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Multi-city and Decat 'i I A I -1 1 . MULTI-CITY STUDY FIELD REPORT FOR CLEVELAND TENNESSEE AND DECATUR ALABAMA - BATTELLE DUXBURY ACTIVITIES for ProjectNumber N1006.72-01 submittedto Conridential July 9,1999 Prepared by ScottC. Macomber BatteHe 397 Washington Street Duxbury, AU 02332 (781)934-0571 Introduction Page:I TABLE OF CONTENTS 1. INTRODUCTION .........................................................................**.,..............1................. 1.1 SURVEY SPECIFIC APPROVAL .................................................................1................ 2. METHODS ..............................................................................................................2................. 3. CHRONOLOGY .......................................................................2.............. 4. IZOULTS ............................................................................4.............. 4.1 SAMPLE MATRIX AVAILABILITY .......................................................5............. 4.2 ONSITE OBSERVATIONS .......................................................................5................ 4.3INSTRUMENTATION RESULTS .................................................................1.0............... 4.4 COMMUNICATIONS ..........................................................................1.2................ 5. PROBLEMS EXPERIENCED AND RECOMMENDATIONS .............................................1.2................ LIST OF TABLES TABLE TABLE TABLE TABLE TABLE TABLE TABLE TABLE TABLE TABLE TABLE 1 MUNICIPALITIES SAMPLED AND APPROVALS GRANTED DURING SURVEY ......................I............. 2 CHRONOLOGY 3 CHRONOLOGY 4 CHRONOLOGY 5 CHRONOLOGY 6 CHRONOLOGY 7 COLLECTED OF EVENTS ON MAY 24,1999...........................................2............. OF EVENTS ON MAY 25, 1999 ...........................................3.............. OF EVENTS ON MAY 26, 1999 ...........................................3............. OF EvENTs ON MAY 27,1999 ...........................................4.............. OF EVENTS ON MAY 28, 1999 ...........................................4............. SAMPLES FROM CLEVELAND TN ..........................................6.............. 8 COLLECTED 9 SAMPLING SAMPLES FROM DECATUR AL ............................................8.............. SITE POSITIONS IN CLEVELAND TN ........................................1.1.............. 10 SAMPLING SITE POSITIONS IN DECATUR AL ........................................................ 11 GPS POSITION VERIFICATION PESULTS .................................................................... FinalFieldRpt ClevelandTN DecaturAL Balteiie 14 14 14 ff4 Introduction Page:I 1. INTRODUCTION The objectiveof thesamplingtaskin thisstudyistocollectrepresentativseamplesfortracelevelanalysisof specifiFcC residualst,o assesssources,dispersionintheenvironment,and human exposurethroughthefood chain.The citieselectedforsamplecollectiownillbe considered'study'or 'controlc'ites.'Study'citieasreconsideredthoseareaswithFC productionfacilitioerslargeindustriaFlC-consumers. 'Controlc'itesdo not containFC productionor consumptionfacilitiaensd arematched to studycitiesbasedon generallocation, populationsize,a.nd drinkingwatersource. During theinitiaplhase of thestudyphone callswere made tomunicipalagenciesrequesting permissiontocollecvtariousmatricesof interestB.ased upon thelevelof cooperationreceived from themunicipalagencies,appropriatseampling strategiewsere'developed.The Quality AssuranceProjectPlan (QAPP) and theSurvey Plan containthedetaileidnfortnatiocnoncerning thematricesforcollectioannd methods to be utilizefdorthisprocess. The fullprojectsamplingscopeisaccomplishedusingtwo fieldteams:1)Battelle'Dsuxbury Personnelcollecdtrinkingwater,POTW, landfilalnd urban airsamples,and 2)Battelle'Msarine SciencesLaboratory(MSL) personnelcollecsturfacewatermicrolayerb,ulkwaterand finfish samples.This reportsummarizes theDuxbury team effort.A separatereportsummarizes the MSL activities. 