Document QXBokgzYqm63LLJvVyyrjNqO6

CG 32 ..VDATe I CODE RT-87G-D PKG _ KZK71 ("l o t ) ( EST WGT ) PROCESSES- APPROVED BY ( >ET-870-D (H) EWK 1-11-82 COMTYP JOB HAHE: 32RT870BMH TYPED BY: JMH - STANDARD HRS.________ _ TIME _//_5_M . PREPARATION NOTES'. EQUIP I MENT j NON-BLEEPING NAME: WATCHUNG RED B USE LBS I NOTE: BO NOT START IF PRESS HILL NOT BE i AVAILABLE WITHIN 3 HRS AFTER MAKING. SUPV ! TO REVIEW WITH P.R. SUPV , RECORD: I PRESS WILL, BE READY______ M_____ /__ PR SUPV. I srm^r^Kim_______ m/ma k in g s u p v . L*-Nt?TE: fjOT5TY PRESS ROOM BEFORE ROPING OFF 1 ---- AREA UNDER V-922 GTE: RUN 15' WATER INTO V-904. PUMP WATER FROM V-904 THRU DISTRIBUTOR. IF WATER DOES CpME OUT OF ALL DISTRIBUTOR HOL WITH FORCE, NOTIFY SUPERVISOR. ! RECORD:___ L___ BATCHES SINCE SPARKLER LAST CLEANED. AFTER 4 BATCHES, CLEAN, DRESS SPARKLER & PRE-COAT WITH 15* DICALITE, F.ILTER AID. QBt^iff FOR S11 2-CHL0R0-4-AMINGTQLUENE-5FDNIC ACID, R S27 3-HYDR0XY -2 -NAPHT H 0 ID ACID DV & DV RECORDER i, CONTROLLER CHART N-CO.DE ACCT LBS 777--A ,! 740-C i 82-0 ] 100G) WATER INTO V- & ADJ TO B-100 DEG F L-#DJ> IN 2-3 'MIN DRESJNATE X . STIR 5 MIN - RECORD PH_^C>/JL_,(9.5-1 0.5) TIR 2 MIN OR LONGER TO DISSOLVE FOR S49 | ( 108 530-A 101 35s (722G) WATER INTO V-922 SODIUM HYDROXIDE IN V-926 i, RUN IN ____, c. iT&/ & % TURN ON AGITATOR L STEAM i DUMP IiTf RGM S2 4-AMIN0T0LUENE , jifMt ! JDH*I NIC 7-D 74G-C 2l 1 08 fZJH ACTIVATED CARBON HP IN FILTER AID TO 21 2t 2 1 4 DEG F WATCH FOAM!! RECORD: YJ=p:_(--} IF NECESSARY ADJ TO -BY SODIUM HYDROXIDE ASSUME 50% STIR 30 MIN AT 212-214 DEG F, THEN SHUT OFF STEAM WATCH FOAM! NOTE: RECORD SPARKLER PRESSURE ...Q.___ PSI. IF NOT ZERO NOTIFY SUPERVISOR, o to LOT= ; COMTYP JOB NAME - 32RT870DMH. PAGE 02 BATE PRINTED: 7/19/82 e q u ip ' II MENT 1 I PAGE 2 OF 4 CG 32 CODE RT--.870-D I USE <H)I LBS I 1>^CIRULATE 15 MIN OR LONGER THRU SPARKLER | ' | N-CODE | ACCT I I LBS ! I 1 UNTIL SQL'N IS CLEAR, MAINTAIN, AT U 90-1 95/ I I BEG F FOR S22v RECORD : START_ *' I I TOTAL MIN.O^--^ CLAR_____ I 1 HT________ .F & REC F ii . 1 I^^MIEASURE SENNITS IN V-928 FOR S39 , I | 1 I i I \ <1 I /i i HYDROCHLORIC ACID J IGH SODIUM jtfTTRITE^IN PT^QR SA WEIGH SODIUM NITRITE IN 5r u M~F0R_SM.