Document QgmmrDzG5L9eQdmxrnx5Jdq6

From: American Laboratories and Research Services, Inc. P.0. BOX 15609 Hattiesburg, MS 39402-5609 601-264-9320 Date: October 9, 1990 To: Mr. William H. Cooper PPG Industries Chemicals Division P.o. Box 1000 Lake Charles, LA 70602 The following analytical results have been obtained for the indicated sample which was submitted to this laboratory: Sample I.D. AA04889 Sample location: PPGHC Collected by: PREJEAN Laboratory submittal date Received by: RLH Cooling Tower Sludge (Hg) Collection date: 09/07/90 09/13/90 Time: 19:00 Validated by: RLH Time: 14:00 Parameter: TCLP Extraction Method reference: SW846-1311 Result: done Date started: 09/20/90 Time started: 11:45 Parameter: TCLP Metals Method reference: SW846 3rd Ed Result: see appended report Date started: 09/27/90 Time started: 09:00 Parameter: TCLP Volatile Organics Method reference: EPA 624 Result: see appended report Date started: 09/30/90 Time started: 21:11 Date finished: 09/21/90 Analyst: MJF Date finished: 10/08/90 Analyst: JSC Date finished: 09/30/90 Analyst: BB SL 046144 Mr. 'William H. Cooper Page: 2 October 9, 1990 Sample I.D. AA048,,9 (continued) Parameter: TCLP Semi-Volatiles Method reference: EPA 625 Result: see appended report Date started: 09/28/90 Time started: 01:06 Date finished: 09/23/90 Analyst: BB Parameter: Selected Volatile Organics Method reference: SW846-8240 Result: see appended report Date started: 10/02/90 Date finished: Time started: 22:34 Analyst: BB 10/02/90 Parameter: Semi-Volatile Organics Method reference: SW846-8270 Result: see appended report Date started: 10/03/90 Time started: 00:15 Parameter: pH Method reference: EPA 150.1 Result: 3.270001 SU Date started: 09/14/90 Time started: 15:00 Date finished: 10/03/90 Analyst: BB MDL or sensitivity: 0.00 Date finished: 09/14/90 Analyst: KEL Data for TCLP Volatile Organics ug/L Component Name Benzene Carbon Tetrachloride Chlorobenzene Chloroform 1,2-Dichloroethane 1,l-Dichloroethene Methyl Ethyl Ketone Tetrachloroethene Trichloroethene Vinyl Chloride Pyridine Concentration Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Component MDL 10 10 10 10 10 10 10 10 10 10 500 Mr. Milliam H. Cooper Page: 2 October 9, 1990 Sample I.D. AA04b9 (continued) Data for TCLP Semi-Volatiles ug/L Component Name 1f 4-Dichlorobenzene Hexachloroethane Nitrobenzene Hexachlorobutadiene 2,4-Dinitrotoluene Hexachlorobenzene Cresols, total 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol Pentachlorophenol Concentration Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Component MDL 10 10 10 10 10 10 20 10 50 50 Data for TCLP Metals mg/L Component Name Arsenic, TCLP Barium, TCLP Cadmium, TCLP Chromium, TCLP Lead, TCLP Mercury, TCLP Selenium, TCLP Silver, TCLP Concentration . 016 2.9 .01 Not Det Not Det Not Det . 041 Not Det Component MDL .005 .1 .01 .03 .04 .005 . 005 . 