbnstn.: K Motslwe:
CONC FO"ND
DETECTION UYIT
PFSSG_OMSZ9 PFSSG-094Sl9 PFS5G-oo4S28 IS.2
RETENTION
TIME
LABELED COMPOUND CWPFOA
IAS FLAG'
SPIKE CONC.
IW)
25.0
CONC. FOUND
l-al
26.7
RIW)'
RETENTION
llME
10,
7.32
AKYS METHOD MLA.o31 Rev 01 Ffos~sI~o*
PERFLUORU`ATSD
FOmllM SURFACYANT AWALYSIS RWORT
L,b "am.: AKYS &NMYTlCAL SERWCES
contract No.:
419,
M&k
soLlo
ssnp40 Receipt D.tm
*5-N0"-2QC!4
Eximcson Date
IQ-Jan-2005
Amlyslr Date:
ZO-Jan-2005
Ex`mct "alum. ,mL,:
2
l",utkl" vohlnn (pL): IS.0
Dhd,o" F.ctcc
N/A
rime: 20:37:02
COMPouND
PFOI PFOS
IAS FLAG 9
COW FOUND
2.45 4.49
DETECnON LIMIT
0.0082 0.0100
CLIENT ID:
24-Nod-2004 15:cfJ
N/A
L7415-2
10.2 2&Ja"-2W5
0 WY)
LCMYMS
c10. z*x XDS
PFSSC~OO7S"O
PFSSC-007S38
PFSSO-007S46
IQ.5
RSTENnON TIME
4.83 6.12
UBELED COMPOUND CISPFOA
(1) " = not *elected (2) R (%) = Pelcew recwery
LAB Fl.Ao*
SPIKE CONC.
bat
2S.O
cow. FWND
fkd
20.0
RWI'
RETENTION
TIME
80.1
4.93
Alms METlK3D MA.031 PFos~sIJu
R." 01 PERFLUORINATED
Foml lN3 SLRFACTANT ANALYSIS REPORT
sample coo9cuon: Pm,.ct Nun: Lab Samph ID: amp* 81u: Inlual ca"b",,on Dal% Inslnumld ID: LC Colwnn ID: SampI* DatalOe: Blank D.,. FII.nar,e: Cal. vu. Da F0.n.m.: x Yohlum:
CLIENTID:
24NoeoO415:35
N/A
L74153
17.0
em?
17.&Arc2005
LGMSlMS
Dim
Cl 8
PFSSG~OOAS30
PFS~GJKI~S~B
PFSSG-WS28
15.4
COMPOUND
LAB FUG'
WNC FOUND
DETECTION LIMIT
RETENI'ION
PFGA PFOS
2.27
O.cu82
7.32
0.22
0.0280
9.22
USELED CGMPGUND ClI-PFOA
(I, " = not ckteued (2, R (%, = Percant recovsry
IAB FIAG'
SPIKE CONC.
@a)
25.0
CONC. FOUND
b-II)
23.8
RWI' 05.1
RETENTtON TIME
7.32
AXVS METHOD PFos.sl_m
Yl.A.031
Rw 01 PERFL"OWN.TED
Form 1M SURFACTANT ANALYSIS REPORT
CLIENT ID:
COMPOUND
PFOA PFOS
RETENTION TlYE
4.84 6.08
USELED COMF+OUND CIWFOA
LAS
FLAG
SPIKE CONC.
Ingl
25.0
ccuc. FOUND
hl)
20.9
RV.1' 83.5
RETENTION
nw
4.84
UPIS YETHOD MIA431 PFos~srJ2
Rw 01 PERFLUORINATSD
Fc.ml1M SURFACTANT ANKYSIS
REPORT
L.b Mm.: u(y.9 ANALYT,CAL SERWCES
MELED coMPO"ND CC-PFO*
(1) u=notds&.ad (2) R(X) = Psrcmt recovery
LAB FLAG '
SPIKE COW.
