Document QJaL3Yzyj2ogXKgXgdNb6Xzyo
J. L. Ledbetter - B-2-N L. F. Steinbech - G-4-E
R. J. Stratmeyer - B-2-N N. L. Sample - B-2-N A. H. Sohwab - JFQ H. A, Partlow - JFQ R. D. McIntosh - JFQ
f -+*-*1*4-, it** hJ e l
bbH ~
J. R. Kellogg - JFQ H. L. Minckler - B-2-S T. M. Patrick - Res. 1 R. E. Keller - Res. 1 D. C. Reed - Res. 1 0. J. Marchand - Res, 1
MONSANTO COMPANY Organic Chemicals Division
To the Qeneral Manager Organic Chemicals Division
Estimate No. 1908 Dept. No. 76001.0000922 Plant - RtD Laboratories
hit fLsJy ~*fi**,
, v-'a. iFU. .-vs..
A9'>/-c '~<C-
c*'": < i 'C.
ax+At A+ l-,-`( ft. ^
<*,( r &!C,tfi
tUc 0
T CAa '-'z j n *"( 6 ` ^
F F fi'
,
PURCHASE BIOMEDICAL GAS CHROMATOGRAPH
Capital Addition
87,000
DESCRIPTION
Purchase biomedical gas chromatograph with all-glass system and multiple flame ionization and eleotron oapture deteotors for the analysis of thermally sensitive and polar materials,
APPROVAL General Manager
H. l. Minoxier
Dafe
EXHIBIT WBP M-27
HONS 034702
LEXOLDMONOOO119
t
Estimate No. 1908 Page 2
NEED FOR THE PROJECT Late in 1966 Swedish researchers reported the presence of poly chlorinated biphenyls in a variety of biological samples. Since that time the Organic Chemicals Division has received a number of requests for Aroclor samples from active pesticide research groups. We also know that the U. S. Public Health authorities have initiated studies to evaluate the significance of this environmental contamination. To assess the validity of these findings, the impact they may have on our Aroclor business, and to avoid restrictive legislation, the Functional Fluids Business Group has begun its own study. The Applied Sciences Section has been requested to develop the necessary analytical methodology for this project. To do this and to do it correctly, we need to purchase a biomedical gas chromato graph. This instrument is designed specifically for this type of analysis and is used by most pesticide researchers, including the Publio Health authorities. Any analytical information we generate will be judged in terms of the techniques and equipment used. By using the tools most familiar to these people, we feel any information we provide will be more effective. The biomedioal-type chromatograph provides an all-glass system with direct injection into a U-shaped glass column which is attached directly to the base of the flame ionisation or elaotron capture detector. This allows high efficiency analyses to be made on pesti cides, steroids, organo metallic* and polyfunctional organic chtmioals which are thermally or catalytically unstable or have polar functional groups that, in the environment of the ordinary gas chromatograph, cause them to decompose or become irreversibly adsorbed. The KD Labs do not at present have such instrumentation. Therefore, we recommend purchase of such a ohromatograph for initial use on the environmental Aroclor project and to broaden the capability of the Applied Sciences Section in the gas chromatographic analysis of unstable organic systems.
HONS 034703
LEXOLDMON000120
Estimate No. 1908 Page 3 STATUS OF THE PROJECT No commitments will be made until this project is approved. RECOMMENDATION It is recommended that this project be approved.
Submitted by E. M. Emery" Group Leader R. E. Keller Research Section Manager T,. "M; Patrick ^Manager R8D Laboratories
mw 8/28/88
HONS 03*704
LEXOLDMONOOOI21
A23C-C
PROJECT AUTHORITY FOR EXPENDITURE
and/or retirement
(THIS FORM TO BE USED FOR AUTHORITIES REQUIRING GENERAL MANAGER AND LOWER LEVEL OF APPROVAL)
PLANT
BUDGET ITEM NO.
DEPT. NO.
DATE
ENG. JOB NO.
Org. RSD , Laboratories
76001-0000922
DESCRIPTION. REASON AND JUSTIFICATION FOR WORK:
8/28/68
AUTHORITY NO.
1908
Purchase Biomedical Chromatograph
PREPARED BY
Marchand
ITEM
REVIEWED BY
GENERAL HGR.
DESCRIPTION
DATE
1. 29-4976, Chromatograph 29-4977, Recorder
29-4978, Integrator
*
PRODi HGR.
APPROVALS
DATE
PLANT MGR. .
.1
DATE
|
OTHER
DATE
EQUIPMENT
TRANS,
NEW
CONTK. WORK
MAT, ft STORES DIRECT SUPP. O'HEAD LABOR
SHOP O'HEAD
TOTAL
7000
7000
1-1908-29/76001-0000922 Life - 5 years (U Bldg.)
