Document O3JRG8Lxk6075r4vL7q1db8qQ

EpidFeFmIIiNNoAlAoLLgyRR,EEP2P2OO0RR-3TTW-05 EpiMMdeeeddmiiiccoaaillogDDyee,ppaa2rr2tt0mm-ee3nnWtt-05 33MM CCoommppaannyy SStt..PPaauull.,MMNN 5555114444 Tile: FFlluuoorroocchheemmiiccaall EExxppoossuurree AAsssseessssmmeenntt ooffDDeeccaattuurr CChheemmiiccaall aanndd FViillmm PPllaanntt Title: EEmmppllooyyeeeess FFiinnaall RReeppoorrtt DDaattee:: AAuugguusstt 1111,,11999999 SSttuuddyy SSttaarnt DDaattee:: SSeepptteemmbbeerr 33,, 11999988 PPrroottooccooll NNuummbbeerr:: EEPPII--0000(066 IIERxReBBmAAppptpprroovvaall((E#4x9p9e85d00i88t22e)d): X IEIxRReBBmAAppptpp:rroovvaall DEDaaxttpeee::diSSteeedpp:tteeXmmbbeerr 33,, 11999988 SSttuuddyy AArrcchhiivvee NNuummbbeerr:: AARRCCHH--002211 PPrriinncciippaall IInnvveessttiiggaattoorr:: CoC-oin-ivnevsetsitgiagtatoorrss:: GGeeaarryyWW..OOllsseenn,,DDVVMM,,PPhhDD'' CPPeearrrrtyyhWAWy...LSLoiogmgapansn,o,nMM,SSR*ZN? CKJKraeriatisnhstyteM.neAJnJ..B.SuHHriaramninpsss,seeonRnn,N,,,PPRhhMNDDP"Z3H! JMMeiiaccnhheeMll.eeBMMu..rrBBiuusrr,llReeNww,,,MMMSPS"H1 ' JJJooehhfnnfCCr.e.HySS.cchhMuaumnmpdpeeerlrt,t,,MMMDDD,,,MMMPPPH1H!4"1 Jeffrey H. Mandel,MD,MPH' SSttuuddyyDDiirreeccttoorr:: JJeefffrferyeHHy.. MMaannddeell,,MMDD,,MMPPHH 1. 3M MMeeddiiccaall DDeeppaarrttmmeenntt,,222200--33WW--0055,,SStt..PPaauull,,MMNN 5555114444--11000000 3M 1. 2. 33MM DDeeccaattuurr,, EEHHSS&&RR,,PP..OO..BBooxx 22220066,,DDeeccaattuurr,,AAllaabbaammaa 3355660099--3.7-210066 2. 33.. 33MM EEnnvviirroonnmmeennttaall LLaabboorraattoorryy,,22--33EE--0011,,SStt..PPaauull,,MMNN 5555114444--I10O0OCC tet4o 1 econ rope cog vomsion | 2512| swsrcsons MMaaddeeAAvvaaililaabbllee bbyy 33MWffofoorrr IIInnssppeeccttiioonn aannddCCopoypiynging aass CCoonnffiiddenetntial Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 EExohibit 2812 State of Minnesota v. 3M Co., 3MA10050434 Court File No. 27-CV-10-28862 22881122..00000011 p1003a0nM6 PPaaggEeeP2t2-0o01f0880556 QQUUAALLIITTYY AASSSSUURRAANNCCEE SSTTAATTEEMMEENNTT TFTiIIlTTmLLPEElOaOnFFt ESSmTTpUUlDoDYyY:e:esFFlluuoorroocchheemmiiccaall EExxppoossuurree AAsssseessssmmeennttooffDDeeccaattuurr CChheemmiiccaall aanndd Film Plant Employees T"GTuhhieedeaalbbioonvveees ssfttouurddGyyowwoaadssEeepxxiaadmmeiimnnieeoddloffogorry qqPuuraaallciitttiyyceaasssssfuuorrraaOnncccceeuiipnnatkkieeoeenppaiilnngganwwdiittEhhnttvhhserossppniimrreiitntotofaflTThhee EEGEppupiiiiddddeeeemlmmiiiinoooelllsoooggfgioiycrcTGRRaeoesssokeedaaGrrErccpohhuipdaa.essmppiTuuohbblleloiigfssyihhneePaddrabrbceyytpiottcrhheteesCwCfhahoeesrmmOdiiceccctaauellpraMMmtaaiinnnouuneffaaaolcctatbuunerrdeeaErrnsnsavAAcsscrssuooornccamiiteaaentttriieoaofnlnlectionn below. EofpittdhheeemddiaaottalaooogbbtytaaTiinanesedkd..GrTTohhueep.ddaaTttehesseoofffinQQauulaarlleiipttoyyrtAAsswssauusrraadnneccteeeraamccittiinvveiidttiiteeossbooenn attnhhiiassciscttuuurddayyteaarrreeefllliiesscttteeiddo of below. SSttuuddyy Inniiitiaattoionn DDaattee::0099/00331/9988 SSttuuddyy CCoommpplleettiioonn DDaattee:: 0083//1111//9999 "TTYYPPEE OOFF AAUUDDIITT:: Protocol, Draft Protocol | 062899 0672899 CE Protocol,Draft Protocol `Addenda, Data File, Draft Addenda,Data File,Draft Final Report Final Report [FFiinnaallRReeppoornt | DDAATTEE OOFF | DDAATTEE FFIINNDDIINNGGSS AAUUDDIITT RREEPPOORRTTEEDD TTOO PPRRIINNCCIIPPAALL IINNVVEESSTTIIGGAATTOORR AANNDD SSTTUUDDYY DDIIRREECCTTOORR 06/28/99 06/28/99 DDAATTEE FFIINNDDIINNGGSS RREEPPOORRTTEEDD TTOO 3aMm MMAANNAAGGEEMMEENNTT 06/28/99 om0o8/o09/o99 | ow08o/o09R/9o9 |_ 008//0099/9999 eAAprrcichdhieivvmiiinnoggl::ogAAyllllarracahwwivddeaattsayasaatnnemdd.tthhe ffiinnaall rreeppoorrtt wwiillllbbeefflieledd iinntthhee OOccccuuppaattiioonnaall MMeeddiicciinnee epidemiology archive system. SSiiggnnaattuurreess((aanndd ddaattee))ooffQQAA AAuuddiitt TTeeaamm Busa9'An'W &a QlDi>s~bxey Aft" 7 - Lan8i. Feg.ww g8//19//1997 8a faq MMaaddee AAvvaaiillaabbllee Subject to Prote bbyy cti v33eMMOfrfodorreIrnIsnIspnpeePcctatilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC 2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00002 3SMMAA1100005800443355 EPLO3a0MMG Page 385 EPI-0006 Page 3 of 85 AABBSSTTRRAACCTT IInntthhee ppaasstt,, eemmppllooyyeeeess aatt tthhee 33MM DDeeccaattuurrcchheemmiiccaall ppllaanntt hhaavvee vvoalluunnttaarriillyy ppaarrttiicciippaatteedd iinn aa fMluuoorroocchheemmiiccaall mmeeddiiccaall ssuurrvveeiillllaannccee pprrooggrraamm.. ~ AAnnaallyyssiissoofftthhee ssuurrvveeiillllaannccee ddaattaa hhaass mnoott sshhoowwnn ssiiggnniiffiiccaanntt aassssoocciiaattiioonnss bbeettwweeeenn tthhee eermrp.lpolyoeyeeess"' cclliinniiccaall cchheemmiissttrryy aanndd hheemmaattoollooggyy tteessttss aanndd eeiitthheerr ttoottaall sseerruumm oorrggaanniicc fflluuoorriinnee o)rr sseerruumm PPFFOOSS ((ppeerrfflluuoorrooooccttaannee ssuullffoonnaattee))lleevveellss.. HHoowweevveerr,,tthhee vvoolluunnttaarryy nnaattuurree ooff tthh:!hhiissttoorriiccaall mmeeddiiccaall ssuurrvveeiillllaannccee pprrooggrraamm ddiiddnnoott pprroovviiddeeffoorraa ccoommpplleettee uunnddeerrssttaannddiinngg ooffthhee ddiissttrriibbuuttiioonnoofffflluuoorroocchheemmiiccaall sseerruumm lleevveellss iinn tthhee DDeeccaattuurr wwoorrkkffoorrccee..TThheerreeffoorree,,tthhee ppuurrppoossee oofftthhiiss ssttuuddyy wwaass ttoo ccoolllleecctt ddaattaa bbyyrarnadnodmolmylyssaammpplliinngg eemmppllooryeeeess iinn tthhee DDeeccaattuurr cchheemmiiccaall ppllaanntt iinn oorrddeerr ttoo ddeetteerrmmiinnee tthhee ddiissttrriibbuuttiioonn ooff eemmppllooyyeeee sseerruumm flluuoorroocchheemmiiccaall lleevveellss aaccccoorrddiinngg ttoo ddeemmooggrraapphhiiccss,,ccuurrrreenntt aanndd lloonnggeesstt hheellddjjoobbss,,yyeeaarrss vvoorrkkeedd aanndd building llooccaattiioonnss.. IInn aaddddiittiioonn,aa rraannddoomm ssaammppllee oofftthhee nneeiigghhbboorriinngg 33AM1 DDeeccaattuurrffiillmm building ppllaanntteemmppllooyyeeee ppooppuullaattiioonn,,llooccaatteedd aatt tthhee ssaammee ssiittee,,wwaass tteesstteedd t0o ddeetteerrnmiinnee fflluuoorroocchheemmiiccaall sseerruumm lleevveellss iinn oorrddeerr ttoo cchhaarraacctteerriizzee tthhee ddiiffffeerreenncceess bbeettwweeeenn tthhee ttwwoo. ppllaanntt ppooppuullaattiioonnss.. AA ttoottaall ooff223322eemmppllooyyeeeess wwaass rraannddoommllyy sseelleecctteedd ffoorr sseerruumm ssaammpplliinngg:: 118866((8800%%)) ppaarrttiicciippaatteedd iinn tthhee bblloooodd ccoolllleeccttiioonn wwhhiicchh ooccccuurrrreedd iinntthhee FFaallll,, 11999988.. Iumn aaddddiittiioonnaall 7777 eemmppllooyyeeeessrreeqquueesstteedd bblloooodd tteessttiinngg ffoorr tthhee ddeetteerrmmiinnaattiioonn oofffflluuoorroocchheermriiccaall lleevveellss.. OOfftthhee random ssaammpplleeooffeemmppllooyyeeeess wwhhoo ppaarrttiicciippaatteedd,, 112266 wweerree ffrroomm tthhee tchhee nniiccaall ppllaanntt aanndd6600 random ffrroomm tthhee ffiillmm ppllaanntt.. TThheerree wweerree 6611 vvoolluunntteeeerrssffrroomm cchheemmiiccaall aanndd 1166 -voolluunntteeeerrss ffrroomm ffiillmm;;tthhuuss,,aallll cchheemmiiccaall ppaarrttiicciippaannttss nnuummbbeerreedd 118877eemmppllooyyeeeess aanndd aallll U{ lImm ppaarrttiicciippaannttss nnuummbbeerreedd 7766eemmppllooyyeeeess.. AAtt tthhe ttiimmee ooffbbllooooddcoclollleeccttiioonn,,eemmppllooyyeeeess rr,2-ssppoonnddeedd t10o.8 attwwoo-ppaaggee qquueessttiioonnnnaaiirree tthhaatt iinnqquuiirreedd aabboouutt tthheiirr ccuurrrreenntt aanndd lloonnggeesstt hheellddjcabbss,,tthhee bbuuiillddiinnggss Sih iorocOhrde ePalmer. OW 530.8308 +" Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00000033 AROS 3MA10050436 yt rin cherie, ndps ossofa nsWoa 3M EPI-OW) Page 4 of85 they had worked in (if chemical employees),and possible routes of oral ngestion of fluorochemicals through cigarette smoking,chewing gum,chewing tobacco and hand washing practices. Sera samples were extracted using an ion-pairing extraction procedure. The Co ---------- On ----TAA To extracts were quantitatively analyzed for PFOS(perfluorooctane sulfon,te),PFHS (perfluorohexane sulfonate),POAA (perfluorooctanoic acid),PFOSAA(N-ethyl JO perfluorooctanesulfonamido acetate)PFOSA (perfluorooctane sulfonate amide), M570 (N-methyl perfluorooctanesulfonamido acetate)and M556(perfluorooc anesulfonamido acetate) using high-pressure liquid chromatography/eIectrospray tanden. mass ssppeeccttrroommeettrryy((HHPPLLCC//EESSMMSSMMSS))aanndd eevvaalluuaatteedd vveerrssuuss aann eexxttrracctteedd ccuurr4v. PPFFOOSS.,PPFHHSS., POAA,PFOSAA and PFOSA levels were determined by Northwest Bioanalytical Laboratory. M570 and M556 levels were determined by the 3M Envirc nmental ory Laboratory. ir ro The overall arithmetic means(and range)and the geometric means and(95% ccoonnffiidence iinntteerrvvaall))ooff tthhee rraannddoom ssaammppllee ooffcchheemmiiccaall eemmppllooyyeeees((nn == 112266))ffoorr tthhee sseevveenn rss prs or 7) fluorochemicals are presented below(in ppm): J Chemical Plant pti atba cones ns. Arithmetic Mean (and Range) a ome mos vou 00 PFOS PPFFHHSS PPOOAAAA PPFFOOSSAAAA MM57700 mow mo gow oom mow onl in OU PPFFOOSSAA M556 1.505 (0.091-10.600) 00..334455 ((00..000055--11..888800)) 11.5366 ((0.0211 --66..776600)) 00.02233 ((00..0011 -- 00.26699)) 0.15511 ((00.008 - 0.99922)) 00..006622 ((0.000.050--000..06611522)) 0.052 (0.001 - 0.406) Geometric Mean (and 950/ > CI) PFOS PPFFHHSS PPOOAAAA PFOSAA M570 PPFFOOSSAA M556 0.941 0.180 0.899 00..0008 0.081 00.001133 0.022 (0.787 - 1.126) ((00..114455-- 00..222233)) ((00..