Document QJNm44wQKYg95mp1bmkXOOZo6

J waiter c. me crone associates, inc. CONSULTING: ULTRAM1CR0 ANALYSIS MICROSCOPY SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 14 June 19.77 Dr. Joseph P. Simko, Jr. Colgate-Palmolive Company 909 Biver Boad Piscataway, New Je rse y . 08854 . . Dear Dr. Simko: Using transmission electron microscopy and selected area electron diffraction, we have analyzed a sample of talc designated as Lot no. 6-1-2. We found no asbestiform minerals in this talc. A general description of this talc is as follows: some of the talc showed shards and rolled talc, the level of fines was moderate and the talc particles were generally equiaxial rather than large thin plates. Thank you for consulting McCrone Associates. If there are any further questions concerning this report, or the data herein, please feel free to contact me. Very truly yours, GEG:jd Bef. MA 5500 G. B. Grieger Senior Besearch Physicist PLAINTIFF'S EXHIBIT CAM-95 2S20 SOUTH MICHIGAN AVENUE CHICAGO. ILLINOIS 60616 312/S42-7100 CABLE: CHEMICRONE QE-CPC00004076 H ^oooow o QE-CPC0Q004077 P R O J E C T COST RECOHD PROJECT TITLE: Talc samples_______________________________ PROJECT NO. ; MA3884 SPONSOR:_______ COLGATE-PALMOLIVE COMPANY_______________ DATE RECEIVED 3/12/74 ADDRESS:________909 River Road________________________________ P.O . NO. : 615139 _________ Piscataway, New Jersey 08854 ______________ COMMITMENTS.'$ Contact: ______Mr. J. P. Simko, Jr._______ SUMMARY OF PROBLEM: Telephone No. Lab Notebook References: No. pp. Initials No. pp. Initials No. pp. Initials Photomicrographic record no. Sample disposal: returned filed (where) discarded Individual1 time \(:Etlxmceluosnivinesot.f oper. below) Date Name Hours Charge ijD O t ; ctjf.ti.*Sr DIRECT COSTS Trave1 , Date ' Traveler Destination Instrument time Date SEM TEM XRD EMP IMP ESCA Outside Services flours Charge Date Photo ~ i%0c r Photo Materials Supplies r <-f ro Company i Charge Summary Cost Individuals $ Instrument Travel Outside Other y Cost Total Charae $ urL ior dtiling , Project Ldr Group Ldr PROJECT LEADER ROUGH DRAFT REPORT RECEIVED IMS TOTAL CHARGE $ O-ft' BILLED TO CLIENT $ ~~7 J (*) INVOICE NO. (S) QE-CPC00004078 Review waiter c. m ccrone associates, ine. CONSULTING: ULTRAM1CR0ANALYSJS MICROSCOPY SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 26 March 1974 Mr. J . M. Simko, J r . Colgate-Palmolive Company 909 River Road Piscataway, NJ 08854 Dear Mr. Simko: As per your request, we have examined three ta lc samples, 85, 120 and 123, th a t you had submitted to us fo r c h ry so tile and trem olite analysis using TEM and SAED methods and have seen no evidence of ch ry so tile or of fibrous amphiboles in any of the samples. . We noted fibrous inorganic m aterial in a l l samples - some of which resembled ch ry so tile or trem olite. However, on consideration of the d iffra c tio n p attern s from these fib e rs , we found them to be nona sb e stifo m mainly "ro lle d ta lc " or h a llo y site (one of the kaolin group of m inerals). have appended representative photomicrographs in order to show ty p ic al m aterial and how closely some of the fib e rs resemble (morphologically) ch ry so tile or one of the amphiboles. Thank you fo r consulting McCrone A ssociates. I f you have any questions regarding the m aterial contained in th is rep o rt, please do not h e sita te to call. Yours sincerely Enclosure RS:smg Ref. 3884 Richard Shimps Research Chemist QE-CPC00004079 Memo from FRANCES EINBINDER . Z0| X ? ' i J U r vS , QE-CPC00004080 waiter c. mecrone associates, inc. CONSULTING: ULTRAMICROANALYSIS MICROSCOPY SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 26 March 1974 Mr. J . M. Simko, J r . Colgate-Palmolive Company 909 River Road Piscataway, NJ 08854 . Dear Mr. Simko: As per your request, we have examined three ta lc samples, 85, 120 and 123, th a t you had submitted to us fo r c h ry so tile and trem olite analysis using TE4 and SAED methods and have seen no evidence of c h ry so tile or of fibrous amphiboles in any of the samples. We noted fibrous inorganic m aterial in, a l l samples - some of which resembled ch ry so tile or trem olite. However, on consideration of the d iffra c tio n patterns from these fib e rs , we found them to be nonasbestiform mainly "ro lle d ta lc " or h a llo y site Cone of the kaolin group of m inerals). I have appended rep resen tativ e photomicrographs in order to show ty p ic a l m aterial and how clo sely some of the fib ers resemble (morphologically) c h ry so tile or one of the amphiboles. Thank you fo r consulting McCrone A ssociates. I f you have any questions regarding the m aterial contained in th is re p o rt, please do not h e s ita te to c a ll. Yours sin c ere ly , Enclosure RS:smg Ref. 3884 Richard Shimps Research Chemist Zfli'O SOUTH MICHIGAN AVENUE CHICAGO. ILLINOl COGIO 3I2/SM2-7T0I - CABLE. CHEf.llCROHE QE-CPC00004081 De c e i v e d H M ? z t o COLGATE-PALMOLIVE COMPANY.... RESEARCH AND DEVELOPMENT DEPARTMENT 909 River Road PisCata-way^ New Jersey 08854 March 8, 197^ Mr. Ian Stewart McCrone Associates 2820 South Michigan Avenue Chicago, I llin o is 60616 Dear Ian: I am enclosing three ta lc samples, labeled Mo. 85, Mo. 120 and Mo. 123, fo r an alysis. Me want you to determine chrysotile and trem olite. Please use TEM and SAED as the method as you did- for the other m aterials we sent you (report dated 2/ 15/ 7^ by Richard Shimtps, Ref. 3805). Please attach the number 615139 on a l l charges b ille d to our company fo r th is work. Many thanks. ' Sincerely JPSrmg Enel C 5137-3 QE-CPC00004082 o O'? i o 0 1 o J. I 1 QE-CPCQ0Q04083 P R O J E C T COS-T RE CORD PROJECT TITLE: SPONSOR:______ ADDRESS: TEM and SAED of 7 talc samples COLGATE-PALMOLIVE CO. 909 River Road Piscataway, New Jersey 08854 PROJECT NO. -, MA 5259 DATE RECEIVED: 3 8 76 P.O . NO. : -634965________ COMMITMENTS: $ 1750 Contact: J. P. Simko Telephone No. (201) 463 1212 SUMMARY OF PROBLEM: Lab Notebook References: No. pp. Initials No. pp. Initials No. pp. Initials Photomicrographic record no. Sample disposal: returned filed (where) discarded Individua 1 time ',tE.i xmceluosnivinesot.fboeploewr.) Date Name Hours Charge DIRECT COSTS Trave 1 Date ' Traveler Destination Instrument time ` Date Hours SEM TEM * > - 4 - 1 1 XRD EMP IMP ESCA Outside Services Charge Date Photo Photo Materials Supplies Company Charge Summary Cost Individuals $ Instrument Travel Outside Other Cost Total Charge & _ ___ _ OK for billing jTrij_;ujit5_Ub TJ./1 lorroup Juur PROJECT LEADER GG____________________ TOTAL CHARGE $ ROUGH DRAFT ________________________ ;______ BILLED TO CLIENT $ _ ___- REPORT R E C E IV E D _________________________ INVOICE NO. (S)____________ QE-CPC00004084 waiter a mecrone associates, inc. ,. CONSULTING: ULTRAMICROANALYSIS - MICROSCOPY SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 11 May 1977 Dr. J. P. Simko, Jr. Colgate-Palmolive Company 909 River Road Piscataway, New Jersey 08854 / < Dear Dr. Simko: The examination of your latest talc sample, utilizing transmission electron microscopical techniques, has been completed. The sample was designated: Colgate, MTR-Talc-Code M-6670-2, Lot No. 5-2-3, Date 5-3-77. This specimen was found to contain, principally, talc with a wide size range but without an excessive amount of material at either extreme of particle size. Talc shards were found as were occasional talc ribbons. Goethite fibers were found with the largest one being about 1. 6 X . 15 cm in size. Goethite is an iron oxyhydroxide and is associated with calcite, quartz, and other minerals. Additionally, goethite may be found as a weathering product of various m inerals, as a direct precipitate in various water sources or from an iron gel. No asbestiform material was detected. If any questions should arise concerning this analysis, please do not hesitate to contact me directly. - Sincerely, RJS:jd Ref. MA 5500 Richard J. Shlmps Research Chemist . 2320 SOUTH MICHIGAN AVENUE - CHICAGO, ILLINOIS 60616 312/842-7100 - CABLE: CHEM1CRONE QE-CPC00004085 waiter c. mucrone associates, ine. CONSULTING: ULTRAMICROANALYSIS - MICROSCOPY SMALL PARTICLE PROBLEMS - SOLID-STATE CHEMrSTRY 9 May 1977 Dr. J. P. Simko, Jr. Colgate-Palmolive Company 909 River So ad Piscataway, Sew Jersey 08854 . Dear Dr. Simko: The transmission electron microscopical examination of your latest talc sample had been completed. The sample bore the following designation: Cogate-preshipment sample, MTS Talc, Code M6670-2, Lot no. 4-26-27, Date 4-26-77. ... This sample was found to consist mainly of nonfibrous talc with a wide particle size distribution but without an excessive amount of fine material. Fibrous aspect talc particles were also found to be present such as shards and ribbons. No asbestiform material was found to be present. . Thank you for consulting McCrone Associates once again. If any questions should arise concerning this analysis, please do not hesitate to call. Sincerely, RJS:jd Ref. MA 5500 Richard J.` Shirnps Research Chemist 2820 SOUTH MICHIGAN AVENUE - CHICAGO. ILLINOIS 60616 - 312/642-7100 CABLE: CHEMICRONE QE-CPC00004086 COLGATE-PALMOLIVE COMPANY A Dtfaii'ein Cvrperatfon RESEARCH AND DEVELOPMENT DEPARTMENT 909 River Road * Piscataway, New Jersey 0SB54 t- June 3 , 19^6 Mr. Gene Grieger McCrone Associates 2820 South Michigan Avenue Chicago, IL 60616 Dear Gene: Enclosed is one sample of ta lc fo r study by TEM and SAED an aly sis, lo t number 5"28-29. I "will telephone you the Purchase Order number as soon as possible. Many thanks. Sincerely, J. P. Simko JPS:da Enc. C 5137-3 QE-CPC00004087 waiter c. me crone associates, inc CONSULTING: ULTRAMiCROANALYSlS MICROSCOPY SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 8 September 1976 Dr. Joseph Simko Colgate-Palmolive Company 909 River Road Piscataway, New Jersey 08854 . Dear Dr. Simlto: ` Using transmission, electron microscopy and selected area electron diffraction we have examined a sample of talc designated as 8-14-15. In this sample we found no asbestiform minerals, neither amphiboles nor serpentines. We found that this sample was very plaiy and did have a large number of fines. We also found that in some cases in these fines there were some indications of rolled talc fibers, which we identified as talc with selected area electron diffraction. If there are any further questions concerning this report or the data contained therein, please contact us. Very truly yours, GRG:fe ref: 5500 QE-CPC00004088 waiter c. mecrone associates, inc, CONSULTING: ULTRAMICROANALYSIS MICROSCOPY SMALL PARTICLE PROBLEMS SOUQ-STATE CHEMISTRY 6 August 1976 M r. J. P. Smico, J r. Colgate-Palmolive Company 909 River Road Plscataway, New Jersey 08854 Dear Mr. Simko: Using TEM and SAED, we have examined a sample of your talc designated as Lot 7-24-25. We found this to be an excellent quality talc, free of asbestiform minerals, both amphibole and serpentine. The talc was generally quite platy and quite acceptable. Thank you for consulting McCrone Associates and if you should have any questions concerning these results, please contact me. Yours sincerely, Gene R. Grieger Senior Research Physicist GRGrfe ref; 5500 2820 SOUTH MICHIGAN AVENUE . CHICAGO. ILLINOIS 60S16.312/042-7100 . CABLE; CHEMICRONE QE-CPC00004089 waiter c. mccrone associates, inc. CONSULTING: ULTRAMICROANALYSIS - MICROSCOPY SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 6 August 1976 Mr. J. P. SImko, J r. Colgate-Palmolive Company 909 River Road Piscataway, New Jersey 08854 . Dear Mr- Simko: This letter records the results of our analysis of a sample of talc designated as Lot 7"18-19. In our first examination, of this talc we found a single fiber of chrysotile. The SAED pattern was extremely weak and does not show up on the print; however, under a 10X magnifier on the negative we were positively able to confirm the fact that this is chrysotile. This would put the relative percentage of chrysotile at approximately 1-2 ppm. Upon request, we subsequently re-examined this m aterial and in our second and third examinations of the same m aterial, taking different samples and different lots from the sample, we did not find any further examples of chrysotile, thus the chrysotile observed in our first examination may well have been contamination from the atmosphere or some other source. In our third examination we did find one particle of antigorite, which is also a serpentine but is not classified as an asbestos mineral- Electron micrographs of the chrysotile fiber and the antigorite particle are also included with this report. We did find a high percentage of talc shards, blocky talc and fibrous talc in this sample and I would estimate that between 20 and 35% was non-platy talc. We are also including some SAED patterns which we feel may help in your future examination of these minerals. Enclosed is a standard talc electron diffraction pattern and a standard chrysotile diffraction pattern, both taken at 200 kV. Thank you for consulting McCrone Associates and if you should have any questions concerning these results, please contact us. Yours sincerely Gene R. Grieger Senior Research Physicist 2820 SOUTH MICHIGAN AVENUE - CHICAG, ILLINOIS 60616 - 312/842-7100 CABLE: CHEM1CRONE QE-CPC00004090 waiter c, me crone associates, inc. QE-CPC00004091 .V.m\fa m ' r-- >" t? W ? -:; 'fi , -* :-`vf.r-*A".,* \vvrfvmB p f e s j > i ,j > g j f " i ' ; " S |H H B v-:; c.?