Document OEvpV2e7739Y6exjw45vZmDZj
BIODEGRADATION (BOD/COD)
TEST SUBSTANCE
Identity:A mixturecontainingperfluorooctanesulfonatweh,ich may alsobe referredtoas PFOS, FC-95, or as a component of FC-3041. (1Octanesulfoniaccid)(CAS # 2795-39-3).
Remarks: The 3M productionlotnumber was 2300. The testsample isFC3041 (cc809-1).Currentinformatioinndicatesitisa mixtureof6% PFOS, 36% diethyleneglycolbutylether,36.05% water,12% Sultonefoamer,9% sodium octylsulfate0,.55% sodium laurylsulfatea,nd 0.4% tolyltriazole.
The followingsummary applies toa mixture with incompletely charactedzed concentrations of impuddes. Data may not accuratelyreflect the biodegradabilityof the tluorachomical component of the testsample.
METHOD:
Method: BOD ProtocolofEAR (2/29/80). Type: Aerobic GLP: No Year completed: -1981 Contact brrie:20 days lnoculum: Stalesewage, Chemolite,Coffage Grove, MN.
RESULTS
BiochemicalOxygen Demand (BOD): 5-Day: 12-Day:
20-Day:
164,000 - 329,000 mg/kg 645,000 mg/kg 642,000 mglkg
CONCLUSIONS
No conclusionsgiven.
Submifter: 3M Company, EnvironmentalLaboratory,P.O. Box 33331, St.Paul, Minnesota,55133
DATA QUALITY
Reliabilitryd:imischranking3. The study lacksdescriptonand recordsofthe method followed.The inoculumisnotproperlycharacterizedT.here isno characterizatioonfthe testsubstance puritya,nd the studylacksanalytical confirmatioonfthe amount offluorochemicaplroportioninsoluton.The testing was conducted on a mixtureofchemicalshavingvadng degrees of biodegradabilitlye,adingtopotentalmisinterpretatioofnthe results.
REFERENCES Thisstudywas conducted by the 3M Company, EnvironmentalLaboratory,St. Paul,MN, Lab Request number 6508S, 1981.
OTHER Lastchanged: 6/26/00
ANALYSIS FORM 1038A
t4LT,ftlA-rEgoo
COiief-AJMAr-zW 0,F
2
3
so rrte_
s
4
5
6 7
@m,
a
9
41
10
11
12 13
14
15 16 17 is 19 20 21 22 23 24 25 26 27 211 1^9 30 31 ..32
23 L4 _ 35
rip
A
0
E
F
i
x
FILE
SEC DAT
RiEsatr9 c, PR 'co
e* A dLe-&4 LAT-4t6
Ar-coR-j)iAIC7?-0
3&7 2,F
T-1
WAronnuntMLaborstorV BOD WorkShm Sompla
Lab Req.No.
Analyst
37@gi
600 Run No
9/-
Arwtya
-!Sr' -Day BOD Readings
t
Date
hi
Sample Dftcription Fe-30ill 4 o r 2 300,
InitiaDlilution
(ce gc>,?-
of Sample dilutedto /00
mi with D Iwater
InitiaDlilutionFactor
(Dilutiofnactor= 1 ifundiluted)
Botdo NO.
fo B,g
Cone.of Somplal
Somple
SIZ&2
Initial Pr@nt 0.0. IDI) D.O. ID2)
2.0
11
'1,0 x-80
-14 -8.0 'T,75*-
12
<O.r
Ict
<
TotalD.O. Depletion
IDI - C121
@i_lo
DepletioDnue To Sompis
;L,80
g-l@
-Day 130D
Avorep
@5
Day
SOD
3:L 4000
D4DO
ttt5g
-Y"lo
B p T E -C, --IILTS
35
2..,8 0 -'E,i;6 6.6.7
4,:-0-.@ 5.5,
oc?0
4
T,DEP. D D'3. BUD
Note:
I Conc. Concentratioonf sample(ml/I009 inSOD bottles. 2. Sample Size ml or g of sample or dilutedsample added to SOD Bottle.
Comments
A.?
2214 Li
E,'OD :fE '3T
5. 4.-7 5 7,1--3
5 E..
U LT ql EDSP e- P-OD
#-j,5- d v
8 -0
BUD T E':-:-'RT U L T.-.
8.
ri
6. 15
TD-EP'
146"@r-
D 1)E@.
210. 55)c@
I Form 19756 PWO--
6*iran M"l Lobbratory .BOD Work Shut -UMPIN
Lob Req. No.
Date Stw"d
4.
Au'*Nno.0
goo 'FtWings-
sernple Dowiption
olel
ln!tw Dilution InitiaDlilutionFactor
tbr
2300
of Semple dilutedto ..1494) mi with Di water Dilutionfactor I ifundiluted)
settle
Cone.of UMPISI
!60 11
&00IV
SN"Plo Siz@2
2-.0
lnithd P.O. (DI)
Prumt 0-0- (D2)
o2 d7'0
TotalaI.0. DWI*Tion
DeplefianDue To So,mplo
-Day SOD
D" SOD
BOD TE@'@T
Conc. Concentratioonf sample(mlA or mgA) inBOD bottles. 2. Sample Size mi org of sampleor dilutedsample addedto SOD Battle.