-,7222-- 11..112200)) ((00..(,00066-00..001111)) ((00..(0,6677 - 00.09988)) ((00..009 --0.001188)) (0.018 -0.029) te late 901 op cion CopCottle Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00004 swsreososer 3MA10050437 EPLO03aGMn. PagEeP1sof-800506 "TThhee oovveerraallll aarriitthhmmeettiicc mmeeaannss((aanndd rraannggee))aanndd ggeeoommeettrriicc mmeeaannss(( 9955%% ccooPnnaffpiidd5eennofcc8ee5 iinntteerrvvaall))ooff tthhee rraannddoomm ssaammpplleeooffffiillmm ppllaanntt eemmppllooyyeeeess((nn == 6600))ffoorr tthh<e- sseevveenn fflluuoorroocchheemmiiccaallss aarree pprreesseenntteedd bbeellooww:: FFiillmm PPllaanntt AArriitthhmmeettiicc MMeeaann (a(anndd RRaanngge)e) GGeeoommeettrriicc MMeeaann(a(anndd 99555: CCID) PPPFFFHOOSSS 000..011277322 ((0000.01001551---00092.4916406))) PPPFFFOOHSSS 000..011133366 (((000.0i111441---0001.06116181))) 0.018) PPPFOOHAASAA PFOSAA 000..000772113 (((000..000000166---0002..22919808))) 0004 (0001-0038) PPFPOOHAASAA PFOSAA 000..000414949 (((000..03013919---000.60622)) 0003 (002-0003) PMMF557O70S0AA PFOSA 000..000202040 (((000..000000111---000..404535448))) 85%of samples <LLOQ PMMF5SO7T0SAA PFOSA 0008...5000%000838of(((s000a..r000s000pl662e---s000<0..001L011L31)))OQ" PLMMFs5LSO5O6S6QA= lower800l..5i00m%00it88ooff(s(0qa.0um00ap0n0lt00ei11ts-a-<t00i3.Lo03nL70f)O7o)rQP*FOSPMMAF555O5ra6S6nAged from800.0.5.00%000033o1f(-s(00a01.m0)0p01l220e--sp00<p0.0m0L40L)4O) Q* LLOQ = lower limit of quantitation for PFOSA ranged from 0.001 - 0.)10 ppm. T"Thhee aabboovvee vvaalluueess sshhoowweedd hhiigghh vvaarriiaabbiilliittyy aaccccoorrddiinngg ttoo tthhee eemmppllooyyeeeess'' ddeemmooggrraapphhiiccss,, wwoorrkk hhiissttoorryy aanndd bbuuiillddiinngg llooccaattiioonnss.. AAmmoonnggtthhee rraannddoomm ssaammppllee((n0 == 112266))ooffcchheemmiiccaall eemmppllooyyeeeess,,cceellll ooppeerraattoorrss hhaadd tthhee hhiigghheesstt ssecrruumm lleevvee ss ooffPPFFOOSS ((ggeeoommeettrriicc mmeeaann == 11..997700 ppppmm))aanndd PPFFHHSS((ggeeoommeettrriicc mmeeaann ==00..669977 ppppmm)).. HHoowweevveerr,.sseerraa ffrroomm cchheemmiiccaall ooppeerraattoorrss aanndd mmaaiinntteennaannccee wwoorrkkeerrss hhaadd tthhee hhiigghheesstt lleevv(ellss ooff ootthheerr fflluuoorroocchheemmiiccaall aannaallyytteess((PPFFOOSSAAAA,,MM57700,,PPFEOOSSAA aanndd MM555566))aa cchhaarraacctteerriissttiicc lliikkeellyy dduuee t10o tthheeiirr wwoorrkk iinn BBuuiillddiinnggss 33 aanndd 44NN wwiitthh fflluuoorroocchheemmiiccaall aallccoohhoollss,,aammiiiieess aanndd aaccrryyllaatteess. FFoorr eexxaammppllee,,cchheemmiiccaall ooppeerraattoorrss hhaadd aa ggeeoommeettrriicc mmeeaann lleevveellooff00.113311 ppppmm ffoorr MM557700 ccoommppaarreedd t10o00..003333 ppppmm ffoorr cceellll ooppeerraattoorrss,,00..004422ffoorr mmiillll ooppeerraattoorrss aanncc 00..007799 ppppmm ffoorr wwaassttee ooppeerraattoorrss.. PPOOAAA lleevveellss wweerree aabboovvee tthhee ggeeoommeettrriicc mmeeaann ooff 11..00)00 ppppm ffoorr eemmppllooyyeeeess wwiitthh ccuurrrreennttjjoobbss ooffcceellll ooppeerraattoorrss((11..442288 ppppmm)),,cchheemmiiccaall oopeerraattoorrss((11..888877 ppppmm)),,mmaaiinntteennaannccee wwoorrkkeerrss((11..009955 ppppmm)),mmiillll ooppeerraattoorrss((11..226666 ppppmm))ianndd wwaassttee ooppeerraattoorrss((11..554422 ppppmm)).. EEmmppllooyyeeeess wwiitthh tthheejjoobb ccaatteeggoorriieess ooffeennggiinneeeern//llaabb aanndd sseeccrreettaarryy MSMuaabddjeeecAAtvvataoiillPaarbbollteeecbbtyyiv33eMMOfrfodorrerIInnIssnppeePccattiiioomnneaavrnn.dd3CCMoo,ppNyyoii.nngg2-aa0ss4CC-oonn6ff3ii0ddee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00000055 33MMAA1100005500443388 EPLO33OMM PaEPgIe-06030o56 had the lowest serruumm fflluuoorroocchheemmiiccaall lleevveellss.. PPFFHSS,,aanndd ttoo aa lleesssseerr eexxtteenntt PPFOOSPS.a,geww6eerroeef85 had the lowest se positively aassssoocciiaatteedd wwiitthh yyeeaarrss wwoorrkkeedd iinn tthhee cchheemmiiccaall ppllaanntt.. TThhee rreemmaaiinniinngg positively fuorochemical analyteess wweerree nnoott roouuttiinneellyy aassssoocciiaatteedd wwiitthh yyeeaarrss wwoorrkkeedd iinntthhee cchheemmiiccaall fluorochemical analyt plant by job ccaatteeggoorriieess.. WWee ddiidd nnoott oobbsseerrvvee aann aassssoocciiaattiioonn bbeettwweeeenn hhaanndd ttoo--mmoouutthh uussaaggee: plant by job or hand clleeaannlliinneessss((ffrreeqquueennccyy ooff wwaasshhiinngg hhaannddss))aanndd sseerruumm fflluuoorroocchheemmiccaall lleevveellss.. or hand c Liikkee tthheeiirr mmaallee ccoouunntteerrppaarrttss,,ffeemmaallee cchheemmiiccaall ooppeerraattoorrss aeppppeeaarreedd ttoo hhaavvee L increased PPFFHHSS lleevveellss wwiitthh yyeeaarrss wwoorrkkeedd.. HHoowweevveerr,,uunnlliikkee tthheeiirr mmaallee ccaouunntteerrppaarrttss., increased there was no aappppaarreenntt mmooddeesstt lliinneeaarr aassssoocciiaattiioonn bbeettwweeeenn PPFFOOSS aanndd yyeeaarrsi wwoorrkkeedd aammoonngg there was no female chemmiiccaall ooppeerraattoorrss.. WWhheetthheerr tthhiissiis dduueettodoidfiffeferreenntt wwoorrkk pprraaccttiicceess,,eexxppoossuurree female che patternsoorr pphhaarrmmaaccookkiinneettiiccss oonnccee aabbssoorrbbeedd,,rreemmaaiinnss ttoo bbee ddeetteerrmmiinneedd.. TThhee ssaammppllee ssiizzee patterns {elf (n= 100 ffeemmaallee cchheemmiiccaall ooppeerraattoorrss iinn rraannddoomm ssaammppllee)),,iissaann iimmppoorrttaanntt,,lliimmiittiinngg itself(n = 1 ffaaccttoorr iinn tthhee iinntteerrpprreettaattiioonn ooff tthheessee ddaattaa.. The ddaattaa aallssoo iinnddiiccaattee ssiiggnniiffiiccaannttllyy lloowweerrsseerruumm fflluuoorroocchheemmiiccaall ieevveellss aammoonngg The employees who hhaavvee oonnllyy wwoorrkkeedd iinn tthhee flilmm ppllaanntt(ii...e..,ddeeffiinneedd aass tthhoosst:.eemmppllooyyeeeess iinn employees who the random sampllee wwhhoo hhaavvee wwoorrkkeedd oonnllyy iinn tthhee ffiillmm ppllaanntt wwiitthh nnoo pprriioorr wwoorrkk oonn tthhee DD--11 the random samp `maker locatedd iinn tthhee ffiillmm ppllaanntt oorr pprreevviioouuss wwoorrkk hhiissttoorryy iinn cchheemmiiccaall..TThhee DD--11 mmaakkeerr uusseess maker locate FX-1801, a mmeetthhyyll FFOOSSEE aammiiddee)).. TThheerree wweerree ssiiggnniiffiiccaannttllyy lloowweerr sseerruurmn fflluuoorroocchheemmiiccaall FX-1801, a levels amoonngg tthheessee eemmppllooyyeeeess wwhhoo hhaavvee oonllyy wwoorrkkeeddiin tthhee ffiillmm ppllaanntt wwhheenn ccoommppaarreedd ttoo levels am those who aarree ccuurrrreenntt cchheemmiiccaall ppllaanntt eemmppllooyyeeeess.. CCoommppaarriinngg tthhee ggeeoommeettrriicc mmeeaannss ffoorr those who cach fflluuoorroocchheemmiiccaallffrroomm tthhee rraannddoomm ssaammppllee ooffcchheemmiiccaall ooppeerraattoorrss aanndd tthhoossee eemmppllooyyeeeess each who only hhaavvee wwoorrkkeedd iinn tthhee ffiillmm ppllaanntt,,wwee oobbsseerrvveedd tthhee ffoolllloowwiinngg rraattiiooss((iinn ppppmm)):: who only PFFOOSS 0(.1.448811//00..111100));;PPFEHHSS((00.442288//00.001155));;PPOOAAAA((11..8888771/00..005522));;PPFFOOSSAAAA((00..001111//00..000022)):; 'M5S7T00((00..222299//00..002222));;aanndd MMS55566((00..004444//00..000033))..EExxcceeppttffoorr PPFFOOSSAAAA,,tthheessee rraattiiooss ssuuggggeesstt M a 10-fold oorr ggrreeaatteerr ddiiffffeerreennccee bbeettwweeeenn cchheemmiiccaall ooppeerraattoorrss aanndd ffiillmm ppllaanntt eemmppllooyyeeeess wwhhoo a 10-fold Sih iorochOrdee Palmer. OW 530.8308 +" Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00000066 