IW)
25.0
CONC. FOUND
InPI
21.3
R(X)'
RErENnoN
TIME
85.2
7.32
AXYB MElHoD PFm-*I-Dz
MLA.03, R." 01 PBRPL"ORlYAlED
Farm 1M SURFACTANT ANALYSIS NEPONT
limp* cQllutlon:
Lab Name: Ayys MALYTICU SEWICES
Fvoject mm.:
CD"lrad No.:
4191
Lab smp* ID:
MddX
SOLlo
Smpl. slzs
SampI* Recalpt D&et
2E-Na\czw4
I"ls.l wllbr-
mte
ExtdRCSO" DSWZ
zwan-2005
kmr"mmi ID:
AndyA D*l*:
21.hn-2005
TIma 22:40:23
LC Column ID:
ExtmCl "OI"nw ,nL,:
2
smp* Dataf#*:
l",esNon "0l"me (p,:
15.0
Blank Dab Fllmame:
rmlu0" FaCtM:
NI.4
Cd. VW. D&a Fs.nml~:
Conc."*ralm "",I. : nplg (dly wdgM basis)
XMdstwe
COMPOUND
LAB FUG '
CONC FOUND
DETECllON LIMIT
PFOA PFOS
0.518 3.40
0.0037 0.0004
CUENr ID:
22NW-2004 14%
NIA
L7415.8 (A)
18.0 21-Ja"-zfJx
g WY1
LC-MSIMS
C18. zo*sx xD0
PFSSf-OWNS
PFSEG-003S34
PFS5C_w8s43
12.4
RETENTION TIME
4.90 6.12
LABELED COMPOUND Cl3.PFOA
LAB FLAG '
SPIKE co+Jc.
(WI
25.0
CDNC. FOUND
IWI
24.6
Rw.)' 93.2
RETENTION TIME
4.90
AXYS YElHaD PFos.S_O?
MU031
Rev 01 PERFL"ORINATED
Form IM SURFACTIIIT
ANbLYsts
REPORT
Sampb CdMkm:
tab N.rnE Ax-is ANUYTEAL 8ERvlCES
Pm,.ct Nun.:
contract No.:
4181
Lab SampI. ID:
MC&IX
souo
smpb she:
Sampb Itawlpl Datw
25-NW-2004
InNhI Cd`bmt!e" 0.0:
ExvaC"O" DItaz
21&n-2035
t"*tNnmnt ID:
A,,rtpb Da,.:
2,.Jan-2005
rime: 20:10:03
LC cotwnn K):
Extract "d"nm ,mq:
2
s.mpt* oatin*:
t+ctton "OI"nw ,pq
15.0
Stank D.ta Flbnam.:
D"Wo" Factor:
N/A
Cd. VW. D.b Fl!an.me:
concentratton ""US : nglg (dry v&M basis)
XUobt"n
COMPOUND
us FUO 3
CONC FOUND
DETSCTtON LlYlT
PFOA PFOS
OS30 3.89
mm2 Cl.0117
CIJENT ID:
22-NW-20041435
NI.4
WGw533-104
17.5
Q (W
21-hRXK15
LC-MS/MS
Cl& zodlax x06
PFSSG~WBSS,
PFSSO~OOSS3.4
PFs50308s28
13.1
RETENTtON TIME
4.04 0.00
USELED COUPDUND CII-PFOA
us FL&S '
SPKE CONC.