>r W mm. . . ':: '' "^ i-f "*'=*.y ' ' fv-jt! ' Sample 7-18-19 1. ! {50, OOOX) 1st run waiter a me crone associates, inc. QE-CPC00004092 waiter c. me crone associates, ine. : QE-CPC00004093 Sample 7-18-19 3rd run SAED - antigorite waiter c. me crone associates,, ine. QE-CPC00004095 a. (30, OOOX) waiter c, me crone associates, inc, QE-CPC00004096 P'/g, o f If waiter c, mecrone associates, inc. CONSULTING: ULTRAMICROANALYSIS MICROSCOPY - SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 8 July 1976 Mr. J. P. Simko, Jr. Colgate-Palmolive Company Research and Development Department 909 River Road Piscataway, New Jersey 08854 . Dear Dr. Simkoj Using transm ission electron microscopy and selected area electron diffraction we have analyzed the sample of talc designated as 6-13-14. In this talc we find no amphiboles or serpentines. We do however find a rather high percent age of fines, some fine rolled talc and fine talc ribbons. This material is not very platy. Repeating again, we did not find any asbestiform minerals in this talc. Thank you for consulting McCrone Associates. If there are any further questions concerning this report or the photographs contained therein please feel free to contact me. Very truly yours GRG:jd Ref. MA 5259 Gene R. Grieger Senior Research Physicist 2020 SOUTH MICHIGAN AVENUE - CHICAGO, ILLINOIS 60616 - 3I2 -S'12-7100 - CABLE: CHEMlCRONE QE-CPC00004097 waiter c. mccrone associates, inc. CONSULTING: ULTRAMICROANALYSIS MICROSCOPY SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 24 June 1976 Dr- J. P- Simko, J r. Colgate-Palmolive Company R&D Department 909 River Road Piscataway, New Jersey 08854 Dear Dr- Simko: . Using transmission electron microscopy and selected area electron diffraction, we have examined a sample of talc designated as 5-28-29. In this talc we did not find any asbestiform m inerals. There were, however, a high portion of fines and an indication of fine talc rolled into fibers. This talc was platy and we have noted in the past that many of these platy talcs tend to form rolls and talc ribbons< Enclosed with this report is a photograph of one of the fine rolled talc fibers. When rolled so tightly the electron diffraction pattern does show some streaking of the spots sim ilar to that of chrysotile which, of course, also has a rolled structure but on an even finer scale. Calculation of the interplanar spacings, however, shows excellent agreement with ASTM data (card 13-558) for the ^002)> axis of talc. Thank you for consulting McCrone Associates. If there are any further questions concerning this report or the data contained herein, please feel free to contact me. Very truly yours, GRG:fe enclosure ref; 5259 Gene R. Grieger Senior Research Physicist 2820 SOUTH MICHIGAN AVENUE CHICAGO. ILLINOIS G061G . 312.'842.7100 : CABLE: CHEMICRONE QE-CPC00004098 waiter a me crone associates, inc. QE-CPC00004099 Q E -C P C 0 0 0 0 4 1 00 waiter c. mecrone associates, inc. CONSULTING: ULTRAMICROANALYSIS MICROSCOPY SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 24 June 1976 Dr. Joseph P. Siinko Colgate-Palmolive Company R&D Department 909 River Road Piscataway, New Jersey 08854 Dear Dr. Simko: Using transmission electron microscopy and selected area electron diffraction, we have examined a sample of talc designated as 42728 4-27-28. This talc contained no asbestiform minerals, neither amphibole nor serpentines. This talc was extremely plaiy: there were fines in this material and a few ribbons, and we found this to be excellent quality talc. If there should be any questions concerning these results, please contact us. . Very truly yours, Gene R. Grieger Senior Research Physicist GRG:fe enclosure ref: 5259 I 2620 SOUTH MICHIGAN AVENUE . CHICAGO. ILLINOIS 6 0 6 1 6 .312/8<I2-7100 . CABLE: CHEMICRONE QE-CPC0Q0Q4101 waiter c. me crone associates, inc. Q E -C P C 0 0 0 0 4 1 02 waiter c. mecrone associates, inc, CONSULTING: ULTRAMICROANALYSIS MICROSCOPY SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 24 June 1976 Dr. Joseph P. Simko Colgate-Palmolive Company R&D Department 909 River Road PIscataway, New Jersey 08854 Dear Dr. Simko: Using transmission electron microscopy and selected area diffraction, we have examined a sample of talc designated as 4-29-30. We found no asbestiform minerals in this talc, but it did seem to have rather a large number of talc shards and there were some indications of bacterial contamination as shown in the accompanying photographs. There were fines in this talc which did not show such morphological perfection and .was not as plaiy as other talcs because of the lack of platiness of this talc. If there are any further questions concerning this report or the data contained herein, please contact me. Yours sincerely, GeneR. Grieger Senior Research Physicist GRGfe enclosure ref: 5259 2020 SOUTH MICHIGAN AVENUE . CHICAGO. ILLINOIS 60616.312/842-7100 . CABLE: CHEMICFIONE Q E -C P C 0 0 0 0 4 1 03 MA 5259 4-29-30 (30,000X) Bacterial debris waiter c. me crone associates, inc. Q E -C P C 0 0 0 0 4 1 04 Q E -C P C 0 0 0 0 4 1 05 COLGATE-PALMOLIVE COMPANY ^ A Dilatsart Cerftrdfstrs RESEARCH AND DEVELOPMENT DEPARTMENT 909 River Road * PiseaPatoay, New Jersey 08854 m y 27, 1976 - Dr. Ian Stewart McCrone Associates 2820 South Michigan Avenue Chicago, ID 60616 { 0/ ^ ^ fW )- Dear Ian, Enclosed i s one sample of ta lc for study by IBM and SAED an aly sis, lo t number 4-29-30* 1 w ill telephone you the Purchase Order number as soon as p o ssib le. Many thanks. r IT CPS:Is ;Enclosure J . P. Simko G y A u J-tM q E-CPC00004106 C5)33-2 Q E -C P C 0 0 0 0 4 1 07 COLGATE-PALMOLIVE COMPANY A Diiauwt Corporation RESEARCH AND DEVELOPMENT DEPARTMENT 909 River Road Piscataway, New Jersey 08854 May 7, 1976 Hr. Ian Stewart McCrone Associates 2820 South Michigan Avenue Chicago, Hi 60616 ' . Dear Ian, Enclosed is a sample of raw m aterial ta lc for TEM, SAED analysis, lo t number lf-27-28. I w ill telephone you the Purchase Order number as soon as possible. Many thanks. JPS:ls Enclosure J . P, Simko Q E -C P C 0 0 0 0 4 1 08 COLGATE-PALMOLIVE COMPANY A Dilation Corporation RESEARCH AND DEVELOPMENT DEPARTMENT 909 River Road Piscdtaway, New Jersey 08854 May 27, I 976 Dr. Ian Stewart McCrone Associates 2820 South Michigan Avenue Chicago, IL 606I 6 _ Dear Ian, Enclosed i s one sample of ta lc for study hy TEM and SAED analysis, l o t number ^-29-30 I w ill telephone you the Purahase Order number as soon as possible. Many thanks. IPS:Is Enclosure J . P. Simko 313B>2 Q E -C P C 0 0 0 0 4 1 09 waiter c. mccrone associates, inc. CONSULTING: ULTRAMICROANALYSIS - MICROSCOPY - SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 3 May 1976 Dr. J . P. Simbo Colgate-Palmolive Company ` R&D Department 909 River Road Piscataway, New Jersey 08854 Dear Dr. Simko; This report .covers the results of the transmission electron microscopical examination of your four talc samples: JF-4-10-11, JC-4-11-12, 12-10-11, and 2-13/14, for asbestiform material. No asbestiform m aterial was detected in any of the four samples. The sample descriptions are as follows: JF-4-10-11 - Platy to chunky talc particles which vary widely in size (small submicrometer to large multimicrometer sizes). Talc shards and some rolled talc are to be noted as are occasional small blocky inorganic particles. No asbestiform material was detected. JC-4-11-12 - The size ranges from quite small (<l/3 im) to large multi micrometer particles. The talc particles vary in morphology from thin platelets to substantial chunky particles with talc shards fairly common and some occasional rolled talc being noted. Small (<l/3 fim) blocky inorganic material is also present. No asbestiform material was detected. 12-10-11 - Platy to chunkier types of talc particles. Some talc shards and ribbons noted. Some quite small blocky inorganic m aterial present, occasional organic m aterial. Infrequent, poorly diffracting, high aspect ratio (>10:1) fibers of uneven morphology (sometimes jagged) which can be positively shown not to be asbestiform m aterial (most likely silicates of varying composition and crystallinity). 2-13-14 - Platy to chunky material is present which is mainly talc but some of the chunky m aterial is not (? quartz or carbonates). Some fibrous aspect ratio talc particles (shards, e tc .) are noted which range to quite large sizes. Also noted were occasional non-asbestiform non-talc fibers. This sample is pre dominantly talc with the other m aterials occurring at very low concentrations. 2820 SOUTH MICHIGAN AVENUE - CHICAGO, ILLINOIS 60616 - 312/642-7100 . CABLE: CHEMICRONE Q E -C P C 0 0 0 0 4 1 10 Dr. J . P. Simko Page two - Thank you for consulting McCrone Associates once again. If you should have any questions regarding these analyses, please do not hesitate to call. Sincerely, Richard J, Shimps Research Chemist RJS:fe ref: 5259 Q E -C P C 0 0 0 0 4 1 11 COLGATE-PALMOLIVE COMPANY A 'Delaware Corporation RESEARCH AND DEVELOPMENT DEPARTMENT 909 Riser Road Piscataway, New Jersey 08854 A pril 6, 1976 Dr. Ian Stewart McCrone Associates 2820 South Michigan Avenue Chicago, Hi 60616 . Dear Ian, Enclosed Is one sample of raw Tnaterial ta lc fo r TEM and SAED analysis. Lot number is -1-6-7. I w ill telephone you the Purchase Order number for charges as soon as possible. Sincerely, if. P. Sijtiko IPS:Is Enclosure C 5138-2 Q E -C P C 0 0 0 0 4 1 12 COLGATE-PALMOLIVE COMPANY A Delaware Corporation RESEARCH AND DEVELOPMENT DEPARTMENT 909 River Road Piscataway, New Jersey 08854 March 10, 1976 Dr. Ian Stewart McCrone Associates 2820 South Michigan Avenue Chicago, IL 6o6l6 Dear Ian: Enclosed i s a single ta lc sample coded CB MS No. 1. Please run TEM-SAED studies. Determine a l l asbestos minerals especially amphibole. Please expedite th is sample. I -will phone you a purchase order No. to cover costs. Sincerely, JPS:ls , Enclosure J. P. Simko, J r Q E -C P C 0 0 0 0 4 1 13 H - - to -- If " A) ''jr-4 1 r Ct4L&*AJ&92 - 1 3 /1 4 Q'*" <*s~L*^GI+- % L /& ? + < * ? _ *^& -l^-~ *< 5 ~ *t^^vC m *'*vtA ou^' Q E -C P C 0 0 0 0 4 1 14 W& jpjS^-i-^^N^LAA L w ' % cfcr? 3 Ou^-U^ fe U ^ t^A- LU^&~ I T P "" H H d H | L o c fe j "fc& >cJ& A ^vJ!& " ts - i^ ^ ^ * - ^ V^vA^ |//w-^iL<i#j ^V ^J0P ^ /^WjfciA^i<yCAdn^s^ * ~ J j 2 o ^'Q-^ved- CW'i? A A r$ & $ b * v \ ^ ~ t b U - y w A a P C l^ - CXAfiL H iA 'd U M ^ 'V U it~ & d b } 1, , O d * < xdfcu& + M[-"U H Z fe .j ^A ^Jfc* U ovvC -cv T U fi-^ c ^ M n -^ A fc ^ ^ jL 0 5 ? fe cU/WA^^ ^ c ^ t i M ^ddb\ L& $< % JhtA4U > y^^nAAAA^trv\ C w d l <=^C r`^S , 45&Cj 4*.4M snA A ) /^0 -$ & d i \j?bc> sv^feP , Sr-rvL*J$ (j~)% ^ jW -2CE A ^fl-^> Q E -C P C 0 0 0 0 4 1 15 ORIGINAL'PURCHASE ORDER 05217-9 . Show this number end prefix on in voices, packing slips and packages. S6 3 3 1 0 COLGATE-PALMOLIVE COMPANY ' A DELAWARE CORPORATION 105 HUDSON S T R E E T . JERSEY C IT Y . N,J. 07302 ATTENuDR: DATJ SHIP TO McCrone Associates 2820 South Michigan Avenue ' 1 1->w ' . ;- '>! ,,V . : -: 25 5 4 G R A N D S T . JE R S E Y C IT Y . N .J . 07302 $14 13 PO? R f V E R R D . F tS C A T A W A Y . N .J . 08334 20 GRA ND ST. JE R S E Y C IT Y . N .J . 07302 . Chicago, I llin o is 6o6l 6 16 RSC e iv in g s t a t io n JEFFER SO N VI LLE . IN D IA N A 471 3 0 . Attn: DISCOUNT TERMS 1 2.-'10 M/30 2 N/30 3 1/10 N /30 Dr. Ian Stewart SHIPPING TERMS 1 l^]] FOB Destination 2 [A ] FOB Shipping P I. (Pro-Pay &BfijScc Balw W A N TE D BY EROsM: I / I /77 10 : 12/31/77 IF A B O V E D A T E C A N N O T BE M E T N O T IF Y 19 22 28 23 1 R E C E IV IN G S T A T IO N K AN SAS C IT Y . K A N . 66105 7 T0 C A R L T O N S T B E R K E L E Y . C A L IF - 9471 0 300 PAR K A V E . N E W Y O R K . N .Y . J0O22 4 _Lt Net Cash Trade 3 F O B S h ip p in g P t. (Collect) C ity_________.________________ ATTN: Receiving Cferk YOU ARE AUTHORIZEO TO FURNISH T h E ARTICLES LISTED HEREON IN ACCORDANCE W ITH THE TERMS AND CONDITIONS OH THE FACE AND Sa CK OF TH IS ORDER. QUANTITY ANDUNIT SYMBOL NUMBA PR ICE This purchase order issued to cover the following a n aly sis: (as required): . 1. Transmission Electron Microscopy ana Selected Area E lectron D iffractio n Analysis on ta l c samples (TEMSAEBA.) 2 - X-ray analysis $300. each sample 50. each This cancels and supersedes .0 . 635737 TAX EXEMPT VENDOR TO PR O TEC T A L L M E T A L PARTS AGAINST CORROSION BY SU ITA B LE P R O T E C T IV E SEALING. -"IKS 'W-TCES ihetincluJc authorised raaswiricivioii charges, jn'st &3 i/eastd FreM'u-iviL spy of ongmol bill of lading. ; . _ . .. ^ o- .. ^ K PACKAGES w ifi p u r c h a s e crder number, s y m b o l number, c o n te n ts ' e n d quantify. A c c e p ta n c e a la. . u e r is t o h o d o o m e d c e r t iiic a lio ii t h a t y o u h a v e r e a d a n d a g r e e d h e fo rm s a n d c o n d itio n s o n live " z : f - W o o f p a y m e n t w il l n o t b e m a d e a g a in s t f r o f o r m a in v o ic e and tiras for heavy loads by telephoning: 201-432-JGOO extension 309. n i !_d f j - , COLGATE-PALMOLIVE COMPANY * f.D t. e J-THe rJ3 IlrV JLiSHY S:.sr. TAX MK7 3E BILLED DXT:-:?TRD BY /.TTACHBD CTTCTi'I^.r: Q E -C P C 0 0 0 0 4 1 16 COLGATE-PALMOLIVE COMPANY A Dt/awan Corporation RESEARCH AND DEVELOPMENT DEPARTMENT 909 River Road Piscataway, New Jersey 08854 A pril 20, 1976 Hr. Ian Stewart McCrone Associates 2820 South Michigan Avenue Chicago, Hi 60616 , .. Dear Ian, Enclosed are 2 raw m aterial ta lc s , l o t numbers 12-10-11 and 2-13-14 fo r TEM and SAED analysis P0 number w ill follow. Many thanks. JFS:ls Enclosure J . P. Simko -o, C 3136-2 Q E -C P C 0 0 0 0 4 1 17 waiver c, m ucrone Q E -C P C 0 0 0 0 4 1 18 respirable 1 5G,OOOX waiter c, me crone associates, inc. Q E -C P C 0 0 0 0 4 1 19 QE-CPC00004120 waiter c. me crone associates, inc, QE-CPC00004121 QE-CPC00004122 V>/VSj I V J ('w''i !'"Ii'K: t\y' \1."ivr\>;,W'*vV^''-'fV''.A1tP-.'/CW/ irvk"-.-*i QE-CPC00004123 respirable . 