3aMMAA1T00005S0044309 lt3M EPI-0006 Page 7 of85 work several hundred yards away from Building 3. This only film plant employee group emer en i AC pony 4s rn had a geometric mean value for PFOS that is approximately 3-4 times higher than the J pooled geometric mean(0.029 ppm)from 64 samples obtained from 18 U.S. blood eso pir ie PCdSr i banks. Thus,we suspect that occupational exposure to PFOS does occur within the film plant although at much lower levels than among employees working at tht: chemical plant. Additionally employees who worked on the D-1 maker have serum PFOS levels approximately 3 times higher than those employees who have never worked on the D-1 UR maker nor have worked in the chemical plant (i.e., the only film plant employees). We did not observe an association between hand-to-mouth usage .)r hand cleanliness(frequency of washing hands)and serum fluorochemical leve s. It is possible eon cued ns rns blsion chs an association might have been masked because industrial hygiene had i istituted an aggressive educational campaign several months prior to the collection of blood samples in this study; thus current practices may not be indicative of past practices. Because the tt 708 mite 0 ee, hm tn half-life ofPFOS is estimated to be 1000days or more,such an association may not be mb ty i discoverable with this study design. A limitation to this study design which must be considered in the interpretation of the data was our inability to more accurately quantify an employee's work history eee. Tetra ir ts onps es 0 experience. Decatur work history records provide department numbers andjob titles but es so pote i io oe me hc. AES they do not provide information regarding where someone worked(e.g., what building(s) ere rl i Des wo iy en oorr wwiitthh wwhhaatt ssppeecciiffiicc fflluuoorroocchheemmiiccaallss))..SSeellff--rreeppoorrtteedd wwoorrkk hhiissttoorryyiinnffoorrnmaattiioonn oobbttaaiinneedd by questionnaire was highly correlated with Decatur work history record information; nneevveerrtthheelleessss,,tthhee ssppeecciiffiicciittyyooffwwhheerree ssoommeeoonnee wwoorrkkeedd aanndd wwiitthh wwhhaatt cchheemmiiccaallss wwaass nnoott I -- known. Because many operations are in batch mode,the likelihood of determining ety id me rei sess gr specificity ofhistorical workload fluorochemical exposure among chemical operators Tes Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00007 S-- 3MA10050440 ErLo03a0Ms PagEePIS-o0r00856 Page 8 of85 wwaass nnoott ppoossssiibbllee. Th present study's sseerra fllouroorocchheemmiiccaal leevveelss,,oobbsseerrvveedd bbyyjjoobb ccatteeggoorriicess aanndd The present study's building location, strongly support tthhe rreeccoommmmeennddaattiioonnss bboormnee ffrroomm rrecceenrtllyy ccoonndduucctteedd building locations, strongly suppor ndusral hygiene assessments, Thessee rreeccoommmmeennddaattiioonnss iinncclluuddee ssppeecciiffiicc eennggiinneeeerriinngg industrial hygiene controls to reduce assessments. The inhalation exposure, aapppprroopprriiaattee ppeerrssoonnaall pprrootteeccttiivvee eeqquuiippmmeenntt t(o0 controls prevent to reduce inhalati overexposure and on exposure, aproprse ppeerrssoonnaall hhyyggiieennee pprraaccttiicceess aammoonngg eemmppllooyyeeeess t(o0 prevent overexposure and appropriate rreemmoovvee sskkiinn ccoonncceennttrraattiioonnss. Finally, PFOS andd PPOOAAAA sseerruumm lleevveellss mmeeaassuurreedd iinn tthhiiss ssttuuddyy aarree:ssiimmiillaarr ttoo tthhoossee hot Finally,PFOS an have been previously reporteedd vviiaa ppaasstt bbiieennnniiaall mmeeddiiccaall ssuurrvveeiillllaannccee ~cctiiivittiiess.. that have been previously report Results of previous epidemiologic studdiieess hhaavvee nnoott aassssoocciiaatteedd tthhee sseerruumm PPFFOOSS oorr PPOOAAAR Results of previous epidemiologic stu Levels observeidn this study population wwiitthh hheeppaattiicc,, lliippiidd oorr hhoorrmmoonnee aabbnnoorrmmaalliittiieess.. levels observed in this study population RioProechseOrder Palmer 34h iCaroaasos 1 OTE Aade Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2288122..00000088 3aMMAA1T0000S500444411 E030wMm FarEPet9-o0l0$056 Pap 9of85 IINNTTRROODDUUCCTTIIOONN Inthe past, eemmppllooyyeeeess aat tthhee 33MM DDeeccaattuurr cchheemmiiccaall ppllaanntt hhaavvee wvoilluunnttaarriillyy In the past, panicipated in a Nuoroocchheermiiccaall mmeeddiiccaall ssuurrvveeiillllaannccee pprrooggrraamm..TThhee ssuurrvesillllannccee pprrooggrraamm participated in a fluor analyzed for otal seerruumm oorrggaanniicc fflluuoorriinnee lleevveellss uunnttiill tthhee mmiidd--11999900''ss wwhh:inn ssecrruumm analyzed for total s perlucrooccttaannee ssuullffoonnaattee((PPFFOOSS))aanndd ppeerrfflluuoorrooooccttaannooiic aacciidd((PPOOAAA))cceetteerrmmiinnaattioonn., perfluoroo quantifiable by higghh ppeerrffoorrmmaannccee lliiqquuiidd cchhrroommaattooggrraapphhyy mmaassss ssppeecctrtorror eetxryy,, bbeeccaammee quantifiable by hi incorporated in the bbiieennnniiaall mmeeddiiccaall ssuurrvveeiillllaannccee eexxaammiinnaattiioonnss.. AAnnaallyy::iiss ooff tthhee incorporated in the surveillance dataa hhaass nnoott sshhoowwnn ssiiggnniiffiiccaanntt aassssoocciiaattiioonnssbbeettwweeeenn tthhee eenmppllooyyeeeess"'cclliinniiccaall surveillance dat chemistry and hemaattoollooggyy tteessttss anndd eeiitthheerr ttoottaall sseerruumm oorrggaanniicc fflluuoorriinnee 'elevveellss[(RRooaacchh.. chemistry and hem 1952; Schuman, 1998822]1 oorrssecrruumm PPFFOOSS lleevveellss[OOllsseenn eett aall.., 11999999]1.. HHoowweevveerr,,tthhee 1982; Schuman, 1 voluntary nature of tthhee mmeeddiiccaall ssuurrvveeiillllaannccee pprrooggrraamm mmaayy nnoott lleenndd istesleflf1t0o a4n1 voluntary nature of approprste charaacctteerriizzaattiioonn oofftthhee ddiissttrriibbuuttiioonn ooff flluuoorroocchheemmiiccaall sseerruusn lleevveellss assiitt iss nnoott appropriate char based on random ssaammpplliinngg mmeetthhooddss.. TThheerreeffoorree,,tthhee ppuurrppoossee ooff tthhiiss ssttu.llyy wwaass ttoo ccoolllleecctt based on random data from th neecceessssaarryy ddiissttrriibbuuttiioonn bbyy rraannddoommllyy ssaammpplliinngg eemmppllooyyeeeess iinn tthhee DDeeccaattuurr data from the n chemical pllaanntt iinnoorrddeerr t0o ddeetteerrmmiinnee tthhee ddiissttrriibbuuttiioonn ooffeemmppllooyyeeee sseerruunn)i flluuoorroocchheemmiiccaall chemical p eves according ttoo ddeemmooggrraapphhiiccss,,ccuurrrreenntt aanndd lloonnggeesstt hheelldd jjoobbss,, yyeeaarrss Nsoorrkkeedd aanndd levels according building locations. In addition,aa rraannddoomm ssaammppllee oofftthhee nneeiigghhbboorriinngg 33MM DDeeccaattuurr ffiillmm addition, building locations. In plant emplooyyeeee ppooppuullaattiioonn,,llooccaatteedd aat tthhee ssaammee ssittee, wwaass tteesstteedd tfoo ddeetteerrmmiinnee plant empl Muorochemical sseerruumm lleevveellss iinn oorrddeerr ttoo cchhaarraacctteerriizzee tthhee ddiiffffeerreenncceess bbeetrwweeeenn tthhee ttwwoo. fluorochemical ppllaanntt ppooppuullaattiioonnss.. The film plant eemmppllooyyeeeess hhaavvee ssecrrvveedd aass aa ccoommppaarriissoonn ppooppuullaa iioonn iinn aa pprriioorr The film plant health sttuuddyy((MMaannddeell aanndd JJoohhnnssoonn., 11999955))dduuee ttoo tthheeiirr((aassssuummeedd))nnoonnooc ccuuppaattiioonnaall health s exposure to ffluuoorroocehheemmiiceaallss.. HHoowweevveerr,,tthheeiir aaccttuuaall sseerruumm fflluuoorrooechheerrrriiccaall lleevveellss hhaadd nnoott exposure to been discernneedd..EEppiiddeemmiioollooggiicc ssttuuddiieess aatt tthhee DDeeccaattuurr ppllaanntt ccaann bbee mmortea ffuullllyy aapppprreecciiaatteedd been discer Sohalto techs Ore aime +. 