1.1 Survey SpeciricApproval Approvalwas grantedinClevelandTennesseefrom thePubliclyOwned TreatmentWorks (POTW), municipaldrinkingwaterplant,and ClevelandFireDepartment(foratmospheric sampling).Permissionwas notgrantedforsamplingatthemunicipallandfillP.ermissionto sample was grantedinDecaturAlabama forthePOTW (includinagirsampling)m,unicipal drinkingwaterplanta,nd municipallandfillT.he DecaturFireDepartment deniedaccesstotheir propertyforatmosphericsampling.Table Ihighlighttshecitievsisiteduringthissurveyand theapprovalsgrantedby municipaldepartments. Table1.MunicipalitieSsampled and ApprovalsGranted During Survey City Decatur,XE Stuidy-orFln Department POTW Control (AirSampling) Study NA Ddnldng Water Plant ClevelandT,N Control I NA = No ApprovalReceived Air samplecollected Mumcipal La I NA FinalFieldRpt ClevelandIN DecaturAL Baltelle methods Page:2 2. MEETHODS ThecollectoifoennvironmentsalmpleissconducteadccordintgoStandarOdperation Procedur(eSsOP's)T.heSOP'susedintheMulti-CiSttyudywerewrittebnyBattelalnedare 94 used totrainpersonalpriortoconductingfielda,;tivitaineds alsoserveasa referencedocuments whilein thefield.These documents,alongwith theQAPP, serveastheguidancedocuments for thecollectioonffieldsamples.The methods used forcollectioanresummarized below. 14 The collectioonfpositiondata(latitudaend longitudew)as completedateach samplinglocation usinga Garmin 12XL GPS unitaccordingtoBattelleSOP 3-164-01.Instrumentaccuracywas validatebdy comparing an acquiredpositionversusa positionof known location.The collection of airsampleswas completedusinga GeneralMetals Model PS- I atmosphericsampler.The samplingwas conductedaccordingto BattelleSOP M3-MC-F-1.1. The use of thissystem allowstheseparatecollectioonf particulataend vapor phase compounds usinga glassfiberfilter 94 forparticulatmeatterand a polyurethanefoam PUF forthevaporphase.Water samplesfrom drinldngwatersuppliesP,OTW'S, and landfillwsere collectedaccordingtoSOP M3-F-2.0. Surfacewater sampleswere collectedviadirectsubmersion,tapwater and drinkingwater suppliedby themunicipalplantwer-ecollectevdiaa valvesystem,and effluenwtas collected 94 usingeithera bucketor smallsamplingbeaker. Sediment samples were collecteudsingBattelle 4I SOP M3-F-7.0. Both sludgeand sedimentwere collecteudsinga stainlesssteelspoon. 3.CHRONOLOGY Tables2 through6 providea detailedchronologyof theeventsthatoccur-reedach day of the survey.The timesrecordedforthecollectioonf each sample matrixhas been transcribefdrom thesample collectiolnog,allothertimeshave bee@ estimatedbased on theeventsof theday. All timeshave been recordedinEasternStandardTime. Table2.ChronologyofEventson May 24,1999 0615 BattellDeuxbury personneldepartBoston. 0900 ArriveinAtlantaG,A and meet withKim Andrews. 1130 ArriveinChattanooga,TN. 1145 Pickup rentalvan and proceedtoFederalExpresstorrtrievseamplingmaterialsA.ll materialpsresentand accountedfor. 1300 Depart Chattanoog@a--apnr-odceed toCleveland,TN. 1400 ArriveinClevelandand check intohotel.Proceedtohave kickoffmeetingoverlunch. Duringthemeetingitisdiscoveredthatmore samplingmaterialasrerequiredforair -sampler. 1500 Arriveatfirestationand placeairsamplingunitbehind buildingforsample collection. 1545 Conductcalibrationfairsamplerand starstamplingfor12hrperiod. 1600 Meet withPaulPittst,heassistanmtanager ofthewaterdivisioonfClevelandUtilities. He providesmaps, directionasn,d infomisthemanagers oftheplantsofour scheduled arrival. 1630 Returntohotel.BattellCeolumbus contactedand more supplieasrescheduledfor shipmentto Chattanooga. FinalFieldRptClevelandTN DecaturAL ..,;p]3agelle P&MifwTochr-oloaTo "& Chronologv Page:3 Table3.ChronologoyfEventsonMay 25,1999 0730 Arriveatthefirestationa,irsamplerdidnotstopatend of 12hrperiod.Sampling event concludedat0745. Cleaned samplerand placedthePTJF and filtebrlanksintothe Isamdler.Blanks remainedin samplerfor-30 seconds,theywere thenplacedinstorage Table 3 Continued -3rshipment. JL%A" tuiivcatClevelandUtilitieWsastewater TreatmentPlant(WWTP). Discusssampling withMr. Mike Ward who was thesupervisofrortheshif@no significainstsuesraised. 1015 CoHect postcentrifugesdludge.Used stainlesssteelspoon forcollection 1030 CoUect chlorinateedffluenstample viaoldsteelpail.Collectioanssistancperovidedby plantemployee. Complete collectioant1055. Followingcollectioonf sample Kim Andrews departedtheteam toreturntoColumbus. 1100 Benchmark discoveredattheWWTP, inquiredabout thecoordinatefsrom theplant employee. He contacteda member of thecityengineeringdepartmentwho providedthe coordinatesforthe benchmark. The coordinatesare,N 35*18'35.0"W 85047154.0@'. 1210 Arriveatfewassee drinkingwaterplant.Spoke withChrisWiles who isthemanager oftheplantwaterqualitylab.Collectraw untreaterdiverwaterand postfiltration -drinkingwaterfrom waterqualitylab. 1420 ArriveatStateaccessarealocatedon lewassee River.Thisaccessareawas used to collectsurfacewaterand sedimentsamples. 1450 Collectsurfacewaterand sedimentsample atSite1. 1520 Collectsurfacewaterand sedimentsample atSite2. 