1 50,OOOX waiter c. mucrone associates, ine. QE-CPC00004124 waiter a me crone associates, Inc. QE-CPC00004125 waiter c. me crone associates, ine. CONSULTING: ULTRAMICROANAIYSIS MICROSCOPY SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 31 March 1976 Dr. J. P. Simko Colgate-Palmolive Research & Development 909 River Road Piscataway, NJ 08854 Dear Dr. Simko : We examined seven samples of ta lc labeled "0925AX6, 0215DX, 1971CB4, 04143 (we believe th is should have been id e n tifie d as 0413), 0326 and 3214." ' These samples were examined in the TEM at approximately 17,000X mag n ific a tio n and also using selected area electron d iffra c tio n (SAED). We were prim arily concerned with the amphiboles and serpentines which we might find in the form of fibrous, asbestos m inerals. None of these were found in these samples. W e did, however, find two other unusual m aterials, photographs of both of which are included. One which appears to be organic from i t s mor phology and d iffra c tio n p a tte rn we believe to be a zinc ste a ra te ; the second we found was sodium chloride. Enclosed with th is report is a SAED p attern of the sodium chloride which we have indexed p o sitiv e ly as sodium chloride. We also examined th is m aterial using the electron microscpe microanalyzer (EMMA-4) and we did, again, find sodium and chlorine as the only elements present. Samples 0925AX6 and 3214 showed le s s of the sodium chloride than the other samples. Thank you for consulting McCrone Associates. If you have any questions concerning th is report, please feel free to contact us. Very tru ly yours Enclosures GRG:smg Ref. MA-5259 Gene R. Grieger Senior Research Physicist seso SOUTH MICHIGAN AVENUE . CHICAGO. ILLINOIS S0SIG . 312 8-12-7100 CABLE: CHEM1CRONE QE-CPC00004126 / waiter c. me crone associates, inc. QE-CPC00004127  *.V- [ r. L' .-V waiter c. me crone associates, inc. Q E -C P C 0 0 0 0 4 1 28 waiter c. me crone associates, no. QE-CPC00004129 ORIGINAL PURCHASE ORDER -O 5 2 1 7 - 1 0 Show this number, sd, prefix on in- peeking . 'ipr a m puiiw i . -- 3 5 Uy you ARE AUTHORIZED TO FURNISH THE AR TIC LE S LISTED HEREOH IH ACCORDANCE W ITH THE TERM S ANO CONDITIONS ON THE FACE AND SACK OF T H IS ORDER. M N T I T Y AND UNIT SYMBOL NUMBER - . P R I C E ' -; Transmission Electron Microscopy and selected area electron ' i 11 ,1 - 1*1 1 - . ' ' Diffraction analysis of 1 talc s s t a p - NOTE: This i s a one -time sample ' ATTENTION: Dre Ian Stewart '. . JieCrone A ssociates le . '. ' - ' . * - ' est, dost ' . .. . . - .. f TAX EXEMPT V E N D O R T O P R O T E C T A L L METTR.L P A R T S A G A IN S T CORROE " ............ _ > --*--n--^ j .... BY SU ITA B LE P R O T E C T IV E SEALING. SELLERS INVOICES that Include authorized transportation charge*, must bs supported by prepaid freight bill o k copy o f original bill of lading. ^ MARK PACKAGES with purchase.order number, symbol number,.contents and quantity. Acceptance of this I order is to bo deemed a certification that you have read and agreed to the terms and conditions on tho back hereof. PAYMENT WILL NOT BE MADE AGAINST PRO FORMA INVOICE. RESERVE UNLOADING space and time for heavy loads by telephoning: 201-432-1300 extension 309. * * i,,, SAMS TAX MOST BE B3XED UlM SS EXEMPTED BY ATTACHED CERTIFICATE: P U i f C '-tA S ItflO i.T IP A K TiM ENT C O P Y Q E -C P C 0 0 0 0 4 1 30 COLGATE-PALMOLIVE COMPANY A Vtinware Cerparatfon RESEARCH AND DEVELOPMENT DEPARTMENT 909 River Road Piscata-way, Near Jersey OSS54 February 27, 1976 Mr, Ian Stewart McCrone Associates 2820 South Michigan Avenue Chicago, 31 606l'6 Dear Ian, * * I am enclosing seven ta lc samples fo r TEM-SAJSB analysis. These are fin ish ed products and I am in te reste d in determining i f any chrysotile or amphibole, sp ecifically trem olite or anthophyllite, are present. The sample codes are as follows: 0925AX6 0215DX 1971CB4 0316CX oMHi-3 0326 321k I w ill contact you concerning, the purchase order number of th is work, I need these re s u lts as soon as possible. Any questions please contact me. Sincerely, J , `P. Simko tfPS:ls QE-CPC00004131  Q E -C P C 0 0 0 0 4 1 32 * "iS. _ ! * H. . iT. : \ mJ. j5 r :V i'< -- rli.. . i'V ij] TJ : ..I ORIGINAL PURCHASE ORDER ' `'S2T7-10 Show this number and prefix on ith voicest packing 34965 Dtl, . COLGATE-PALMOLIVE COM PANY 1(Te,0 BI LL T O a Delaware: corporation M Loo 10S HUDSOK S T R E E T , JERSEY C IT Y , N.J_ 07302 ATTENTONl SHIP TO i__ !__ L..________ L _ i _ . ___ MsCrone Associates T[ 2820 South Michigan Avenue i Ohioage, I llin o is 606l6 D ISCO U N T TERM S c1 2 /1 0 N / 3 0 2 [ j N /30 ' 3 C 1/10 N /30 SH IPPIN G TERM S . 1 1 F O B D e s tin a tio n 2 j2 F 0 3 Shipping P t. * Bi( P r e - P a y i3 f/J 5 e e B elo w A WANTEDBY /ASAP / . IF K AB\)Ve DATE CANNOT' BE MET*NOTIFY . 25 as- gresne st. X14 9P0IS9CRAITVAEWRARYD..N.j: 06654 13 2JE0RGSREAYNDCISTTY.. N.J. 07302 16 JRINSEFDCPIAHENfRVASlNO4G7N1VS3T0ILALTEIO.N 19 RKEACNESAIVSINCGITSYT,AKTAIONN. 66105 22 7B1E0RCKAERLLETYO.NCASTL.IF. 947T0 26 3N0E0WPYAORKRKA.VNE.Y.. 10022 23 4 r " N et Cash - 1 5 Trade 3 F O B S h i p p h E P t . (Collect) C ity ATTN: R eceiving C ierk YOU ARE AUTHORIZED TO FURNISH THE ARTICLES LISTED HEREON IN ACCORDANCE WITH THE TERMS AHO CONDITIONS ON THE FACE AND BACK OF TH IS ORDER. QUANTITYAND' UNIT SYMBOLNUMBER , PRICE Transatission E lectrsn liieroseapy and selected area electron - ....... - ' d iffra c tio n analysis f 7 t a l c 'samples. .......... ----- Note: This, i s a one time req u est. ....... ........i------- ......ATTENTION: Dr.' Ian Stewart ' ' ............ . ...... ............. .......7 " ...... MeCrone' A s s o c ia te s ..................... . - j & ................... ----- ------ -------- est* cost: $17i>0 .. ........... .. --L...--- ---r- -- ..........- :- '............................ `p T 7 5 ( E ) ( E M p f ^ ................................- ........ VENDO R TO PR O TEC T A LL M E T A L PARTS AGAINST CORROSION BY SUITABLE P R O T E C T IV E SEALING. SELLERS INVOICES that include authorized transportation charges, must be supported by prepaid freight bill or copy of original bill of lading. ' ' MARK PACKAGES with" purchase order number, symbol number, contents and quantity. Acceptance, of this . order is to be deemed a certifiedflan that you have read and agreed to the terms and conditions on the . bock hereof. PAYMENT WILL NOT BE M a DE AGAINST PRO FORMA INVOICE. RESERVE UNLOADING space and time for heavy loads by telephoning: 201-432-1300 extension 30?. Q E -C P C 0 0 0 0 4 1 33 TERMS AND CONDITIONS .WARRANTY -- The Seller expressly warrants and agrees th at there has been compliance ivith and no violation of any trademark rights, patent righhs, copyright, or of any rule, law or regulation of the Federal Government or of. any State or any o f their respective agencies or political subdivisions, in the manufacture, production , sale and or shipm ent of the goods hereunder; and the Seller will indemnify and hold Purchaser harmless from any or all costs, damages, fines or expenses (including counsel fees and fees of expert witnesses) which may be incurred by the Purchaser by reason of any claim or suit avidog out of the infringement of any trademark, patent right or copyright and/or by reason of any citation, claim or suit for damages and/or penalties brought against the Purchaser based upon any injuries, damages or violations resulting or claimed to have resulted from any alleged infringement or defect in such goods or ingredients or parts thereof. EQUAL EMPLOYMENT OPPORTUNITY -- The Equal Employment Opportunity Clause Section 202 of Executive Order 11246 as amended related to Equal Employment Opportunities and Implementing Rules and Regulations of the Secretary of Labor are incorporated herein by specific reference. CHANGES IN ORDER -- This order cannot be changed, modified or discharged in any manner except by agreement in w riting sighed hy a duly authorized representative of the Purchaser. The Purchaser reserves the rig h t to (1) make changes in the order (2) cancel all or any p a rt of the order at any time by notice in writing. The Purchaser shall not be responsible for costs incurred by the Seller in connection with this order, after the date of receipt of the change or cancellation notice. Unless the Seller presents to the Purchaser an itemized statement of claim against the Purchaser within twenty (20) days afte r the receipt of notice of such change or cancellation, the Seller shall be conclusively deemed to have waived all claims against the Purchaser with respect thereto. . CANCELLATION FOR SELLER'S DEFAULT -- Should the Seller fail (1) to effect delivery on or before the specified delivery datc(s) (2) to deliver goods in all respects conforming with the requirements (3) to duly perform Seller's obligation under each and all of the' term s and conditions of this order; the Purchaser may cancel this order in whole or in part. W ithout prejudice to the foregoing, the Seller agrees to report promptly to the Purchaser any delays in performance or in shipment of the goods covered by this order. SPECIFICATIONS. DRAWINGS. ETC. -- All specifications, drawings, plans, designs, samples, or othor documents referred to in this order shall he deemed an integral p a rt of this order as fully as if set out in full herein and Seller w arrants th a t all deliveries and/or performances hereunder shall conform thereto, each delivery and/or per formance being subject to the inspection and approval of the Purchaser, whether or not any prior paym ent snail have been made thereon by the Purchaser. NONCONFORMING MATERIAL - If Seller delivers defective materia! or material noi conforming io the agree-upon specifications. Ferchascr may {lj hold such material at Seller's expense pending instructions as to disposal, (2) return it to Seller at Seller's expense, ox (3) utilize-it in the I'orm received or after up-grading or other operations are performed on it, ct utilise, it in a different manner or in different proportions willi other products llnm was istlemlud, and Seller will be liable for any diminution in the value to Purchaser of the material and for any incidental or other damages suffered by Purchaser resulting from such defectiveness or nonconformity. No replacement of defective or nonconforming material will be made by Seller unless authorized by Purchaser. LIABILITY FOR DAMAGES --Whenever Seller shall, by virtue hereof, hare property of the Purchaser in its posses sion. the Seller shall be deemed an in su rer thereof and shall be responsible for its safe return to the Purchaser. ASSIGNMENT-- This order shall not be assigned or transferred without prior written consent of the Purchaser. W A ITER -- Purchaser shall not be deemed to h are waived any of its rights hereunder unless such waiver shall have - been signed by a duly authorized representative of the Purchaser. No such waiver, unless expressly stated there in. shall be effective as to any delivery or other transaction which may occur subsequent to the date of the waiver, nor as to any continuance of a default after such date. LABOR AND/OR MATERIAL -- With respect particularly to orders covering labor and material, Seller agrees to start . work immediately, to proceed with the utm ost dispatch and to complete all of the work under this order. All such work shall be performed in strict accordance with Purchaser's " General Conditions for ConLract Work" Specification No..0920-GE. nor shall 'work be perm itted to start on Purchaser's property until required Insurance Certificates have -' been received by Purchaser.' Time is hereby declared to be the essence .of this order. Prices shown are firm and n ot subject to adjustment because of increase or decrease in material prices and/or wage rates and/or freight rates and/or ' other items of cost. The acceptance of the.final payment by Seller shall be held to be a waiver and discharge of any and . . all .claims and demands against the Purchaser for- compensation and damages on account of any .matter arising out of *Or in connection with th Contract or the perform ance o f the work. Any extra or additional work performed by Seller ' shall be on a. fixed price basis or cost plus fee basis and m ust be in each case, first authorized in w ritingby Purchaser. Seller's rates for such purposes shall be as set forth in a quotation from Seller prior to starting any such extra or additional work and confirmed by Purchaser's prior written authorization. - .' QE-CPC00004134 ST 4 (1073. ( I) To ba complatad by pureboiar und glvan to ond ntflllHd by vattdar. Hand inafrvCttoni on both of thll Carllfrlola. THIS CERTIFICATE M A Y N O T BE USED IN CO N N EC TIO N W IT H THE PURCHASE OP SERVICES MAY RE REPRODUCED fc ta tp u f -N rn i ip r a p tt DIVISION OF TAXATION SAUS TAX EXEMPT USE CERTIFICATE FORMST4 PURI HASEK S CERlINCAlt OF AlllllORIIY NUMStN I 3I - 8 5- 39`3/OQl (Noma of Vandor) Addran .C b s t* * i City 3 -M /7 C // Stota Hp Tha undersigned purchaser certifies that It is not required to pay the New Jersey Sales and/or Use Tax on the purchase or purchases covered by this Certificate because the tangible personal property pur. chased will be used for an exempt purpose. Said tangible personal property will be used for the following exempt purpose: . ,i!Qr. USfi.,.Gr.... consum ption d ir e c tly and e x c lu siv e ly in re se a rc h and developm ent in th e experim ental" 'o r ``lahbirtitbJiy'' SenSei............................................................................... The exemption on the sale of said tangible personal property to be used for the above described exempt purpose is provided in subsection N.J.S.A. 54:32B-j 6-N | ($ee averse for listing o f principal exempt uses of tangible personal p ro p e rty a n d f ill in th e b lo c k w ith proper subsection c ita tio n ). I. the undersigned purchaser, have read and complied with the instructions and rule* promulgated pur suant to the New Jersey Sales and Use Tax Act with respect to the use of the Exempt Use Certificate, and it is my belief that the vendor named herein is not required to collect the sales or use tax on the transac tion or transactions covered by this Certificate. The undersigned purchaser hereby swears (under the penalties for perjury and false swearing) thot all of the information shown In this Certificate is true. COLGATE - E A IM O L IV E COMPANY A VENDOR SHOULD READ A N D COMPLY W IT H THE INSTRUCTIONS G IV E N O N BOTH SIDES OF A N EXEMPTION CERTIFICATE. (S ig n a tu ra of o # n a r,J 9 a rfn B r. afffcar o f corporation, ate.) , W a lte r L . B o m -- P u rc h a s in g D e p a rtm e n t ........105ii.H )i^pn.S^eet...... .......................... (Addreu of Purehaiar) J&TSey C i t y , H . J . 