3. C204a30s Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00000099 3SMwAA1T0000s500444422 EPLO30TMMG PageF,1P010-0708056 iifftthhee ddiissttrriibbuuttiioonnssooffeemmppllooyyeeee sseerruumm fflluuoorroocchheermmiiccaall lleevveellss aatt bbootthh tthhee cchheemmiiccPaaallgeaann1dd0of85 ffiilmm ppllaannttss aarree bbeetttteerr uunnddeerrssttoooodd.. MMEETTHHOODDSS DDeessccrriippttiioonn ooff DDeeccaattuurr FFaacciilliittyy T"Thhee 33MM DDeeccaattuurr ssiittee iiss llooccaatteedd iinn DDeeccaattuurr,, AAllaabbaammaa wwhhiicchh sstaarrtt-zdd pprrooddusccttiioonn iinn tthhee aearrllyy 11996600''ss.. TThhee ssiittee ccoonnssiissttss ooff ttwwoo ppllaannttss,,SSppeecciiaallttyy FFiillmm ""ffiillmm pplaannt"" aanndd `SSppeecciiaallttyy MMaatteerriiaallss""cchheemmiiccaall ppllaanntt"".. BBootthh ppllaannttss aarree iinn tthhee SSppeecciiaallttyy MMaatteerriiaallss MMaannuuffaaccttuurriinngg DDiivviissiioonn((SSVMIMMDD)).. TThhee cchheemmiiccaall ppllaanntt iiss llooccaatteedd sseevveerr iill hhuunnddrreedd yyaarrddss ddiirreeccttllyy eeaasstt ooff tthhee FFiillmm PPllaanntt.. TThhee mmaaiinn bbuuiillddiinnggss llooccaatteedd oonn tthhee ssittee ~rree BBuuiillddiinnggss 11,.22,, 33,,55,.1144,,1155,,1177,,1199.,3311,,3366,,3388..4400,,442,24488.,,4499,,5511,,5577,,5599 aanndd 6611 ((sseece AAppppeennddiixxAA)).. BBuuiillddiinnggss 1144,, 1155 aanndd 1199aarree ccoonnssiiddeerreedd ffiillmm ppllaanntt bbuuiillddiinnggss.. BBuuiillddiinnggss 11,,22,,33.,3311.,3388.,4400,, 4422,,4488,,4499,,5511 aanndd6611 aarree ccoonnssiiddeerreedd cchheemmiiccaall ppllaanntt bbuuiillddiinnggss.. BBuuiillddiinn;; 5 iiss tthhee bbooiilleerr hhoouussee tthhaatt ccoonnttrroollss ssiittee uuttiilliittiieess ssuucchh aass cchhiilllleedd wwaatteerr,, ppllaanntt sstteeaamm,,ppllaann nniittrrooggeenn aanndd bbrreeaatthhiinngg aaiirr.. BBuuiillddiinngg 55 ii s llooccaatteedd ssoouutthhwweesstt ooff tthhee cchheemmiiccaall ppllaanntt.. BBuuiillddiinngg 1177 sseerrvveess aass tthhee mmaaiinntteennaannccee aanndd ssttoocckkrroooomm bbuuiillddiinngg llooccaatteedd jjuusstt wweesstt ooff BBuuiillddiitt g5 sseerrvviicciinngg `mmaaiinnllyy tthhee cchheemmiiccaall ppllaanntt.. BBuuiillddiinnggss 3366 aanndd 5$77 aarree ssiittee wwaasstteewwaatteerr ttrree tttmmeenntt bbuuiillddiinnggss llooccaatteedd eeaasstt oofftthhee cchheemmiiccaall ppllaanntt.. "TThhee mmaajjoorr pprroodduuccttiioonn bbuuiillddiinnggss iinn DDeeccaattuurr ffiillmm ppllaanntt aarree BBuuiilldd- nnggss 1144,, 1155 aanndd 1199.. PPoollyyeesstteerr aanndd nnoonn--ppoollyeesstteerr ffiillmmss aarree pprroodduucceedd iinn BBuuiillddiinngg 1144.. MMaaiinntttennaannccee,,lloocckkeerr rroooommss,,aannddddiinniinngg ffaacciliiltiietsaiarerseaalll llooccaatteedd iinn aarreeaass ooff BBuuiillddiinngg 1144.. RReesiinn uusseedd iinn ffiillmm pprroodduuccttiioonn iiss mmaannuuffaaccttuurreedd iinn BBuuiillddiinnggss 1155 aanndd 1199.. TThhee oonnllyy pprroocceessss,n tthhee ffiillmm ppllaanntt uussiinngg fflluuoorroocchheemmiiccaallss iiss rruunn oonn tthhee DD--11 ffiillmm lliinnee((ccaalllleedd tthhee DD--11 mmaakkee )).. TThhee pprroocceessss Sohalto techs Ore aime +. 3. C204a30s Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00001100 3sMuAa1t0o0os5a0a4s4s3 EPL003s0Mm6 uses FX-1801 in the production of film used or a limitedd nnuummbbeerr ooff products. PPaCauggreeErP11eI1n0-to10lf08y80,556 products. Currently, uses FX-1801 in the production of film used for a limite other pprroocceesssseess iinn tthhee ffiillmm ppllaanntt susee fflluuoorroocchheemmiiccaallss iinn pprroodduuccttiioonn.. no other "The three major products produced in thhee cchheemmiiccaall ppllaanntt arree pprroottee-cttiivvee cchheemmiiccaallss,, The three major products produced in t performance cchheemmiiccaallss,,aanndd fflluuoorrooeellaassttoommeerrss.. TThhee tthhrreeee pprroodduucctt ggrroouuppss aarree rreeffeerrrreedd t1o0 performance as focus factories. Fluorroocchheemmiiccaallss iiddeennttiiffiieedd iinn tthhiiss ssttuuddyy aarree uusseedd iinn aallll ffooccuuss ffaaccttoorryy Fluo as focus factories. groups to some extent. Production for alll fooccuuss ffaaccttoorriieess ttaakkeess ppllaaccee iinn BB.aiiklldiinnggss 22,.33.,44., groups to some extent. Production for al f 38,40, 42,49, 511 aanndd 6611.. TThhee cchheemmiiccaall ppllaanntt''ss mmaaiinn ooffffiiccee aarreeaass,, wwaarreehhoouussee aanndd qquuaalliittyy 38,40,42,49,5 control lbs are llooccaatteedd iinn BBuuiillddiinngg 11.. TThhee cchheemmiiccaallppllaanntt'ssddiinniinngg ffaacciilliittyy aanndd lloocckkeerr control labs are rroooommss aarree llooccaatteedd iinn BBuuiillddiinngg 3311. Raw materiiaallss aanndd iinntteerrmmeeddiiaatteess ffoorr eeaacchh pprroodduucctt ggrroouupp mmaayy fflloow: tthhrroouugghh mmaannyy Raw mater ifferent prroodduuccttiioonn bbuuiillddiinnggss bbeeffoorree tthheeyy aarree ppaacckkaaggeedd ffoorr sshhiippppiinngg.. TThhee ffllooww ooff different p protective cheemmiiccaallss ffoollllooww aa ppaatthh sstaarrtiinngg aat BBuuiillddiinngg 33 ttoo BBuuiillddiinnggss 2200.7-4499 ttoo BBuuiillddiinnggss .protective ch 3.4.38 or 511.. TThhee pprrootteeccttiivvee cchheemmiiccaallss ggrroouupp iiss tthhee pprriimmaarryy pprroodduuccere0or 3,4,38 or perfluorooctane ssuullffoonnyyll fflluuoorriiddee((PPOOSSFF))aanndd ppeerrflluuoorroohheexaannee ssuullffoonnyyll fflluuoorriiddee((PPHHSSFF)) perfluorooctane based chemistry.. OOccttyyll mmeerrccaappttaann oorr hheexxyyll mmeerrccaappttaann iiss rreeaacctteedd wwiitthh cchhlioorrinnee aanndd based chemistry ammonium fflluuoorriiddee ttoo pprroodduuccee ooccttaannee ssuullffoonnyyll fflluuoorriiddee((OOSSFF))oorr hheexxaannee ssuullffoonnyyll ammonium fluoride (HSF) inn BBuuiillddiinngg 33 aanndd iiss rreeffeerrrreedd ttoo aass tthhee '`cceelll ffeeeedd'.. TThhee cceellll ffeeeedd iiss sseenntt ttoo fluoride (HSF)i Buildings 2 andd 4499 wwhheerree ittiiss rreeaacctteedd iinn eelleeccttrroocchheemmiiccaall cceellll ssyysstteemmss ttoo pprroodduuccee PPOOSSTF: Buildings 2 an or PHSF. POSF is tthhee mmaajjoorr ssuullffoonnaattee bbaasseedd fflluuoorroocchheemmiiccaall pprroodduucceedd aott DDeeccaattuurr.. PPHSSFF POSF is or PHSF. 1s produced maaiinnllyy ffoorrffiirre ssuupppprreessssiioonn lliiqquuiiddss.. MMoossttoofftthhee PPOOSSFF pprroodduucceedd iiss ppiippeedd ttoo is produced m Building 3 where aammiiddeess,,allccoohhoollss,,aaccrryyllaatteess aanndd ootthheerrfflluuoorroocchheemmiiccaall ppoollyymmeerrss aarree Building 3 where produced. Thesee fflluuoorroocchheemmiiccaall ppoollyymmeerrssaarree tthheenn uusseeddiinn aalll pprroodduuccttiioonn bbuuiilkdiinnggss ttoo produced. Thes pprroodduuccee iinntteerrmmeeddiiaatteess aanndd ffiinniisshheedd ggooooddss.. Sih iorochOrdee Palmer. OW 530.8308 +" Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00001111 rose 3MA10050444 Epto3annMs "The performance chemicals arc mostly made up of inert liquids aarndd firePPaaggeeEP11I22.0o00f0880556 The performance chemicals are mostly made up of inert liquids fire Suppressiioonn lliiqquuiiddss..TThhee iinneertt lliiqquuiiddss ffoollllooww aa ppaatthhssatratritinnggaatt BBuuiillddiinnggss :2'.oorr 4499ttoo suppress BBuuiillddiinnggss 4400oorr 4422.. IInneerrtt lliiqquuiiddss ccoonnssiisstt ooff mmoossttllyy ppeerrfflluuoorroonnaatteedd aallkkaannee~s.aanndd ddoo nnoott ccoonnttaaiinn ssuullffoonnaattee oorr ccaarrbbooxyylliicc aacciidd ccoommppoouunnddss.. FFiirree ssuupppprreessssiioonn lliiqquuiidd::. aarree pprriimmaarriillyy based oonn ssuullffoonnaattee cchheemmiissttrriieess ssttaarrttiinngg wwiitthh PPOOSSEFaanndd PPHHSSF.. FFiirree ssuupppprreessssiioonn pprroodduuccttss based aarree mmaaddee iinn BBuuiillddiinngg 33 aanndd ppaacckkaaggeedd iinn BBuuiillddiingn4g4,. FFlluuoorroocchheemmiiccaallss aarrce uusseedd iinn tthhee pprroodduuccttiioonn oofffflluuoorroocellaassttoommeerr pprroodduuccttss.. TThhee ffiirrsstt part of the fflluuoorrooeellaassttoommeerrss iis ccaalllleedd llaatteexx,, wwhhiicchh iiss pprroodduucceedd iinn BBuuiillddiinng;ss 44,,3388 aanndd 5511. part of the "The latex iiss tthheenn ccooaagguullaatteedd,,wwaasshheedd aanndd mmiilllleedd iinn BBuuiillddiinnggss44 aanndd 6611.. ?P'OOSSFF bbaasseedd The latex comppoouunnddss aarree tthhee pprriimmaarryy fflluuoorroocchheemmiiccaallss ooffiinntterreesstt uusseedd iinn tthhee mmaajjoorrttyy ooff com fflluuoorrooeellaassttoommeerr pprroodduuccttss,. PPOOAAAA iiss aallssoo uusseeddiin aa lliimmiitteedd nnuummbbeerrooffffluuoorrooeellaassttoommeerr pprroodduucctt rruunnss.. PPOOAAAA iiss uusseedd iinntthhee pprroodduuccttiioonn ooffllaatteexx tthhaatt iiss eevveennttuuaallllyy ccooaagguullaatteedd,, wwaasshheedd.,aanndd mmiilllleedd iinn BBuuiillddiinngsg44saanndd 6611.. TThhiissPPOOAAAA ccoonnttaaiinniinngg pprroodduucctt iiss urunn iinnffrreeqquueennttllyy,,oonnllyy sseevveerraall ttiimmeess ppeerr yyeeaarr.. PPOOAAAA iiss aallssoo aa bbyy--pprroodduucctt wwiic.hhiinn tthhee eleccttrroollyyttiicccceellllss aanndd iiss ccaarrrriieedd tthhrroouugghh uuppttoo pprroodduucctt.. It iiss bbeelliieevveedd ttoo bbe.