Document Oz06Z5v42QKOvyMpY8VLa4npX

A R ^ r O 40| ACUTE TOXICITY TO FISH TEST SUBSTANCE Identity: Perfluorooctanesulfonylamido(ethyl)acetate; may also be referred to as PFOSAA, FC-128 or as the major component of FC-127, FC-129, FC-109, or FC-109-X. (Glycine, N-ethyl-N[(heptadecafluorooctyl)sulfonyl]-, potassium salt, CAS # 299151-7) Remarks: The test sample is FC-128. Current information indicates it is a mixture of 86% test substance and 14% C4-C7 fluoroalkyl carboxylate compounds. METHOD: Method: Not noted. Type: Static acute GLP: No Year completed: 1974 Species: Pimephales promelas Supplier: Not noted. Analytical monitoring: pH and DO Exposure period: 96-hours Statistical methods: Graphed Test fish age: Not noted. Length and weight: Average length = 2 inches Average weight = 1.5 g Pretreatment: Not noted. Test conditions: Dilution water: Carbon Filtered city water Dilution water chemistry: Not noted. Stock and test solution preparation: Individual weights Concentrations dosing rate: Once Stability of the test chemical solutions: Not noted Exposure vessels: Type not noted. 16L volume. Number of replicates: one Number offish per replicate: Not noted Number of concentrations: five plus a negative control Water chemistry during the study: Dissolved oxygen range (24 - 96 hours): 5.0 - 6.1 mg/L (control exposure) 4.0 - 5.7 mg/L (40 mg/L exposure)* pH range (24 - 96 hours): 000334 7.0 - 7.1 (control exposure) 6.7 - 7.0 (40 mg/L exposure)* * 40 mg/L test group data given because total mortality occurred in the 50 mg/L test group by 72 hours and all data was not collected. Test temperature (24 - 96 hours): 72 to 74F RESULTS Nominal concentrations: Bk control, 10, 20, 30, 40, and 50 mg/L Element value: 96-hour LC50 = 34 mg/L (C.l. not calculated) All element values based on nominal concentrations CONCLUSIONS The test sample 96-hour LC50 for fathead minnow was determined to be 34 mg/L. Submitter: 3M Company, Environmental Laboratory, P.O. Box 33331, St. Paul, Minnesota, 55133 DATA QUALITY Reliability: Klimisch ranking 3. This study lacks documentation and information on the methodology. Sample purity was not properly characterized. REFERENCES This study was conducted by the 3M Company, Environmental Laboratory, St. Paul, MN, completed on May 18, 1974. OTHER Last changed: 5/18/00 FORM 10620-PW O v .i* . >cc: LAB REQUEST BOOK - 42-5W File: Water and Wastewater * REQUEST FOR LABORATORY WORK Lab Rei*uest No- <=?? 5 4 " TO: ENVIRONMENTAL ENGINEERING LABORATORY - BUILDING 53-6N Requestor Lab Personnel Name: D .fc O C n Y X _____ Request D a te ______ Project N o .. #Prob. No. . Code Description: ~ V c . A ~ 2 g _ p f t t d U T _______ Sample D a te :_______________ Date Needed: Hold Sample F o r . .Days Est. T im e :. . Hrs. Date Rec'd. Sample:. Analyst: MTE Y Date Completed:__ Hrs. Spent: \0 p'R;,. A s s o*\ 5 -/ S -.Z V ________ S Sample Description fa -lx s Total Hardness, mg/l as CaCCh Calcium Hardness, mg/l as CaC03 "P " A lkalinity, mg/l as CaCCh " M " A lkalinity, mg/l as CaCC>3 pH Sulfate, mg/l as SO4 Nitrate, mg/l as NO3 Chloride, mg/l as Cl Silica, mg/l as S1O2 Fluoride, mg/l as F Ortho Phosphate, mg/l as P Total Phosphate, mg/l as P Total Chromium, mg/l as Cr Hex. Chromium, mg/l as Cr Total Cyanide, mg/l as CN Ferrocyanide, mg/l as CN Iron, mg/l as Fe Manganese, mg/l as Mn Surfactant, mg/l as LAS Phenol, mg/l BOD, mg/l COD, mg/l (Short, Long, Dilute) Total Suspended Solids, mg/l Volatile Suspended Solids, mg/l Turbidity, mg/l Silica Total Solids, mg/l Total Volatile Solids, mg/l Conductivity, mhos Total Bacteria, N o./100 ml Total Coliform, N o./100 ml Fecal Coliform, N o./100 ml Fecal Streptococcus, N o./100 ml Ammonia Nitrogen, mg/l as N Kjedldahl Nitrogen, mg/l as N Oil and Grease, mg/l KV><1SAM Q t A u u k V c - Z H - if , . LC. & 0 ________ e v ___________ ._______________________ i0 _______C L - ;* *r p7 0003:16 3 m Cartoonltsi Pap W h ite -- E nviron m ental Engrg. Lab C anary -- E nviron m ental Engrg. Lab Pink -- E n viro n m en tal Engrg. Lab G oldenrod -- Requesters Copy 740101 ENVIROWENTAL ENGINEERING LABORATORY ^IJEST COPY AVAILABLE aqmat,c TOX,cm **x Type Test_ <j4>tndf * ^tatlC____ ___ ) Test Organlte FnfJiea/J MinrirwX, Date S ta rte d `n -/-V - 7 T iro Started______________ P lo tte d LC^ M aterial Tested /y ? -!s.s Pou)de/' Avg. eig h t /, 5 j S ite a Twr-Ues Date Completed -- ti -1&-1H___________ S*i hTM 9.___________________________________ D ilu tio n Water f i M e J - c ftv j uvrtdf 24 hrs 48 hrs .72 hrs 96 hrs % Survival co n s*/