ml)
25.0
CaNC. FOUND
(W)
25.0
RI%)' 100
RETENTtDN IlYE
4.04
Aws MSTNDD IlllAmi PFos.SIJ2
Rrv 01 PERFLUDRINMED
Lab Name: Aws ANALYTICAL sERvlcEs cmtmct No.: Mamx
Extracttm Dale: Adysts D.k Ext"ct "ot"me ,mL,: t",ecuon "ohm. (IJL): Dltutton F*ctor: concHltra(ron ""ita :
Form IN3 SURFACTANT ANAL"S18 REPORT
amp* colNctlon: Pro)ut N.mc Lab sampt. ID: Sampl. sb.0: Inlttal C.ttb"tlon D.t.: tmtr"m."t ID: LC Column ID:
amp* DabIt*: stantcD.h Ft*n.m.: Cd. hr. Data Fhnam.: K Mobtun:
CLIENT ID:
22-Nov.2,X415:,5
NIA
L711W (A)
to.1 17Jan.2w5
o (dry)
LC-MS/MS
Discnvery ct.2
PFS5GJO4S32
PFs5c~cws19
PFs5G~c4Ms2s
11.4
COMPOUND
LAS FtAD '
CDNC FWND
DETECTION LllllT
RETENTIDN TINE
PFDA PFDS
0.322
o.cJm4
7.32
3.18
0.0163
9.22
LASELED COMPOUND C%FTDA
(1) U=notdetesed (2) R ($4) = Percent remvery
LAB FUD '
SPlKE CONC.
WJ)
25.0
CDNC. FWND
(WI
26.2
RW' 105
RETENTION TINE
7.32
AXYS METHOD M.A-0.Y FFm_sr_o2
Rw 01 PERFLUORINATED
Fmn IN3 SURFACTANT ANALYSIS REPORT
Samp* Cosution:
Lab NW".: AXYS ANM-,,lCAL SERWCES
ProjuA Name:
Cont"ct No.:
4191
Lab Smplb ID:
Merk
SOLID
SampI. skw
SampI. Recdpt Dab:
ZbNo"-ZoM
bllhl cdlbrmson D.lw
Exlnclion Date
14Ja~2005
IMtNmMt ID:
Analysis Datx
,7&"-2005
Tim: 17:44:40
LC w"mn ID:
Extract Volume (mL):
2
sample Damnl.:
In)utllm volum. ,pL,: 15.0
Blank Da`s, FS.runn:
DSutiD" Factor:
NIA
Cd. VW. Data FSwanw
Cwlca"Wtlo"
unnr : "g/g (dry tight b&S)
x Mc4shne:
CONPOUND
LAS FM'
CONC FOUND
DETECTION LIMIT
PFOA PFOS
0.315 2.65
O.WT2 oms7
CLIENT ID:
RETENTION TIME 7.32 922
LASELED COMPOUND CK3-PFOI
IA3 FLAG'
SPKE CONC.
(WI
25.0
CONC. FOUND
(WI
25.6
RW1'
RETENTION
TIME
102
7.32
AWS METHOD YLA4.W Ffos_s~~Ln
Rev O< PERFLUORINATED
Form IrJz SURFACTANT AMLYSB
REPORT
Lab N.mc AXYS ANALYTICAL SERVICES
COMPOUND
PFOA PFOS
LAB FIAG '
CONC FOUND
0.270 1.03
CLIENT ID:
22-Nw-2004 N/A
1o:cn
L7415-8
18.7
0 (dry)
2wan-2005
LC-MS/MS
cis. atlax XOS
PFS5G~OOW49
PFSX_w8S34 PFS5o_OOSS43 15.1
RETENTION TlHE
4.02 0.08
LASELED COMPOUND C13PFOA
(1, u=rddetEcled (2) R (%I = percenl mm"=ry
LAS FLAD'
SPIKE CONC.