07302 QE-CPC00004135 INSTRUCTIONS FOR USE OF EXEMPT USE CERFICATS 1. Good Faith --In general, vendor who accepts an exemption certificate in "good faith" is relieved af.liobility for collection ar payment of tox upon transactions covered by the certificate. The question of "good faith" is one of fa d and depends upon a consideration of all the conditions surrounding the transaction. A vendor is presumed to be fomilior with the low and the regula tions pertinent to the business in which he deals. . In order far "good faith" ta be established, the fallowing conditions must be met: . (oj The certificte mpst contain no statement or entry which the vendor knows, or has reoson to know, is false or mis leading. '' (b) The.certificte must be an officially promulgated certificate farm ar a substantial and proper reproduction theieof. (c) The certificte must be doted ond executed in accordance with the published instructions, and must be complete and regular in every respect. ' The vendor may. therefore, occept this "goad faith" Exempt Use Certificte On a basis far exempting soles to the signofory pur chaser provided that: . (d) The purchaser's Certificate of Authority number, indicating thot the purchdser is registered with the New Jersey bivisian of Taxation, is entered an the face of the Certificate. (e) The purchaser has entered oil other information required on the form. -. (f) The vendor hos no reosop to believe that the property to be purchased is of a type noTardinarily Used in the purchaser's business far the purpose described in this Certificte. 2 . Improper C e rtific te -- Soles transactions which o r* not supported by ptoperly executed exemption certificates shot! be deemed to be toxoble retail sales. The burden af proof That the tax was not required to bp collected is upan the vendor. 3 . Correction o f Certificate -- In general, vendors hove 60 days after dale of sale to obtain a corrected certificate where the originol certificate locks moteriol information required ta be set forth in soid certificate ar where such information is Incorrectly stoted. . 4 . A dditional Purchases by Sam e Purchaser--This Certificate will servato coyer additional purchases by the sam purchaser o( the some gnerol type of property. However, each subsequent sales slip or purchase invoice biec On this Certificate must show the purchaser's name, address and Certifcate af Authority number for purposes af verification. 5. Retention of Certificles Certificates must be retained by the vendor far a period a f not lessThan three years from the date a! the lost sale coveredby the certificate. Certificates must foe in the physicot possession of the vendor and available for in spection an or before the 60th day following the dat of the transaction to which the certificte relates. .. 6 . The mast common exempt uses far which the Exempt Use Certificate {Form.ST-4) is applicable ore the. la Hawing: Sales of machinery, opparolus ar equipment for use or consumption directly ond primorily in the production, generation, transmission ar distribution of gas. electricity, refrigeration, steam or water for sale ar in the operation af sewerage systems. JN.J.S.A. 54:328-8 (m) (2)| ' ' Soles of tangible'personal property purchased far use ar consumption directly and exclusively in. research and development in the experimental ar laboratory sense. Such reseorch ond development shall not be deemed to include the ordinary testing or inspection af. molerais.ar products for quality control, efficiency surveys, management studies, consumer surveys, advertising, promotions ar research in connection with literary, histrico] or similar projects. {N.J.S.A-' 54:326:8 (n)j Sales or use of wrapping paper, wrapping twine, bags, cartons, tape. rope, tobis, nonreturnoble containers, reusobte milk cantinrs and.all other wropping supplies when such use is incidental to the delivery of personal property which has been sold. |N J.S .A . 54-.326-B (o)| . Sales of materials, such as chemicals and cotolysts. used ta induce ar couse a refining ar chemical process, where such molerais ore an integrator essential port gf the processing operation, but do not become a component port of the finished pro duct. |N.J.S,A. 54:326-8 (l)| The sole af advertising materials to be publishedin a newspaper. N.J.S.A. 54;-8 (ee)j . The use af property far market sampling by the purchoser. [NJ.S.A. 54:32B-11 (4)] ** REPRODUCTION OF EXEMPT USE CERTIFICATE FORMS: Privole reproduction of Exempt Use Certificates moy be mode without the prior permission of the Division of Taxation. STATE OF N E W JERSEY, DEPARTMENT OF THE TREASURY. D IV IS IO N OF TA XA TIO N Pest O ffice Box 9 9 9 , Trenton, N-J- 0 6 6 2 5 QE-CPC00004136 QE-CPC00004137 QE-CPC00004138 QE-CPC00004139 t-I. ' h V.- *'ftt COLGATE-PALMOLIVE COMPANY A "DtlavMrt Cerporafhn RESEARCH AND DEVELOPMENT DEPARTMENT 909 River Road Piscata-way^ New Jersey 08854 February 27, 1976 Me. Ian Stewart McCrone Associates 2820 South Michigan Avenue Chicago, Hi 606l6 . . . Dear I a n ,' I am enclosing seven ta lc samples fo r TEM-SAED analysis. These are fin ish ed products and I am in te re ste d in determining i f any chrysotile or amphibole, sp ecifically trem olite or anthophyllite, are presen t. The sample codes are as follows: ' 0925AX6 0215DX 1971CBU 03I 6CX O ialt-3 ' 0326 3214 I w ill contact you concerning the purchase order number of th is work. I need these re s u lts as soon as possible. Any questions please contact me. Sincerely, QE-CPC00004141 CCKOW O !I fff* 3 QE-CPC00004142 PRO JECT COST PROJECT TITLE analyze for asbestos SPONSOR: ADDRESS: coI*TE--PATMT.TW. CO. 909 River U------------m.utr-- --08854- RECORD m 7673 PROJECT NO.: --------2__7__7_9 DATE RECEIVED: _______ _ P.O. NO. : rS p . s COMMITMENTS: $________ Contact: J . P. Stofco_________________ _ Telephone No. : SUMMARY OF PROBLEM: Lab Notebook References: No. PP. Initials No. PP. _ Initials No. PP. Initials Photomicrographic record no. _________ Sample disposal: returned filed (where) discarded DIRECT COSTS (Exclusive of oper. I Individual time time on inst. below) Travel Charge Summary Date Name Hours Charge Date Traveler Destination Cost ' Individuals $ Instrument Travel Outside Other Instrument time Date SEM TEM XRD EMP IMP ESCA EMMA MOLE Hours Charge Date Company Photo Photo Materials Supplies Total Charge $ Cost OK for billing ' . i * J T L VJJ C U L . J-lL IL Group Ldr ? .O- \LftAsLAJOij CHARGE $ BILLED TO CLIENT $ . `t-l-.-f--aH. ,I ------ * |1^ 3-J0'J0'O j/ 0 H - i t s I 11 j o' INVOICE NO. (S)______ PROJECT LEADER: ^ QE-CPC00004143 waiter c. mecrone associates, inc. CONSULTING: ULTRAMICROANALYSIS MICROSCOPY SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 13 February 1979 Dr. Joseph P. Sirrko, J r . Colgate Palmolive Company 909 River Road PIscataway, New Jersey 08854 Dear Dr. Sirrko: Using transm ission electron microscopy and selected area electron d iffra c tio n we have analyzed a sample of sodium carbonate for a sh estiform m inerals. The procedure we used for th is sample was to dissolve the sodium carbonate in'approxim ately 500 nil of water and f i l t e r onto a 47 mm f i l t e r . We then washed the f i l t e r to remove any excess sodium carbonate and, using ajSoxhlet extractor, dissolved the f i l t e r . We did not find any asbestiform minerals in th is sample, e ith er amphibole or serpentine. In fa c t, the f i l t e r was extremely clean indicating th a t the predominant portion of th is sample was water soluble. We thank you for consulting McCrone Associates and i f there are any further questions concerning th is report or the data contained herein, please fe e l free to contact me. Very tru ly yours, GRG:jd Ref. MA 7673 Gene R. Grieger Senior Research Physicist 2B20 SOUTH MICHIGAN AVENUE . CHICAGO, ILLINOIS 60 616.312 /842 -710 0 . CABLE: CHEMICRONE QE-CPC00004144 PURCHASE REQUISITION - METROPOLIT AN AREA ORIGINAL PURCHASE ORDER Show this number and prefix on in voices. packing slips and packages. 630290 COLGATE-PALMOLIVE COMPA A DELAW ARE CORPORATION 105 HUDSON S TR E E T . JERSEY C IT Y . N.J. 07302 'J ! DATE SH IP T O . . .. - - '- ' ! McCrone Associates ............. - - - ........ R S C f V E D - '! 2 S i 3 7 3 > 2 5 SO G R E E N E S T . X JE R S E Y C IT Y . N .J. 07302. 909 R IV E R RQ. 14 F IS C A T A W A Y , N . J . 0 0 6 5 4 1 ; 2820 South Michigan Avenue Chicago, I llin o is - 20 G RAND ST. 13 J E R S E Y C I T Y . N . J . 0 7 3 0 2 16 R E C E IV IN G S T A T IO N JEFFERSO NVJLUE, IN D IA N A 47130 19 R E C E IV IN G S T A T IO N KANSAS C IT Y .-K A N . 86105 D ISCO U N T TER M S 1 2 /1 0 N /30 2 N /30 3 1/10 N /3 0 4 Net C ash 5 Trade SH IPPIN G TERM S 1 0 FOB D estination 2 Q FO B Shipping P t. (P re -P a y fi B ilU See B elow 3 0 FO B Shipping P t. (C o lle c t) C ity V *N T D BY ASAP ) IF A SO V E lD A Tfe. C A N N O T B E M E T N O T IF Y 22 710 C A R LT O N ST. B E R K E L E Y . C A L IF . 947T0 26 300 P A R K A V E . NEW Y O R K . N .Y . 10022 23 A TTN : R eceiv in g C lerk YOU ARE AUTHORIZED TO FURNISH THE ARTICLES LISTED HEREDH IN ACCORDANCE W ITH THE TERMS AND CONDITIONS ON THE FACE AND BACK OF TH IS ORDER. SELLERS INVOICES that include authorized transportation charges, must be supported by prepaid -freight bill or copy of origtnal bill of lading. ' MARK PACKAGES wiih purchase order number, symbol number, contents and quantity. Acceptance of this order is to be deemed a certification that you have reed and agreed to the terms and condi Iions on the back hereof. PAYMENT WILL NOT BE MADE AGAINST PRO FORMA INVOICE. RESERVE UNLOADING space and time for heavy loads by telephoning: 201434.1300 extension 30?. ,________________________________ ___________ ________ ____ _______ ______ ------ ---- ------ -- --- ~ -------- 1 r ~ < ;ATE- PALMOUVE C MPANY <r QE-CPC00004145 TERMS AND CONDITIONS WARRANTY -- The Seller expressly warrants and agrees th at there has been compliance with and no violation of any trademark rights, patent rights, copyright, or of any rule, law or regulation of the Federal Government or of any State or any of their respective agencies or political subdivisions, in the manufacture, production, sale and or shipm ent o f the goods hereunder; and the Seller will indemnify and hold Purchaser harmless from any oral! costs, damages, fines or expenses {including counsel fees end fees of expert witnesses) which may lie incurred by the Purchaser by reason of any dais or suit arising o u t of tile infringement of any trade murk, patent right or copyright and/or by reason o f any citation, claim or suit for damages and/or penalties brought against the Purchaser based upon any injuries, damages or violations resulting or claimed to have resulted from any alleged infringement or defect . in such goods or ingredients or parts thereof. EQUAL EMPLOYMENT OPPORTUNITY -- The Equal Employment O pportunity Clause Section C-L' of Executive Order 112=16 as amended rcinwd rc Equal Employment Opportunities and Implementing Pules and Peculations of the Secretary of Labor arc incorporated herein by specific reference. ,, CHA NGES IN ORDER -- This order carmot be changed, modified or discharged in any m anner except by agreement in writing- signed by a duly authorised representative of the Purchaser. The Purchaser reserves the right to (1) make changes in the order (2) cancel all or any p art of the order at any time by notice in writing. The Purchaser shall not be responsible for costs incurred by the Seller in connection with this older, after the date of receipt of the change or cancellation notice. Unless the Seller presents to the Purchaser an itemised statem ent of claim against the Purchaser within twenty (20) days after the receipt of notice of such change or cancellation, the Seller shall be conclusively deemed to have waived all claims against the Purchaser with respect thereto. ' CANCELLATION. FOR SELLER'S DEFAULT -- Should the Seller fail -(1) to effect, delivery on or before the specified delivery date(s) (2) to deliver goods in all respects conforming with the requirements (3) to duly perform Seller's obligation under each and all of the terms and conditions of this order, the Pnrchas-. r may cancc-1 this order in whole or in part. W ithout prejudice to the foregoing, the Seller agrees to report prom ptly ta the Purchaser any delays in performance or in shipment of the goods covered by .this order. SPECIFICATIONS, DRAWINGS, ETC. -- All specifications, drawings, plans, designs, samples, or other documents referred to in this order shall be deemed an integral p a rt of this order as fully as if set out in full herein and Seiler w arrants th a t all deliveries and/or performances hereunder shall conform thereto, c-ach delivery and/or per formance being subject to the inspection and approval of the Purchaser, whether or not any prior payment shall have been made thereon by the Purchaser. NONCONFORMING MATERIA!. - If Seller deliver.': defective material or material not conforming to the agrec-upon specifications, Purchaser may (11 hold such material at Seller's expense pending insb-.v.