Document Oz0mpKa8VRENdYDwenDENwm5M

CODE 21-D Luiua& < DATE ) L2JB3 Tl o t I 4448* LBS. < EST WT ) PROCESSES < ) YE-721~D <M> APPROVED BY: FWP 11/08/82 COMTYP JOB NAME: 01YE721DMM BLENDED BAC>r CG 01 , PGf t c o deT * EQUIP MENT NAME: MOLYBDATE RED PREP 1 J i/, I OBTAIN FOR S-12 I "W\ OBTAIN FOR S-34 I W. I OBTAIN FOR S-38 I * | OBTAIN FOR S-40 i I OBTAIN FOR S-44 |I/OBTAIN FOR S-47 WEIGH IN- d p t r ^L, h AK T4MWM2 OPTR____ , MK _ 359 | \ WEIGH IN: OPTR MK if, T-3jjO, 3i I OPTR ____ , MK _1_, T-__,__, ______% --I 358 RUN 10" <500 G> WATER INTO V-358 4 1*0 j RUN V-359 INTO V-351 & PUMP IN V-351 4 ADJ TO 55* <2600 G) n* SIFT IN N-108-A FROM S 1 'VSTIR 5 MIN & RECORD: PH 0.0) ADJ TO PH 9.8-9.9 6 RECORD; PHjfj." W'1I RUN INTO V-351 FROM BADGER METER OPTR 32^-___ * MK________, JJt **r PUMP FROM V-351 TO V-358 FLUSH V-351 6 PUMPING LINES WITH y WATER INTO V-358 ADJ TO 74" <3530 G> AT 67-69*F RECORD; VOL'W_' 6 _J?j*F STIR 5 MIN & RECORD: PH33l <7 2-7.4) & G/ML 1.055-1 .058) -NOTE IF G/ML OUT OF LIMITS FILL OUT CHECK LIST & ATTACH. TAKE 1 GJT SAMPLE* SV RUN 20J <996 G) WATER INTO V 5 RECORD--N-^i--EL. STORAGE TANK TO PUMPJRQM. Cir c l e QNEy>42 410 411 420 424 C42 cite? wmraj s u p v : *STORAGE TANK MUST CONTAIN AT LEAST 1900 GAL: 402*39'" , 410*20', 4l1=38', 420*20' 424=20", 425=25" ^STORAGE TANK MUST HAVE STIRRED AT LEAST 20 MIN SINCE LAST ADDITION OR ADJUSTMENT WSTORAGE TANK MUST BE ISOLATED UNTIL ALL PUMPING FOR THIS BATCH IS COMPLETE. SET METER FOR 300 G 6 PUMP TO SV LOT:___ ecu ip MEN? I CQMTYP JOB NAME: 01YE721DMM PAGE 02 DATE PRINTED:1 i/08/82 USE N- ACCT LBS CODE LBS AT APPROX 100 G WHILE CONTINUING TO PUMP, CHECK PH & DENSITY* RECORD BELOW. IF NOT IN RANGE, STOP PUMPING & SEE SUPV. * PH:3LL.. (2.2-3.7) * DENSITY: icZiLYl G/ML <1.270-1.328) IF S-23 OK & WHEN S-22 COMPLETE, RECORD ^DENSITY JJA. G/ML ON TRAPPED SAMPLE FROM END OF S-22 PUMPING. USING DENSITY FROM *-24, FIND METER SETTING FOR SECOND PUMPING IN TABLE BELOW. NOTE: TABLE ACCOUNTS FOR 300 G ALREADY PUMPED IN S--0CA9, CIRCLE DENSITY 6 SETTING IN TABLE BELOW, xxxx TABLE xx* 1 G/ML 1 1.270 1 1.271 1 1.272 1 1.273 I 1.274 1 1 .275 i 1.276 1 1 .277 1 1 .278 1 1.279 1 1.280 i 1 .281 i 1 .282 i 1.283 i 1.284 i 1.285 i 1.286 f 1.287 i 1.288 i 1.289 i 1 .290 SETTING 1 G/ML 1259 1 1.291 1253 1 1.292 1248 1 1.293 1242 ! 1.294 1236 1 1.295 1231 t 1.296 1225 1 1.297 1219 1 1.298 1214 1 1.299 1208 1 1.300 1203 i 1 .301 1198 1 1.302 1193 t 1 .303 118? I 1.304 1182 I 1.305 1177 1 1.306 1171 i 1.307 1166 f 1.308 1161 i 1.309 1155 i 1.310 1151 i 1.311 SETTING 1 G/ML 1146 1 1 .312 1141 1 1.313 1136 1 1 .314 1131 1 1.315 1126 1 1 .316 1121 1 1 .317 1116 1 1.318 1112 r 1.319 1107 1 1.320 1103 1 1 .321 1 098 1 1 .322 1094 1 1 .323 1089 l< 1084 1 1.325 1080 1 1.326 1076 1 1 .327 1070 1 1.328 1066 I 1 .329 1061 1 1 .330 1057 1 1.331 1053 1 1 .332 SETTING 1049 1045 1040 1036 1032 102? 