Document QeOkLzn0q6Jk20R96aGbQBx8
From:
American Laboratories and Research Services, Inc.
P.0. BOX 15609
Hattiesburg, MS 39402-5609 601-264-9320
Date: September 29, 1990
To: Mr. William H.Cooper PPG Industries
Chemicals Division P.0. Box 1000 Lake Charles, LA 70602
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
Sample I.D. AA04886
Sample location: PPGHC
Na Formate TK Sludge tL'
Collected by: COOPER
Collection date: 09/06/90 Time: 12:40
Laboratory submittal date: 09/13/90 Time: 19:00
Received by: JSC
Validated by: RLH
Parameter: TCLP Extraction Method reference: SW846-1311 Result: done Date started: 09/14/90 Time started: 17:15
Parameter: TCLP Volatile Organics Method reference: EPA 624 Result: see appended report Date started: 09/19/90 Time started: 14:46
Parameter: Total Metals Method reference: SW846 3rd Ed Result: see appended report Date started: 09/20/90 Time started: 09:00
Date finished: 09/15/90 Analyst: MJF
Date finished: 09/19/90 Analyst: BB
Date finished: 09/29/90 Analyst: JSC
SL 45846
Mr. William H.CooperPage: 2 September 29, 1990
Sample I.D. AAU4886 (continued)
Parameter: Percent Ash Method reference: EPA Result: 25.7 % Date started: 09/24/90 Time started: 12:00
Parameter: Density Method reference: Result: 1.21 g/ml Date started: 09/17/90 Time started: 12:00
Parameter: pH Method reference: EPA 150.1 Result: 11.95 SU Date started: 09/17/90 Time started: 11:00
Parameter: TCLP Metals Method reference: SW846 3rd Ed Result: see appended report Date started: 09/20/90 Time started: 09:00
Parameter: Semi-Volatile Organics Method reference: SW846-8270 Result: see appended report Date started: 09/20/90 Time started: 11:48
MDL or sensitivity: 0.01 Date finished: 09/24/90 Analyst: ATT
MDL or sensitivity: .01 Date finished: 09/17/90 Analyst: KEL
MDL or sensitivity: 0.00 Date finished: 09/17/90 Analyst: KEL
Date finished: 09/25/90 Analyst: JSC
Date finished: 09/20/90 Analyst: BB
Parameter: Selected Volatile Organics
Method reference: SW846-8240
Result: see appended report
Date started: 09/19/90 Time started: 17:07
Date finished: Analyst: BB
09/19/90
Parameter: TCLP Semi-Volatiles Method reference: EPA 625
Result: see appended report Date started: 09/17/90 Time started: 14:52
Date finished: 09/17/90 Analyst: BB
SL 045847
4
Mr. william H.Cooper Page: 3 September 29, 1990
Sample I.d. AAi/-*886 (continu d)
Data for Total Metals mg/Kg
Component Name
Arsenic, total Barium, total Cadmium, total Chromium, total Lead, total Mercury, total Silver, total Antimony, total Thallium, total Beryllium, total Nickel, total
Data for TCLP Metals mg/L
Component Name
Arsenic, TCLP Barium, TCLP Cadmium, TCLP Chromium, TCLP Lead, TCLP Mercury, TCLP Selenium, TCLP Silver, TCLP
Data for TCLP Semi-Volatiles ug/L
Component Name
1,4-Dichlorobenzene Hexachloroethane Nitrobenzene Hexachlorobutadiene 2,4-Dinitrotoluene Hexachlorobenzene Cresols, total 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol
Concentration
Not Det 110 7 130
Not Det Not Det
14 Not Det Not Det Not Det
480
Component MDL
.1 5 1 3 8 .1 2 10 10 2 5
Concentration
Not Det .9
Not Det .09 .15
Not Det .024
Not Det
Compon nt MDL
. 005 .1 .01 . 03 .04 .005 .005 .03
Concentration
Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det
Component MDL
10 10 10 10 10 10 20 10 50
'S1 045848
--
Mr. William H.Coope Page: 4
September 29, 1990
Sample I.D. AAv-*886 (continued)
Data for TCLP Semi-Volatiles (continued)
Component Name
Concentration
Pentachlorophenol
Not Det
Component MDL so
Data for TCLP Volatile Organics ug/L
Component Name
Benzene Carbon Tetrachloride Chlorobenzene Chloroform l,2-Dichloroethane 1,1-Dichloroethene Methyl Ethyl Ketone Tetrachloroethene Trichloroethene vinyl chloride Pyridine
Data for Semi-Volatile Organics ug/Kg
Component Name