(no)
25.0
CONC. FOUND
Ino)
21.5
RlW)' 00.1
RETENIIDN TlYE
4.82
AXYS METNOD MIA431 PFcls~sIpP
Rev Ot PERFLUORINATED
Form lAi2 SURFACTIHT
ANALYSIS REPORT
satnpb col-n:
Lab Name: Axys #Nunlcu
SERWCCS
Pm)Bct Nmn.:
conmcd NC.2
4191
Lab Sampb ID:
Y.tdx
SOLID
Sampb Sk?.:
sampb Race,* Da&c
20.Nov.2W4
I"Nid C.Obrrlum Da&z
ExtmcSoon Da,.:
14.J~W2000
I"`tNm.nt ID:
*Nlyrb Date
V-Jd"-2000
Tlmc 2052:40
LC column ID:
Extract Volume (mL):
2
Sampb Dabfib:
I",-
"ol"m* @L,: 15.0
Bhnk Dab Flbnanw:
Dlltilon Factor:
NI.4
Cd. VW. Dab Flbname:
ca"unt"om
""on : "g/g (dry wei~td baoio)
x Mrlbtww
COMPOUND
LAS FLAO'
CONC FOUND
DETECTION LIMIT
PFOI PFOS
0.900 0.19
O.OiMO 0.0349
CLENT ID:
2%NW-2004 11:20
N/A
I.74159
17.1 w.b"-2005
9 WY)
LCMSlMS
Discnv.3lyCIo
PFSM~Ooe33
PFS5CQD4S19
PFS5G-OOGi3
20.1
RETENTION TlME
7.32 9.22
UBELED COMPOUND CIW'FOA
LAS FLAG '
SPOE CONC.
(WI
25.0
CONC. FOUND
m9)
21.5
RW)' 06.2
REYENTlON TWE
7.32
AK% YEmoD Ffo5_8,_D2
ML&m,
Rev ol PERFLUORINATSD
Lab Nun.: AXYS ANALvllcu
c-
"0.:
Mlbh:
Smpl. Rewlp, Date:
Ext-
Dse:
Analysis Da-
Extncl"ol"m.
@IL):
I",*cthm volum (IaL):
q iltih F.tir:
C0Ke"lntlo"
units :
SERVICE*
Form IN2 SURFACTANT WLYSIS
REPDR,
s.mp* colleenon:
Pro@3 NUna:
Lab SunpIe ID:
smpl. SIZW
l"lll.4 C.llbntion D&K
lMburn.nl ID:
LC Column ID:
samp,. DNaRl.:
Blank Data Flham.:
Cal. VW. Data FS.,,mm:
K Mom"":
COHPouND
LAR FLAG'
CONC FWND
DwEcnotd LIMIT
PFOA PFDS
0.173 1 .a7
0.0043 0.0138
CLIENT ID:
3aHI-Nou-M0( 1230 NIA
L7454.1
17.6 2O.hW2W5
0 (dry1
LC-MSIMS
CIB. ZorbaxXDs
PFSSG_oO7SS1
PFSSG-W7S38
PFSSG~oO7S.48
11.2
RETENnoN TIYE
4.93 6.12
LABELED COMPOUND MS-PFOA
UB FiAG'
SPIKE CONC.
(WI
25.0
COW. FOUND
(WI
26.5
RI%)'
RETENTION
nhw
ma
4.93
CUENT ID:
30-NW-200413:lO WA
l.7154-2
18.5 M-Jan-2005
o (dry)
LCMSJMS
Cl& ~axxos
PFSSGJQ7SU PFSSG-W7s38
PFs50~007S46 1, .4
RETENTION TIME
LAS FLAG'
SPIKE CONC.
@Of
25.0
CONC. FOUND
(WI
22.9
R(4'
NETENTlON
TIME
91.0
4.90
AWS METHOD Yu-031 Pfos~sr~Dz
Rev 01 PERFLUORINATED
Lab Yam.: UYS *N.UWNXL SERVlCES
co*cl WC..:
4101
Matrkc
saLm
Fomt lU3 SURFACTANT ANALYS,S REPORT
smpl. Cooedlon: Pmju4 Null.: Lab samph ID: ' smp* Bb:
PFOA PFOS
IAS FUG *
CONC FOUND
1.00 4.70
OETECllON LlMlT
OlJX.3
CLIENT ID:
3o-N~200113:35 NIP, L745+3 (A) 17.5 20-h".2045 LCM?JMS C13.**xXDs PFSM-007SS3 PFB50~007s3o PFS5G~007S4`3 14.0
0 PY)
RETENTION TIME
LABELED COMPOUND C13PFOA
LAS FLAO'
SPIKE CONC.
