Document O3Jk6JMkNwRNDXq2Ldz7yVDnw
CG 40
CODE RT-531-D
jp 1,5 1981 FZKZB
( DATE )
< LOT )
PROCESSES
APPROVED BY
( >ET-531-D <N) EWK 11-24-81
COMTYP JOB NAME: 40RT531DMN
TYPED BY: JMH
EST. WT, M3* LBS.
F4ir- fftetiSTANDARD HRS. _____
TIME
.M
PREPARATION NOTES: SUPV1R NOTE: DO NOT USE V-3Q3 FOR NAP.HTHANILS WHEN CAMPAIGNING DALAMARS YC-39-A, YC-40-A, YT-839-P, YT-840-P, YT-858-D, AND YT--B68-D.
SEMI-BLEEDING
EQUIP KENT
NAME: NAPHTHANIL RED LIGHT
USE I N-CODE ACCT LBS LBS
BTAIN 4-NITR0-2-AMINOTOLUENE FOR `S6 OBTAIN 3 -HY DRG X Y- 2 -N APT H YL AM1DE FOR SI 8 CLEAN, DRESS, CLOSE 24* CLARIF PRESS -
5 FRAMES
504-C | 150-C |
UN JJL* <486 G) WATER INTO
UN IN HYDROCHLORIC ACID FROM V-324
m_*___t____ ___ i
Clip IN FROM SI
LOT
4-NITR 0-2-AMIN OT QLU E NE
______
Ml-
28-D 504-C
1 262//
STIR 15 MIN TO, WET ^SSf___________.
ADJ TO
<102O G> AT 40-45 DEG F
f\/X330 |
I 5BPH0N IN SODIUM NITRITE IN 7-10 MIN
t ^|
, r.,,LU--X
i
STIR 5 MIN 4, RECORD: CR__,L_< + >, KI,,^L__< + ) I
I
i NOTE: <1> IF CR-, KI- ADD 204 *AS IS* I !
I INCREMENTS HYDROCHLORIC ACID ASSUME 32%
i RECORD: CR___<+> KI________ ( + )
Ii
I (2) IF CR+, KI- ADD 104 *AS IS* INCREMENTS |
|
ODIUM NITRITE
ASSUME 33% t_______
RECORD: CR^_____ < + ) KI_,.__< + >
.
I!
STIR 10 HIM AT 40-45#F MAINTAINING +CR, +KI|
50ft SI 3 RECORD: TIME START..JL4C-
i
i 57-A
725-A '
28-D
725-A
i 95 I I
I 1 |___ _
t SLURRY DICALITE FILTER AID IN 40 GAL WATER |
IN DRUM & PRECOAT CLARIF PRESS
j
5 1 777-A 1 ,1 1
5
WHEN S11 STIR COMPLETE DUMP IN ACTIVATED
CARBON 4 ybUMP IN DICALITE FILTER AID
| STIR 30 MIN AT 40-45 DEG F
ASSUME 33%
1 MAINTAINING +KI FOR ,S23.
,
j RECORD: START_,,_iiJj___KI___X____ < + )
15 1 |
10 | _____1 _____ 1
113-B
777- A 725-A
57-A
1 IS
1 1 10 1 __
1____
IUN 13* <177G) WATER INTO V-330
| \y i SLURRY TRISULPHCIL SOAP D IN 25G WATER 4,
' ,4"T,0UR IN
S8 1 DUMP IN 3-HYDRQXY~2~NAPTHYLAMIDE FROM S2 6
I STIR 30 MIN OR LONGER TO WET,
LOT
] RECORD: START,,,,,,?.
_____
.1 Ou j p <?-- ----------------- ---
16 J77..
211382;
39-A | 16 I
150-C | 370
N38128
EQUIP MENT
3 CG 4Q CODE RT-531-D (N>
. "*1%,.
I USE T"n -35d eT ACCT
I LBS
LBS :
PUN < WlMtfr) WATER INTO V-302
POUR IN SODIUM HYDROXIDE
ASSUME 50%
PHON IN ACETIC ACID & STIR 3 MIN
I
7/) H.____ \*A RECORD PH,,/._(6.7~7.5> IF NECESSARY ADJ TO|
I 6,7-7.5.
ACETIC ACID ASSUME 70%i _
RECORD PH____ SODIUM HYDROXIDE ASSUME 50%I
J 7-D ! //
II | x: 30-D 1
II I 30-D ! I 7-D I.