-tions as to disposal, (2) return it to Seller at Sclkrb expense, or (3) utilize it in the form received or after up-grading or other operations are performed on it, or utilize it in a different manner or in different proportions with other products than was intended, and Seller will lie liable for any diminution in the value to Purchaser of the material ansi for any incidental o, other damages suffered by Purchaser resulting from such defectiveness or nonconformity. No replacement of defective or nonconforming material will be made by Seller unless authorized by Purchaser. LIABILITY FOR DAMAGES -- Whenever Seller shall, by virtue hereof, have property of the Purchaser in its posses sion. the Seller shall be deemed an insurer thereof and shall he responsible for its safe retu rn to the Purchaser. ASSIGNMENT-- This order shall not be assigned or transferred without prior w ritten consent of the Pnrclinscr. WAIVER -- Purchaser shrill not he deemed to have waived any ,of its rights hereunder unless such v.niver shall have been signed by a duly authorized representative of the Purchaser. No such waiver, unless expressly stated there in. shall be effective as to any delivery or other transaction which m ay occur subsequent to the date of the waiver, nor as to any continuance of a default after such date. LABOR AND/OR MATERIAL -- With respect particularly to orders covering labor and material, Seller agrees to start work immediately, to proceed with the utm ost dispatch and to complete all of the work under this order. All such ' work shall be perform ed in strict accordance with Puvchaser's " General Conditions For Contract Work1' Specification . ` No.0920-CE, nor. shall work be permitted to start on Purchaser's property until Veq'uired Insurance Certificates have . been received by Purchaser. Time is hereby declared to be the essence of this order. Prices shown are firm and n o t subject to adjustm ent because of increase or decrease in material prices and/or wage rates and/or freight rates and/or other items of cost. The acceptance of the final payment by Seller shall be held to be a waiver aud discharge of any and all-claims and dem ands against the Purchaser for compensation and damages on account of any m atter arising o n t of or in connection w ith the Contract or the performance of the work. Any extra or additional work performed by Seller shall be on a fixed price basis or cost plus fee basis and must be in each case, first-authorized in writing by Purchaser. .Seller's rates for such purposes shall be as set forth in a quotation from Seller prior to starting any such extra or additional work and confirmed by Purchaser's prior written authorization. ' QE-CPC00004146 11 <(0M. * |) h Im bf unborn wrf |l( n to 9*4 fotolito# by vaiiOor oo# KuhuHoi or ball I 4M C w M fltaH . TMtt ciwnncATt may not H UIIO IN CONNKTWN WITH TIM HMCHAH Of KtVKn MAY BE REPRODUCED fctatr nf Nrin 3rrari? WVIIfOM OF TAXATION SAW TAX ixim pt u$ citnncATa FORMST-4 fUl IIASI-t N c i m i t K AH or A in m it iiY n i i m u k 131-815^9^/001 The undersigned purchaser certifies that it 1 not required to pay tho Now Jersey Solo* and/or Use Tax an the purchase or purchases covered By tfili Cortlflcot* because tho tangible pononal pieporty pur chased will bo used for on exempt purpose. Said langlblo porionol property w ill bo used for tho following exempt purpose^ . f o r USO O r consum ption d i r e c t l y snd e x c lu s iv e ly in re s e a rc h and developm ent In th e e x jf *im *n til 01* la b o ra to ry iW O ie. ...................................................... ................. Tho oxomptlon on tho sale of M id tangible personal property to bo uiod for tho above described exempt purpoio 1 provided In subsection N.J.5.A. S4i32B-| j fSee reverie sid0 for litfbo of principal exempt u n i of fanglbfo personal properly and All In the block with proper wbiocffon cHaWont. - I, the undersigned purchaser, have road and complied with tho instructions and ru in promulgated por tuari to tho Now Jortoy Sale* and Use Tax Act with respect to tho uto of tho Exempt Uio Certificato, and it it my belief that the vendor named herein It not required to collect the talet or ute tax on the transaciton or. transactions covered by thli Certificate. The undertigned purchater hereby wear (under the penatilo for perjury and false swearing) that all of the Information shown In this Certificate It true. A VINCO* HOMO MAO ANO COMH.Y WITH THIINSTRUCTIONS (NVSi ON OOTH MOM Of AN BMMntON CMTStCATf. : C O L O A T E -n iM O L IV E COMEMW NAMI oe PtCHAJM(>nolilsi 1D ir it to o f T a x a tio n ) r (WanoiiKo of awntriitortnor, offleor of corporation, oh.) . . W a lte r I, jf o r n - - ^ c h a 8 in g Department ...... ............................................................................................. lAMnn et puMhrnw) Je rse y C it y , H. J . 07302 QE-CPC00004147 INSTRUCTIONS FOR USE O f EXEM PT USE CERTIFICATES I Good Faith In general. a vendor who accept! on exemprian certificate in "good faith" if relieved of liability for ceriectiofs or payment of (ah upon transactions covered by the certificate The question of "good forth" it one of fact and depend opon a conuderarian of oil thr conditions surrounding the transaction. A vendor it presumed to be familiar with the law and the regula tion! pe- rment la rhe business in which he dealt. - tn a rd e r lo r "good faith1' ro be established, the fallow ing condition! mutt be met: - (o) the certificate mutt Conrom no tlatemenl or mrry which the vendor knows. or hot reaton to liltow, if false o r 'mis leading . (b) The certificare muir be an officially promulgated Certificate form or a iirbitontiol and proper reproduction thereof. (c) The certificate mutt be doled and executed in accordance with the published Instructions, ond mustbecompfete and regular in every respect. '" . The vendo may. therefore. accept this "goad faith'1Exempt Die Certificate on a b ad l for exempting tales to the signatory pur chaser provided that: . " (d) The purchaser's Certificate of Authority number, indicating that the purchaser Is registered with the New Jersey Dividon of Taxation, is entered on the face o f the Certificte. (e) The purchaser hat entered all Other information required On die form. ' (f) The vendor hot no.reqson to believe that the property to be purchased It of a type not ordinarily used In the purchaser's busmen for rhe purpose described In this Certificate. ' 7- fritproper Certificte-Soles transactions which or* Ml supported by property executed exemption certificates shall be deemed to be to xable retail soles. The burden of proof thor the fox was not required to be collected It upon the vendor. 3. Cerrecren of Certificate In general, vendors have'60 days after dote of sale to obtain a corrected certificate where the original certificar* locks material information required to'be sel forth in sold Certificate or'where Stich Information is incorrectly stated. ' 4. Additional Purchases by Same Purchaser--This Certificate will serve to cover additional purchases by the tome purchaser of thy some general type of properly. However, each subsequent sales slip, or prchbtt Invoice based'oh this Certificate must show lb purchaser1! name, address ond Certillcote of Authority number fdr'prpofdi Of vsirttiicatian. ' ' ' -: 5. Reten lien of Certificte* Cerlificolet mutt be retained'by the vendor for a period af not less than three years from the date of the tasr'vate covered by the Certificate. Certificates must be In the physical possession of the vendor and available far in spection on ar before the 60th day (allowing the dale of the transaction to which the certificate relates. 6. thf most mu,man exempt uses lor which (he Exempt Use Certificate (Farm ST-4)is applicable ore rhe fallowing: Sales af machinery, apparatus or equipment far use or consumption directly and primarily in the production, generation, 'transmission or distribution a f gas, electricity, refrigeration, steam or water far sale or in the operation a f sewerage systems. IN.J.S.A. 54:32B-a'(m) (2)| Sates of tangible perianal properly purchased far use ar consumption directly and exclusively In research and development in the experimental or laboratory sent*. Such research ond developrKenr shall not be deemed to include the ordinary testing ar inspection of materials ar praduers far quality control, efficiency surveys, management studies. Consumer surveys, advertising, promotions or reseorch in connection with literary, historical ar slmjlor projects. (N.J.S.A. 94)321-8 (n)j Sales or use of wrapping paper, wrapping twine, bags, cartons, tape, rope, labels, nonreturnable containers, reusable milk containers and all other wrapping supplies when such us* it incidental to the delivery of perianal property whkh hot been Id. INJ.S.A. 54:328-8 (o)| . ' Sales al materials, such os Chemicals and cotolytrs. used to induce or cause a refining or chemical process, where such materials are an inregral or esHntial part af the processing operation, but da notbecame a component part of the finished pro* duel. IN.J.S.A. S4.-328-8 (t)| - - The sale af advertising molerais to be published in o newspaper. |N.J.S.A. 54i*0 (ee)| The use of property for market sampling by the purchaser. IN.J.S.A S4i32B-t I (4)| REPRODUCTION O f EXEMPT USE CERTIFICATE FORMS: Privte reproduction of Exempt Use Certificte! may be mode without the prior permistin a f the Division of Taxation. 5TATI OP NIW JERSEY, DEPARTMENT OP THE TREASURY, DIVISION OP TAXATION Peel Office Bex W , Trenlen, N.J. 0MR5 QE-CPC00004148 waiter c. mecrone associates, inc. CONSULTING: ULTRAMICROANALYSIS MICROSCOPY SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 13 February 1979 Dr. Joseph P. Simko, J r . Colgate Palmolive Company 909 River Road Pis cataway, New Jersey 08854 Dear Dr. Sinko: Using transm ission electron microscopy and selected area electron d iffra c tio n we have analyzed a sample of ta lc designated as #32. We found th is sample to be extremely p laty , although there were indica tions of ro lle d shards because of the p la tin e ss, but we did not find any asbestiform minerals. t We thank you for consulting McCrone Associates and i f there are any fu rth er questions concerning this report or the data contained herein, please fe e l fre e to contact me. Very tru ly yours, GRG:j d Ref. MA. 7673 Gene R. Grieger Senior Research Physicist 2820 SOUTH MICHIGAN AVENUE . CHICAGO. ILLINOIS 6Q616 312/842-7100 - CABLE: CHEMICRONE QE-CPC00004149 PURCHASE REQUISITION - METROPOLITAN AREA ORIGINAL PURCHASE ORDER ' O ' 5T21-11 Show this number mid prefix on in voices, packing slips and vackaees. 630318 *n'v.ls-**rm -T/irrr!r T O ^,, EPA 89982 COLGATE-PALMOLIVE COMPANY; A DELAW ARE C FP ftA TIN 105 HUDSON S TR E E T . JERSEY C IT Y . N.J. 073tk t/A sh \ SH IP TO HeGrne Associates 2 5 BG c r e e n e s t . JERSEY CITY. N.J. 07302 %14 909 RIVER RD. P1SC ATAWAY. N . J . 0BB54 I 220 South Michigan Avenue i Chicago, Illin o is D ISCO U N T TERM S 1 2/10 N /30 2 N /30 3 l/lO N /3 0 4 Net C ash 5 Trade SH IPPIN G TERM S 1 [ FOB D estination 2 FO B Shipping P t. (P re -P a y B ilJ)5ee B elow 3 [ FO B S h ip p in g P t (Collect) C ity 13 20 GRAND ST. JERSEY CITY. N.J. 07302 16 R E C E I V I N G S T A T I O N JEFFERSONVILLE. INDIANA 47130 19 RECEIVING STATION KANSAS CITY. K A N . 66105 22 7 1 0 C A R L T O N S T . BERKELEY. CALIF. 94710 26 300 PARK AVE. NEW YORK. N.Y. 10022 23 A TTN : R eceiv in g C lerk YOU a r e AUTHORIZEO TO FURNISH THE ARTICLES LISTED HEREON IN ACCORDANCE W ITH THE TERMS ANO CONDITIONS ON THE FACE AND SACK OF TH IS ORDER. Q U A N T IT Y A N D UNIT SYMBOL NUMBER PRICE ..................___________ 1 Sample of Talc Code #32 fo r Microscope and Selected. Area r. ' -Electron D iffractio n analysis fo r asbestos m in erals. i . `cost approx* $300 1 Sample sent under separate cover* j ji1 NOTE: This is a one time re q u e st^ j i i , i; i .] f T "t.................... ........... .... ___ i . ... ............. -- -- ..... --\.K i\i'G fL " :--- -------- ---------------------- -------------- ; L^x ^ 1 \S 5>cD - ` iTAX EXEMPT 1 ]L MAIL |NV05CS|S) o: VT {$ ' CGr C V fi/& /2 - .. CaloaVo-PolwolWa Co.1 939 fevor ***. ` ` ..... . . --- ............... ..... 13o ' - VENDO R TO P R O TE C T A LL M E T A L PARTS AGAINST CORROSION BV S U IT A B L E P R O T E C T IV E SEALING. SELLERS INVOICES that jnejude authorized transportation charges, must.bo supported by prepaid freight bill oj copy of original bill of losing. .. ' 1" MARK-PACKAGES with purchase'order number^ symbol number contents and quantity* Acceptance-of this order is to be deemed a certification that you have read and agreed to the terms and conditions on the back hereof- PAYMENT WILL NOT BE MADE AGAINST PRO FORMA INVOICE. RESERVE UNLOADING space qnd time for heavy loads by telephoning: 201-434-1300 extension 309. :JV QE-CPC00004150 TERMS AND CONDITIONS WARRANTY -- The Seiler expressly warrants and agrees th at there has been compliance with and no violation of " any trademark rights, patent rights, copyright, or of any rule, law or regulation of the Federal Government or of any State or any of their respective agencies or political subdivisions, in the manufacture, production, sale and or shipm ent of the goods hereunder; and the Seller will indemnify and hold Purchaser harmless from any or all costs, damages, fines or expenses (including counsel fees and fees of expert witnesses) which may be incurred by the Purchaser by reason o f any claim or suit arising o ut of the infringement of any tradem ark, patent right or copyright and/or by reason of any citation, claim or suit for damages and/or penalties brought1against the Purchaser based upon any injuries, damages or violations resulting or claimed to have resulted from any alleged infringement or defect in such goods or ingredients or parts thereof. EQUAL EMPLOYMENT OPPORTUNITY -- The Equal Employment Opportunity Clause Section 202 of Executive O rder 11240 as amended related to Equal Employment Opportunities and Implementing Rules and Regulations of the Secretary of Labor arc incorporated herein by specific reference. CHANGES IN ORDER -- This order cannot, be changed, modified or discharged in any manner except by agreement in w riting signed by a duly authorised representative of the Purchaser. The Purchaser reserves the right to (1) make changes in the order (2) cancel all or any p a rt of the order a t any tim e by notice in w riting. The Purchaser shall not be responsible for costs incurred by the Seller in connection with this order, after the date of receipt of the change or cancellation notice. Unless the Seller presents to the Purchaser au itemized statem ent-of claim against the P urchaser within twenty (20) days after the receipt of notice of such change o r cancellation, the Seller shall be conclusively deemed'to have waived all claims against the Purchaser with respect thereto. CANCELLATION FOR SELLER'S DEFAULT -- Should the Seller fail (1) to effect delivery on or before the specified delivery date(s) (2) to deliver goods in all respects conforming with the requirements (3) to duly perform Sellers obligation under each and all of the terms and conditions of this order, the Purchaser may cancel this order in whole o r in part. W ithout prejudice to the foregoing, the Seller agrees to report promptly to the Purchaser any delays in performance o r in shipment of the goods covered by .this order. SPECIFICATIONS, DRAWINGS, ETC. -- All specifications, drawings, plans, designs, samples, or other documents referred to in this order shall be deemed an integral p a r t of this order as fully as if set out in full herein and Seller w arrants th a t all deliveries and/or performances hereunder shall conform thereto, each delivery and/or per formance being subject to the inspection and approval of the Purchaser, whether or not any prior paym ent shall have been made thereon by the Purchaser. ' NONCONFORMING MATERIAL - If Seller delivers defective materia! or material not conformitig to the agrcc-upon specifications, Purchaser may (1) hold such material.at Seller's expense pending instructions as to disposal, (2) return it to Seller at Seller's.expense, or (3) utilize it in the form received or after up-grading or other operations are performed on it, or utilize it In a different manner oi in different proportions with other products than was intended, and Seller will be iinblc for any diminution in the value to Purchaser of the material and for any incidental or other damages suffered by Purchaser resulting from such defectiveness or nonconformity. No replacement of defective or nonconforming material will be made by Seller unless authorized by Purchaser. LIABILITY FOR DAMAGES -- Whenever Seller shall, by virtue hereof, have property of the Purchaser in its posses sion, the Seller shall be deemed an insurer thereof and shall be responsible for its safe return to the Purchaser. ASSIGNMENT -- This order shall not be assigned o r transferred without prior w ritten consenL of the Purchaser. WAIVER -- P urchaser shall not be deemed to have waived any of its rights hereunder unless such waiver shall have been signed by a duly authorized representative of the Purchaser. No such waiver, unless expressly stated there in, shall be effective as to any delivery o r other transaction which may occur subsequent to the date of the waiver, nor as to any continuance of a default after such date. LABOR AND/OR MATERIAL -- With respect particularly to orders covering labor and material, Seller agrees to start work immediately, to proceed with the utmost dispatch and to complete all o f the work under this order. All such work shall be performed in strict accordance with Purchaser's " General Conditions for Contract Work" Specification . No.0920-GE, nor shall work be perm itted to start on Purchaser's property until required Insurance Certificates have bee'n received by Purchaser. Time is hereby declared to be the essence of this order. Prices shown are firm and not subject to adjustm ent because of increase or decrease in material prices and/or wage rates and/or freight rates and/or ' other items of cost. The acceptance of the final paym ent by Seller shall be held to be a waiver and discharge of any and . all claims and demands against the Purchaser for compensation and damages on account of any m atter arising o ut of ' or in connection with the Contract or. the performance of.the' work: Any extra o r additional work- performed by Seller shall be on a fixed price basis or cost plus fee basis and must be in each case, first authorized in writing.by Purchaser. Seller's rates for such purposes shall be as set forth in a quotation from Seller prior to starting any such extra or ' additional work and confirmed by Purchaser's prior written authorization. QE-CPC00004151 II t (10. 1) t* tihi|i>tlid by ywrAgfif uml fin a b m r i b M by tftf. jaiiftMriiHi a baci W b TH CHWKATf MAY NOT M Ulto IN COMMOTION WltH tHI HMCHAU OMNVKfl ----------------------- .I MAY t E REPRODUCED ftta tr f H rm rrari DfVIltON OP TAXATION Ain TAX IXIMFT SI CIRTWCATB FORMST-4 ruxi itAiri s ititttk 'A lt t e AimtniNY nummo 131-815-S9*/001 >, (Nom of VdM AOOnm city Do The undoriignod purchater certtflei that it li not required to pay the Now Jertey Sal and/or Uw Tax on tK* purthote or purchaiet covtfod. by thli Ctrllfleol# boeaui* tho langlblo pereonal proporty pur- thated w ill bo uied for an exempt purpooe. Sold tangible personal proporty w ill bo uiod for tho following exempt purpoeei .fO r UBG o r conouwption d ire a tly aid exclu ilv ely lh r* March and develojment in th e exlwflmtt&ttr r lab o rato ry eniev ............................................................. Tho exemption on tho n i t of m M tanglblo personal proporty to bo uied for tho abovo detcrlbed oxompt purpato It provldod In (ubiectlOfl NJ.S.A.. $4i32B-| | fSoo reverie ride for firth* o f p rin cip a l oxompt vtoi o f tangible perromf pro p o rty and t ill In tho WoeIt wHh p ro p o t tvb ro d fo n cH alha). I. tho undoriignod purchoier, have road and complied with tho Initrudloni and rule* promulgated purtuant to tho Now Jonoy Sale and Uto Ton Act with roipoct to tho u*o of tho Exempt Lite Certificate, and it it my belief that the vendor named heroin In not roqulrod to collect tho taloi or u*e tax an tho traniactlon or. traniactlont covered by thli Cortiflcato. Tho underolgnod purchaser hereby iw ean (under tho ponaltloi fo r perjury and folio (wearing) thot a ll of the information hown In thli Cortlffeafe It true. COLGATE- EA W O LIVE CCMEAHY A VINCO IHOUtD MAO ANO COMnr WITH till INITMiCttONt o tv e t on (oth s w tt o r an RtMmoN cmrtncAti. NAMI o r WRCHAHR (Ot rMflM rCirMon of TmoHen) (Ngnafvr* ot o w ntrjm tnor, otBmr etcoraoreffM, ite.) . W a lte r L . B om - - Purch a sin g Department .................................................................................................... tAodr... of rumhomr) Je rse y C it y , H. J . 07302 Q E -C P C 0 0 0 0 4 1 52 INSTRUCTIONS FOR USE OF EXEMPT USE CERTIFICATES I C e e d Faith In general. a vendor who occepli an exemption certificte in "good foilh" it relieved of (ability l o t coHection ar paym rnt of tox upan trontocliont covered by the certificte The question af "good foith" it on* o ff a d a n d depend open o consideration of nil the condition! surrounding the Iron taction. A vtndor it presumed to be fam iliar with the low and H it raigolo* nom pertinent to.lhe butinett in which he dealt. - In order for "good foith" to be eiloblithed. the fallowing condition!.mult be met (o) the certificte mutt contom no ttoiemeni or entry which the vendor knows, or hot reason fo know, it ( d ie or'm it- leoding . (b | The certificle mutt be on officially promulgated certilicole term or o tubtlanliol and proper reproduction thereof. (<) The certificte mutt be doted ond executed in oCcOrdonca with the pubtilhed Intlrucfioht, and m u tlb e complete ond regulor in every respect- ' The vendor may. therefore, occept ihlt "good foith" Exempt Ute Certificate on a b ath for exempting M le i to Ih t signatory pur- choier provided that: ' |d ) The purchaser't Certificte of Authority number, indicating (hot the pUrcftOier It rtgtiterad with the New Jersey Division of Taxation, it entered on thefoceof the Certificate, (e) The purchoter hoi entered oil other informoHon required on the form. . (f I The vendor hot no reoton to believe that ihe property to be purchaied it of a type not ordinarily uied In Hm purchaser's butinett for the purpote detcribed in thlt Certificate. ' 7 - Im p ro per Certificte - Soles IromacHont which are not supported by properly executed exemption certificat thoH be deemed to be to coble retail tolai. The burden of proof that ihe fox w ot not required to be collected It upon the vender, ' .t ' . ... . 3 . Correction e f Certificle - In general, vendort hove `6 0 doyt offer dole o f tale to obtain o corrected certificte where the original certificle lackt material information required to `be tet forth in told certificte or where tuch Information it Incorrectly ttoted- '' t . A d d itio n al Pureh o t e l by Same Purchaser --Thit Certificate will terve to cover oddirtonctlpurchotei by the tome purchoter ol the tome general type di property. However, each subw'quent tblei sHp O rp0rchd's*invb|i`bated on' thit Certificate mutt show' Ihe purchoter't name, addreii ond Certificte of Authority number forfwjrpbtes of verifiedtioh. ' 5 . R eten tio n a t Certificate Certificates. mutt be retained by the vendor fur a period of not le thon three years from the dole of the tast.iale covered by ihe certificle. Certificle! mutt be in the physical pptieislon of the vendor ond ovariable for in- tpeclton on or before Ihe AOlh day tallowing the d a ft of the trontoction to which Hie certificlo relate!. 6 . (ht- niml iitiiinmn exempt utei lot which the Exempt U i* Certificate (Form $ T -4 )ii applicable ore Ih t following: Sales of machiiteiy. apparatus or equipment for ute or comumption directly ond primarily in the production, generation, "froministion or diftribulion ol got. electricity, refrigeration, iteom or woler for tale or in the operation of teweroge tyrttm t. (N.J.S.A. 54i32B-8 (m)(2}| ' So let of. tangible pertonol property purchoied for ute or contumplion directly ond exclusively in research ond development in-the .experimental-pr laboratory- tente. Such reteorch ond development tholl not be deemed to include the ordinary fettfng or inipedion of moteribli or product! for quolity Control, efficiency turveyi. monogement-itudiei, consumer surveys, advertising.- prom olioni or reteorch in connection with Hierory, historical or limitar project). (N.J.S.A. 3 4 i3 2 F 8 (n)j S o lti or ute of wrapping paper, wrapping twine, b ag t, corlont, lope, rope, fo b tlt, nonreturrloble container!, reusable milk container! ond oil Other Wlopping luppllei when luch ute it incidental to the delivery o f pertonol property which hot been told. N J.S .A . 54:326-8 (o)J - Solet of moterioli, tuch a t chemicolt ond cololytlt, used to. induce or cote o refining or chemical process, where tuch moterioit or on integral or essential part of the practising operation, but do not become o Component pari of Hie finished pro duct. |N.J.S. A, 5 4 :3 2 6 8 (t)j .` ' The rale of advertising materloli.to b.e.published in o newspaper. (N.J.S.A, 5 4 r8 fee)) The use of property for market sampling by the purchoter. [N.J.S.A 54i32B-t 1 (4)| . . R* * ' I REPRODUCTION OF EXEMPT USE CERTIFICATE FODMSi Private reproduction of Exempt Ute Certificate! moy be made without the prior permission o fth e Olvition of Toxalion, 5TATI OF MIW JIRSIY, DRPARTMINT OF TH TREASURY, DIVISION OF TAXATION Fwt Office lex 999, Tremen, N.. 06925 Q E -C P C 0 0 0 0 4 1 53 waiter a mucrone associates, ine. CONSULTING: ULTRAMICROANALYSIS MICROSCOPY SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 13 February 1979 Dr. Joseph P. Simko, J r . Colgate Palmolive Company 909 River Road Piscataway, New Jersey 08854 ' Dear Dr. Simko: Using transmission, electron microscopy and selected area electron d iffra c tio n we have analyzed three samples of ta lc . These ta lc s were designated as H.S., P .B ., and X.L. These samples of ta lc were dispersed in approximately 10 ml of fsopropyl alcohol and deposited onto a TEM g rid . The grid was then analyzed at 200 kV and 20.000X. We found a l l three samples to be completely free from asbestiform m inerals. The samples were extremely p la ty and there were indications of ro lle d ta lc shards, fragrance and coloration pigment, but we found no asbestiform m inerals. Thank you for consulting McCrone A ssociates. I f there are any fu rth er questions concerning th is report or the data contained herein, please fe e l free to contact me. Very tru ly yours, GRG:jd Ref. MA 7673 Gene R* Grieger Senior Research Physicist 2820 SOUTH MICHIGAN AVENUE - CHICAGO. ILLINOIS 60616 . 312. 842-7100 CABLE: CHEMICRONE Q E -C P C 0 0 0 0 4 1 54 COLGATE-PALMOLIVE COMPANY A Dtatoare Corporation RESEARCH AND DEVELOPMENT DEPARTMENT 909 Rivtr Road Piscataioay, Neto Jersey 08854 January 10, 1979 Mr. Ian Stewart McCrone A ssociates 2820 South Michigan Avenue Chicago, IL 60616 Dear Ia n , I have sent under sep arate cover th re e samples of Talc fin ish ed products fo r asbestos an aly sis. These are complex form ulations with th e exception of th e Heaven Sent. I 'v e attached the form ulations fo r your inform ation. We've applied o p tic a l microscopy and x-ray d iff r a c tio n and have found no evidence of fib e rs or amphiboles. In the Peachbloom and Illum ination samples, however, th e re are in terferen ces with th e x-ray and p a r tic le s coating to th e ta lc mailing o p tic a l microscope study d i f f i c u l t . Please use the b est techniques you can to determine p re ^ n c e of asbestos m inerals. The data are required fo r a p o te n tia l le g a l case. I would appreciate you giving them th e b est p r io r ity you can. A purchase order w ill follow separately. Sample I .D .'s are: ! Sincerely yours, JPS:Is Attachment C 5137-3 Q E-O PC 00004155 FORMULATIONS Peachtloom Magnesium S ilic a te E/V Talc T O 2 Zinc S tearate Kaolin Cosmetic Ochra Red Oxide Illum ination Korean Talc Zinc S tearate Red Oxide Concentrate Cosmetic Brown Concentrate Cosmetic Tan Concentrate M icrocei Marcol tO Heaven Sent Talc Magnesium Cartonate 35# 36 10 10 19 1 1 68 3 3 8 8 3 6 96 3 JPSMs 1/10/79 Q E -C P C 0 0 0 0 4 1 56 a i j ; . uyi . >ni oN ~ M tT i-n -5OLST/. ORIGINAL PURCHASE ORDER Show this number and prefix on in voices, packing /jAh 630319 COLGATE-PALMOLIVE COMPAN A DELA W ARE CORPORATION ^ tOS HUDSON S T R E E T , JERSEY C IT Y , N.J. 07302 ATifeRfiO f/shf SH IP TO McCrons A ssociates 2820 South Michigan Avenue Chicago, I llin o is 25 m 13 16 19 ae G REN E ST. JERSEY C IT Y , N .J. 07302 903 R IV E R RD. P 1S C A TA W A Y. N .J . 