1535 Collectsurfacewaterand sedimentsample atSite3. 1630 CollectSiteI tapwaterfrom room 107 ofBaymont Hotel. 1700 Commence spikingof fieldspikesamples 1820 Preparesamplesfor shipping. 2015 CollectSite2 tapwaterfrom an Amoco gas station/conveniencsetorelocatedatthe intersectioonf Routes 60 and 75. 2145 CollectSite3 tap waterfrom Tennessee Jack'sCaf6. Table 4. Chronology of Events on May 26,1999 0800 CoHect GPS locationsatthethreetap watersites. 0830 DepartforChattanooga. 0915 ArTiveinChattanooga. 0930 Finalizeshippinglogistic(sS.amples were repackedingarbagebags becauseof leaking water).Copiesmade of Chain of Custody Sheets 1115 Rendezvous withRosanna Buhl atthe ChattanoogaAirport. 1200 ShipClevelandTN samplesviaFederalExpresstotheirrespectivdeestinationsP.icked _up airs lersupplies(filterPsU,F'S, and fieldspikesamples). 1210 Depart forDecatur, 1430 Receivephone callfrom Marcia Nishioka.T.he clientand DecaturUtilitiemsanager Kem Carr agreedto a confidentialiatgyreementthatwould allowus to samplefrom the POTW and thedrinkingwaterplant. 1440 CallKem Carr toconfirmsamplingapprovaland inforihnim thatwe areexpectingto beginsampling withintheday. 1510 ArriveattheDry Creek WWT? and meet withEd Buyers theplantsupervisorB.egin calibratioonf instrument. FinalFieldRpt ClevelandTN DecaturAL Baltelle ftffingTm:hnolov To Kb* Results Page4: oil lRi 1540 Air samplinginitiated. 1600 Arriveathoteland beginpreparingwater-samplingbottlefsorthefollowingday. Table 5. Chronology ofEvents on May 27,1999 Table 5. Cont:mued atDry Creek WWTP. Collectairsample,airsamplerstoppedautomatically aitr.1J2Lhours.Clean unitand collecQtC samplesincludingan extrafieldspikesample. 0910 Collecteffluenstample using500rni-samplecollectotrhatthefacilitpyrovided.The samplewas collectefdrom thespillwaythatledtothedischargepipe. The effluenits disch d -500 feetintotheriverwhere thechannelexists. 1015 lim Meares collecteldiquidsludgefrom a collectiotnankusinga plastijcar.No GPS locatiornecorded;thecollectiotnankwas -500yds from theairsampling location. 1045 ArriveatDecaturWater Plant.Collectraw and finalprocesseddrinkingwater. Samples collectedinthewaterqualitylabof thefacilitRyi;chardBlackwood was the techniciaonn duty duringourcollection. 1125 Collectquietwaterbody sample from theNorthwestcomer of FlintCreek. The area was locatedacrossfrom theDecaturCouniryClub. Itw'asnorthof Country Club Lane S.E.bv -200-300 yards. 1300 Collectsurfacewaterand sedimentsatsites1,2,and 3 from theRiverwalkMarina complex locatedon theTennesseeRiver. 1410 t-oll-etcatpwaterfrom Site2 locatedattheDecaturBoat Harbor (withinRiverwalk comple 1435 ArriveatMorgan County Landfill.Presentsitemanager RichardTerry,with a request lettetrhatwas requiredpriorto ourcollectioonf samples.Followinga tersediscussion we proceededtothe leachatepond unsupervisedand colleclteachatesample. 1550 CollectSite3 tapwater from a Texaco gas station/convenienscteoreon Route 67 in Decatur. 1635 CollectedSiteI tapwaterfrom room 207 oftheHampton Inn. 1710 Fieldspikesamples were processed,samples segregateda,nd coolerspackaged for shipping. Table 6.Chronology of Events on May 28,1999 0645 Depart forChattanc>oga, 0945 Arrivein Chattanooga,paperwork completed forsample shipment,coolersrepackaged forshipment. 1030 ArriveatFederalExpressand shipallsamplesand equipmenttothererespective esfinatons 13 DepartChattanooga forBoston. 4. RFSULTS The initiaslurveyoftheMulti-CityStudy resultedinthecollectioonfthemajorityof the samples describedinTables 3 through 5 of the QAPP. Also collectedbut not includedinTables 3 through5 ofthe QAPP were samples forthe clientand a thirdlaboratoryspecifiedby the client.The collectioonf thesesamples tiipledthenumber of water and sediment samples taken. The samples were collectedand processed inthe same manner asthoseintended forBattelle. The foIlowingsectionsdescribethe resultsof the sample collectioenfforthatoccurredduring FinalFieldRpt ClevelandTN DecaturAL '0'62'Balreiie 94 ResWts Page:5 thissurveyT.able7sand8 providaelisotfthesamplecsollectiendcludisnagmplinlgocations and sample ID's.Tables7 and 8 do not containtheQualityAssurancesamplescollectedalong with authenticsamples. 