Document QkVw7Vv8e3qKZwbE8kOd80Jjk
* CG.'^Oi CODE YE-698-D
< DATE > -ENDED B
L2H1.9 5527# LBS* f ( EST WT )
PROCESSES ( ) YE-698-D (T)
APPROVED1 FWP 10/15/82
COMTYP JOB NAME: 01YE698DMT
EQUIP MENT
NAME: MOLYBDATE ORANGE
1 USE |
1I ACCT
1 LBS
N-CODE |1 LBS
PREP 1
351 o
OBTAIN SODIUM SULFATE FOR S-13
2 | CALCULATE 6 SET ON BADGER METER F#R. S-16
I i-NlTRIC ACID WEAK)
, ,fo
3^0)BTAIN SODIUM CHLORIDE FOR S-33
T A IN SODA ASH FOR S-37
5^1>0jBTAIN SODIUM SILICATE FOR S-39
<xd>t5BTAIN SODA ASH FOR S-43
TT \ OBTAIN ANTIMONY TRIOXIDE FOR S-46
WEIGH SODIUM CHROMATE INTO V-35 OPTR_____, MK A OPTR_____, MK
I 84
1- .U.
1 734 I 146 1 237 1 350 I 70
i54i
108-A
3 3-D 4-A 3-A
32-D 3-A
711-B
10-D
]! 84
1 |1 60 1 734 11 146 1 237 !1 350 ! 70
1'
! 1885
I
359 v3
WEIGH IN SODIUM MOLYBDATE-SCliUT OPTR_____, MK Mf, T-
DPTR ___ , MK____ , T"
sjzrxjtm' io` (soe &) w at er in t o v -s s s
14*<pRUN V-359 INTO V-351 6 PUMP IN V-351
Sjf \ ADJ TO 55" (2600 G)
...
laH^SiFT IN N-108-A FROM S i j **
\#<\ STIR 5 MIN & RECORD: PH/_Sl7_(920-40.0)
15>TADJ TO PH 9.8-9.9 6 RECORD: PHX-V-
| | (CAUSTIC SODA SOLUTION) '
ASSUME 50%
1 U^
ASSUME 66%
ADD N-33-D FROM S 2 USING BADGER METER
I rrl ADJ TO 66" (3/21 G) AT 67^69*F
| | RECORD: VOLfA-* 6
F
i STIR 5 .MIN-i RECORD : PH^JsU 7.4-7.6) 6
I | G/ML/ifjO__ (1 .080-1 .083)
| | NOTE IF G/ML OUT OF LIMITS FILL OUT CHECK
i | LIST 6 ATTACH. TAKE 1 GJT SAMPLE
423-D I 303 I
7-D l_. 3 3-D
SV 20" (996 G) WATER INTO V-J 5 I RECORD N-41-D STORAGE TANK TO PUMP FROM. L^ClRCLE ONE: 402 410 411 420 424 425
20^1 CHECK WITH CU SUPV: i ^STORAGE TANK MUST CONTAIN AT LEAST 2376 1 GAL; 402=49", 410=25", 411=48*, 420=25", | 424=25", 425=31" | ^STORAGE TANK MUST HAVE STIRRED AT LEAST | 20 MIN SINCE LAST ADDITION OR ADJUSTMENT
| *STORAGE TANK MUST BE ISOLATED UNTIL ALL ,P PUMPING FOR THIS BATCH IS COMPLETE SET METER FOR 300 G 6 PUMP TO SV
NOV 4 1982
LOT*:. ,, EQUIP ME NT i
COMTYP JOB NAME: 01YE693DMT PAGE 02
DATE PRINTED:{/Ti
USE
N- I ACCV
I LBS
CODE I LBS
SV" I 22 I""AT"" APPROX"?0O~G~WHILE "CONTINUING_TO_PUMF'T"
5I | CONT I
II !23| II II [24 j II II I| I|
CHECK PH & DENSITY. RECORD BELOW. IF NOT IN RANGE, STOP PUMPING & SEE SUF'V. * PH : ______ (2.2-3.7) DENSITY: _________ G/ML (1 .270-1 .328) IF S-22 OK 6 WHEN S-21 COMPLETE, RECORD DENSITY _______ G/ML ON TRAPPED SAMPLE FROM END OF S-21 PUMPING. USING DENSITY PROM $-23, FIND METER SETTING FOR
SECOND PUMPING IN TABLE BELOW. NOTE: TABLE ACCOUNTS FOR 30 G ALREADY PUMPED IN S-21. CIRCLE DENSITY 6 SETTING IN TABLE BELOW.
** TABLE ***
I I I |
I I I I I |
%
1 G/ML 1 1 .270 1 1.271 1 1 .272
SETTING 1 G/ML 1678 1 1 .291 1 670 1 1 .292 1663 l 1 .293
SETTING ! G/ML
1534 f 1.312
1527 1 1.313
1521
1 1.314
SETTING! 1410 1 1404 | 1399 i
I 1 .273 1656 1 1 .294 1515 I 1.315 1394 1
1 1 .274 1649 1 1 .295 1509 1 1.316 1388 1
1 1.275 1641
1 1 .296 1 503
I 1 .317
1383 1
1 1.276 1 634 I 1 .297 1497 f 1.318 1378 I
1 1.277 1627
1 1.298 1490
! 1.319
1372 |
1 1 .278 1620 I 1 .299 . 1484 ! 1.320 1367 !