-aa rreessuulltt oo f ele iinnccrreeaasseedd ooxxiiddaattiioonn wwiitthhiinn tthhee cceellllss.. PPOOAAAA wwaass pprroodduucceedd iinn BBuuiillddiinngg 22 aanndd ssuubbsseeqquueennttllyy wwoorrkkeedd uupp iinn BBuuiillddiinngg 33 mmoorree tthhaann 2200 yyeeaarrss aaggoo aanndd hhaadd nna:)tt bbeeeenn pprroodduucceedd in DDeeccaattuurrssiinnccee tthhee ttiimmee oofftthhiiss ssttuuddyy.. PPOOAAAA pprroodduuccttiioonn iisseexxppeecctteedd ttoo rreessuummee iinn in BBuuiillddiinnggss 22 aanndd 4499iinn tthhee nneeaarr ffuuttuurree.. Seeti Fecte Cre pamhvG2ae iosos Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00001122 3MMAAT100005S04I4S5 ssa Sample Size Determination i3M EPI-0006 Page 13 of 85 Three critical factors were considered to decide the sample size or this study. First, it was important that a sample be randomly chosen from the emp ogee populations of both the chemical and film plants. Second, the sample size was drivt n by the need to provide confidence that the exposure in the film plant is small relative t)that of the chemical plant. Third, the sample size had to adequately characterize the exposure levels within the chemical plant workplace. In addition, all employees in the chemical and film plant had to be offered the opportunity to know their fluorochemical le, els via blood testing, although they may not be part of the random sample. The rand.)m sample size in this study of more than 200 subjects was based on: 1) the lower 95% c mfidence bound of the hypothesized mean difference between the serum fluorochemica levels of the chemical plant; and 2)to allow for adequate characterization of serum f1UOTOchemlcal differences byjob and building within the chemical plant(see study pr()tocol for details). There was an added degree of uncertainty in estimating sample size be,-ause approximately 10 percent of the film plant employees may have had pr or work experience in the chemical plant. Also, an unknown number of film pl int workers had worked on the D-1 maker where a PFOS-based fluorochemical(FX 18H.a methyl FOSE sect amide)has been used. etme sey neg et 1b The random sample waschosen by the following methods: a)a I full-time current chemical and film plant employees were identified via a current plant foster that listed departments and supervisors; b)using a random number generator algorithm. a sample of employees was chosen which was proportionate to the number of emp oyees who worked in the various chemical departments,auto and chemical markets group Decatur EHS&R, Dyneon,and the film plant. We included in the random sample all identified Decatur Te Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 usizous 3MA10050446 2881122..00013 .3M EPI-CAM page tects Page 14 of85 site employees who were assigned to the wastewater treatment plant(Bt,ildings 36 and 57). Altogether, there were 232 employees randomly chosen to participate in the study ((TTaabbllee 11)).. AA ttoottaall ooff 118866((88007%,))ppaarrttiicciippaatteedd aanndd 4466((2200%%))rreeffuusseedd.. TThhee ffiilmm ppllaanntt random sample had the lowest participation rate(71%). In addition to I -1e 186 random sample participants,there were 77 employees from the chemical(n =61)and film(n = 16) plants who requested their serum be tested for fluorochemical level :. Hereafter. these individuals will he called the "volunteers." Emplovee Study Participation Study participation required the following: 1) a signed consent f )rm by the employee,2)a written response to a brief questionnaire(Appendix B)t iat inquired about current and past work history along with the frequency of hand washing and use of gum, chew (tobacco)and cigarette habits of the employee while at work, and 3) a venipuneture with the collection oftwo vials of blood(approximately 2)cc)for the determination of the seven fluorochemicals. The study protocol was approved by the 3M IInnssttiittuuttiioonnaall RReevviieeww BBooaarrdd ((IIRRBB)).. Each randomly chosen employee (film and chemical)received; letter of invitation to participate that wasjointly signed by the plant manager(N r. Jim King)and tthhee 33MM MMeeddiiccaall DDeeppaarrttmmeenntt ddiirreeccttoorr((DDrr.. LLaarrrryy ZZoobbeell)).. TThheerree wwaass ppllaa iitt--wwiiddee communication which described the purpose of this study and encoural.ed employee participation. All study participants, who were either randomly chosen or who volunteered, were informed of their own individual results by a letter s.:nt to them from the 3M Medical Department in July, 1999. Aggregate results of the sti dy were also communicated at that time to the employees. Te Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 raza 3MA10050447 2881122..00014 03M rom EP{-0006 revs Page 15 of85 Fuorochemica Ansyses Fluorochemical Analyses All lod ws collie i the month of October nd Never, 1998 at he All blood was collected in the months of October and Novemb -r, 1998 at the Decatur plane by ModAceess (in oceupaional elt clini oct in Decatur, AAllaabbaammaa) Decatur plant by MedAccess(an occupational health clinic located in Decatur. und er he directiono f C a th y Simpson, RN wh ceri fued he blood blood 1 t o tain hethe scrum serum under the direction of Cathy Simpson, RN who centrifuged the -) obt nd hen sipped the samples 0 he Medical Depriment 5. Pal MN). Spit and then shipped the samples to the 3M Medical Department(St. Paul MN). Split ample s wre ca talog ued by Diane M ads en and ean Burs and then then sts-nt to cther either samples were catalogued by Diane Madsen and Jean Burris and to Northwes Bioanalytical (Dr. David Vollmer for determination o per oroocane orooctane Northwest Bioanalytical(Dr. David Vollmer)for determination of per lu ufone (PFOS), pefluoocane slfnste amide (PFOSA), pfu chen slforste ate sulfonate(PFOS),perfluorooctane sulfonate amide(PFOSA), pernuo ohexane sulfon (PHS). peruoroctnoi cid (FOAA)snd ctl perlsoronctan uorooctane ulonamido ulfonamido A)and N-ethyl perfl (PHIS),perfluorooctanoic acid(POA ces (ROSA) orto 3M Enirnmena Laboratory (Dr. Kats Hansen) for acetate(PFOSAA)or to 3M Environmental Laboratory(Dr. Kris Hamen)for deeminaion of N-methyl perflaoratanesafonamdo sete (M70) snd determination of N-methyl perfluorooctanesulfonamido acetate(M5-/',)) and ppeerrfflluuoorrooooccttaanneessuullffoonnaammiiddoo aacceettaattee((MM555566)).. Ibo oratories, sr pes were ced usin a on Sng exrcion In both laboratories,sera samples were extracted using an ion-I airing extraction proces. The xtats were quantal anlycd ox PFOS, PFHS. POAA. procedure. The extracts were quantitatively analyzed for P1rOS,PFH~,POAA. PFOSAA, PROSA,MST0 and M336 ushigih prnessgure quid PFOSAA,PFOSA,M570and M556 using high-pressure liquid cchhrroommaattooggrraapphhyy//eelleeccttrroosspprraayy ttaannddeemm mmaassss ssppeeccttrroommeettrryy((HHPPLLCC//EESSMM i3MMSS))aanndd alate versus an extsted curve, There were minor differences bracen the evaluated versus an extracted curve. "There were minor differences bei weer the altel methods wed st Northwest Bioanalytical snd 3M Environ mal Laorstoy, analytical methods used at Northwest Bioanalytical and 3M Environm -ntal Laboratory. Most notably, Northwest Bioanalytical valued analyte eels versa curve ered Most notably,Northwest Bioanalytical evaluated analyte levels versus a curve extracted from human sea. Endogenous levels ofcertain uorochenicwaelres Jeermined in the from human sera. Endogenous levels ofcertain fluorochemicals were Jetermined in the ndard mat nd addition) furoochmical was spiked nto the mat ix. The total standard matrix and additional fluroochemical was spiked into the matix. The total amountofcach peific fuorochemica endogenous + spiked) was sd 0 consrc sn amount ofeach specific fluorochemical(endogenous+spiked)was u&A to construct an exacted sundard curv. Forth analysis conducted he 3M Enviro wal extracted standard curve. For the analysis conducted at the 3M Enviroimental Sih io roche Orde Palmer. OW 530.8308 +" Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00015 3aMAAt1o0o0s5o0d4d4s8 Epio3aoMe Laboratory, th difficulties presented by the endogenous levels of fluo ochemicPPaaalggeePinP1lo6oI-o0f085056 Laboratory, the difficulties presented by the endogenous levels of fluo ochemical in Ssaammpplleess ooff "bbllaannkk"" tteesstt mmaattrriixx wweerree cciirrccuummvveenntteedd bbyy uutiilliizziinngg rraabbbbiitts s1 rfaa aassaa ssuurrrrooggaattee mmaattirni,x. PPrreevviioouuss