4.1 Sample Matrix Availability Per clienitnstructionos fooditemswere collecteduringsurvey.Due toschedulingand permit issuesno finfiswhere collecdturingthissurvey.The collectioonfPOTW influenwtas not collecteadteitherClevelandor Decaturdue tohealthconcerns.Both POTV influentstreams availablfeorsamplingcontainedbiologicahlazards.In bothcitiest,hestaffatthefacilities indicatetdhatthechlorinatiopnrocessoccursfollowingsecondarytreatment. Neitherlandfillleachatenor an alternativseample was collectefdorthemunicipalitoyf Cleveland,'fN. The reasoningthatan alternativseample was not soughtafterisbased on the followinginformation.A discussiowniththemanager ofthelandfililnFebruaryresulteidnthe denialof permissionto collecta sample. During thisdiscussionitwas revealedthattheleachate fro'm thelandfililspumped tothePOTW fortreatment.During subsequentdiscussionwsith ClevelandUtilitieasn offerwas made toremove a manhole coverthatwould allowus accessto theleachateas.iitspumped infrom thelandfillH.owever, becausewe had not been granted permissionitwas decidedthatwe would not collectheleachatesample.With thesample unattainablaend theleachatepumped from thelandfililtreasonedthattheleachatewould not be migratingfrom thelandfilalnd enteringanearby watersource.Therefore,no alternativseite was collected. Also to be collectedb,ut not includedin theQAPP, was a sample of quiet/undisturbesdurface water.This sampleisintendedforuse in a long-termtransporsttudythatiscurrentlybeing, conducted.In Clevelandwe were unabletocollectthissample becauseaccesswas unavailable tothepond selectedas a samplingsiteasitwas locatedon privateproperty.A sample was collecteadtFlintCreek inDecatur. 4.2 Onsite Observations Cleveland,TN: The drinkingwaterplantwithdrawallocationisapproximately2 miles east/northeaosfttheplantintheHiwassee River. The locationofthesurfacewater siteisatthe end of Eades or Eads road. One spellingwas observedon a localstreetsignand theother displayedon a localmap. The siteisa small stateaccessarealocatedat'thetipof thepeninsula. The areaappearedhighlyutilizebdy thelocalpopulationforrecreationalctivities. Decatur,AL: The PiverwalkMarina complex where surfacewaterand sedimentswere collecteidslocatedadjacentto theHighway 72 bridgethattraversetsheTennesseeRiver into Decatur.Thisareaisa highlyactivemarina complex, severalpeoplewere observedfishingfrom thebanks. Severaldead catfishwere observedalongtheshore.A semi-softshelletdurtloef unknown specieswas observedatSite2. At theMorgan County Landfilltheleachatesample was collectefdrom a recentlyconstructecdollectiopnond. Thispreviouslysampled pond FinalFieldRptClevelandTN DecaturAL Batteiie Rowns Tft-@stmia" TO Iva& ResWts Page: 6 (December 1998)was surroundedby vegetationand accesswould have been extremelydifficult. The pond sampledduringthissurveycontaineda varietyof wildlifleivingin and or aroundit. Severalturtlesm,ultitudesof insectsand larvae,and variousbirdswere observedfeedingatthe pond. Table 7.CollectedSamplesfrom ClevelandTN Matrix Sample ED DrinkingWater Processed DrinkingWater Processed DiinkingWater Processed DrinkingWater Processed DrinkingWater Processed DrinkingWater Processed DrinkingWater Processed DrinkingWater Processed DrinkingWater Processed DrinkingWater Processed DrinkingWater Processed DiinkingWater Processed DrinkingWater Processed DrinkingWater Processed DrinkingWater Unprocessed DrinkingWater Unprocessed DrinkingWater Unpmcessed DrinkingWater Unprocessed DrinkingWater Unprocessed DrinkingWater Unprocessed DrinkingWater Unprocessed DrinkingWater Unpmcessed DrinkingWater Unprocessed DrinkingWater Unprocessed DrinkingWater Unprocessed DrinkingWater Unprocessed DrinkingWater Unprocessed DrinkingWater Unprocessed Tap Water Site#1 Tap Water Site#1 Tap Water Site#1 Tap Water Site#1 Tap Water Site#1 Tap Water Site#1 Tap Water Site#1 Tap Water Site#1 Tap Water Site#1 Tap Water Site#1 Tap Water Site#1 Tap Water Site#1 Tap Water Site#1 MC-121B MC-122B MC-123B MC-124B MC-125B MC-121K MC-122K MC-123K MC-124K MC-125K MC-121H MC-123H MC-124H MC-125H MC-1 15B MC-116B MC- I17B MC- I18B MC- I 19B MC-115K MC-1 16K MC-117K MC-1 18K MC-119K MC-115H MC-117H MC-118H MC-119H MC-126B MC-127B MC-128B MC-129B MC-130B MC-126K MC-127K MC-128K MC-129K MC-130K MC-126H MC-127H MC-128H ApproximateTotal Volume Collecte(dL)or *SedimentMass (g) LocationCoHected I lewasseeDrinkingWater Plant I Mwassee DrinkingWater Plant I Hiwassee DTinkingWater Plant I lewassee DrinkingWater Plant I Mwassee DrinkingWater Plant 1 Hiwassee DrinkingWater Plant 1 I-IiwasseDerinkingWater Plant I lewassee DrinkingWater Plant I I-IiwasseDerinkingWater Plant 1 I-IiwasseDerinkingWater Plant I lewasseeDrinkingWater Pl!nt I IfiwasseeDrinkingWater Plant I lewasseeDrinkingWater Plant I HiwasseeDrinkingWater Plant I Hiwassee DrinkingWater Plant I I-IiwasseDerinkingWater Pl!nt I lewasseeDrinkingWater Plant 1 HiwasseeDrinkingWater Plant I lewassee DrinkingWater Plant I Hiwassee DrinkingWater Plant