1 1 .279 1614 ! 1.300 1478
t 1.321
1362 1
1 1 .280 1607
1 1 .301
1473
I 1.322 135? !
1 1 .281
1600
1 1.302 1467
1 1.323 1351 I
! 1.282 1593 1 1 .303 1461 < 1 1,324 1346 !
1 1.283 1586 1 1 .304 1455 1 1.325 1341 !
! 1 .284 1580
! 1 .305 1449
I 1.326
1336 f
1 1.285 1573
1 1.306 1444
1 1.327 1331 1
! 1 .286 1566 ! 1 .307 1438 1 1.328 1326 !
1 1 .286 1566 I 1 .307 1438 ! 1.328 1326 !
1 1 .287 1 559 1 1 .308 1 432 1 1.329 1543 I
1 1 .288 1553 1 1 .309 1427 1 1.330 1537 1
1 1 .289 1 546 1 1 .310 1421
1 1.331
1532 |
,I --1-.-2--9-0------1 -5-4-0-------1 ---1 .3--1-1------1--415--- -1 --1--,3-3--2------1-5-2--6--.-1 |
25 [ SET METER 6 PUMP _,,^.*G (RECORD FROM TABLE)
I
I FLUSH LINE WITH WATER INTO SV FOR APPROXIMATELY I
I 30 SECONDS
I
261 ADJ LEAD NITRATE TO 76* <3625 G) AT 67-69*F.
|
I RECORD: ______ ____ *F
-
I
271 STIR 5 MIN & RECORD PH: ______ (2.2-3.7)
I
281 IF NECESSARY ADJ TO PH 3.0-3.1
ASSUME 66%|
I 6 RECORD PH: .______
ASSUME 50% I
i NOTE: DILUTE N-7-D 10:1 WITH WATER BEFORE ADDING!
291 RECORD: ________ G/ML.(1.143-1.144) IF OUT OF SPEC!
I FILL OUT CHECK LIST & ATTACH.
.
I
301 STIR AT 67-69*F FOR S-31. TAKE 1 QT SAMPLE.
!
41-0 | 511.0 57-A
33-0 7-0* |__c-:v
* **#
X
4
DUP050059963
V COT: . ;,'.ERUIP
;HENT I jV-
H1-3V-. -I:
si.%
C.OMTYP JOB NAME: OfYE698DMT PAGE 02
LBS
AT APPROX 100-G WHILE CONTINUING TO PUMP,
CHECK PH $ DENSITY, RECORD BELOW, IF NOT
IN RANGE^ STOP PUMPING & SEE SUPV,
X jPH':
"^^T2 2-3,7)
DENSITY SljjjLll G/ML <1,270-1 ,328)
IF S-22 OK 6 WHEN S-21 COMPLETE, RECORD DENSITY jJLA/> G/ML ON TRAPPED SAMPLE ROM END OF S-21 PUMPING,
USING DENSITY FROM S-23, FIND METER SETTING FOR SECOND PUMPING IN TABLE BELOW.- NOTE: TABLE ACCOUNTS FOR 30 G ALREADY PUMPED IN S-21.
CIRCLE DENSITY G SETTING IN TABLE BELOW, TABLE *#**
j | | j
J j | | | |
i |
| CODE I LBS I.
J 1 G/ML SETT I! I 1 1 .270 1644 1 [ 1 .271 1637 1 1 1 .272 1 63 1 I 1 ,273 1623 1 [ 1 .274 1616 1 1 1 .275 1609 ! ! 1 .276 1602 1 i 1 .277 1595 i i 1 .278 1588 1 ! 1 .279 1582 ! 1 1 .28 1575 I J 1 .281 1568 1 ! 1 .282 1562 ! I 1 .283 1555 1 1 1 .284 1549 1 1 1 .285 1542 i ! 1 .286 1 535 1 t 1.287 1528 1 1 1,288 1522 ! ! 1 .289 1515 1 ! 1.290 151
I : G/ML I 1.291 i 1.292 I 1.293 f 1.294
I 1.295 I 1.296 I 1.297 I 1.298 I 1.299
SETTING 1504 1487 1491
1485 1479
1473 1 467 1461
1455
`.302 1.303 1 .304 1 .305 1 .306 1 .307
1 .308 1 ,309 1 .310 1.311
143& 1432 1426 1420 1416 1410 1 404 1399 1393 1387
G/ML 1 .312 1 ,313 1.314 1 .315 1 .316 1.317 1 .318 1.319 1.320 1 .321 1 .322 1 .323 1 .324 1 .325
1.326 1-.327 1 .328
1 ,329 1 .330 1 .331
1 ,332
SETTING!
1382 I 1376 1 1371 i 1367 1 1361 1
1 356 I 1351 i 1 345 ! 1340 1 1 335 ! i 330 1 1324 i 1319 1
1315 I
1310 1
1305 1 1300 .1
1295 1 1290 I 1285 !