INFORMATION FOR RETIREMENTS
SUMMARY OF ITEMS TO BE RETIRED
INFORMATION FOR EXPENDITURES
CLASSIFICATION OP AMOUNT AUTHORIZED
PROJECT SUMMARY
1. INSTALLED COST
6. CAPITAL EXPENDITURE
7000
2. VALUE NOT RETIRED *. VALUE TO BE RETIRED
.9 REPAIR OR OTHER EXPENSE
..... . 10. LEASEHOLD IMPROVEMENTS
.4 ACCRUED DEPRECIATION
ON VALUE TO BE RETIRED
| DEPRECIATED VALUE
f <)!)
8. AMT* EXPECTED FROM
SALE. TRADE-IN; ETC.
>. numi MI NT LOSS (.*>
XU TRANSFERRED EQUIPMENT
12. DISMANTLING EXPENSE <
:
13. TOTAL AMT. AUTHORIZED '
7000
fl ; f: ff* -I 11 *! 1
P 1ft
8 ?... UVH IOft CAPITAL APPWOVA1
ur;r.' FORM A-B23-I TO DETAIL RETIREMENTS
Ut PROJECT TOTAL (ORIG OR REV.I
......... 1 t--:-------
IS. LESS PREVIOUSLY AUTH;
t, PROJECT TOTAL ^ THIS REQ.
; (u.i5> *
17. LESS TRANSFERRED EQUIP*
18. NET CASH REQUIRED
! (16-17)!
I =IS. AMOUNT AUTHORIZED
(16)
j , i ..
.
MON-MT-008602
7000 7000
7000 7000
LEXOLDMONOOQ122
RSD Laboratories - South Second Street
September 13, 1368 Hewlett-Packard Company
r, Eiaery V*. Tucker
Purcnaso Order AT-9430
Vernon Fox Stores - J.F.Q. Plant
Sometime ago an instrument containing a radioactive source material was lost before reacidng the Research department, At that tiraa we instigated the following procedure for subsequent orders of like material or equipment:
"This order requires SPECIAL handling* Upon receipt of this equipiaehf ih the JFQ Storeroom, please inform:
Dr. Scott Tucker Station 3439
Please deliver this equipment DIRECTLY to:
Dr. Scott Tucker . Lab 213, U Building
DO HOT LEAVE EQUIPMENT AT ANY DELIVERY STATIONS."
Attached is a Xerox copy of the Purchase Order. Since there is not space on the order to type this statement, will you please take action to insure that the procedure ia carried out.
0, J. Marchand raw
MON-MT-008603
LEXOLDMONOOQ123
UcQuiSiYiOi] TO PURCHASING DEPARTMENT
INSTRUCTIONS TO REQUISITE |R
1. THIS FORM MUST BE TYPEWR.lTEN
2. DO NOT fill IN SHADED AREAS
3. REMOVE'1ST. COPY FOR YOUR FILES
DEl. MO'O.
ESt. COST
I/13/G8 2 wks. $6785
INQUIRY NO.
iii knowni Hewlett-Packard ' 8 r2` SYTYrentwood TJIycTT
L St . Louis, Mo. 63144 ' ~ Attn: Hr. Lou Anderson
REMARKS
PURCHASE Ot^\yi->vU*^A
DATE IOC. NUMBER
RENQUUMISBITEIRON
AT- 9-3
r.o o. poini
FREIGHT TCfiMS
Route EMERY AIR FREIGHT
TEAMS
1
2011 Kosciusko St. Louis, Ho. 63177
P.C. MC OR HIM NO. QUAN1ITV
1. 1 2. 1 3. 1
UNIT
ea. Model 402 Basic Dual Flame Ionization Detector Gas Chromatograph
ea. Model 71-27A Moseley single-channel recorder
ea. Option 03 Electron Capture Detector .with high temperature NT63 foil (installed)
ea. Recorder Option 07 - Disc Integrator (installed)
$4000 $1100 $1000
$ 685
A.E.C. License No. 24-01.113-14-Amencjlment 07
NOTE:
CONFIRMING ORDER
This order was verbally placed by our Dr. E. Emery to Mr, h. Anderson to an instrument; however, no Purchase Order was issued.
SALES TAX
use iax
EXEMPI
ORDERED
; f.E.O.C. MATERIAL TO
Marchand j ir-APii.vci.il Appiiovji
S. Tucker,
STANOAROS APPROVAC
Pi a}isJ=AiuJL,
Lab
213
OEPI.
70001-0000922
DATA REQUIRED
gi: number'
MAIN sun Cl ASS
17-19
2 64
30} 1 *00
71-U
--..... - ---
1 " - -------- --
-- - --.. - .....
- -............ . ..._
i.... -- -............... . f------------ ~ ... -------- --
VENDOR NO.
2C. -49^o - Chromatog rap n 21 14977''- 'Re'cbrder' 2 -49]T8~ - Integrate
r
..j________
i
--------I1~-------1__
RECEIVING REPORT PURCHASING APPROVAL
JOB NUMBER
1-1908-29
OrOOR.. 7/67
MON-MT-008604
flFOUi<;moMF'<; ropv
LEXOLDMONOOQ124