Document QXkmbeYBeDo3meZJrvka50xLE
CODE RT-698--D ` PKG ^
vNOy-J*^0 1982 L2J45 i^LBS.
'.T^DATE 7
LOT 7 \
< ESI WT
`
PROCESSES
APPROVED^*:
< > RT-698-D (0) EWK 03/22/82
COMTYP JOB NAME: 32RT698DM0 . S7 /%
STANDARD HRS,___________ ..TIME
,
PREPARATION NOTES- _L--^_____________________________________
NON-BLEEDING
EQUIP ' MENT
, NAME: WATCHUNG RED B-
PREF' 'i .
RECORD: _________ BATCHES SINCE SPARKLER LAST!
CLEANED. AFTER. 4 BATCHES, CLEAN, DRESS
I
SPARKLER & PRECOAT WITH 154= DICALITE
FILTER AID J
OBTAIN FOR $11,2-CHLORPt 4-AMINOTOLUENE-5^
SULFONIC Ato/
IN FOR S40 3-HYDROXY-2-NAPHTHOIC ACID
INSTALL pV K CV RECORDER G CONTROLLER CHART
NOTE : NOTIFY PRESS ROOM BEFORE ROPING. OFF /
AREA UNDER V-922
TE: RUN 15* WATER <ENT.O V-904. PUMP WATER
FROM V-904 THRU.DISTRIBUTOR. IF WATER DOES
NOT COME OUT OF ALL DISTRIBUTOR HOLES WITH
FULL FORCE, NOTIFY SUPERVISOR
I J/H RUN,
X494G? WATER* INTO V-%g? U HEAT TO
1 . ixBO-100 BEG F
ADD IN 8-9 MIN DRESINATE X
r i. ;STIR 5 MIN L RECORD: PK^JZiL.-(9.5-1 0.5)
S^\ STIR 20 MIN OR LONGER TO DISSOLVE FOR S50
j I
8S 530-B^bS?
922 UN 35* (721G) WATER.INTO V-922 3 IGN'SODIUM HYDROXIDE IN V-92<
, . . j TURN ON AGITATOR L STEAM 6 DUMP IN FROM S2 \
CMtA'MWfQ U2-CHL0R0
__LOT
4 A4--AMMTIWNOnTTOLUENE
4100%
lLek\
5-SULFONIC ACID
7-P 740-C
212 1086.
DUMP IN ACTIVATED CARBON
t l4f>SUMP IN FILTER AID IVPn>EAT TO 212-2.14 DEG F
WATCH-FOAMi i i
|15^T RECORD: BY_j*rI< + > IF NECESSARY ADJ TO
| j/J-BY
ASSUME 503
25 1
|16>n STIR 30 MIN AT 212-214 DEG F, THEN SHUT OFF i lySTEAM. WATCH FOAM. RECORD: SPARKLER PRES-- | / SURE _Q___ F'SI IF NOT ZERO NOTIFY SUPVR.
11y \ CIRCULATE 15 MIN OR LONGER THRU SPARKLER | | UNTIL SOL'N IS CLEAR. MAINTAIN*^!. 190-195^ FJr~
| I FOR SI 9. RECORD: STARxU-&-SJfc- TOTAL MIN^_! I ! CLARITY^^^L HTF & RECjf^L_ F i
113-B 777-A
7-D
i'jOVlOjg^
25. I
"'s
LU I = *______ _ uun I I r JUP PtMI'lC - J*ruol/ng
.1 n sr .*mm W *
EQUIP j ,s I WENT j I 1*A6E 2 OF 3
| USE CG 32 CODE RT-698-D (O) I LBS
904/CVj
2* (5SG) WATER INTO V-904/CV
4 | I^T WHEN 21? COMPLETE, PUMP IN V-922 THRU
I I SPARKLER. MAINTAIN V-922 AT 190-195 DEG F
I 1 RECORD: START^4tel^T0TAL MIN,/i2:___ _
I I
| f
902 . I 2^mT*RUN 65* C1696G) WATER INTO V-902
5 UrfWH DUMP IN CALCIUM HYDROXIDE 6 STIR TO SMOOTH I
I N-CODE I
ACCT LBS
MXSC 4
1 2IK1h EASURE SL3J&1 UNITS IN V^928 FOR J35., I
| [HYDROCHLORIC ACID
M__\J?______ iZQxSJZ^ I
|&S*'fwElGH SODIUM NITRITE IN PT .FOR S3S _>
h--AQ.___ _,sJc_Zfe__% 1
'I WEIGH SODIUM NITRITE IN DR^M FOR^43
922 WHEN- S19 COMPLETE, STOP PUMP & INSERT V-9221
?~ OT PLUG.