I I-IiwasseDerinkingWater Plant I Mwassee DrinkingWater Plant I Hiwassee DrinkingWater Plant 1 Hiwassee DrinkingWater Plant I I-IiwasseDerialdngWater Plant I I-EwasseeDrinkingWater Plant I lewassee DrinkingWater Plant, I -lewasseeDrinkingWater Plant I Baymont Hotel I Baymont Hotel 1 -Baymont Hotel 1 -Baymont Hotel I Ba_ymo ntHotel I Baymont Hotel 1 Baymont Hotel I -Baymont Hotel I Baymont Hotel 1 Baymont Hotel I Baymont Hotel I Baymont Hotel I -Baymont Hotel FinalFieldRpt ClevelandTN Decatur AL Batteiie fttonsTOL*nolcw To Vvoo* Results Page:7 Matrix Table 7. Continued Water Site4r2 Tap Water Site#2 Tap Water Site#2 Tap Water Site#3 Tap Water Site#3 Tap Water Site#3 SurfaceWater Site#1 SurfaceWater Site#1 SurfaceWater Site#1 SurfaceWater Site#1 SurfaceWater Site#1 SurfaceWater Site#1 SurfaceWater Site#1 SurfaceWater Site#1 SurfaceWater Site#1 SurfaceWater Site#1 SurfaceWater Site#1 SuifaceWater Site#1 SurfaceWater Site#1 SurfaceWater Site#1 SurfaceWater Site#1 SurfaceWater Site#2 SurfaceWater Site#2 SurfaceWater Site#2 SurfaceWater Site#3 SurfaceWater Site#3 SurfaceWater Site#3 Sediment Site#1 Sediment Site#1 Sediment Site#1 SedimentSite#2 Sediment Site#2 Sediment Site#2 Sediment Site#3 Sediment Site#3 Sediment Site#3 POTW Effluent POTW Effluent POTW Effluent POTW Effluent POTW Effluent POTW Effluent POTW Effluent POTW Effluent POTW Effluent POTW Effluent POTW Effluent SampleED MC-129H MC-130H MC-131B MC-131K MC-131H MC-132B MC-132K MC-132H MC-101B MC-102B MC-103B MC-104B MC-105B MC-101K MC-102K MC-103K MC-104K MC-105K MC-IOIH MC-102H MC-103H MC-104H MC-105H MC-106B MC-106K MC-106H MC-107B MC-107K MC-107H MC-1 10B MC-IIOK MC-IIOH MC-1 IIB MC-111K MC-IIIH MC- I12B MC-112K MC-1 12H MC-139B MC-140B MC-141B MC-142B MC-139K MC-140K MC-141K MC-142K MC-139H MC-141H MC-142H ApproximatTeotal LocatioCnollected VolumeCollecte(dL)or *Sediment Mass (g) I Baymont Hotel I Baymont Hotel I Amoco Gas Station 1 Amoco Gas Station I Amoco Gas Station TennesseeJacksCaf6 I TennesseeJacksCaf6 I TennesseeJacksCaft T -lewasseeRiver I HiwasseeRiver I HiwasseeRiver I I-liwasseReiver I HiwasseeRiver I -lewasseeRiver I luwasseeRiver 1 lewasseeRiver 1. HiwasseeRiver I -lewasseeRiver I Hiwassee Rivei- 1 Hiwassee River I Hiwassee River 1 Hiwassee River I Hiwassee River I Hiwassee River I Hiwassee River I Hiwassee River I Hiwassee River I lewasseeRiver I Hiwassee River 200* Hiwassee River 200* Hiwassee River 200* Hiwassee River 200* I-IiwasseReiver 200* IiiwasseeRiver 200* Mwassee River 200* Hiwassee River 200* I-IiwasseReiver 200* I-liwasseReiver 1 ClevelandMunicipalPOTW I ClevelandMunicipalPOTW I ClevelandMunicipalPOTW I ClevelandMunicipalPOTW I ClevelandMunicipalPOTW I ClevelandMunicipalPOTW I ClevelandMunicipalPOTW I ClevelandMunicipalPOTW I -ClevelandMunicipalPOTW I ClevelandMunicipalPOTW I ClevelandMunicipalP FinalFieldRpt ClevelandTN Decatur AL Baneiie ftwrw Tm*noto" To Vfo* ResWts Page:8 Matrix SampleED POTW Sludge POTW Sludge POTW Sludge Urban Air (Vapor) Urban Air (Particulate) MC-144B MC-144K MC-144H MC-146 MC-147 Table 8. Collected Samples from Decatur AL Matrix Sample ID Drinking Water Processed Drinking Water Processed Drinking Water Processed Drinldng Water Processed Drinking Water Processed Drinking Water Processed Drinking Water Processed Drinking W terProcessed Drinking Water Processed Drinking W terProcessed Drinking Water Processed Drinking Water Processed Drinking Water Processed Drinking Water Processed Drinking Water Unprocessed Drinking Water Unprocessed Drinking Water Unprocessed Drinking Water Unprocessed Drinking Water Unprocessed Drinking Water Unprocessed Drinking Water Unprocessed Drinking Water Unprocessed Drinking Water Unprocessed Drinking Water Unprocessed Drinking Water Unprocessed Drinking Water Unprocessed Drinking Water Unprocessed Drinking Water Unprocessed Tap Water Site#1 Tap Water Site#1 Tap Water Site#1 Tap Water Site#1 Tap Water Site#1 Tap Water Site#1 Tap Water Site#1 Tap Water Site#1 Tap Water Site#1 Tap Water Site#1 Tap Water Site#1 MC-221B MC-222B mc-223B MC-224B MC-225B MC-221K MC-222K MC-223K MC-224K MC-225K MC-221H MC-223H MC-224H MC-225H MC-215B MC-216B MC-217B MC-218B MC-219B MC-215K MC-216K MC-217K MC-218K MC-219K MC-215H MC-217H MC-218H MC-219H MC-226B MC-227B MC-228B MC-229B MC-230B MC-226K MC-227K MC-228K MC-229K MC-230K MC-226H ApproximatTeotal VolumeCollect(eLd)or *SedimenMtass (g) 200* 200* 200* I Filter 1 PUF LocatioCnollected Cleveland Municipal POTW Cleveland Municipal POTW Cleveland Municipal POTW Cleveland Fire Department Cleveland Fire