hll
25.0
CONC. FOUND
IW)
25.7
R(X)'
RETENTION
IlME
103
4.03
AXYS wlHoo pFos_hl_ol
YLA.03, Rev a, PERFLUDRINATED
Form 1An SURFACTM ANAL1818 REPORT
Lab Nme: AXYS ANALYWX,. SERWCES
C-NO.:
4101
MlldE
SOUD
sampb coautban: Pm,.ct Nan,.: Lab sample ID: s.mp* Sk.:
SampI. Raeipl Dab:
0~~*004
lnllhl C.Obntion Da,%
Exh-ac.nD" Dam BJm~ls oak`: EAraL "dwn. (ma): I"jealon "ol"nu &L,:
la&w2005 2c-Jan-2W5 2 15.0
nm9: 18:4,:17
Inchwn.nt 1D: LC cobmm ID: Samph Oataft*: Shk D.rn Fu.n.me:
Dilulii Factoc
N/A
Cd. VW. Data FoeMn:
concmt*n
unns : n&, (dty w-aighl bask)
x Md`tllm:
COMPOUND
L&E FLAG *
CONC FOUND
DETECTION LIMIT
PFOI PFDS
1.21
wx47
5.30
o.mwo
CLIENT ID:
3c-NW-2Da4 ,335
WA
WG14832.104
17.7 20.JSn-xx)s
a W-Y)
LC-MSIMS
C18. zorhax xos
PFSSO-007S4,
PFs5G_oo7S38
PFSSGJO7531
14.7
RETEN'tlON llME
4.03 6.12
C13PFDA
(1) " = not detected (2, R (X, = PBrcelll ceco"*ly
IAS FIAG'
SPIKE CONC.
ha)
CONC. FDVND
hl
Ro()'
RETENTIDN
TIME
AXYS Ys7HoD PFo3~sr-m
YIAOJ,
RWOl PERFL"oRmATED
Form W2 *"RFAcmMT
ANALYSIS REPORT
Samph Co0ution:
lab W.mm Ax-is ANALYrlCAL 8ERvlcs8
Conbad NC
4191
MIIIW
SOLID
smpl. Receipt Dab EmactIon Da,*: Andysir D.W
03-tMC-2CQ4 1%&n-2005 2UJa"-*W5
Exlnct "c4"rn. ("L,: 2
l",ectk" "olurn (pl.,: 15.0
Time: 21:2s:19
Prc.Jmt mm.:
Lab s.mp* ID: sample SIZE Inn,*, callbra"o" D.*: lnrbumm, ID: LC Colunn ID: sampI9 mtmi,.: SI."k mla Fu."am.:
Dilu"on Fsstoc
NIA
C.I. WM. 0.u F,iwum.:
Conse"lm"c.n ""lb : ngrg (dry wei@l basis)
H M*t",*:
CLIENT ID:
30-Nuv-2004 14wl
N/A
L74s44
18.2 2O-h*2005
g (dry)
LCMSMS
cm. zcrbabaxXDS
PFSSG-0075%
PFs5GJm7S38
PFs50Jm7s46
12.2
PFOA PFOS
0.859
O.OMS
430
4.75
0.018,
8.08
LAS FUG *
SPIKE cow.
(W)
25.0
COW. FOUND
(W)
22.0
RW' 88.0
RE7ENTmN TIME
4.90
Axw MslHOD WA431 PFOS-*1-D?
