Document Oz3e53dQo9VzyYMJmZZyr4wxv

A R a a 6 -c r? \5 ACUTE TOXICITY TO FISH (RAINBOW TROUT) TEST SUBSTANCE________________________________________________ Identity: A mixture containing perfluorooctanesulfonate, which may also be referred to as PFOS, FC-95, or as a component of FC-203. (1Octanesulfonic acid) (CAS # 2795-39-3). Remarks: The 3M production lot number was not noted. The test sample is FC-203. Current information indicates it is a mixture of 1.34% PFOS, 35% diethylene glycol butyl ether, 37.85% water, 20% ethylene glycol, 2.66 % Sultone foamer, 3% sodium octyl sulfate, 0.1% sodium lauryl sulfate, and 0.05% tolyltriazole. The following summary applies to a mixture with incompletely characterized concentrations of impurities. Data may not accurately reflect toxicity of the fluorochemical component of the test sample. METHOD:_________________________________________________________ Method: Not given. Type: Continuous flow GLP: No Year completed: Not given. Species: Salmo gairdnen Supplier: Not given. Analytical monitoring: pH, and DO Exposure period: 96-hours Statistical methods: Not given. Test fish age: Not given. Length and weight: Not given. Loading: Not given. Pretreatment: None Test conditions: Dilution water: Not given. Dilution water chemistry: Not given. Lighting: Not given. Stock and test solution preparation: Stock solution of 160 g/L prepared, then diluted with dilution water to prepare the sample concentrations. Concentrations dosing rate: Flow-through Stability of the test chemical solutions: Not given. Exposure vessels: Not given. Number of replicates: Not given. Number of fish per replicate: Not given. Number of concentrations: five plus a blank control Water chemistry during the study: pH range (0 - 96 hours): 7.3 - 7.8 Dissolved oxygen range (0-96 hours): 7.2 - 9.0 mg/L 000506 RESULTS Nominal concentrations: Bk control, 25, 50,100, 200, and 400 mg/L. Element values: 96-hour LC50 = >400 mg/L Element values based on nominal concentrations Remarks: Testing was conducted on the mixture as described in the Test Substance Remarks field. The values reported apply to that mixture and not the fluorochemical proportion alone. CONCLUSIONS___________________________________________________ The test sample 96-hour LC50for rainbow trout was determined to be >400 mg/L. No mortality or sublethal effects observed at this concentration. Submitter: 3M Company, Environmental Laboratory, P.O. Box 33331, St. Paul, Minnesota, 55133 DATA QUALITY___________________________________________________ Reliability: Klimisch ranking = 3. Testing lacks record of methodology used and data sheets. Sample purity was not properly characterized and the study lacks analytical confirmation of the amount of fluorochemical proportion in the solution. REFERENCES___,_________________________________________________ This study was conducted by the 3M Company, Environmental Laboratory, St. Paul, MN. O T H E R __________________________________________________________ Last changed: 6/27/00 00050V TC-ZOZ ^ U A U C ^ M ^ iT `'i'b BEST copy ava ila ble LC SO XXJiAM jCi to ^'fytyudC ( J a ^ w v o ,,qcljaJ L - i& 2 i> __ C o ^ L J k ^ L p t o - u ? //tA o i i^ a o c r -C* : M g V ^& z J ra M X ^ *2*} fr h K *Q & x& r- aJr 4 o Q rv ig / E o ulm ^JQ As [A s Q O c f- fc u x ) ko cbujcrvMiA V^oXjl^>,, ^ ^ t -9 K<j< ^^4< Ca-^&kj XM-JUa^______ ______________________________________________________ bx& oc ' * 2 s , 5 P , [q <o if3 j & o a - ^ y 4o<g JLd^^ ye- ( L . Jl ivjo vy v A jAj ^ > U o ''T-^rryj ~~1~ -^~ Q J r Q y 4 ff <3k X c a X ' __ ^ CuL^ fcr ^t r / - '-JiL -ts p K ~ ^> 0 - 7- 0 _px|_____ l~ _ _______l_y__________________ ________ jCjJ h . ..J t& * r!fG l^ & 0 S ..... i h l 2>C W 5 S" 60S00 Av \J K - \y ' \, ; a ia x n iv A v A d o o is a a v< '"^'v ^>' V ' I / V ,. \ V \ v- Q .' i * *"T - ! - V r '"' ,, ~-i r \\ r ~-- n ' -x> yr C-. V X > >; i f ii >- - -V r y -iir A' " _C Y ...rV A, A 1,bV.Vi v';. J { VV l: y ro ' < y y / ~ Vi V r; -r 3 ''ri fV , ' j- - ( 'V O f ' \< 1v ^ \ F r - ' A ' y c , r-w-' gto ,-' C\ i r,-1' '~v \ - :KA' -, - V.. *+'v.y V ~ V-C r-r'f' v- r- A siC r:: ^r _ 'A .** -'-'-'SV- ' ,< .r. ' '' ' -V CK A m f " " sa r H. : a v ~ ' ot >^ .A ' < * Y V i i ' ' * -"A-.: .>-7 ' ^ ' - A ' ' K . ;,. v t - -,Ar'-;------n y r ^ T 0\ v-j. s ' "' ; y .; ' i y a > j -K V i'if.'- r c-c-os,-' V " y i . M ; ~V KC ' T' r \ V qYTT" ' y i ' .*> A - a ;r./--. a A ' . .' < -, v * y, . " y n i vA H -TfV. >a t t T <,r r 0O ~oaJ OS- - 5 < f" OV>Ot>-y ^yyy< y\^ f ~ V ^ ktoo^ J/(f*