rreessceaarrcchh hhaadd sshhoowwnn tthhaat rraabbbbiit sseerraa ccoonnttaaiinnss tthhe l[oowwe( sstt lleevveell ooff eennddooggeennoouuss fflluuoorroocchheemmiiccaallss wwhheenn ccoommppaarreedd too sseerraa ffrroomm bboovviinnee,, rraatt,, -mnoonnkkeeyy aanndd hhuummaann.. AAss aa qquuaalliittyyccoonnttrrooll cchheecckk,,tthhee 33MM EEnnvviirroonnmmeennttaall LLaabboorraattoorryy::crreeeenneedd PPFOOSS lleevveellss iinn aapppprrooxxiimmaatteellyy 1100%% ooff tthhee sseerraa aannaallyyzzeedd aait NNoorrtthhwweesstt BBiiooaannaa yyttiiccaal.l. WWhhiillee mmoosstt oofftthhee rreessulutss aaggrreeeedd too wwiitthhiinn 2255%%,,1144 ooff tthhee 4400ssaammpplleess cchheecckkeedd sshhoowweedd lloowweerr((>> 2255%%))vvaalluueess wwhheenn aannaallyyzzeedd aatt 33MM.. IIttiss eexxppeecctteedd tthhaat tthhessee ddiissccrreeppaann-,iicess aarree dduuee ttoo ddiiffffeerreenncceess iinn ccuurrvvee ssllooppee aanndd iinntteerrcceeppttss aarnissiinngg ffrroomm tthhee aannaallyyttiiccaall ddiillffeerreenncceess ddeessccrriibbeedd aabboovvee.. GGiivveenn tthhaatt NNoorrtthhwweesstt BBiiooaannaallyyttiiccaall ssaattissffoaccttoorrillyy ccoommpplleetteedd aa nneetthhoodd vvaalliiddaattiioonn ffoorr PPFFOOSSususiinngg hhuummaann sseerraa aanndd ggiivveenn tthhaatt mmoosstt vvaalluess wweerree iinn cclloosseesargerceeemnentt wwiitthh tthhoossee oobbitaaiinneedd bbyy tthhee 33MM EEnnvviirroonnmmeennttaall LLaabboorraattoorryy uussiinngaga rraabbbbiittsseers.o ccuurrvvee,,ddaattaa ffrroomm bbootthh llaabboorraattoorriieess wweerree ccoonnssiiddeerreedd aaccccuurraattee ttoo wwiitthhiinn tthhee ppaarraammeetteerrss ddo ffiinneedd bbyy tthheeiirr mmeetthhooddss.. DDeettaaiillss ooffbbootthh llaabboorraattoorriieess'mmeetthhooddss aanndd ffiinnaall rreeppoorrttss aarreerreeppoorrtteeddeellsseewwhheerree. [(VVoollllmmeerr,, 11999999:; HHaannsseenn,, 119999991]. DDaattaa AAnnaallyyssiiss EEaacchh eemmppllooyyeeee''ss qquueessttiioonnnnaaiirree ddaattaa aanndd ccoommppuutteerriizzeedd wwoorrkk hhii sttoorryy rreeccoorrddss wweerree rreevviieewweedd ttoo ddeetteerrmmiinnee wwhheetthheerr tthhee eemmppllooyyeeee wwaass::aa))aa ccuurrrreenntt cchheemmiicc ilt eemmppllooyyeeee ((rreeggaarrddlleessssooffaannyy wwoorrkk eexxppeerriieennccee iinn tthhee ffiillmm ppllaanntt)):; bb))aa ffiillmm ppllaanntt(mmppllooyyeeee wwiitthh nnoo hhiissttoorryy iinn cchheemmiiccaall;;orrc))a ffiillmm ppllaanntt eemmppllooyyeeee wwiitthh pprriioorr hhiissttoorryy iinncxe1memiiccaall.. EEmmppllooyyeeeess wwhhoo wweerree ccoonnssiiddeerreedd DDeeccaattuurr'ssiittee'eemmppllooyyeeeess((ee..gg..,ssaaffeettyy iinndduussttrriiaall Sohalto techs Ore aime +. 3. C204a30s Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00001166 3sMuAa1t0o0os5o0s4s4e9 Erio3TMnM hygiene) and who stated they currently worked in oneormore chernici | buildiPPnaagggseeEwP11e177r-0o0e7f0880556 hygiene)and who stated they currently worked in one or more chemic,I buildings were ccoonnssiiddeerreedd ttobo bee cchheemmiiccaall eemmppllooyyeeeess iinn tthheeddaattaa aannaallyysseess.. EEmmppllooyyeeeess wweerree aasskkeedd ttoo pprroovviiddee tthheeiirrccuurrrreenntt aanndd lloonnggeesstt--hheellc( jjoobb.. AA rreevviieeww ooff tthheesseejjobb tiittleess bbyy aann iinndduussttrriiaall hhyyggiieenniisstt((PPWWLL)),,eeppiiddeemmiioollooggiissttss((GGWW ),,JJMMBB))aanndd ooccccuuppaattiioonnaall hheeaalltthh nnuurrssee((CCAASS))ccaatteeggoorriizzeedd tthhee eennttrriieess iinnttoo eeiigghhttjoobbc lalsassiiffiiccaattiioonnss ffoorr tthhee cchheemmiiccaall ppllaanntt:: cceellll ooppeerraattoorrss,,cchheemmiiccaall ooppeerraattoorrss.,eennggiinneeeerrss//llaabboorrsatoorryy,, mmaaiinntteennaannccee, mmiillll ooppeerraattoorrss.,sseeccrreettaarriieess.,ssuuppeerrvviissoorrss//mmaannaaggeemmeenntt aanndd wwaassttee ooppeerraattoorrss.. FFiillmm ppllaanntt ccuurrrreennttjjoobbss((aanndd lloonnggeesstt hheelldd jjoobbss))wweerree ccaatteeggoorriizzeedd iinnttoo ffoouurrjjoobb ccllaasss iffiiccaattiioonnss:: eennggiinneeeerrss//llaabboorraattoorryy.,ffiillmm pprroocceessssoorrss,, mmaaiinntteennaannccee aanndd aaddmmiinniissttrraattiivvee.. TThheessee ccllaassssiiffiiccaattiioonnss wweerree ddoonnee pprriioorr t0o aannyy ddaattaa aannaallyysseess.. TThhee iinnddiivviidduaula'ls's i;ssuuaalljjoobb aassssiiggnnmmeenntt wwhheenn hhee/fsshhee wwoorrkkeedd oovveerrttiimmee wwaass nnoot aannaallyyzzeedd aass mmoosstt ppee -ssoonnss rreeppoorrtteedd tthhiiss wwaass tthhee ssaammee aassththeeiirr ccuurrrreenntt((oorr lloonnggeesstt hheelldd))jjoobb.. EEmmppllooyyeeeess wweerree 1sskkeedd oonn tthhee ssttuuddyy qquueessttiioonnnnaaiirree ttoo iinnddiiccaattee tthhee nnuummbbeerrooffyyeeaarrss tthheeyy hhaavvee wwoorrkkeedd iinn Cchheerr iiiccaall.. TThhiiss iinnffoorrmmaattiioonn ccoorrrreellaatteedd wwiitthhaa rreevviieeww ooffrreeccoorrddss ffrroomm tthhee eeppiiddeemmiioollooggyy uunniitt''ss DDeeccaattuurr wwoorrkk hhiissttoorryy ddaattaabbaassee ffoorr tthhoossee eemmppllooyyeeeess wwiitthh 77000000 lleevveell ddeeppaarrttmmeenntt czooddeess:,tthhuuss tthheessee: sseellff--rreeppoorrtteedd ddaattaa wweerree uusseedd ttoo aasssseessss yyeeaarrss wwoorrkkeedd iinncchheemmiiccaall.. OOnn tthh:,-ootthheerr hhaanndd,, yyeeaarrss wwoorrkkeedd iinn ffiillmm wweerree ccaallccuullaatteedd ffrroomm tthhee eeppiiddeemmiioollooggyy unniits's DDeeccistuurr wwoorrkk hhiissttoorryy ddaattaabbaassee bbeeccaauussee tthhiiss iinnffoorrmmaattiioonn wwaass nnoott rreeqquuesetsetdoeondn tthhee ssttuuddyy qquueesstt oonnnnaaiiree.. CChheemmiiccaall eemmppllooyyeeeess wwhhoo hhaadd wwoorrkkeedd pprreevviioouussllyyiin tthhee ffiillmm ppllaanntt wweerrtc iiddeennttiiffiieedd aanndd ccllasassifsiiedfaaissettodo tthheeiirr ttiimmeeooffsseerrvviiccee iinn tthhee ffiillmmppllaanntt((<< 11998800,,11998800--11998899 aanndd 11999900--11999988)).. AAggee wwaass ccaallccuullaatteedd ffrroomm tthhee eemmppllooyyeeee''ss ddaattee ooff bbiirrtthh ffrroomm tthhee cppiiddeemmiioollooggyy uunniitt''ss DDeeccaattuurr wwoorrkk hhiissttoorryy ddaattaabbaassee.. BBooddyy mmaassss iinnddeexx((kkgg//mm?2)) wwaass ccaa ccuullaatteedd bbaasseedd oonn tthhee iinnffoorrmmaattiioonn pprroovviiddeedd bbyy tthhee eemmppllooyyeeee oonn tthhee qquueessttiioonnnnaaiirree.. AAnn iinnd(eexx ooff hhaanndd--ttoo-mmoouutthh ccoonnttaacctt wwaass ccaallccuullaatteedd bbaasseedd oonn wwhheetthheerr tthhee ppeerrssoonn ssmmookkeedd cciigg::rreettteess,,cchheewweedd MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbtyyiv33eMMOfrfoodrrerIInnIssnppeePccattiiioomnneaavrnn.dd3CCMoo,ppyNyoii.nngg2-aa0ss4CC-oonn6ff3ii0ddee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00001177 3MA10050450 3MA10050450 Patsw3M F.PI-0006 ttoobbaaccccoooorr cchheewweedd gguumm.. AAnn iinnddeex ooff hhaanndd wwaasshhiinngg wwaass bbaasseedd oonn wwhheerthheerr oorr not the Page 18 of not the 85 eemmppllooyyeeee ssaaiiddtthheeyy aallwwaayyss wwaasshheedd tthheeiirr hhaannddss bbeeffoorree eeaattiinngg wwhhiillee aatt wwozr)krk.. TThhrroouugghh tthhee uussce ooffSSAASS aanndd JIMMPP aanndd eemmppllooyyiinngg ssttaannddaarrdd ssttaattiicsttiiccaall tteecchhnniiqquueess ((ssttuuddeenntt'ss ttetsestt,,cchhii ssqquuaarree,, AANhOOVVAA,,ssiinnggllee aanndd mmuullttiivvaarriiaabbllee rreeggrreessssii )mn uussiinngg lliinneeaarr aanndd nnoonnlliinneeaarr aannaallyysseess)),, ddaattaa aannaallyysseess ccoonncceennttrraatteedd oonn tthhee ffoolllowliongwiii~ssnuueegss::11))ccoommppaarree rreessppoonnddeerrss aanndd nnoonnrreessppoonnddeerrss iinn tthhee rraannddoomm ssaammppllee bbyy tthheeirr ddeemmooggrraagf hhiicc cchhaarraacctteerriissttiiccss ((ee.2g..,aaggee.,ggeennddeerr,, yyeeaarrss wwoorrkkeedd));;22))ccoommppaasree mmeeaann sseerruumm fflluuoorroocehheermmii a:al lleevveellss wwiitthhiinn tthhee cchheemmiiccaall ppllaanntt bbyy aa))eemmppllooyyeeee ddeemmooggrraapphhiiccss.,bb))sseellff--rreeppoorrtteedd wwoorr:,hhiissttoorryy ddaattaa bbaasseedd ffrroomm tthhe ssttuuddyy qquueessttiioonnnnaaiirree iinncclluuddiinngg ccuurrrreennttjoobb,.lloonnggeessti--hheelldd oobb., yyeeaarrss wwoorrkkeedd iinn cchheemmiiccaall aanndd iinn wwhhiicchh cchheemmiiccaall bbuuiillddiinnggss:; c))wwoorrkk hhiissttoorryy ifnoforrnmtaat oonn ssuupppplleemmeenntteedd wwiitthh ddaattaa ffrroomm tthhee 33MM eeppiiddeemmiioollooggyy uunniitt'ss ccoommppuutteerriizzeedd ccoommpprreehheennssii,:e wwoorrkk hhiissttoorryy rreeccoorrdd