1280 1
! 1 i 1 1 1 1 i 1 1 1 1 1 ! 1 1 i f
1 ! 1 1
SET METER G PUMP
ROM TABLE)
1 i
I 1
FLUSH LINE WITH WAT? 0 SECONDS
ADJ LEAD NITRATE TO 3625 G <76'
APPROXIMATELY 1 I1
2/245 G 74.5"
1 t1
247) AT 6)?~49*F 7 RECORD:
< 330=r/BLOCK) ij iCmP v,.1 .vyA w if
1-3.7 >
11
1281 IF NECESSARY ADJ TO PH 3.0-3.1
i1
2& RECORD PH: " _'J__
-D PH
i1
ASSUME 667.1
I
ASSUME 50% J. "TET .!
1 DENOTE: DILUTE N-7-D 10:1 WITH WATER BEFORE ADDING!
I
129! RECORD: idSL-2- G/ML <1.143-1.144) IF OUT OF SPEC! REFILL OUT CHECK LIST & ATTACH,
I
30T SnTrIiFR AT 67-69F FOR $-31* TAKE 1 RT SAMPLE,
41 -D
33-D 7-D
i 5110 !asie
!___ I1 !7 I
DUP050059964
LOT;._____ COMTYP JOB NAME: 1YE698DMT
EQUIP " I MENTf
PAGE 03
DATE PRINTED:1415/82
USE
N- ACCT
LBS
CODE LBS
5v ]^T i OBTAIN 1 QT SAMPLES OF S-18 & S-30 SOLUTIONS
*5 I"' CONTI
I
I I
I I | I
I h TITRATE TWICE I NOTIFY SUPV IF ML N-IO-D IS NOT IN RANGE | 7.1-7.4 OR IF THE TWO TITRATIONS DIFFER BY
I MORE THAN 0.10 ML N-iO-D (IF YES, FLUSH ALL I EQUIPMENT & REPEAT TITRATIONS). DO NOT
I' PROCEED IF N-IO-D TITRATION IS OUT OF RANGE | ADJUST V-358 FOR A TITRATION PH OF | FROM FINAL IN-LINE TITRATION.^ECO I PH Z Q I & ML N-IO-D J__JX
______ __________________________ ;____________________,___________
132*1 WHEN S-31 TITRATION OK , STRIKE
SV ' I BOTH UNDERSURFACE DISTRIBUTORS INTO SV IN
6 ...| 16-18 MIN
| , | RECORD; START L
t o t a l min _____*____:
I | NOTE: STRIKE TIME UP WHEN 1/2 VAT BOTTOM SHOWS
I | & BUBBLES APPEAR INSi&HT GLASSES
I3j5-KIMMEDIATELY DUMP IN N-4-A FROM S 3 & SET TIMER
I L- FOR 15 MINUTES |3<i DURING S 33, WASH IN V-358 l^TSTin 2 MIN 6 RECORD PH^-_/0_< 1.8-2.5) I L. PBXS,,,dbn(MUST BE + )
|3<frT STIR TOTAL OF 15 MIN FROM S-33 It | RECORD: TEMPJZ__*F (67-73*F) I 3^-DUMP N-3-A FROM S-4
58 L STIR 3 MIN
I 'Z&Qr' POUR IN N-32-D FROM S-5
2 MIN
lAf^JURUN IN LIQUID ALUM USING BADGER METER
STIR 3 MIN t, FLUSH ALUM LINE WITH WATER
DUMP IN N-3 FROM S-6
STIR 4 MIN-FOR S-48
``
33-D 7-D
1
734 115-D 367
390 7
45^T RUN IN HYDROCHLORIC ACID USING WEIGHT 6 FLOW* **
| CONTROL PANEL
MK Jfc____
Vfl
!^T DURING
S-44
SIFT
N-711-B
MMKl/ FROM S- 7
INTO
V-390
*/
WITH AGITATOR ON.IN 1-2 MIN
STIR 1-2 MIN TO MILKY SOLUTION
SV |j J#H'"'WHEN S-44 COMPLETE, IMMEDIATELY RUN IN N-711-B
8 | I SOLUTION GRADUALLY OVER 5 MIN PERIOD INTO SV
| | WATCH FOAM!!! IF FOAMING IS EXCESSIVE, STOP
UNTIL FOAM SUBSIDES,
JDUMP IN BLANC FIXE N
WHEN SCHEDULED, DUMP IN BLEND BACK LISTED ON
TOP OF PAGE 1 >
RECORD: CODE _.2r___, LOT___rETZ"-,,
STIR 20 MIN^ /
RECORD; PH5.8-6.0) ,
|5*H IF NECESSARY, ADJ TO PH 5.8-6.0
ASSUME 50%
||
J, RECORD: pH-___ tET_._____
ASSUME 66%
154*1 FLOOD TO 153* (7298 G) & STOP AGITATOR
28--D l 105 28-D
330i/ 12 28-A 33
7-D 33-D
<T ip T R
D/
TJ^\ ........
DUP050059965