E;Mments
l@4
T'IfE P@::
0 D--
I..:,Fwm
in*Md Dgution Fwtoo
lootdo,
Coom of
-1@ O@
Gs
ti@utod
7:r
it
40
-3@il
7
m wit und*
bay
A vwago :Boo.
Conc. Concentraotnio@f"sam pis(rnla.omrg A)@ih80 ti 2. Sample Size mi.or'gof sample or dilutedsampleadded to SOD Bottle.
2214
*wm
197M
PM
ribw"nmenteLl-aboratorv' SOD Wo* Shoot-BWnks, 'Controakr,WSundards
LabRequat No.
Analyst
/,t,),
S"d Type a Source
Dow Ste
12-13-91
concentration
Flunt4o. If .,I.I -
AN*IM
- Day SOD Readings
NonseededDilu6m -Waur Blank
lnhw D.O. (Al)
9Q
Seeded Dilution-Waur Blank lopftm)
Battle NO.
lnithdD.O. (CI)
go
Seed Convois
Botdo NO.
Somple sit@
prowt 0.0. fA2)
i@o
Pruent D.O. (C2)
InitiaDl.O. lei)
D.O. Dq"tlm,' (Al -A2)
qo
D.O. Depletion (Cl -C2)
o- 55
Pr@t D.O. IB2)
Av- D.O. Depletion
(A, X2)
0, 3E3
Avwop D.O. CWpWflon (El -E2)
.61
0.0. D@Wation
@60
ILO
1
Gluom -GlutemiAccidStandwd
Bottle NO.
sampi* size
Inioel0.0.
Prsmt D.O. ID21
13
12S
o
7,0
<1,4 s- -3.s@o
SA"4d inytow um Hyd.owo, Pa.ti.slawStffndord (updu.od)
odttle NO.
Swnpk Size
InitiaDl.O. (DI)
pl@ t D.O. (D2)
"P",pt**13
el TotalD.O. DhW&don (Di -D2)
D -45-
TotalDa. Depletion (Di - D2@
ols 0,.r
kt4444A,@,
Oq"tion Due To gtwwwd
6.I-ey 300 pya
DepletiontkW 4:.
Day Ave op SOD -*'S- -Dy
00 >mg zx
-Day
INHD--
2C33)
,Z
Form 19755 PWO
6,446
""TAY
ltoi@@tM. Lob43tator k Shiist
oft,and StmW6*
Lob Request No. 0
Aknelyst Arco
3 v4moonva"n
NonindDeidlutWiaotneB.rlank
RotN"o*.
lnh0w.0. 4A,)
Dm Surted
BOD'Ru'Nno@.
DOY. 800 ReadinP
-1
crz.
pi 10.0.
IA2)
D.OD.eoWt"': (Al-A2)
C)
-1 Li
Awwap D.O.
Depletion
tAl A2)
I aQ
S"ded
Dilution
- Water Blank (opdonw)
so
Prominit
0.0.'
(C2)
D.O.
D%AMI"
(Cl
C2)
o
Awwap
D.O.
Depletion
S-"d Controls..
Botoo.w..
Samoa sin
od:
Initial 0.0. lei)
Pr@nt D.O. 1621
0.0. owletion
GlucosGelufamAictidStendwd
Bot"e No.
SempleSize
InitiDa.lO. IDI)
Pt tD.O. (D2)
.7,0
-,A
ila@lmydiropi,P@,O,WatgS dl.d(apd..md)
00"10 NO.
SONP'*
InitialD.O. (Di,)
Po@ t D.O. (D 2)
-0,9*ro19755 PVWO
TotalD.O. D@pWdon IDI -02)
DepletioDnue'.. To Standwd
Dy so 0
-70
Total DD. Dopkidon (Di D21
Of Flo
30
30
pwa H&08nZ"
Deplation4W* soa#W
Dy Sol).--
L r7lO
A.&P
2f.33)
1(0 -imenimLaborstw
'I@o@t@o .-EindStiit@"
.2-2
O,M
@Lib'Request No.
Date Started
Seed Type Source
&t:@, (j
adnolo
of18"d iconcentration 1 0/.0
wateerlm*
SOD Run NO. Analyn
Day BOD Readings Date
&mle No.
i.ih 0.0. (AlI
p am t0.0. (A2)
C3o
D.O.Depletion (Al A2)
go
'AlviiDr.iOw. Ow"on
(Al A21
Seeded Dilution -Waftr Blank, (aption#A)
-70.
'767
sonm NO.
kthw D.O.
D.O. Depletion (C-1 C2)
36
Avwap D.O. PW*tion
ILI -C2).
@7,
S"d Confiols
Bottl* No@.
SN"Ple size
ID
60.
InMal D.O..
Pramt D.O. (B2)
,:oore-). ------f
D.O. Ddko4d*n IBI 82)
Glt4cose - Glutemic Acid Stands So .itio@No. son*m .size 0.0.
13
7.0
WtialD.O.
No.
Swnpiesize.,.
sq
19755PWO
plow tD.O.
47.70
1 D.O. iotion
D2)
Total0.0. Dw"an
Depletion Due To Stendard
q. A3
-BW pay
41a 3
3'4(. -j
Dopmtiongo*
Day
-T*4k@ndwd
A--map Dev
40
2.C!3
Dw
Z, og