Rev 01 PERFLUORINATED
Form w2 SURFACTANT ANALYSIS REPORT
smlp* Coli~lon:
l..b Nmne: NWS c31ALYllCAl. SERVICES
PmJwt Name:
ca"IRC( NO.:
4191
L.b smpl. ID:
YatIbc
SCXID
Sample Skw
smnple Recdpl oale
03.OeGzaN
lnltlal CallbnHon 0.b:
Extncllon oat.:
19-Jan-2cm
In*bumo", ID:
AlulysiJ Dalw
2c-Jsn-2005
Tlw: 21:41:02
LC Column ID:
Extract "Ohm. fIrI`,:
2
sm@* L7atafs.:
I",.clbarl Volume w,:
15.0
Btmk D&J m.nm.:
q htion tw2ic.K
N/A
C.1. VW. mla FIlmulna:
Conca"lrwtkIrl ""It8 : w!9 wY-Q+aht bsw
% Molsbtm:
COMPOUND
IAS FUO (
CONC FOUND
PFOA PFOS
1.72
0.0048
8.42
0.0209
CLIENT R):
30Nov-27llul42?5
NIA
L7454-5
16.6 2warr2M)5
D (dry)
LW?JMS
C18. Zwbax XDS
PFSSGJVTSS5
PFSSG~OWS39
PFS50_007S48
17.4
RETEHTION TIME
4.80 6-W
UBELEO COMPOUND CSPFOI
(1, " = not delecled (2) R (X) = Percent rem"elY
IAS FLAG *
SPIKE CONC.
IWI
25.0
CONC. FOUND
b9)
23.5
RW' 93.9
RETRNTION TINE
4.90
C0MP0UN0
PFOA PFOS
LAS FUG'
CONC FOUND
0.411 4.70
o.cmt 0.0075
30N0&?00414:00
NM
L764-0
10.0 2o-Jan-ZoQo
o (dry)
LC-MsiMS
mo. Zorba* xos
PFSSD-SS7SSS
PFS5G_oo7S38
PFSSD~007W
11.0
RETENTION THE
4.86 0.03
LABELED COMPOUND Ct%PFO*
UB FLAG '
SPIKE CONC.
(W)
20.0
cow. FOUND
@I)
25.4
R(X)' 102
REnanON nw2
4.06
Lab Name: Axys ANALYTICAL sERvtcEs
contrut NO.:
4191
MaWI:
SOUD
Sample Rmelpt Oat.:
05Dso2004
ENtdion oat%
1SJarr2uo.5
Analysis 0It.x
21.Jan-2005
The: 0:0230
Exlract volume (IIlL)
2
I"jOcticm "ohm* 011,: 15.0
0ll""on FYIOC
NIA
Conwncn"on ""Ns : rig/g (dry weight basis)
CoMPOUNll
LAS FUG'
CONC FOUND
PFOA PFOS
O.OST 5.80
DEi-ECTtON "Yrr
O.WXS wJosG
CLIENT ,D:
JO-NC+2ow I!315
WA
L74W7 (A,
17.4 *o-Jan-2005
0 WY)
LCMSMS
c1s. z-
XDS
PFSSG~OO7SW
PFs50~007s38
PFS5G~OO7SS4
13.8
RETENTION TIME
4.9s 6.12
IASELELI COMPOUND C13PFW
LAS FLAG *
SPlKE CONC.
hl)
25.0
CONC. FOUND
ow
22.6
RIW' 90.5
RETSNTION TIME
4.9s
AXYS YEllioD Mu031 Rev 01 pFos~s,~o2
PERFLUWNATED
Form IAl2 SURFACTANY ANALYS`S REPORT
Lab N.mm ANY8 ANALYncAL SERvlCEs
ccsneti NO.:
4191
Y.tflx:
SOLID
smpl. R.dpl chtc moec-2004
Exwactlo" Data:
19&w2W5
Analyrb Date:
2o-Jan-zuo5 rime: 18:54a
Extract Vohns (mL): 2
l~lon "Ol"me (PL): 15.0
DlluWon Factor
NIA
CcHlcentrath ""na : nglg (dry weight basis)
COMPOUND
LAS FUO'
CONC FOUND
PFOA PFOS
o.oao 3.31
DEYECYION LlYlT
CLIENT ID:
RETENYION
TIME 4.80 6.09
LASELED COMPOUND tl3PFOA
LAS FUO *
SPIKE CONC. bwl
25.0
CONC. FO"N0
bxl)
14.0
R WI' REYSNY,ON T)ME
58.5
4.00
CLIENT ID:
CONC FOUND
0.206 8.28
DETECTION UNIT
O.OOJ6 0.0139
RETENT,ON TIME
4.90 6.09
lABELED COMPO"N0 C139FOA
(1) u=nddetected (2) R (%) = Partent recw*ly
LAB FUG
SPME CONC.