Department Approximate Total Volume Collected (L) or *Sediment Mass (g) I I I I I I I I I I I I I I I I I I I I I I 1 1 I I I I I I I 1 1 I I I I I I Location Collected Decatur Water Plant Decatur Water Plant Decatur Water Plant Decatur Water Plant Decatur Water Plant Decatur Water Plant Decatur Water PIant Decatur Water Plant Decatur Water Plant Decatur Water Plant Decatur Water Plant Decatur Water Plant Docatur Water Plant Decatur Water Plant Decatur Water Plant Decatur Water Plant Decatur Water Plant Decatur Water Plant Decatur Water Plant Decatur Water Plant Decatur Water Plant Decatur Water Plant Decaur Water Plant Decatur Water Plant Decatur Water Plant Decatur Water Plant Decatur Wat- Plant Decatur Water Plant Hampton Inn Hampton Inn Hampton Inn Hampton Inn Hampton Hampton Inn Hampton Inn Hampton Inn Hampton Inn Hampton Inn Hampton Inn Final Field Rpt Cleveland TN Decatur AL Baiefifie A;lk ...PuainTLe,c*nWoT"oV/m* Resvlts Page:9 Matrix Tap Water Site#1 Tap Water Site#1 V..-us Table 8.Continued 'I*apWater Site 4r2 Tap Water Site#2 Tap Water Site#3 Tap Water Site#3 Tap Water Site#3 SurfaceWater Site#1 SurfaceWater Site#1 SurfaceWater Site#1 SurfaceWater Site#I SurfaceWater Site#1 SurfaceWater Site#1 SurfaceWater Site#1 SurfaceWater Site#1 SurfaceWater Site#1 SurfaceWater Site#1 SurfaceWater Site#1 SurfaceWater Sit-#-I SurfaceWater Site#1 SurfaceWater Site#1 SurfaceWater Site#1 SurfaceWater Site#2 SurfaceWater Site#2 SurfaceWater Site#2 SurfaceWater Site#3 SurfaceWater Site#3 SurfaceWater Site#3 Sediment Site#1 Sediment Site#1 Sediment Site#1 Sediment Site#2 Sediment Site#2 Sediment Site#2 Sediment Site#3 Sediment Site#3 Sediment Site#3 POTW Effluent POTW Effluent POTW Effluent POTW Effluent POTW Effluent POTW Effluent POTW Effluent POTW Effluent POTW Effluent POTW Effluent SampleID MC-228H MC-229H MC-230H MC-231B MC-231K MC-231H MC-232B MC-232K MC-232H MC-201B MC-202B MC-203B MC-204B MC-205B MC-201K MC-202K MC-203K MC-204K MC-205K MC-201H MC-202H MC-203H MC-204H MC-205H MC-206B MC-206K MC-206H MC-207B MC-207K MC-207H MC-210B MC-210K MC-210H MC-21 1B MC-211K MC-21 IH MC-212B MC-212K MC-212H MC-239B MC-240B MC-241B MC-242B MC-239K MC-240K MC-241K MC-242K MC-239H MC-241H ---Xp-proximTaotealVolume Collecte(dL)or*Sediment Mass (g) I I I I I 1 I I I I 1 I I I I I I I 1 I I 1 I I I I I I I 200* 200* 200* 200* 200* 200* 200* 200* 200* I I I I I 1 I 1 I I LocatioCnollected Hampton Inn Hampton- Inn Hampton Inn Decatur Boat Harbor Decatur Boat Harbor DecaturBoat Harbor Texaco Gas Station Texaco Gas Station Texaco Gas Station Tennessee River Tennessee River Tennessee River Tennessee River Tenne&see River Tennessee River Tennessee River Tennessee River Tennessee River Tennessee River Tennessee River Tennessee River Tennessee River Tennessee River Tennessee River Tennessee River Tennessee River Tennessee River Tennessee River Tennessee River Tennessee River Tennessee River Tennessee River Tennessee River Tennessee River Tennessee River Tennessee River Tennessee River Tennessee River Tennessee River Dry Creek WWTP Dry Creek WWTP Dry CreekWNVTP Dry Creek WWTP Dr@ Creek VAVTP Dry Creek WWTP Dry C k VAVTP Dry Creek Vv'ArrP Dry Creek VVNTP Dry Creek V;WTP FinalFieldRpt Cleveland TN Decatur AL Ago, Battelie V.,;p iiiFiffiTnfgftffdnTfnfVrM Results Page: 10 Matrix Sample ID POTW Effluent MC-242H POTW Sludge -nr%,mxr vi..i.-- MC-244B MC-244K Table 8. Continued MC-244H Qwet SurtaceWater' MC-284B Quiet SurfaceWater' MC-284K Quiet SurfaceWater' MC-284H LandfillLeachate MC-235B LanllllLleachale MC-235K LandfillLeachate MC-235H Urban Air (Vapor) mc-246 Urban Air (Paniculate) MC-247 'Samples notpartof theMutti-CityStudy Approximate TotalVolume Collected(L)or *Sediment Mass (g) I 200* 200* 200* I I I I I I I Filter I PUF Location Collected k WNVTP Dry Creek WWTP Dry Cre k WWT? Dry Cre WWT? FlintCreek FlintCreek FlintCreek Morgan County Landfill an County Landfill Morgan County Landfill Dry Creek WWTP Dry Cmek VIVVTP 4.3 Instrumentation Results Air samples were collected using a General Metals Model PS-1 air sampler. According to SOP M3-MC-Fl. 1 the airsampler calibrationisacceptable ifitiswithin 10% of the expected results. To determine the acceptable resultsa calibrationwas conducted in Duxbury prior to the initiation 2 of the study. The initiaclalibrationcurve resultedin an R value of 0.997. The calibration 2 curves generated in Cleveland and Decatur had R values of 0.997 and 0.996 rrspectively.The percent differencein recorded values from the initialcalibrationranged from -1.92% to 3.70% for Cleveland