^ M,,j_____ 3&J3BLX 28-D | 438 397 43 1-2^1 RUN 2" <530 WATER INTO V-9i^/CV |22^TWHEN SI 7 IS COMPLETE, PUMP. IN V-922 THRU i i SPARKLER, MAINTAIN V-922 AT 190-iy5,. RECORD: START_A_t_^TOTAL MIN_. i I 9"?o I WHEN S22 COMPLETE, SHUT OFF PUMP-AND INSERT) 6 f22 FOOT PLUG 'i RUN IN 10' <2090 WATER & HEAT TO 190-195 FI i CIRCULATE 15 MIN THRU SPARKLER l ! S#"4/CV 7 I AND PUMP V-922 THRU SPARKLER INTO V-S58W/CV: 1 .} 902 8 I \WZ\ I RUN 65' <16960 WATER INTO V-902 SODIUM HYDROXIDE IN V-926 6 RUN IN M_Jl Ij E____I Ol Ll -/. - DUMP IN FROM S3 3-HYDROXY- LPT ^-NApiTHDIC ACID I^Arf^J>PCr70-90 DEG F &~STIR TO DISSOLVE _m_ i i >i U i______i j 7-D j 8.2-C i 399 994 12 w/cvi 10 I RUN IN 5* <104G) WATER & HEAT TO 190-195 F j I CIRCULATE 15 MIN THRU SPARKLER . I ___1_____ __________ THRU' SPARKLER INTO V-93H/CV ! OUT SPARKLER INTO V-$i4/CV | ALKANQL XC IN 20G WATER AT 150-160! HOT WATER MIXER IN DRUM & POURIN. I HEAT TO 165-170 F FOR S38 .I 32 I 133-B I 32. RUN Tj8*T <3280 WATER INTO V-932 6 AD.J TO 't DEG F'. W I ADD IN 6-7 MIN DRESINATE X 135 ) STIR-5 MIN & RECORD PH.._____ _<?,5-10,5) 136 ) STIR 20 MIN OR LONGER TO DISSOLVE FOR S59 !1 33* V T 530--A 378 f \.... DUP050102116 __uun i i r j u u rHnt = i a i,yunh t-HUt W5 Dfl I t PKINjED: 7/19/82 C5U2P i USE N-CGDE ACCT rlENT PAGE 3 OF. 4 CG 32 CODE RT-870-D CH) LBS LBS --l~--I--*r~ NOTE: IF N-740-C SOL. WAS PUMPED DIRECTLY FROM SPARKLER TO CV S21.,24B,29 OMIT S37 6381 137 ! RUN 1* (95G> WATER INTO . | j j I PUMP V-904 AT 165-170 DEG F THRU UNDERSUR- | | FACE DISTRIBUTOR INTO CV AFAP <12-15 MIN) 1 j RUN IN N-28-D HYDROCHLORIC ACID FROM Si 8 IN] ! 12-15 -MIN, MAINTAIN 165-170*F IN CV. |j IR 15 MIN AT 165-170 DEG F ADJ TO 46* (4347G) AT 32-38 DEG F ^ ECORD : TEHP__DEG f, V0LUME_ij^__ * || 154X330] j| 57"A j /7&Z> i 7 ... RUN IN N-725-A SODIUM NITRITE FROM SI 9 AFAP1 | (5--1^0 MIN) 6 RINSE IN FT 'J ] NQTE: PROCESS HAS A VERY LOW N-2S-D EXCESS J CHECK CR VERY CAREFULLY J| STIR 20 MIN AT 32-38 DEG F MAINTAINING/- . | +CR, +KI FOR S44. RECORD, TIME START^I^pspfl ' _ CR___^:'_^, KI NOTE: j 1)' IF CR-, KI-- ADD 20* "AS IS" INCREMENTS j 57-A I; ! RECORD CR______< + > KI____ HYDROCHLORIC ACID ' ASSUME 32% 2) IF CR+, KI- ADD 205= "AS is INCREMENTS- RECORD CR______ < + ) KI.__.__<-f-) 28-D 1______ SODIUM NITRITE ASSUME 33% 725-A DUMP IN CALCIUM CHLORIDE i 1026 1 20-A 1026 45 1 ADD FOR MAINTAINING 32-38 DEG F. THRU S55 132X330] 57-A FILL PT APPROXIMATELY 1/2 FULL 'WITH 90-110*1 T WATER FROM HOT WATER MIXER ] Ju mp in s t r o n t iu m n it r a t e ] STIR 30 MIN OR LONGER WITH LIGHTNlN MIXER ] TO SOLUTION FOR S58 | 68 1. 