1023 1019 1015 1010 1006 1003 995 991 98? 983 979 975 971 96? %\ I ii 0<T| SET METER & PUMP jffS__G (RECORD FROM TABLE) FLUSH LINE WITH WATER INTO SV FOR APPROXIMATELY SECONDS ADJ LEAD NITRATE TO 3244 G \(68"-242^245 i, 66.5" 247) AT 67-69F CORD: __^jL__*F & ICE CONSUMED <3304/BLOCK) STIR 5 MIN & RECORD PH: 3*f__ <2.2-3.7) xx USE TITRIMETER TO ADJUST N-41-D PH xxxx IF NECESSARY ADJ TO PH 3.0-3.1 ASSUME 66% & RECORD PH:c Jl <!L_ ASSUME 50% OTE: DILUTE N-7-D 10:1 WITH WATER BEFORE ADDING RECORD: G/ML (1.128-1.129) IF OUT OF SPEC FILL OUT CHECK LIST & ATTACH. STIR AT 67-69XF FOR S-33. TAKE 1 QT SAMPLE. 330X___ 41 -D 57-A 4094 33-D IJ!?/... 7-D l,,_ DUP050059738 1.01= 4QUIP MENT |TYP JOB NAME: 01YE721DMM PAGE OBTAIN 1 QT SAMPLES OF S-19 & S-31 SOLUTIONS & TITRATE TWICE NOTIFY SUPV IF ML N 10-D IS NOT IN RANGE 9.5-9.9 OR IF THE TWO TITRATIONS DIFFER BY MORE THAN 0.10 ML N-10-D (IF YES, FLUSH ALL EQUIPMENT 6 REPEAT TITRATIONS). DO NOT PROCEED IF N-10-D TITRATION IS OUT OF RANGE ADJUST V-358 FOR A TITRATION PH OF FROM FINAL IN-LINE TITRATION, RECORD LOWEST PH_______ & ML N-10 _D ^ ^ WHEN S-32 TITRATION OK, STRIKE V-358 THRU BOTH UNDERSURFACE ^TRIBUTORS INTO SV IN 44-46 MIN RECORD: START&&__., TOTAL MIN__~ NOTE: STRIKE TIME UP WHEN 1/2 VAT BOTTOM SHOWS I ^1 & BUBBLES APPEAR IN SIGHT GLASSES | IMMEDIATELY DUMP IN N-4-A FROM S 2 & SET TIMER I Jr FOR 15 MINUTES IDURING S 34, WASH IN V-358 I2l STIR 2 MIN 6 RECORD PH_/&1_< 1.7-1.8) | PBXS,__7^__(MUST BE + ) .>37 1 STIR TOTAL OF 15 MIN FROM S-34 & I VT RECORD- TEMP__"3/__F (67~73F) DUMP N-3-A FROM S-3 'vsf' i STIR 3 MIN ` ` POUR IN N-32-D FROM S-4 ,1 STIR 2 MIN ,, i RUN IN LIQUID ALUM USING BADGER METER STIR 3 MIN & FLUSH ALUM LINE WITH WATER 4'DUMP IN N-3 FROM S-5 STIR 4 MIN FOR S-49 RUN IN HYDROCHLORIC ACID USINGG WEIGHT & FLOW. . I - CONTROL PANEL MK ______, 2/LoL%1 ZrJtl* MMKi/ ______ t / RING S-45 SIFT N-711-B FROM S 6 INTO V-390 WITH AGITATOR ON IN 1-2 MIN STIR 1-2 MIN TO MILKY SOLUTION WHEN S-45 COMPLETE, IMMEDIATELY RUN IN N-711-B SOLUTION GRADUALLY OVER 5 MIN PERIOD INTO SV WATCH FOAM!!! IF FOAMING IS EXCESSIVE, STOP UNTIL FOAM SUBSIDES. DUMP IN BLANC FIXE N WHEN SCHEDULED, DUMP IN BLEND BACK LISTED ON S TOP OF PAGE 1 RECORD: CODE, LOT, __________________________ * fl VSTIR 20 MIN / RECORD: PH_M!A._<5.8-6.0) IF NECESSARY, ADJ TO PH 5.8-6.0 ASSUME 50X & RECORD: PH-.^Lfe?.____ ASSUME 66X H FLOOD TO 153* (7298 G) 6 STOP AGITATOR II START W' j FINISH /08/S2 USE LBS DUP050059739