|
RUN IN 10* C20OG)'WATER & HEAT.TO 190-195 FJ
! I CIRCULATE 15 MIN- THRU- SPARKLER
I
904/CVU25AI PUMP V-922 THRU SPARKLER INTO V-904/CV
Oil
*.
if -
' " 'i --` --
I WEIGH SODIUM HYDROXIDE IN &.nTr \`A
M_
L%
S4J,,
1 .; 1
\37A\
I'-** 1
RQULATE 15 MIN THRU SPARKLER
95 r~ 1
1
J
1 7-D i 194 #f (
} I
MP V-922 THRU SPARKLER- INTO V-904/Cy
WHpT MTY BLOW OUT SPARKLER INTO V-904KCV
UR IN IGEPAL CO-430
- "tj I 63 } 979-D I 48
I HEAT TO 165-170 DEG F FOR S34
'-T '
I NOTE: IF N-740-C SOL'N WAS PUMPED DIRECTLY I
QM SPARKLER TO CV OMIT STEPS 37 6 38
J'
CV
IN 1* <95G) WATER INTO V-JzSZi
I
12 WHEN S32 COMPLETE, PUMP V-904 AT `165-170 F I
j THRU UNDERSURFACE DISTRIBUTOR INTO CV AFAP I
I <12-15 MIN). MAINTAIN 165-170 DEG F IN CV I .
} i^RECORD: START__,_______ __TOTAL MIN_________ ___ I -
135*1 RUN IN N-28-D FROM S22 IN 12-15 MIN
L
}36^VSlTIR 15 MIN AT 165-170 DEG F. \ :.
I
13^1 ADJ TO 46* (4347G) AT 32-38 DEG F [ L^RcCORD: TEMPjSS_fL_DEG F,VOLUME__________*
r,|<4X330
IZST SdN IN N-725-A FROM S23 AFAP (5-10-MIN)
1
I >r & RINSE IN PT'
J
|;3T STIR 30 MIN AT 32-38 DEG F MAINTAINING 1 I
I +CR, +KI FOR S40. RECORD TIME START_____,__1
I CR_.________ < + ), KI__l______:<+)'
I
I NOTE: N-28-D HYDROCHLORIC ACID XVS IS LOW |
I FOR THIS PROCESS. BE VERY CAREFUL WHEN
I
I CHECKING CR+-. IF YOU LOSE +CR, YIELD WILL I
I BE LOW.
* ^i
f *
~=:-<-kr
l
i ,, ; 57-A 1l&>
I. V.:;..-
: 1 HS&i I*1
DUP050060887
LOT=> -ikj'f.
es u iPT
WENT I
COMTYP JOB NAME = 32RT698DM0 PAGE 03
_________________ _________ ______
7" !"TM"'
11
I PAGE 3 OF. 3 CG 32 CODE RT-698-D <0)
DATE PRINTED: 8/10/82
I USE I LBS
N-CODE I ACCT j LBS
,Cy -12
CQNT r.