03 Data for Selected Volatile Organics mg/Kg Component Name Chloromethane Bromomethane vinyl Chloride Chloroethane Methylene Chloride 1.1- Dichloroethene 1.1- Dichloroethane trans-1,2-Dichloroethene Chloroform 1.2- Dichloroethane Concentration Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Component MDL 10 10 10 10 5 5 5 5 5 5 SL 046146 Mr. William H. Cooper Page: 4 Qctob r 9, 1990 Sample I.D. AA04few9 (continu d) Data for Selected Volatile Organics (continued) Component Name Concentration l,lf1-Trichloroethane Carbon Tetrachloride Bromodichloromethane 1.2- Dichloropropane t-l,3-Dichloropropene Trichloroethene Dibromochloromethane 1.1.2- Trichloroethane Benzene c-1,3-Dichloropropene Bromoform Tetrachloroethene 1.1.2.2- Tetrachloroethane Toluene Chlorobenzene Ethylbenzene Xylene, total c-1,2-Dichloroethene 1.1.1.2- Tetrachloroethane Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det 6 Not Det Trace Not Det Not Det Not Det Not Det Not Det Component' MDL 5 5 5 5 5. 5 5 5 5 5 5 5 5 5 5 5 5 5 5 Data for Semi-Volatile Organics ug/Kg Component Name Phenol bis(2-Chloroethyl) Ether 2-chlorophenol 1.3- Dichlorobenzene 1.4- Dichlorobenzene l,2-Dichlorobenzene bis(2-Chloroisopropyl) Ether N-Nitroso-di-n-propylamine Hexachloroethane Nitrobenzene Isophorone 2-Nitrophenol 2.4- Dimethylphenol bis(2-Chloroethoxy) Methane 2.4- Dichlorophenol l, 2,4-Trichlorobenzene Naphthalene Hexachlorobutadiene 4-Chloro-3-methylphenol Concentration Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Component MDL 300 300 300 300 300 300 300 300 300 300 300 300 300 300 300 300 300 300 300 SL 046147 Mr. William H. Cooper Page: 5 October 9, 1990 Sample I.D. AA04& j (continued) Data for Semi-Volatile Organics (continued) Component Name Concentration Hexachlorocyclopentadiene 2.4.6- Trichlorophenol 2-Chloronaphthalene Dimethyl Phthalate Acenaphthylene Acenaphthene 2.4- Dinitrophenol 4-Nitrophenol 2.4- Dinitrotoluene 2.6- Dinitrotoluene Diethylphthalate 4-Chlorophenyl-phenylether Fluorene 4.6- Dinitro-2-methylphenol N-Nitrosodipheny1amine 4-Bromophenylphenyl ether Hexachlorobenzene Pentachlorophenol Phenanthrene Anthracene Di-n-Butylphthalate Fluoranthene Pyrene Butylbenzylphthalate 3,3'-Dichlorobenzidine Benzo(a)anthracene bis(2-Ethylhexyl) Phthalate Chrysene Di-n-octyl Phthalate Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(a)pyrene Indeno(1,2,3-c, d)pyrene Dibenzo(a,h)anthracene Benzo(g,h,i)perylene Benzidine alpha-BHC beta-BHC delta-BHC gamma-BHC Heptachlor Aldrin Heptachlor Epoxide Endosulfan I Dieldrin 4,4'-DDE Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Trace Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Component MDL 300 300 300 300 300 300 1500 1500 300 300 300 300 300 1500 300 300 300 1500 300 300 300 300 300 300 600 300 300 300 300 300 300 300 300 300 300 2400 300 300 300 300 300 300 300 300 300 300 SL 046148 Mr. William H. Cooper Page: 6 Ccrooer 9, 1990 Sample I.D. AA046_9 nrmued) Data for Semi-Volatile Organics (continued) Component Name Endrin Endosulfan II 4,4'-DDD Endosulfan Sulfate 4,4'-DDT Methoxychlor Endrin Aldehyde alpha-Chlordane gamma-Chlordane Toxaphene Aroclor-1016 Aroclor-1221 Aroclor-1232 Aroclor-1242 Aroclor-1248 Aroclor-1254 Aroclor-1260 l,2-Diphenylhydrazine N-Nitrosodimethylamine Concentration Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Component MDL 300 300 300 300 300 300 300 300 300 600 300 300 300 300 300 600 600 300 300 Comments: Reference Lab Report No. R1461. If there are any questions regarding this data, please call. Kicxy-L. Hatton, Vice President Reviewed By: ^f W. Pinson, resident Ph.D. SL 046149