0B&54 20 GRAND ST. JE R S E Y C IT Y . N .J. 073 02 R E C E IV IN G S T A T IO N J E F F E R S O N V iU L E . IN D IA NA 471 30 R E C E IV IN G S TA T IO N K A N S A S C I T Y * K A N . 5 05 D ISCO U N T TERM S 1 2/10 N /30 2 N /30 3 1 /1 0 N /30 4 Net C ash 5 Trade SH IPPIN G TERM S 1 HD FOB D estination 2 Q FO B Shipping P t. (Pr&~Pay& B tfljS e c B e /o w 3 F O B S h i p p I n g P t . (Collect) C ity 4I F A B O V E D ' ;? .H O BE MET N O T IF Y 22 26 23 | J be^-- - "" |7 1 0 C A R L T O N S T . I b E R K E L E Y . C A L IF . 94710 300 PAR K A V e . NEW Y O R K . N .Y . 10022 A TTN : R ec e iv in g C lerk YOU ARE AUTHORIZE!) TO FURNISH THE ARTICLES LISTED HEREON IN ACCORDANCE W ITH THE TERMS AND CONDITIONS pN THE FACE AND BACK OF TH IS ORQER, q u a n t it y a n d u n it sym bol number PRICE Three ta lc samples fo r microscope analysis fo r asbestos m inerals cooed P.B, IL, and H .S .. . co st approx. $1000 : Samples sen t under sep arate cover a t 'enion Mr. Ian Stew art / HOTS: This i s a one time req u est. MAIL INVOICES) to: JX.EXEM EL .i ' v>o _ AAr ^Coueio-PcMsvo 4. - Please send invoice to Helena K ubinstein ATTEMTIOhV C? Rjvor Hoad Pscatawr/, N. J- 03C54 Mr. Herb Schneider. .. V E N D O R T O P R O T E C T A L L METBrbr-iaAR X S A G A I N S T C 0 RRJ3 S J - Q N -B - y - g O T f A B L E P R O T E C T I V E S E A L I N G . \ t \ J o -ni -- tA. -V -c CL-9) x k t- - Ohjvo . SELlERS INVOICES that include authorized tramportotion charges, must bB supported by prepaid freight bil! ot^cO{.GATE PALMOLIVE ^COMPAN^ copy of original bill of lading. . . c .r. MARK PACKAGES with purchase order number, symbol number, contents and quantity. Acceptance ottiiis oorder Is to be deemed certification that you have read and agreed to the terms and conditions on the back hereof. PAYMENT WILL NOT BE MADE AGAINST PRO FORMA INVOICE. RE6CftV UNLOADING spaee and time fafhoqyy bydc by telephoning1 2flK d M TT3pQ ffrtQ'mon zyassawi -- `a m mi Q E -C P C 0 0 0 0 4 1 57 A TERMS AND CONDITIONS WARRANTY -- The Seller expressly warrants and agrees that there has been compliance w ith.and no violation of any trademark rights, patent rights, copyright, or of any rule, law or regulation of the Federal Government or of any State or any of their respective agencies or political subdivisions, in the manufacture, production, sale and or shipment of the goods hereunder: and the Seller will indemnify and hold Purchaser harmless from any or all costs, damages, fines or expenses (including counsel fees and fees of expert witnesses) which may be incurred by the Purchaser by reason o f any claim or suit arising out of the infringement of any trademark, patent right or copyright and/or by reason of any citation, claim or suit for damages and/or penalties brought'against the Purchaser based upon any injuries, damages or Violations resulting or claimed to have resulted from any alleged infringement or defect in such goods or ingredients or parts thereof. EQUAL EMPLOYMENT OPPORTUNITY -- The Equal Employment Opportunity Clause Section 202 of Executive Order 11246 as amended related to Equal Employment Opportunities and Implementing Rules and Regulations of the Secretary of Labor are incorporated herein by specific reference. CHANGES IN ORDER -- This order cannot be changed, modified or discharged in any maimer except by agreement in Writing signed by a duly authorized representative of the Purchaser. The Purchaser reserves the right to (1) mal-.c changes in the order (2) cancel all or any p a rt of the order a t any tim e by notice in w riting. The Purchaser shall not be responsible for costs incurred by the Seller in connection with this order, after the date of receipt of the change or cancellation notice. Unless the Seller presents to the Purchaser an itemized statem ent of claim against the Purchaser within twenty (20) days afte r the receipt of notice of such change or cancellation, the Seller shall be conclusively deemed to have waived all claims against the Purchaser with respect thereto. CANCELLATION FOR SELLER'S DEFAULT -- Should the Seller fail (1) to effect delivery on or before the specified delivery d atc(s) (2) to deliver goods in all respects conforming w ith th e requirem ents (3) to duly perform Seller's obligation under each and all of the terms and conditions of this order, the Purchaser may cancel this order in whole or in part. W ithout prejudice to the foregoing, the Seller agrees to report promptly to the Purchaser any delays in performance or in shipment of the goods covered by this order. SPECIFICATIONS. DRAWINGS, ETC. -- All specifications, drawings, plans, designs, samples, or other documents referred to in this order shall be deemed an integral p a rt of this order ns fully as if set out in full herein and Seller w arrants that ali deliveries and/or performances hereunder shall conform thereto, each delivery and/or per formance being subject to the inspection mid approval of the Purchaser, whether or not any prior payment shall have been made thereon by the Purchaser. NONCONFORMING MATERIAL - If Seller delivers defective material or material not conforming to the agree-upon specifications. Purchaser may (1) hold such material at Seller's expense pending instructions as to disposal. (2) return it to Seller at Seller's expense, or (3) utilize it in the form received or uftei tip-grading or other operations are performed on it. or utilize it in a different manner or in different proportions with other products Ilian was intended, and Seller wiU be able for any diminution in the value to Purchaser of the material and for any incidental or other damages suffered by Purchaser resulting from such defectiveness or nonconformity. No replacement of defective or nonconforming material will be made by Seller unless authorized by Purchaser. LIABILITY FOR DAMAGES -- Whenever Seller shall, by virtue hereof, have property of the Purchaser in its posses sion. the Seller shall be deemed an insurer thereof and shall he responsible for its safe return to the Purchaser. ASSIGNM ENT -- This order shall not be assigned or transferred without prior written consent of the Purchaser. WAIVER -- Purchaser shall not be. deemed to have waived any of-its rig h ts hereunder unless such, waiver shall have been signed by a duly authorized representative of the Purchaser. No such waiver, unless expressly stated there in. shall be effective as to any delivery or other transaction which may occur subsequent to the date of the waiver, nor as to any continuance of a default after such date. LABOR AND/OR MATERIAL -- With respect particularly to orders covering labor aiul material. Seller agrees to start work immediately, to proceed with the utmost dispatch and to complete all of the work under this order. All such work shall be.performed in strict accordance with Purchaser's " General Conditions for Contract Work'1Specification No".0920 CE. nor shall work be permitted to start on Purchaser s property until required Insurance Certificates have -been received by Purchaser. Time is hereby declared to be the essence of this order. Prices shown are firm and not subject to adjustment because of increase or decrease in material prices and/or wage rates and/or freight rates and/or other items of cost. The acceptance of the final payment by Seller shall be-held to be a waiver and discharge of any and all daim s.and demands against the Purchaser for compensation and damages on account of any m atter arising o ut of or in connection with the Contract or the performance of the work. Any extra or additional work performed by Seller ' shall be on a fixed price basis or cost'plus fee basis and rffust be in. each case, first authorized in writing by Purchaser. Seller's rates for such purposes shall be as set forth in a quotation from Seller prior to startingany such extra or additional work and confirmed by Purchaser's prior written authorization- 1 QE-CPC00004158 *r4(1077. M >1 t t ba i m p k l f j by ym hgH i ihmI i>*n ta an (atalm * by raaOaf. I ( j (nihvtKam an b a d af <Mt Catrifkata. THHISWUCItTMrHoTTIHNHKICANOTAHICNMHIACAYTMKMMOT or sakvicn MAY BE REPRODUCED #ta!r itf Nrui 3rrart{ wvmoN or taxation Mill TAX IXIMPT USI CIKTtnCATB FORM ST-4 ru i HAST* Y (.cittrKAlt or aiuihmiiiy nhmwr 1 3 1 -8 lg -5 f)*j/0 0 1 (Maataaf Y m i t r ) City Oof* The undersigned purchaser certifies that II ( nor required to pay the Now Jersey S alt* and/or Dm Tax on the purchase or purchase* covered by th li Certificate because th* tangible personal property pur* chased will bo used for an exempt purpose. Said tangible personal proporty w ill bo used for iho following exempt purpose* .fOJ? Ufl O r conovwnprtlon d ir e c t ly ad t c lu ilv o ly in rt a re h and d *v lo jo n t in th e x p e r t n e n t ll 6Y lih b r a t t t iy iW tii*. ............................................................................. Tho exemption on tho iolo of aid tangible personal property to bo used for Iho above described exempt purpose It provided In subsection N.J.S.A. 54i329-[* | (5w rovono dd for listing o f principal axampl uses of tangible p o rto o o l property and HU In fhe block wUh propor subsection cHerMonJ. I. iho underilgned purchaser. have road and complied with tho Instructions and ruin* promulgated purluant to iho Now Jersey Salt* and the Tax Act with reipect to tho use of the Exempt the Cortlflcato, and it I* my bellsf that tho vendor named heroin I* not required to collect the Mil* or u m tax on the transac tion or transactions covered by thlo Certlflcat*. The undersigned purchaser hereby swears (under the penalties for perjury and fatso swearing) thot a ll of tho informaffon shown In this Cortlflcato It true. OCAXOIVtMVMINIHrNTVDtOOOWHNkITCSHSOIHITTOWHHUIILCS1DANKSXTMTtI*W.ADCOTfIAOANNNDS C O L O A T E -B U M Q L IV E CCMBANY NAMI OEMKCHASCK(e* neliM DlrMofl efTmotton) (Stanolitra af WMrjiartMr. effkxr of larpwmhm, ate.) , . w a ite r L . B o m --P u rch asin g Departm ent ............................................................................... .................... lAodran af fw*ewr) C it y , H. J . 07302 Q E -C P C 0 0 0 0 4 1 59 SM INSTRUCTIONS FOR USE OF EXEMPT USE CERTIFICATES I G o o d Foilh In general. o vendor who occepts on exemption certifico! in "good foith" it relieved of Mobility for coMecfiofl or poym m r of tax upon transactions covered by the certificte The queelion of "good faith" it one of fact and depends upon a consideration nf all the candilioni surrounding the transaction. A vendor It presumed to be fomltior with the low ond H it regulo1 liant pertinent to the bunneu in which he dealt. -. In order lor "good foilh" lob e etloblithed. the following eondiliant mutt be melt (o) The certificle mutt contoin no tlolement or entry which the vendor knowtr or h a t reoton fa know. It folie oc'mit- leoding (b) The certificte mutt be an officially promulgated certificte form o r a tubiiontiol and proper reproduction thereof. (O The certificte mutt be doted and executed in accordance with the publithld Instructions, and mutf be complete an d regulor in every retpecl. . -, The vendor moy, therefore, accept thii "good faith" Exempt Ute Certificte on a b a tll far exempt!tig latei to the tignafory pgrchofer provided thof: (d) 1h purtho tor's Certificot* of Authority number, indicating thot the purchaser It registered with the Mew in i e y Divdan of Toxption, It entered an the foce o l the Certificte. (e) The purchaser h at entered ol) other information required on the form. - .{() The vendor hot no reoton to believe that the properly to be purchclted it of o type not ordinarily used In the purchaier't business far the purpose described In this Certificle. 1. Im p roper C e rtific a te - Sotes transactions which ore not supported by properly .executed exemption certifico lei lhaH be deemed lobe toxoble retail tales. The burden of proof thol the tox wen not required lo b e collected ft upon the vendor, 3. Correction of Certifcale In general, vendors hove `0 doyt after daie of tale to obtain a corrected certificate where the original certifico I locks material information required to`.be tel forth in told certificte or where such in formation it incorrectly stated. 4. A d d itio n al Pu tchaeei b y S a m * Purchaeer--This Certificte will serve to cover odditjhpl.pyrchpiei by the tom purchoter ol the tome general type of property. However, each tubieqUenl t d lii Up orpuirchqitf'in^^ on th ii Certificte mutt show lha purchaser'! nome. o dd rettond Certificate of Authority number foVprpotes'ofienfi'cd'tlon. " . . . . 5. t e le n lien ef Certificte Certificle! mutt be retoined by the vendor far a period of not te n thon three yoo'rt from the dote of theldit vole covered by the certificate..Certiflcot#i mutt be In th*. phytfeo! possession of the vendor ofld available for in* vpeettan on or before the 60th doy following the date of the transaction to which the certificte relates. 6. f h r mov i imimnn exempt uses lot which the Exempt Ute Certificle (Form ST-4) it applicable ore the following: Sales ol mochineiy. apparatus or equipment for ute dr tOniOmpiibh directly ond primarily in the production, generation, transmission or distribution of got, electricity, refrigeration, tleom or w o lir for late or In the operation of sewerage tystemt. IN.J.S.A. 54:32B-8 im )(2)j Sale! o f tangible personal properly purchoted for ute or consumption directly and exclusively in rettorch ond development in the experimento! or taboralary tente. Such research ond development shall not be deemed to include the ordinary l*iting or inipectiori'of moterials o r produc'd (or quolity control, efficiency surveys; management Studies. Consumer surveys, odverliting, promotions or research in connection with literary, hiiforicot or similar pra*cti. [N.f.S.A. 34i328-8 (n)| Soles or use of wropping p o p ir, wrapping twine, bags, corldns, toper rop*, (obeli, nonrehrrnoble conlolnert, reusable milk containers orid oil other wrapping supplies when such use is incidental to the delivery of personal property which h at been sold. |N J.S.A. 54:328 8 (o)| Soles of moierials, such os chemicols and catalysis, used to induce or couse a refining or chemical process, where such materials ore on integral or eitentiol part of the.proceulng operation, but do not become o component part of the finished pro duct. IN J .S .A . 