be)
CONC. FOUND
IWI
R(X)'
RETENTION
TIME
I 2-2
smlp* Data",.: Blank Dab FIlmam+: Cal. VW. D.ta Fi*n.m: x Molst"n:
CONC FOUND
DETECTION LNml
RETENTION TlME
4.93 6.08
LABELED COMO"ND CIWFOA
us FIAG'
SPME WNC.
w
25.0
CONC. FOUND
IW)
25.9
RW'
RETENTION
TIME
1D3
4.93
12.3
AXYS MEnloD EOS_St~DZ
MIA-031 Rev 01 PERFLUOI?INATED
Form i/v2 SURFACTANT ANALyslS
REPORT
CUENT ID:
L&J Na,na: AXVS ANclLyTlCM SERVICES nm: 23:05:5*
Proja Name
M/A
Lab Smpk ID:
SmpN sii:
Inmd caobnoon D*:
I"sbumsnt ID:
LC Column ID:
sample Deafo.:
SI."k Data wen.m:
Cal. "or. oata Fo*n*me:
CoMPO"ND
PFOA PFOS
LAS Fuo'
CONC FOUND
3.63 6.24
DETEC'"ON LIMIT
0.0430 0.0208
RETENTION TIME
4.66 6.06
LASELEO COMPOUND CKLPFOA
(1) u = notdetecied (2) R(X) = Penxnt mm"efY
LAS FUG '
SPIKE CONC.
(WI
25.0
CONC. FOUND
MO)
19.8
R(W' 79.0
RETENTION TINE
4.66
AKYS METHOD MIA431 Pfcs~sl~m
RDV 01 PERFLUORINATED
FOtTlll&C? SURFACYANY ANALYSIS REFORT
Lab Nam.z AK-is ANALYTICAL SERVICES
CollkKt No.:
4101
uatrk:
souo
S.t"pk R.c.ipt D.ta:
21-oec-2004
Erhct,on 0.t.z
21&"-X105
Andyed oale:
2,.Jan-2005
llmw 20:3*:47
Ertract Volum (mL):
2
I"*on "OI"m# @Lb 15.0
Muk." Facdw:
NIA
l%tk3&8tlon"~.'
rg/Q (dry Might bask)
CoNPouND
LAB FUG '
CONC FOUND
PFOA PFOS
cl.167 2.88
DETECTION LIMIT
0.0001 0.0038
CLIENT ID:
RETENTION TIME 4.08 6.12
LmELEO COMPOUND ClS-PFO*
LAE FLAO'
SPIKE CONC.
InO)
25.0
CONC. FOUND
Ino)
22.4
RIW' 80.7
R"ENTlON TlWE
4.00
AltYS METHOD MU431 PFo8~S,Jx
R.vOl PERFL"oRINAYS~
Form w-2 SURFMXM
BAALYSIS REPORT
L& ~.m.: AXYS ANALYTICAL SERVICES
COMPOUND
PFOA PFOS
21.Jan-2005
nm8: 23:10:3s
2
15.0
N/A
n#* (dry weigh1 bark)
LAS FUD `
CONC FOUND
0.230 3.81
DETECTION LIMIY
o.ce30 o.olw
CLIENT ID:
1o-LwF2006,311
N/A
L7503-2
IS.0 21 -Ja"-xJx
0 WY)
LC-MS/MS
ClS. zwbax XDB
w55DJo5s51
PFS5OJW33.l
PFssO~D&3S43
10.6
RETENTlON TIME
4.04 6.0s
-LED
COMPOUND
cls.PFo*
IAS FLAS *
SPINE CONC.