ddaattaabbuassee ffoorr tthhee DDeeccaattuurr ssiitte,,aanndd dd))ppeerrssoonnaall hhaabbiittss((aallssoo iiddeennttiilileedd oonn tthhee ssttuuddyy qquueessttiioonnnnaaiirree))tthhaatt wweerree hhyyppootthheessiizzeedd to iinnccrreeaasseetthhe lliikkeelliihhoooodd ooffoorraall iinnggeessttiioonn ooff fflluuoorroocchheemmiiccaallss((ee..gg..,hhaanndd wwaasshhiinngg,,cciiggaarreetttee ssmmookkiinngg,,cchheewwiinngg t(oobbaacc:0o aanndd cchheewwiinngg gsuumm)):;aanndd 33))lliikkeewwiissee,,ccoommppaarree mmeeaann sseerruumm fflluuoorroocchheemmiiccaall lleevveellss wwiitthin tthhee ffiillmm ppllaanntt bbyy ssiimmiillaar ffaaccttoorrss,. TToo pprreevveenntt mmiissccllaassssiiffiiccaattiioonn ooffppootteennttiiaall wwoorrkkppllaaccee eexxppoossuurree eexxppeerriieennccee ttoo flluuoorroocchheemmiiccaallss wwiitthhiinn tthhee flilmm ppllaanntt,,wwee aannaallyyzzeedd ssasmmpp eessffrroomm ffiillmm ppllaanntt eemmppllooyyeeeess aaccccoorrddiinngg ttoo tthhoossee wwhhoo hhaavvee aanndd hhaavvee nneevveerr wwoorrkkeedd iinn tthhee -hheermoiiccaall ppllaanntt aass wweellll aass tthhoossee wwhhoo wweerree iiddeennttiiffiieedd aass hhaavviinngg wwoorrkkeedd oonn tthhee DD--11 mmaakkeerr ooccaatteedd iinn tthhee ffiillmm ppllaanntt.. FFiillmm ppllaanntt eemmppllooyyeeeess wwhhoo hhaadd nneevveerr wwoorrkkeedd oonntthhee DD--11 mmaakkeerr ftoorr eevveerr wwoorrkkeedd iinn cchheemmiiccaall aarree hheerreeaafftteerr rreeffeerrrreedd ttoo aass ""oonnllyy ffiillmm ppllaanntt eemmppllooyyeeess.."" BBeeccaauussee tthhee sseerruumm ddiissttrriibbuuttiioonnss ffoorr PPFOOSS..PPFFHHSS.,PPOOAAAA,,PPFFOO;SAAAA,,MMS5T700,, PPFFOOSSAA aanndd MM555566 aappppeeaarreedd lloogg nnoormmaallllyy ddiissttrriibbuutteedd((a sskkeewweedd ddiisstrribb iitoinon))., nnaattuurraal lloogg {trraannssffoorrmmaattiioonnss oofftthhee flluuoorroocchheemmiiccaallss wweerree ppeerrffoorrmmeedd too ccaallccuullaatteeggeelmmeettrriicc mmeeaannss Sohalto techs Ore aime +. 3. C204a30s Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00001188 3aMtAo1o0s05o0s4s5t1 EPLO33GMM ((e(suEm n)d statistical calculations regarding central tendency weree primariPPlaayggeebEaP11s199e-.od00f10880556 arily based In xVn and statistical calculations regarding central tendency wer prim oonn tthhee ggeeoommeettrriicc mmeeaann..TThhee rraannddoomm vvaarriiaabbllee XX iiss ssaaiidd ttoo hhaavvee aa lloogg nnecrmmaall ddiissttrriibbuuttiioonn iifflloogg XX iiss nnoorrmmaallllyy ddiissttrriibbuuttede.d,tthhaatt iiss,iiffXX iisoofftthhee ffoorrmm e"Y wwhheerree YY ii. .nnoorrmmaall((ii..e.,tthhee `nnoorrmmaal bbeellll sshhaappeedd ccuurrvvee)).. TThhee ppeerrttiinneenntt pprrooppeerrttiieess ooffaa lloogg nnoorrmmaall ddiistrriibbuuttiioonn ccaann tthheenn bbeeddeerriivveedd ffrroomm pprrooppeerrttiieess oofftthhee nnoorrmmaal ddiissttrriibbuuttiioonn.. TThhee mmeeaann aanndd vv:,rniaannccee aarree ooff tthhee nnoorrmmaallllyy ddiissttrriibbuutteedd YY.,tthhaatt iiss.,ooff lLoogg XX.. TThhee lloogg nnoorrmmaall ddiissttrriibbuuttiioonn ffii iddss aapppplliiccaattiioonnss iinn aa wwiiddee vvaarriieetdy'ooffffiieellddss iinncclluuddiinngg eexxppoossuurree aasssseessssmmeennttss iinn nnaattuurree((wwhheettieerr ooff hhuummaannss., mmaammmmaallss,, eettcc)).. PPrroovviiddeedd iinn AAppppeennddiicceess CC aanndd DD aarree tthhee hhiissttooggrraammss ooff tthhee sseevvee ir flluuoorroocchheemmiiccaallss aass mmeeaassuurreedd ffoorr eemmppllooyyeeeess iinn tthhee cchheemmiiccaall aanndd ffiillmm ppllaannst,s,rreessppeeccttiivveeli-uussiinngg ssttaattiissttiiccss ddeerriivveedd ffrroomm tthhee nnoorrmmaall ddiisstrriibbuuttiioonn aalloonngg wwiitthh tthhee nnaattuurraall llootg" ttrraannssffoo mmaattiioonn oofftthhee ddiissttrriibbuuttiioon.n. TThhee SShhaappiirroo--WWiillkk WW tteesstt ssuuggggeessttss tthhee nneecceessssiittyy ooff tthhee floogr ttrraannssffoorrmmaattiioonn.. MMeeaassuurreess ooffcceennttrraall tteennddeennccyy rroouuttiinneellyy pprreesseenntteedd tthhrroouugghhoouutt tthiiss rreeppoo tt wwiilll iinncclluuddee tthhee aarriitthhmmeettiicc mmeeaann aanndd rraannggee,,aanndd tthhee ggeeoommeettrriicc mmeeaann aannddaassssoocciiaatteedd 9955f ccoonnffiiddeennccee iinntteerrvvaall.. CCoommppaarriissoonnssooffggeeoommeettrriicc mmeeaannss wweerree ccoonndduucctteedd uussiinngg tthhee ss uuddeentn'ts't tteesstt wwiitthh sstuattiissiticcaall ssiiggnniiffiiccaannccee ccoonnssiiddeerreedd aatt pp << .0055.. AAllll fflluuoorroocchheemmiiccaall mmeeaassuurreemmeennttss wweerree rreeppoorrtteedd iinn ppaarrttss ppeerr mmii.lliioonn((ppppmm))ttoo tthhee tthhiirrdd ddeecciimmaall ppooiinntt.. FFoorr ssttaattiissttiiccaall ppuurrppoosseess,,sseerruumm fflluuoorroocchheemmiiccaall vvaa uueess tthhaatt wweerree lleessss tthhaann tthheelloowweerrlliimmiittooffqquuaannttiittaattiioonn((LLLLOOQQ))wweerree aassssuummeedd tthhee mmiiddppooiirrtt bbeettwweeeenn zzeerroo. aanndd tthhee LLLLOOQQ.. OOFftthhee ttootteall nnuummbbeerr((nn == 118866))ooffeemmppllooyyeeeess ccoonnssiiddeerreet.<.ttoo bbee ccuurrrreennttllyy wwoorrkkiinngg iinn cchheemmiiccaall wwhhoo ppaarrttiicciippaatteedd iinn tthhee ssttuuddyy((112266 ffrroomm tthhee rraannddooamr ssaammppllee aanndd 6600 Vvoolluunntteeeerrss)),,tthhee ffoolllloowwiinngg nnuummbbeerrss((iinn ppaarreenntthheesseess wwiitthh ppeerrcceennttaaggee))hhiidd rreeppoorrtteedd LLLLOOQQ''s bbyy tthhee mmeeaassuurreedd fflluuoorroocchheemmiiccaall::PPFFOOSS((11.,00..551%/).):; PPFH'fS1S((11.,((.55%%));,PPOOAAAA((00., 00%%n)):;PPFFOOSSAAAA((4499,,2266%%)):,MM557700((00.,00%%));;PPFFOOSSAA((3366.,1199%%));;aanndd MM55_`66((88.,44%%)).. OOfftthhee Sohalto techs Ore aime +. 3. C204a30s Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00001199 satoosessz 31VIA10050452 u3M EPI-0006 Page 20 of85 ct roy ply consis tecomen il 0i ns total number(n =76)ofemployees considered to be current film plant 60in the random ssaammppllee aanndd 1166 vvoolluunntteeeerrss)),,tthhee ffoolllloowwiinngg nnuummbbeerrss((iinn ppaarreenntthheesseess))hhaadd rreeppoorrtteedd LLLLOOQQ''ss bbyy tthhee mmeeaassuurreedd fflluuoorroocchheemmiiccaall:: PPFFOOSS((11,,11%%));;PPFFHHSS((22,,22%%));;PPOOAAfAk((00,,00%%));; P'PFFOOSSAAA((299,,38%%));;MM557700((0,,0%%));;PFOOSA ((6655,,866%%))and MM55566((332,,422%%)).. WWee cchhoossee. not to analyze PFOSA among the film plant employees because 85% ol* them had serum PFOSA measured at less than LLOQ which resulted in minimum variability for statistical ccoonnssiiddeerraattiioonnss.. TThhee LLLLOOQQ ffoorrPPFFOOSSAA rraannggeedd,,bbeettwweeeenn aannaallyysseess,,ffrroormr 00..000011 t10o00..001100 ppm. Analyses focused on the random sample but aggregate data analyses were also conducted for all participants(random sample and volunteers)stratifiec by the two plants. ests RESULTS Compt ion al pons ses Comparison ofrandom sample responders and nonresponders company eer ned nd dete. Ange hems RReessppoonnddeerrss((nn == 118866))aanndd nnoonnrreessppoonnddeerrss((nn == 4466))ffrroomm tthhee rraannddoomm ssaammppllee wweerree. compared by age, gender and years worked and found to be alike. Among the chemical rraannddoomm ssaammppllee,,tthe average age wwaass 422 yyeeaarrss ccoommpaarreedd to 433 for nnoonnrreessppoonnddeerrss.. pd sonepveowrne.koneegs.6 us. Thre asi Responders and nonresponders have worked,on average,16 years. There wasa similar5 ft ml oye or sondern egies aren to 1 ratio ofmale tofemale employees forthe responders and nonresponders among ens eno chemicalemployees. AAR Re FFiillmm ppllaanntt eemmppllooyyeeeess wwhhoo rreessppoonnddeedd wweerree,,oonn aavveerraaggee,,4466 yyeeaarrss ooffaaggee.,hhaadd worked 19 years and the ratio of male to female was 5 to 1. Nonresponders were 48 yyeeaarrss ooff aaggee,,hhaadd wwoorrkkeed 2255 yearss and had a 77 to 1 malee to female ratio.,. Thuuss,, aioe Grn nonresponders in the film plant random sample were slightly older, worked longer and a pes ee wr mis. greater percentage were males. te late 901 op cion Cop Cottle Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00020 ownioosi50 3MA10050453 Erto3amMme PageE2P1I-o0f080S56 Page 21 of Overall Findings "The arithmetic mmeeaann((aanndd rraannggee))ooffththee rraannddoomm ssaammppllee aass wweellll:iisstthhee ggeeoommeettrriicc The arithmetic mean and (95% ccoonnffiiddeennccee iinntteervravla)olof)fcchheemmiiccaall eemmppllooyyeeeess((nn == 112266))ffoorr tthhee sseevveenn mean and(95%n ffluuoororchoemcichalesaamrreeipprcreesaseenlnttesedd bbeellooww((iinn ppppmm)):: CChheemmiiccaall PPllaanntt AArriitthhmmeettiicc MMeeaann((aanndd RRaannggee) GGeeoommeettrriicc MMeeaann(a(anndd 9955% CCII) PPFFOOSS PRES 0345 (0005-880) PFHS 0180 (045-0223) PFHS PPOOAAAA PFOSAA 0023 (0001-0269) PFOSAA 0008 (0006-0011) PFOSAA MMS57700 PPFFOOSSAA MSS 00% (0001-0406) Mss6 0022 (0018-0020) M556 11..550055 ((00..009911--1100..660000)) 0.345 (0.005 -1.880) 11..553366 ((00..002211 --66..776600)) 0.023 (0.001 - 0.269) 00..115511 ((00..000088 -- 00..999922)) 00..006622 ((0.000.050--000..60611252)) 0.052 (0.001 - 0.406) PPFFOOSS PFHS PPOOAAAA PFOSAA MM557700 PPFFOOSSAA M556 00.994411 0.180 00.889999 0.008 00..008811 00.001133 0.022 ((00..778877-- 11..112266)) (0.)45 - 0.223) ((00..7'2222--11..112222)) (0.