and 0% to 6.56% for Decatur, respectively. The locationof each sampling sitewas determined using a Garrnin 12 XL GPS, the resultsare presented in Tables 9 and 10. The accuracy of the GPS unitwas verifiedpriorto departure from Duxbury by comparing a benchmark atBattelleversus the measured location determined by the instrument. The difference the true and measured coordinates was 0.01 kilometers. Following shipment to Tennessee the instrument was reinitialized-.Thiswas conducted atthe Baymont Hotel on May 24h. Within several minutes of the process,the unitwas displaying maps and locationsof the localarea,which indicatedthatitwas working properly. The results of the verificationsfor each sampling day are presented in Table 11. The resultof the verificationfor Cleveland was a differenceof 0.11 kilometers between the "true" and measured coordinates. Although the verificationisbeyond the acceptance criteriat,he positiondata forthe day willbe considered valid because itappeared thatwhile the instrument was receiving data,the Department of Defense might have adjusted the satellitseelective availability.The instrument did not record a constant position over a five-rriinutpeeriod and the positionappeared to change in a regulated step manner. The resultof the verificationin Decatur resultedin a differenceof 1.68 kilometers between the true" and measured coordinates. The reference point thatwas used for the verificationwas that "of the discharge forthe plant. During the verificationthe plant manager suspected that the referenceposition was thatof the plant outflow located onsite. Based on the substantial FinalFieldRpt Cleveland TN Deca= AL Baiteiie 14 14 14 In IN Resulu Page-.11 differenicnpeositiofnusrthienrvestigatwiaosnconductedS.ubsequentlyithas been discovered thatthepositionistheterminatiopnointof thedischargepipe*locat6dintheriver.Based on this informationverificatiwoans notpossibleforthatday. According theQAPP theminimum distanrebetween sedimentsamplingsitespositioniss500 feetapart.The followingresulthsave been calculateudsingtheGarmin GPS. The distancefrom ClevelandSite1 toSite2 is229.6',thedistancefrom Site2 toSite3 is196.8'and thedistance from Site1 to Site3 is360.8'.Sampling atClevelanddidnotmeet theQAPP requirements.The distancefrom DecaturSite1 toSite2 is951.2',thedistancefrom Site2 to Site3 is754.4'and thedistancefrom Site1 to Site3 is1,148'. Table 9.Sampling SitePositionisn ClevelandTN Sampling Location Hiwassee DrinkingWater Plant Baymont Hotel Amoco Gas Station Tennessee JacksCaf6 Hiwassee River Site#1-1 lewassee RiverSite#2 Hiwassee River Site#31ClevelandMunicipalPOTW ClevelandFireDepartment T= Transcribedatainlog Latitude N 35016'01.5" N 35011'34.2" N 35011'44.1" N 35011'38" N 35"'20'38.2" N 35"'20'40.3" N 35020'40.8" N 35018'35" 35009'19.5" Table 10.SamplingSitePositionisnDecaturAL Sampling Location DecaturWater Plant Hampton Inn DecaturBoat Harbor Texaco Gas Station TennesseeRiver Site#1 TennesseeRiver Site#2 TennesseeRiver Site#3 Dry CreekWV*ITP (EffluenStample) Dry CreekWVn? (AirSample) Morgan County Landfill FlintCreek Latitude N 34036'14.7" N 34034'41.4" N 34036'57.2" N 34035'26.9" N 34037'03.2" N 34037'07.1" N 34037'00.1" N 34*37'31.5" N 34037'20.4" N 34037'19" N 34033'59.4" Longitude W 84045'31.9" w 84053'28" W 84053'2@0-.9@"i W 84053'28.2" W 8405I'l0.4" W 94*51'10.8" W 8405 I'l3.1" W 84047'58.2" W 84052'41.9" Longitude W 86057'41.7" W 87'01'13.5" W 86058'16.1" W 87001'50.3" W 86058'08.T' W 86058'18.7" W 86058'21.3" W 86'59'55.7" W 86059'53.8" W 87006'Or2" W 86057'55.6" Address 114 ValleyRoad Routes 60 and 75 Routes 60 and 75 Routes60 and75 Eads BluffRoad Eads BluffRoad Eads BluffRoad Lower RiverRoad 555 Oc2ee Road Address Market Street Route 67 RiverwalkMarina Route 67 RiverwalkMarina RiverwalkMarina RiverwalkMarina leghway 20 FEghway 20 Highway 20 Country lubRoad Table 11.GPS PositionVerificatioRnesults CalibratioLnocations Waypoint PositionatPOTW GPS Derived Position Difference ClevelandTN N 35018'35"/ W 84047'54" N 35 018'35"/ W 84047'58.2" 0.11 kilometers- bearing93* DecaturAL N 34038'10"/W 86059'09" N 34037'31.4"1W 86*59'55.7" 1.68kilometers- beating470 FinalFieldRpt ClevelandTN DecaturAL Balteiie Puwnlg Tochmlogy Tc,Vbf* Problemsuperienmdand rmmn=dations Page:12 4.4Conununications Durintghecompletioofnthefielsdurveys,everaclonversatiroengsarditnhgesamplinegffort were noted.These communications were conductedbetween Battellsetaffand various municipalemployeesor thepublic. In Cleveland,TN, ChiefGaylor oftheCFD was informedthata donationtotheSt.Jude's