.TURN ON
AGITATOR $, ADD ICE, THEN
SHUT OFF AG.TTAT-0R
2X33 |
PUMP DV THRU CLARIF PRESS INTO DV USED IN
S 23. MAINTAINING TEMP AT 40-45*F. RECORD:
TART; _r
. TOTAL MIN___iJL___
O'tE: DO NOT USE V-303 - TOO SMALL
WHEN S23A CLARIF COMPLETE WASH DV <S4>
LINES PUMP & PRESS FOR 20 MIN'-QR TO A -CR.
TEST ..ON A SAMPLElJr'mtjAL PRES\EFFLUENT
" 4ICHEVER COMES FIRST. CObbECT WASHINGS IN
DV (S23> RECORD: START y^CR
(-0R+)
N S24 IS COMPLETE TEST DV(S23> ASSUME 33%|___
t. RECORD; KI_,,:3t_J + ) TMP___(40-45* F) !_
W?GH SULFAMIC ACID IN RUBBER BUCKET AND I
INSE IN AND STIR 5 MIN.
i 10
RECORD; KI_,,n__. MUST BE - & IF NECESSARY I
l Jj TO -KI WITH SULFAMIC ACID ADJ TO_______ _* (1925 G) AT 40-45 DEG F
1 1X330
57-A |.
725-A 57-A
395-D '395-D
57-A
1
Kto/OS 2J
RUN 39* (390 G) WATER INTO
|
INSTALL TEMP CHART i, SET AGITATOR AT 16 RPMI
HEN SI9 STIR COMPLETE, POUR IN SODIUM
I
I
HYDROXIDE IN 3-4 MIN.
ASSUME 50% I^220 i
HEAT TO 128-132 DEG F AFAP f, STIR 5 MIN TO |
|
SSOLVE. STOP AGITATOR.
|i
7-Dl | 110
IMMEDIATELY RUN V-33 AFAP INTO CV.. NO
I TAT I ON IN CV4 RECORD: SiW\,,XlZd
TOTAL MIN ____ JX-- I$4 I POUR IN ACETIC ACID 4 STIR 5 MIN.
X:
j JX
. M____ 7_______ ,____kZSAX
...I
\W\ RECORD; PH..^/*_M0.5-11.0) ASSUME 50%
NECESSARY ADJ TO PH 10.5-11.0
iGRD: PH___,,___ _
ASSUME 7%
138 IN V-302 AFAP
Ip^iJUMP IN BARIUM SULFATE
35
i3SH HJ TO 78-32 DEG F AND RECORD:
DEG F AND REC___#&___DG F
WHEN S28 COMPLETE, COUPLE DV UNDERSURFACE IN 65-7 MIN. MAINTAIN CV AT 73-82 DEG F.
>ORD; STARTTOTAL MIN
_____
"STIR 5 MIN, DISCONNECT TRANSFER LINE AT CV
& RECQftfti DIAZO_rX!-. <+/-> ^SE2^r__(MUST BE +) PH_%jfe_(4.2-4.6)
IF NECESSARY STIR TO - DIAZO RECORD:
START___________ _ TOTAL MIN____________
RECORD: DIAZO__________MUST BE -
BASE __________MUST BE +
PH _______ (4.2r4.6)
30-D 7-D
30-D
65-A
150 35
DUP050047515
CPHTYP JOB NAME : 40RT531DMN
'PAGE 03
DATE PRINl ED:MM/DD/YY
iQUIft~T MEN?' J HI SC i
T --
- ( f Hcoii T ACCT
I AGE 3 OF 3 CG 40 CODE RT-531 -D (N) | LBS I
! LBS
ADD 3SG WATER AT 130-140* TO RUM FROM HOT ! 30 |
11 ! i WATER MIXER ADD BLANCOL N &STIR FDR S43 1
I
/0>
ft IN N-567-B SOLUTION FROM S42 HEAT, TO i94-196,JjG.F IN 5S-60 MINJiT
'CRD: HT /fX---DEG F AND REC_XTii_DEG F WHEN S44 HEATING COMPLETE, RUN IN ALUMINUM i IJJLFATE SOLUTION THRU BADGER METER* NOTE? | 120
. KRINSE IN LINE AFTER N-115-D SOL'N RUN IN. i m IJWPIR 30 MIN AT 194-196 DEG F
' FLOOD TO BO" (7928G) AND STOP AGITATOR
VAT
I V-3031 V-31 51V-3171 /^2 \ V-323
S4 (486G) I 20*1 14" I 14" |f14*M| 14" SO (1020G) I 43"J 30" I 30* i\ 30*/l 30"
i i
I 115-D |
I
60
START
FIN
OPTR
//*?
T 1
____ __________ i ____ SJ2k-_v
I I
t
MM 4T0
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