Phenol bis(2-Chloroethyl) Ether 2-Chlorophenol 1.3- Dichlorobenzene 1.4- Dichlorobenzene l,2-Dichlorobenzene bis(2-Chloroisopropyl) Ether N-Nitroso-di-n-propylamine Hexachloroethane Nitrobenzene Isophorone 2-Nitrophenol 2.4- Dimethylphenol bis(2-Chloroethoxy) Methane 2.4- Dichlorophenol 1.2.4- Trichlorobenzene Naphthalene Hexachlorobutadiene
Concentration
Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det
22 Not Det
10 10 10 10 10 10 10 10 10 10 500
Concentration
Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det
610 Not Det
2400
Component MDL
300 300 300 300 300 300 300 300 300 300 300 300 300 300 300 300 300 300
0
1
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Mr. William H.Coopej. Pag : 5
September 29, 1990
Sample I.D. AAU4886 (continued)
Data for Semi-Volatile Organics (continued)
Component Name
Concentration
4-Chloro-3-methylphenol
Hexachlorocyclopentadiene 2,4,6-Trichlorophenol 2-Chloronaphthalene Dimethyl Phthalate Acenaphthylene Acenaphthene 2,4-Dinitrophenol 4-Nitrophenol
2,4-Dinitrotoluene 2,6-Dinitrotoluene
Diethylphthalate 4-Chlorophenyl-phenylether Fluorene
4,6-Dinitro-2-methylphenol N-Nitrosodiphenylamine 4-Bromophenylphenyl ether Hexachlorobenzene Pentachlorophenol Phenanthrene Anthracene
Di-n-Butylphthalate Fluoranthene Pyrene
Butylbenzylphthalate 3,3'-Dichlorobenzidine Benzo(a)anthracene
bis(2-Ethylhexyl) Phthalate Chrysene
Di-n-octyl Phthalate Benzo(b)fluoranthene Benzo(k)fluoranthene Benzo(a)pyrene Indeno(1,2,3-c,d)pyrene Dibenzo(a,h)anthracene Benzo(g,h,i)perylene Benzidine alpha-BHC beta-BHC delta-BHC gamma-BHC Heptachlor Aldrin Heptachlor Epoxide Endosulfan I Dieldrin
Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det
4700 Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det
Compoi
300 300 300 300 300 300 300 1500 1500 300 300 300 300 300 1500 300 300 300 1500 300 300 300 300 300 300 600 300 300 300 300 300 300 300 300 300 300 2400 300 300 300 300 300 300 300 300 300
^ ^50
Mr. William H.Cooper Page: 6
September 29, 1990
Sample I.D. AAu4886 (continued)
Data for Semi-Volatile Organics (continued)
Component Name
4,4'-DDE Endrin Endosulfan II 4,4'-DDD Endosulfan Sulfate 4,4"-DDT Methoxychlor Endrin Aldehyde alpha-Chlordane gamma-Chlordane Toxaphene Aroclor-1016 Aroclor-1221 Aroclor-1232 Aroclor-1242 Aroclor-1248 Aroclor-1254 Aroclor-1260
1,2-Diphenylhydrazine N-Nitrosodimethylamine
Concentration
Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det
Component MDL
300 300 300 300 300 300 300 300 300 300 600 300 300 300 300 300 600 600 300 300
Data for Selected Volatile Organics mg/Kg
Component Name
Chloromethane Bromomethane Vinyl Chloride Chloroethane Methylene Chloride 1.1- Dichloroethene 1.1- Dichloroethane trans-1,2-Dichloroethene Chloroform 1.2- Dichloroethane 1,1,1-Trichloroethane Carbon Tetrachloride Bromodichloromethane 1.2- Dichloropropane t-1,3-Dichloropropene Trichloroethene Dibromochloromethane 1.1.2- Trichloroethane
Concentration
Not Det Not Det
650 Not Det Not Det Not Det Not Det Not Det Not Det
14 Not Det Not Det Not Det Not Det Not Det
5 Not Det Not Det
Component MDL
10 10 10 10 5 5 5 5 5 5 5 5 5 5 5 5 5 5
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Mr. William H.Cooper Page: 7 September 29, 1990
Sample I.D. AAo**886 (continued)
Data for Selected Volatile Organics (continued)
Component Name
Benzene c-1,3-Dichloropropene Bromoform Tetrachloroethene 1.1.2.2- Tetrachloroethane Toluene Chlorobenzene Ethylbenzene Xylene, total c-l,2-Dichloroethene 1.1.1.2- Tetrachloroethane
Concentration
Not Det Not Det Not Det
280 Not Det Not Det
6 Not Det Not Det Not Det Not Det
Component MDL
5 5 5 5 5 5 5 5 5 5 5
Comments: Reference Lab Report No. R1440.
If there are any questions regarding this data, please call.
SL 045852