5 4 :3 2 8 8 (t)| ' ' The sole of advertising moterlols to be published in o newspaper. IN.J.S.A. 94i-8 (ee)| 1 The use of properly far market tompling by th* purchaser. (N.J.S.A 54i328 11 (4)| > j * , * ' I REPRODUCTION O f EXEMPT USE CERTIFICATE FORMSi Private reproduction of Exempt Ute Certificates moy be mode without the prior permission of the Division of Taxation. STATI OP NtW JIRSIY, ORPARTMINT OP THI TRIAIURYr DIVISION OP TAXATION Poet Off! lax 991, Tramen, N.J, OMIS N QE-CPC00004160 X -<S4tA_ J^ v u -e r^ ' i^u U. Q E -C P C 0 0 0 0 4 1 61 COO 00COO QE-CPC00004162 'F V S PROJECT COST talc PROJECT TITLE: CYPRS INDUSTRIAL MINERALS CO SPONSOR: ADDRESS: 651 Metuchen Rd South P la in fie ld , NJ 07080 RECORD MA PROJECT NO. : DATE RECEIVEdT P.O. NO.: # 0 7 5 COMMITMENTS: $ Contact: Mn\ l i e TM ' f!1\ < > & >iT H SUMMARY OE PROBLEM: Lab Notebook References: No. pp. Initials No. pp. Initials No. pp. Initials Photomicrograph.ic record no. / Telephone No. . Sample disposal: returned filed (where) discarded DIRECT COSTS (Exclusive of oper. . Individual time time on inst. below) Travel Charge Sumra Date Name Hours Charge Date Traveler Destination Cost l oerwrvvJa. = -- ___ X ~ l fW F ~ & b s L JhtfM L ____H.___ iJS iS J ___ *___ -_____ 1 Instrument time Individuals $ Instrument Travel Outside Other Total Charge $ Date Hours Charge Date Company Cost .SEM TEM XRD EMP IMP ESCA EMMA MOLE Photo Photo Materials Supplies OK for billin Project Ldr Group Ldr _ 3. ^ rf TOTAL CHARGE fr p p BILLED TO CLIENT $Z-------------INVOICE NO. (S)^ ^ ) fs& A a*p-i RME PROJECT LEADER: A %C L AB\ - QE-CPC00004163 ; &'i \ /. / v\ , Oo ; -\ * iij: /;: J. \ ' -V-- fW a, r i i jh x A l '1 j -.-' yr.\ (A A ' j J - . ........................ ;) , </ A A _ y_ /A j-A f V 'A -a , , x..i /'7 i il ^ .,- v f Ay. *' v :P / /' ~-d-P--tr-i \ If i \ Z 0 l 6 S / . > ' : V: :' . AsV\ dc f la v/ ^ ia A V V , J / [ A /l AV. ; *' V 5 jo : A i(.X0 ili, k- i . ! A 4 . L- X ; A 4 / .. A ^ u C - U l i' I i r ? s ? j( & -7 l l \ 4 4 . .. : - W .: - -r mi i ,-TfL - ;L ^V V va,, / C '-; '- r ' V . r f - M . J W & /(A ^ *11 l > s 4 - | . O , I d /. f - l l . -JV-I r s ^ ^ - 4 --OO^L. , | A j f / \ f l A ')J V. !. 'H..'I. ^/ a_.-Ui ^. .. 4 .a , aaU m '1 ''A' \ r! i -AVi.:- ':-^/SA' ri V X -*--- Ar tA , K i y- r 'V )'1 \t .. ;- :.i : QE-CPC00004164 w a ite r c. m ccrone associates, inc. CONSULTING: ULTRAMICROANALYSIS MICROSCOPY SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 25 February 1983 Mr. K eith B. Lehman Cyprus In d u stria l Minerals Company 651 Metuchen Road South P la in fie ld , New Jersey 07080 Dear Mr. Lehman: I have completed ny asbestos analysis on a ta lc sample labeled "Monoblend", Lot 1120965A RM3833 and submitted under your purchase order #45079The sample -was examined w ith the transmission electron microscope. The sample contained no detectable asbestos. The lim it of detection fo r the method is approximately 0.1% per weight o f asbestos. Thank you for consulting McCrone A ssociates, please contact me i f you have any questions. Sincerely, Richard M. E llis , J r . Research Microscopist RME:fe Ref: 9863 2320 SOUTH MICHIGAN AVENUE - CHICAGO, ILLINOIS 60616.312/842-7100 CABLE CHEMICRONE QE-CPC00004165 j t e g y p r u s in d u s tria l M in e ra ls C o j$ |jj |y OMih How1S tm t ! \jomAOqd \a, Giffrocniq 90071 4^-.J . -.Tj 12131 483-3700 Purchase Order < ' Ship To: s.^ r Acknowledgement Requested K e ith B. Lehman CYPRUS INDUSTRIAL MINERALS 651 M etuchen Road - : So. P la in f ie ld , N .J. 07080 Vendor A` ' ' *:"?:. ; ` ',w &&': L !_; W alter McCrone A s s o c ia te s In c . 28 28 S o u th M ich ig an Ave. .. C h icag o , ILL 606 07 ' ' .' A ttn : R ic h a rd M. E l l i s , J r . . .tK Date To: 2/9/83 Quantity Ordered Quantity Received '/b'BSCriptiQn Invoicein tripJteata ... ` ' ' - SAME Date Required ASAP Unit Price Terms N et 30 Total Please run '..youKu^egular test ,,for asbestos fibers, on enclosed sample. ^--TYri- . .. Please use in v o ic in g fo r/th e y e a r 1983. Ak 3 >fi/ 45079 A b o v e oxd e r futnbse m u s t a p p e a r on all papers and packages relativ to tills order, f' g . Approved CYPRUS ' ' . QE-CP000004166 w aiter c. mccrone associates, inc. CONSULTING: ULTftAMICROANALYSIS MICROSCOPY SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY . 22 epterriber 1981- M r . Vern Alltus Cyprus IndustrialMinerals Company 651 Metuchen Road South Plainfield, New Jersey'07Q80 Dear Mr. Alltus; I have completed m y asbestos analysis of a talc sample labeled.Jtyonpblend, . ' lot number 812065. .' The sample w a s examined`with.the transmission electron microscope. No asbestos minerals were detected. The' analysis has a detection limit of approximately 0.1% by weight. - Thank you for consulting McCrone A ssociates', please contact itje if you have any questions. . ' RME/pi M A .9863 Richard M. Ellis, Jr. Research Mi oroscopist 2820 SOUTH MICHIGAN AVENUE CHICAGO, ILLINOIS 60616 312/842-7100 * CABLE CHEM1CRONE QE-CPC00004167 Cyprus Industrial Minerals Company 651 Metychen Road South Plainfield, N.J. 07080 Telephone (201) 754-4880 TWX 710-997-9528 August 21, 1981 L - Mr. R ick E l l i s W alter C. McCrone A s s o c ia te s , In c . 2820 So. M ichigan Ave. C hicago, I l l i n o i s 60616 Dear Mr. Ellis: E n clo se d h e re w ith p le a s e f in d one (1) sam ple o f Mono b le n d , L ot No. 812065. P lease perform th e u su al t e s t fo r asb esto s and re tu rn the re s u lts to our o ffic e . Very tr u ly y ours, CYPRUS INDUSTRIAL MINERALS KBL/hbt E nclosure K e ith B. Lehman A sst. P la n t Supt. CYPRUS Q E -C P C 0 0 0 0 4 1 68 w a ite r c. m ccrone associates, inc. CONSULTING; ULTRAMICROANALYSIS . MICROSCOPY SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 28 August 1981 Mr. Vern Alltus Cyprus In d u s tria l M inerals Company 651 Metuchen Hoad South P la in fie ld , New Jersey 07080 Dear Mr. A lltu s: ' I have completed my asbestos analysis of a sample of Cyprus Mono blend ta lc Lot #712165. The sample was analyzed by transm ission elec tro n microscopy and e le c tro n d iffra c tio n . The sample contained no detectab le asbestos m in erals. The lim it of d etection is approximately 0.1% by w eig h t. ' Thank you for consulting McCrone A ssociates. I f you should have any questions concerning th is an aly sis, please contact me. ' . Sincerely, ' Richard M. E llis , J r . Research Microscopist RME: fe Ref-. 9863 2B20 SOUTH MICHIGAN AVENUE CHICAGO. ILLINOIS 6D616 * 312/8+2-7100 CABLE CHEMICRONE QE-CPC00004169 waiter c, mecrone associates, inc. CONSULTING: ULTRAMICROANALYSIS MICROSCOPY SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 29 APfil 1981 Mr, Yejm Alltus Cyprus Industrial Minerals Company 651 Metuchen Road . South Plainfield, NJ Q7080 Dear Mr, Alltus: . I have, completed jny asbestos analysis of a sample.' of Cyprus Monoblend Talc lot #311865 received by HS on 20 March 1981, The sample was analyzed by transmission eleqtfcin .micro scopy and electron diffraction. The sample contained no detectable asbe.stos minerals, Thank you for consulting McCrona Associates,' Please contact us if you have any questions, Sincerely, . RME:jr Ref. MA 9863 Richard M, Ellis Research. Miproscopist' 2820 SOUTH MICHIGAN AVENUE . CHICAGO, ILLINOIS 60S1G 312/842-7100 CABLE: CHEMICRONE QE-CPC00004170 waiter c. me crone associates, inc. CONSULTING: ULTRAM1CR0ANALYSIS MICROSCOPY SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 29 April .1981 Mr, V e m Alltus Cyprus Industrial Minerals Company 651 Metuchen Road . South Plai,nfield, NJ 07080 ' Pear Mr, Alltus; . I have completed my asbestos analysis ,of a sample of Cyprus Monoblend Talc Ipt #311865 re.csi.yed b y ps on 20 M arch 1981, 'The sample was analyzed by transmission electron .miebb" scopy and electron diffraction, The/ sample contained no detectable asbestos, minerals. Thank you for consulting McCrone Associates, Please contact us if you have any guestions, Sipceyelyf . RME;jr Ref. MA 9863 Rich^td M, S l lis Research M icroscopist' 2820 SOUTH MICHIGAN AVENUE . CHICAGO, ILLINOIS 60616 312/642-7100 . CABLE: CHEMICRONE QE-CPC00004171 Cyprus industrial Minerals Company Scu tw. VtLjy H -^5 To Walter C. Me Crone From Vem All.us__,__________ Subject Colgate Samples 1 Interoffice Correspondence Dale ______ March 20, 1981 Inclosed" are two d ifferen t samples of M eterial to be tested and the re s u lts returned here to me as per our reo ien t conversation. LOT # 511865 i s a new lo t. I s t i l l have not recieved the return of which I requested returned to me. a CYPRUS QE-CPC00004172 waiter c. me crone associates, inc. CONSULTING: ULTRAMICROANALYSIS MICROSCOPY SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 25 March 1981 Mr. V e m Alltus ' Cyprus Industrial Minerals Co. 651 Metuchen Road South Plainfield, New Jersey 07080 . ' _. Dear Mr. Alltus: I have completed my asbestos analysis of a sample of Cyprus Monoblend Talc Lot #110865 received by us on 11 March 1981. " The sample was analyzed w i t h the transmission electron microscope (TEM) and electron diffraction. The sample contained no detectable asbestos minerals. A few fibers of a clay mineral, sepiolite or attapulgite, were seen. '' , Thank you for consulting McCrone Associates. Please contact us if you have any questions. .Sincerely, RMErgb Ref: 9863 Richard M. Ellis, Jr. Research Microscopist 2820SOUTH MICHIGAN AVENUE .CHICAGO, ILLINOIS 60816.312/842-7100 . CABLE: CHEMIcRONE QE-CPC00004173 9 QE-CPC00004174 e QE-CPC00004175 PR O JECT COST RECORD PROJECT TITLE: talc sample for asbestos TEM) SPONSOR:______ L.YPKT.TS INDUSTRIAL MINERALS--CO---------- ADDRESS: -? 2 0 0 -gnuLh Altuu Way - P.0. Box 3419 nglewood, Colo--- ST55" PROJECT NO!. : MA 1119' DATE RECEIVED: _ n -- f -- - ir t -- i r . P.O. NO.: TK.-UU/4-S----- COMMITMENTS: $ "3D------ Contact:________ Dr. Kenneth. W. Olson Telephone No. O303'1 740 SUMMARY OE PROBLEM: Lab Notebook References: N o ._____pp. _____ Initials _ No. _____ pp. _____ Initials _ N o .____ _pp. _____Initials _ Photomierographie record no. Sample disposal: returned _______ filed (where)__ discarded_____ "' :' DIRECT COSTS Individual time Date Name (Exclusive of oper. time on inst. below) Hours Charge Travel Charge Summary Date Traveler Destination Cost Individuals $ Instrument Travel Outside Other Instrument time Date SEM TEM XRD EMP IMP . ESCA EMMA MOLE Hours Charge Date Company Photo Photo Materials Supplies Total Charge $ Cost OK for billing ' ' i _j l u Group Ldr .A. *. ' ';.m . ,:s:*' TOTAL CHARGE $ '________ _ BILLED TO CLIENT $ 3 J o INVOICE NO. (S) 3 PROJECT LEADER: _ DPP ^ "f`Jr, ... . `,m i QE-CPC00004176 f J& t) w a ite r c. m ccrone associates, inc. CONSULTING: ULTRAMICRQANALYSIS * MICROSCOPY SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 21 October 1982 Dr. Kenneth W. Olson Cyprus In d u stria l Minerals Company 7200 South Alton Way Englewood, Colorado 80155 Dear Dr. Olson: Our laboratory has completed the asbestos analysis of ta lc sample "Altac 400, 052582" under your purchase order TK-0074-82. No asbestos was detected. Approximately 0.1 to 0.15 grams of m aterial was suspended in 10 mis o f .01% methyl cellulose. This was ultrasonerated for 15 minutes and a drop o f the supernatant liquid was placed cm a carbon coated transm ission electron microscope g rid . The sample was then examined by transmission electron microscopy. Enclosed with th is report are electron micrographs of the ta lc . I f you have any questions regarding th is analysis, please do not h esitate to c all. Sincerely, DPP:fe Enel. Ref: 11196 Deborah P. Palenik Manager, Electron Optics Group 2820 SOUTH MICHIGAN AVENUE CH1GAGO. ILLINOIS 60516 312/S42-7100 CABLE CHEMICRQNE QE-CPC00004177 w a ite r c. m ccrone associates, inc. CONSULTING: ULTRAMICROANALYSIS MICROSCOPY SMALL PARTICLE PROBLEMS SOLID-STATE CHEMISTRY 21 October 1982 Dr. Kenneth W. Olson Cyprus In d u stria l Minerals Company 7200 South Alton Way Englewood, Colorado 80155 Dear Dr. Olson: Our laboratory has completed the asbestos analysis of ta lc sample "Altac 400, 052582" under your purchase order IK-0074-82. No asbestos was detected. Approximately 0.1 to 0.15 grams o f m aterial was suspended in 10 mis of .01% methyl cellulose. This was ultrasonerated fo r 15 minutes and a drop o f the supernatant liq u id was placed on. a carbon coated ' transm ission electron microscope g rid . The sample was then examined by transmission electron microscopy. Enclosed with th is report are electron micrographs of the ta lc . I f you have any questions regarding th is analysis, please do not hesitate to call. Sincerely, DPP:fe Enel. Ref: 11196 Deborah P. Palenik Manager, Electron Optics Group 2820 SOUTH MICHIGAN AVENUE CHICAGO. ILLINOIS 8DG16 * 312/842-7100 CABLE CHEMICRONE QE-CPC00004178 Cyprus Industrial M inerals Com pany Tate Division 7200 S o u th A lton W ay. P .0 . Box 3419 E nglew ood. C olorado 80155 303-740-5444 J u ly 20, 1982 Ms. D eborah P a le n ik W a lte r C. McCrone A s s o c ia te s 2820 South M ichigan Avenue Chicago, I l l i n o i s 60616 D ear Ms. P a le n ik : Enclosed, p le a se fin d ta lc sample " A lta ic 400, 052582" fo r a n a ly sis fo r asb esto s and a sb estifo rm m inerals using th e TEM-SAED m ethod in y o u r l a b o r a t o r y . As p e r o u r te le p h o n e c o n v e rsa tio n o f Ju ly 20, 1982, t h i s work i s to be done u sin g ou r P.O. #TK-0074~82 and i s to c o s t $300.00. As we a r e e a g e r to o b t a i n th e r e s u l t s o f y o u r a n a l y s i s , we hope t o o b t a i n y o u r r e p o r t so o n . S incerely, K enneth W. O lso n , Ph.D . KWO/mc E n clo su re C. R . Moebus QE-CPC00004179 waiter c. me crone associates, inc. Q E -C P C 0 0 0 0 4 1 80 waiter c, mecrone associates, inc. GE-CPC00004181