246-B/E ] 68 J i. WHEN S28A COMPLETE, 'STEAM EJECT V--93T/931 FROM 58 INTO 'V-902 . OUR IN N-725-A SODIUM NITRITE FROM S20 ADD AMMONIUM CHLORIDE 213 1 165-A ] 213 1 CV IMMEDIATELY COUPLE V-902 THRU UNDERSURFACE 1 15 DISTRIBUTOR INTO CV IN 18-22 J1IN. RECORD: \ START^V!5/%_ TOTAL MIN_Z^P_______ _ 1i PT DURING S52 WEIGH SODIUM HYDROXIDE IN PT. | 16 7-P ] 140 DILUTE TO MAXIMUM VOLUME (+/-100G) FOR S56 ] | CV WHEN S52 COMPLEfE, STIR 30 MIN 6 RECORD: 1 17 DIAZ0_L-2!h.__< + ) BASE__i_____< + ) 1 PH^,,jrjf2_<5.0-6,0) TEMP_1&L_< 32-38 F) i RUN SODIUM HYDROXIDE IN PT'FROM S54 THRU 1 DERSURFACE LINE, RINSE IN PT 6 STIR 15 MNi RECORD: DIAZO . BASE_t:_____( + ) | PH 5l ^_(9.0-9.8) ] RUN IN STRONTIUM NITRATE N-246-B,ESOL'N | ROM S48 6 RINSE IN PT ?j STEAM EJECT IN V-932 FROM S36 STIR 5 MIN 6 RECORD: PH(9.0-9.8) ] ] % I DUP050102117 -H j i-- H* 1 il -oi ' Sm Co Ii ! i i o -j x. COMTYP JOB NAME = 32RT87DDMH PAGE 04 DATE PRINTED:'" /i9/82 PAGE 4 OF 4 CG 32 CODE RT-870-D (H) USE 7~n "c o d e~ i A COT LBS I LBS I IF PH BELOW 9.9 ADJTO PH 9.0-9.SWITH { N-7-D ONLY. RECORD PH _ i 3DIUM HYDROXIDE ASSUME 50% | IN I QCTANOL ! HEAT TO 193-195 DEG F IN 70-J5 MIN & RECORD! ' '1T_/Jl&__DG F ANDREC_/5L4.__DEG F [ STIR 60 MIN-AT J93-L95 DEG F. .' { .RECORD: START * I T AFTER 20 MIN S64 SflR RECORD: . PH I8r& (8.8-9.3) PH BELOW 8.8/ ADJ TO PH^8.8-9.3 WITH N-7-D ONLY. RECORD PH___ WJ?-- ASSUME 50% I AFTER S64 STIR, FLOOD TO 180-190" I (+/-18,000G) AND STOP AGITATOR I 33 &> I 7-D 588" A 38 7-D SCI I WHEN INSTRUCTED BY PROCESSING AREA HALFWAY i 1 I I I THRU PRESSING, DUMP IN, STIR 5 MIN & STOP [ 10 i 538-A ] 10-- I i AGITATOR. RESUME PRESSING. - .! \' i ! ! \ DUP050102118 DUP050102119 k- Co7>S: Zl 'P'fO -c- X^ / V^::4 De u m srevc/t. g~z> MgmftEK Cfj G<^K- u>E!& ft , X e>T ._ ,^'^a W?*i 'X^9L. . .~T`!#t.Ui'&Y 3*0*- isrM' :rv*<- . *(,*?*.*:% `7*?r Net S/?oss T#VK der ^-/eid/o 3ar 32-5" ,3LC 3:S52i ' 55H<? ^JSJ' 3&o m 1=) iq L-e F*rsr v>; : - -- 0"S "3 fcJe* -L>Q/^a 3150 33 J qq 3 /--i-' rtf ; V > | IO%3 /O^A.. -. .*- * ?':/;' " - f A/- A c^r o$<& .... ;Sv3^^ 24^" /J* jL ifa&Q /6> a.<rc .. -{ : 9? ..... -- -- ................. ........- 2.L& J4> a& <? . /T &lLC j S 2. sc 5LSL aS? . mv i . DUP050102120 DUP050102121 DUP050102122 DUP050102123