Hospitalwould be sentdirectlfyrom Columbus intheirname. We must ensurethatthiseffortis completed.PaulPittstheAssistanMtanager ofClevelandUtilitieWsater Divisionprovided maps tothefacilitiaensd reiteratehdisofferto allowus to samplethelandfillleachateas itis pumped to thePOTW. On May 21, 1999 a callwas receivedfrom Kem CarrofDecaturUtilitieisndicatintghathe would not allowthesamplingtooccuratthePOTW orDrinkingWater Plantifhe was not informedof theclient.FollowingtheconversationM,arciaNishiokawas contactedand made aware of thesituationI.n responsetothesituatiointwas decidedby theclientand Battelltehata confidentialiatgyreementrevealingtheidentityoftheclienwtould be draftedand offeredt.o W. Carr.A conversatiobnetween Ms. Nishiokaand Mr. Carrresultedinan agreementinwhich the client'isdentitwyas revealedinconfidence,and in r-etumwere allowedtocollectsamplesatthe POTW and thedrinkingwaterplant.The agreementwas completedon Wednesday May 26, 1999. Lateron May 26"'duringa conversatiobnetween W. Carr and ScottMacomber, the samplingteam leaderW,. Carrindicatedthathe wanted tospeakto theclientdirectlyM.r. Macomber indicatedthathe would informtheprojectmanager of thesituationO.n May 27thW. Carrdirectlcyontactedthemanager of thelocalmanufacturingplantforfurtherinformation. Mr. Carr'semployees atthePOTW inquiredseveraltimesaboutwhat we were lookingfor duringour visitothefacilityD.uring thecalibrationftheairsamplerMichaelDeck, an assistanstupervisoarttheplantasked ifwe were samplingforMolybdenum. He revealedthat thefacilithyad dischargeexceedencesin therecentpastdue tolocalindustryinput. Therewere no otherpertinenctonversaitonssurroundingthecollectioonf samplesatthevarious facilititehsatwere sampled. During thecourseof collectinsgurfacewatersamplesinboth Decaturand Cleveland,members of thegeneralpublicinquiredaboutthesamplingeffort.In each casea generalanswer was offeredand allinterestepdartieswere satisfied. 5. PROBLEMS EXPERIENCED AND RECOMMENDATIONS During thecollectioonfsamplesfrom ClevelandTN and DecaturAL thefollowingQAPP deviationwsere encountered 9 The QAPP Section12.2statesthat"sampleswillbe shippedattheend of each collectiodnay fornext-daydelivery".In bothcitielsogisticaplroblemspreventedthesamplesfrom being shippedon thesame day thattheywere collected.Clevelandsamples were collecteodn Tuesday May 25h and shippedon Wednesday May 26th.Decatursamples were collecteodn FinalFieldRpt ClevelandTN Decamr AL Baftelie, LAk.* A Pmblem expaiencemdd mmmmenfttions Page: 13 ThursdayMay 27d'andshippedon FridayMay 28'h.Battellperojectleadershave indicated thatsamplescan be chilled(onice)overnightand shippedthefollowingday when adequate timeisavailablea,nd thatthischange toprotocolwillbe addressedinan addendum tothe QAPP. The samplescollecteidn Decaturwere shippedon FridayMay 28thand were not specifically marked fora Saturdaydeliveryr,esultinign a 4-dayperiodintransitS.amples were delivereTduesday June!l,"P.riortothenextsurveylogisticparleparationwsillbe inplace forSaturdaydeliveryto recipienltaboratories. F4 Battelle'Ssampling Task QualityAssuranceOfficer,Rosanna Buhl,conducteda fieldaudit duringthesesurveysand has preparedan internarleporttoimprove fieldoperationsand ensure fullcompliancewiththeQAPP and SOPS. In responsetoBattelle'isnternaaludit,thefield,crew willredesignseveralfieldlog formsto helpfacilitattiemelyand accuratedatarecording. FinalFieldRpt ClevelandTN DecaturAL miffeiie ftwnr rm*nobffv To %oW* FielRdeportAddendum - ClevelanTdN, and DecaturA,L AtmosRheriScuElingDetailTsh.efollowidnegtaialrse-incluhdeerdetocomplettehefielrdecorwdidi respectto samplerpositioning. Cleveland,TN: The airsampleratthissitewas positionedapproximately4 feetfrom thefiredepartment headquarterslocatedat555 S. Ocoee Street. Decatur,AL: The airsamplerinDecaturwas positionedapproximately3 to4 feetfrom theDry Creek wastewatertreatmentplant. SurfaceWater S=Iiniz. The followingdetailasreincludedhereto completethefieldrecordwithrespect to sitecharacteristics. Cleveland,TN: The surfacewatercollectedateach of 3 within2 inof shoreinca.0.5in depth.Resuspended bottom sedimentswere avoidedineach case. Decatur,AL: The surfacewatercollectefdrom thelocalriversystemwas collecteadteach ofthe3 sites within2 in of shoreinca.0.5 indepth. Re-suspendedbottom sedimentswere avoidedineach case. Additionallya,single"quiescent"watersitewas sampled withinFlintCreek accessedfrom Country Club Road. The sample was alsocollectedwithin2 m of shoreinca.0.5 m depth.Re-suspendedbottom sedimentswere avoided. K:@ Ba(tAleDuxbury Operations Date