| I NOTE i> IF CR-,KI- ADD 20* *AS IS* INCRMTS |
I 1 HYDROCHLORIC ACID
I
I I RCRD: CR_______( + ) KI____< + > ASSUME -32%
. I 3.yI
i I 2) IF CR+,KI- ADD 20* ;*AS IS* INCREMENTS. |
1 i SODIUM NITRITE
|
1 LjaetfD: CR
( + ) KI ___ < + ) ASSUME "33%
|
14DUMP IN FROM S3 & STIR 10 MIN
LOT
3-HYDR0XY-2jiNAPHTH0IC ACID
i__JL.\
| DUNLIN ^fixi^^HLDRlDE
^
lA^TAD^-FOR MAINTAINING 32-38 DEG F THRU S46
l*"448"j ^X330|
28-D
i
,
725-A I,_____ 82-C | 994
20-A | 448 57-A }&%sh
902 1 N725A SODIUM NITRITE FR S24 INTO V-902 J
13 IN AMMONIUM CHLORIDE
I
165-A 245
CV
I IMMEDIATELY AFTER S44 COMPLETE, WITH V-902 I
|
14
I AGITATOR ON
PUMP V-902 THRU UNDERSURFACE I L
!
i DISTRIBUTOR INTO CV IN 18-22 MIN. MAINTAIN !_______ | 57-A
32-38 DEG F^ N CV . RECORD STARJ.*#*#^..
1; J<TOTAL MIN,,j&fc____
-------
14^1 SJ*ff 3 MIN 6 RECORD: RH^iTiS___ (510-6.0) j
1 j>-i'EMP__
i.DEG F <32-38 DEG F)
I
i^T> RUN IN. PT SODIUM HYDROXIDE FR S28 THRU UN- |
J j ^\ DERSURFACE. LINE, RINSE IN PT"& STIR 15 MIN.|
RECORD PH:i*^<9.-9.8) , IF-PH IS BELOW 9.0L
JR | ADJ TO E'H-9.0-9.8 SODIUM HYDROXIDE .
I / <&,\\
\77reZ/?pf~- m39*VF" . A^ . sh.: ASSUME 550077. I / oO I
ND RECORD: PHiL_ DIA|0^1___<-)
1I
MASE__3L___< +) HYDROCHLORIC ACID ASSUME 323 TEAM EJECT V-%| FROM S8 INTO CV `
-I___ ___ I J*
OUR IN I OCTANOL
I 32
r^THEAT TO 173-175 DEG F IN 55-65 MIN AND.-
j
J
SZ-C .j JO
i 96
l
28-D I______
!588--A I
32
1 1 run Tun: f
g ni ifir R*}^ffiTmiE ~i alrriHf j
1
DURG S52 HEATG, RUN 10*<268G) WTR INTO V902I
I
URN ON AGITATOR 6 STEAM h DUMP IN BARIUMj 110 I
CHLORIDE
II
CV .J&f'i|1 WHHEEANT ST5O2 1C5O5M-1P6L0ETED,EGSTFRI6KESTUIR-9.0T2O ADTISS15O5L-V1E60' F 1
|
16 THRU UNDERSURFACE DISTRIBUTOR INTO CV IN, 2-3 MIN. RECORD: START^i^-TOTAL MIN_JL___
HEAT CV TO 193-195 DEG F IN 10-15 MIN
STIR 60 MIN AT 193-195 F. RECORD ^TART/2^^
AFTR '20 MIN S59 STIR RECORD PHjk-> C8.8-9.3)
IF NECESSARY, ADJ^TO PH 8.8-9.3 ASSUME 507 &__
AND RECORD : Ph M.___
ASSUME 327.
AFTR S59 STIR FLOOD TO 180-190* (+/-18000G)
.\ 16-B \ no
4 \ i 1
7-D I. 28-D
AND STOP AGITATOR
:
WHEN INSTRUCTED BY PROCESSING AREA HALF WAY
J THRU PRESSING, DUMP IN I OCTANOL, STIR 5
| MIN 6 STOP AGITATOR* RESUME PRESSING.
10
588-A
1
,, STA. Jt'JiO.
m
DUP050060888
(
4<
#
'*> *>
/
f
i
5
DUP050060889
DUP050060891
DUP050060892
DUP050060893