Ino)
25.0
CONC. FOUND
lncl)
24.0
RW'
RETENTION
TIME
So.5
4.04
COMPOUND
PFOA PFOS
IA0 FIAG '
CONC FOUND
1.30 3.03
DETECTION LIMIT
0.0501 O.OWl
CLIENT n:
lboac-2004 13:40
N/A
L7003.3
16.5 21-JaMW5
0 WY)
LCMSlMS
Cl& zolbax XDB
PFS5.eSSSS52
PFS5G-WBW
PFS5G_oOSS43
20.8
RETENTION TINE
4.00 O.l2
lA0ELED COWOUND CCLPFOA
IA0 FUG *
SPIKE CONC.
InO)
25.0
CONC. FOUND
hl)
10.0
RW' 70.4
RE"%-llON TIME
4.08
COMPOUND
LAS FUO *
CONC FDUHD
DETECllDN LIMIT
RETENTION TIME
UBELED COMFOUYD C,%PFOA
UB FIAO'
SPIKE CONC.
w
25.0
CDNC. FOUND
ow
21.8
R(W)* 87.2
RETENTK)N TIME
4.86
CLIENT R:
LAS FLAG '
sample ColbctkN Pro,.ti Name: Lab smpl. LD: Sample Ska: 1"nl.l Callbmlh Dmtc Inslrumml ID: LC ColYtn" ID: smpl. D&m.: Blank 0.l. Filaname: C.I. "IT. DJta Fomain*: %lAdm
CONC FOUND
DETECnON LIMR
1.91
0.0019
B.so
0.0189
%-Ccc-2cw ,430
WA
L7503-5
15.9 21 -Ja"ao5
9 WY)
Lc-MrnS
cm zorbal XDS
PF5sGpxm4
PFS5GJMSS34
PFS5G-ODSS43
20.1
RETENTION
none
4.86
8.12
lABELED CoMFa"ND C134'FOA
(1, "="Mdeteded (2) R (%I = Percent recovery
LAB FIAG'
SPIRE CONC.
w
25.0
CONC. FOUND
b9)
21.8
RW)' 87.0
RETENTION Tmle
4.86
AXYS MElHoD PFos_srm
wA-o31
Rev 01 PERFLUORSWTED
FGml IM SURFACTAN,
ANALYSIS REPORT
Samph Cdhdlon:
bb NanI.: AXYS ANAL-
SERVICES
Pmjed N.mw
Ccmtid No.:
4191
lab Sampk ID:
Nabi:
SOLID
SampI* Sk.
Sample Realpt Datw
21-DK.2004
kdud Cdbrdion Dak
Extrxhn Ddc
21-.la"-2005
*dnlmolO ID:
Anaiydr Dde
22-Jan-2005
Tim*: 0:08:29
LC Cdumn ID:
Exlnd "dum* (ml.,:
2
Samph Dddih:
Injsdion Volume (pL): 15.0
Blank Ddw FOm~ma:
Dilution Factor:
NIA
Cd. vu. Data F0.n.m.:
Conunb.tio" unit9 : "s/g (dry weight bark)
XMddU~
COYPO"ND
us
CONC
DETECTlON
FUG'
FOUND
UNIT
PFOA PFOS
0.852 7.10
0.0028
0.0289
CLIENT ID:
Is-DaGm
14:3a
N/A
L7503.5
15.0 *1J*"-ZCC5
o W-d
LCMSMS
ClO. ZorbaxXDB
PFSSG-OS3SSS
PFS5G_OOSSM
PFSJG~OOBS43
19.8
RETENTIDN TIME
4.84
6.08
LABELED COMPOUND CIJPFOA
(1) "="ddaed~ (2) R (%) = Percent mavery
us
SPIKE
FUG'
COW.
WA
25.0
CONC. FOUND
IWI
18.7
RI%))'
74.9
RETENIION TIME
4.84