(106 - 0.011) ((00..006677 -- 00..009988)) ((0.0(10.9--000..00011988)) (0.(118 -0.029) "The arithmetic mean (and range) ofthe random sample as well as the geometric: The arithmetic mean(and range)ofthe random sample as well as the geometric `mmeeaann aanndd((9955%% ccoonnffiiddeennccee iinntteerrvvaall))ooff tthhee ffiillmm ppllaanntt eemmppllooyyeeeess((nn == 6600))ffoorr tthhee ssiixx ffluuoorroocchheemmiiccallss aarree pprreesseenntteedd bbeellooww.: FFiillmm PPllaanntt AArriitthhmmeettiicc MMeeaann((aanndd RRaannggee)) GGeeoommeetrriicc MMeeaann((4anndd 9955%% CCTI)) PPFFOOSS PPFFHHSS PPOOAAAA PFPFOOSSAAAA MM557700 PPFFOOSSAA 00..117722 ((0.001.5--000..19944566)) 00.002233 ((00.00011 --00..221100)) 00..007711 ((0.000.6--000..02299688)) 00..000044 ((00..000011 -- 00..003388)) 00..002200 ((00..000011 --00..445544)) 8855%% ooffssaammpplleess << LLLLOOQQ** PPFFOOSS PPFFHHSS PPOOAAAA PPFFOOSSAAAA MM557700 PPFFOOSSAA. 00..113366 ((00..111144--00..116611)) 0.014 ((00.011 - 0..001188)) 0.049 ((0.003.9--000..30066922)) 00..000033 ((00..00022 -- 00..000033)) 00..000088 ((0.0110.6--000..00011611)) 8855%% ooffssaammpplleess << LLLLOOQQ** MSS 0008 (00001-0307) _ MSS6 0003 (0002-0008) M556 0.008 (0.0001 -0.307) M556 0.003 (0.002 - 0.004) LLOQ = ower limit of quantitation for PFOSA ranged fom 0.001 - 0.010 ppm. LLOQ=lower limit ofquantitation forPFOSA ranged from 0.001 -0.010 ppm. BBeceaucsetathheueaabsboovevee vvaalluueessmmaayybbee hhiigghhllyy vvaarriiaabbllee bbyy eemmppllooyyeeeess''ddeemmooggrraapphhiiccss,,wwoorrkk hiissttorryy aanndd ppeerrssoonnaall hhaabbiittss,,ssuubbsseeqquueenntt aannaallyysseess wwiillll ffooccuuss oonn eeaacchh lplaanntt sseeppaarraatteellyy.. MMaaddee AAvvaaiilaabbllee `Subject to Prote bbyy cti v33eMMOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CC4oo,ppNyyoii.nnggC 2aa-ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 281122..002211 3SMMAA1100008500445544 EPLO33XMMS Tables 1 - 21 provide the results from the chemical plant. Tables 22 - 29 proviPPdaaeggeeEth2P2e122-0o0/f0680556 Tables 1 - 21 provide the results from the chemical plant. Tables 22 - ?9 provide the rreessuullttss ffrroomm tthhee ffiillmm ppllaanntt. ChCheemmiiccaall PPllaanntt PPrroovviiddeedd iinn ttaabblleess 22 aanndd 33 aarre tthhee ddeemmooggrraapphhiicc cchhaarraacctteerriissttiiccss bbyy tthhee nnuummbbeerr ooff cchheemmiiccaall eemmppllooyyeeeess((aanndd ppeerrcceenntt))ffrroomm tthhee rraannddoomm ssaammppllee((nn == 112266)),, vvoolluunntteeeerrss((nn ==6600)) aanndd aallll cchheemmiiccaall ppaarrttiicciippaannttss((bbootthh rraannddoomm ssaammppllee aanndd vvoolluunntteeeerr,, nn == )18866)).. TThhee ddiissttrriibbuuttiioonnooffddeemmooggrraapphhiicc cchhaarraacctteerriissttiiccss bbeettwweeeenn tthhee rraannddoomm ssaammplpe aanndd vvoolluunntteeeerrss wweerree ccoommppaarraabbllee aalltthhoouugghh tthhee rraannddoomm ssaammppllee hhaaddaa hhiigghheerr ppeerrcceennttaaggeeooffcchheemmiiccaall ooppeerraattoorrss((3377%%))tthhaann ddiidd tthhee vvoolluunntteeeerrss((22885%%)).. T"Thhee mmeeaann,,mmeeddiiaann,,rraannggee aanndd ggeeoommeettrriicc mmeeaann oofftthhee rraannddoomm ssic tmrpilplee,, vvoolluunntteeeerrss aanndd aallll cchheemmiiccaall ppaarrttiicciippaannttss,, iiss pprroovviiddeedd iinn TTaabbllee44 ffoorr tthhee sseevveenn fflluuoorroocchheemmiiccaallss.. TThhee rraannggee ooffPPFFOOSS wwaassffrroomm 00..009911- 1100..660000 ppppmm.. AAlltthhoouugghh tthhee ggeeoommeettrriicc mmeeaannss wweerree. ccoonnssiisstteennttllyy hhiigghheerr ii n tthhee rraannddoomm ssaammppllee tthhaann vvoolluunntteeeerrss,, oonnllyy wwiitthh PPFFOOSSAA ddiidd tthhee g`geeoommeettrriicc mmeeaann ddiiffffeerr ssiiggnniiffiiccaannttllyy bbeettwweeeenn tthhee rraannddoomm ssaammppllee((00..0011%? ppppmm))aanndd tthhee vVoolluunntteeeerrss((00..000066 ppppmm)).. IItt sshhoouulldd aallssoo bbee nnootteedd tthhaatt aammoonngg tthhee rraannddoonmn ssaammppllee,,ffiivvee eemmppllooyyeeeess hhaadd sseerruumm PPFFOOSS lleevveellss >> 55 ppppmm ccoommpparaerdettodo nnoonnee aammoonngg tthhee vvoolluunntteeeerrss.. BBeeccaauussee tthhee ddeemmooggrraapphhiicc cchhaarraacctteerriissttiiccss aanndd ggeeoommeettrriicc mmeeaannss ddiidd nnoott ssuubbssttaannttiiaallllyy ddiiffffeerr bbeettwweeeenn tthhee rraannddoomm ssaammppllee aanndd vvoolluunntteeeerrs,s,ssuubbsseeqquueenntt taabblleess wwiillll reeppor)rtt oonn eciitthheerr tthhee rraannddoomm ssaammppllee aand/noradallllc/chheeommiiccraall ppaarrttiicciippaannttss.. TThhee vvoolluunntteeeerrss wwiillll nnx> bbee pprreessecnrteedd. sseeppaarraatteellyy.. PPrreesseenntteedd iinn TTaabbllee 55 aarre tthhee ddeemmooggrraapphhiicc cchhaarraacctteerriissttiiccss oofftthhee rraannddoomm ssaammppllee ooff cchheemmiiccaall eemmppllooyyeeeess bbyy ccuurrrreennttjjoobb ccaatteeggoorryy((cceellll ooppeerraattoorr,,cchheemmiiccaall ooppeerraattoorr,, eennggiinneeeerrf/llaabb,,mmaaiinntteennaannccee,,mmiillll ooppeerraattoorr,,sseeccrreettaarryy.,ssuuppeerrvviissoorr//mmaannaaggeemmeenntt aanndd wwaassttee. MSMuaabddjeeecAAtvvataoiillPaarbbollteeecbbtyyiv33eMMOrffdoorrerIInnIssnppeePccattiiioomnneaavrnn.dd3CCMoo,ppyNyoii.nngg2a-ass04CC-oonn6ff3ii0ddee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00002222 3MA10050455 3MA10050455 EPLo3s%mM operator). Supervisorsimanagement (mgmt) and wast operators were thee oldePPstapawEi22Pt3Ig3h0-o01fe0880556 oldest with were th operator). Supervisors/management(mgmt)and waste operators mill operatorss tthhee yyoouunnggeesstt.. MMiillll ooppeerraattoorrss hhaavvee wwoorrkkeedd ccoonnssiiddeerraabbllyy l1e:s55s yyeeaarrss,,oonn mill operator average, tthhaan aalll ootthheerrjjoobb ccaatteeggoorriieess.. TThhiiss iis ttobbee ecxappeecctteedd ssiinnccee mmiillll osppeeraaitoorriisas ann average, entry lleevveell ppoossiittioonn ffoorr nneeww eemmppllooyyeeeess.. TThhee nnuummbbeerr((aanndd pprrooppoorrttiioonn))ccffffeemmaallee entry employees wweerree ssiimmiillaarr bbeettwweeeenn tthhee cchheemmiiccaall ooppeerraattoorrss aanndd tthhee eennggiinneeccrrf/laabb ggrroouupp.. employees Provided iinn ttaabbllee6iis tthhee mmeeaann,,mmeeddiiaann aanndd ggeeoommeettrriicc mmeeaann ffoorr eeaacchh oofftthhee sseevveenn Provided fuorochemical lleevveellss bbyy ggeennddeerr,,hhaanndd--ttoo--mmoouutthh ccoonnttaacctt,,wwaasshh hhaannddssaarrdA wwhheetthheerr tthhee fluorochemical individuaall hhaadd wwoorrkkeedd oonnllyy iinn tthhee cchhemeimcail ppllaanntt.. GGeeoommeettrriicc mmeeaann lleevevls ffoorr mmaalleess wweerree. individu sgniiffiiccaanntllyy hhiigghheerr tthhaann ffeemmaalleessffoorrPPEFOOSS,,PPFFHHSS,,PPOOAAAA aanndd MMS5T700.. WWee ddiidd nnoott sign obseerrvvee,,aass hhyyppootthheessiizzeedd,,tthhaatt hhaanndd--ttoo--mmoouutthh ccoonnttraacctt((vviiaa uussee ooffcciagarreettte,s,cchheewwiinngg obs ttoobbaaccccoo oorrcchheewwiinngg gguumm))aanndd lfeesssffrreeqquueenntt hhaanndd wwaasshhiinngg rreessuulltteedd iinn hhiigghheerr ffluuoorroocchheemmiiccaall sseerruumm lleevveellss.. AAllssoo,,hhaavviinngg wwoorrkkeedd oonnllyy iinn cchheemmiiccaallddii3nonott rreessuulltt iinn hhiigghheerr sseerruumm ffluuoorroocchheemmiiccaall lleevveellss.. WWee ddiidd oobbsseerrvvee tthhaat tthhe ffuurrtthheerr bbaacckk iin ttiimmee tthhaatt cchheemmiiccaall eemmppllooyyeeeess wwoorrkkeedd iinn tthhee ffiilmmplpalnatn,t,tthhe llaarrggeerr tthheeiirr ggeeoommeettrriicc::mmeeaann vvaalluueess were, aass mmeeaassuurreedd iinn tthhiiss ssttuuddyy.. FFoorreexxaammppllee,,tthhee ggeeoommeettrriicc mmeeaann vvaalluueess ffoorr cchheemmiiccaall were, eemmppllooyyeeeess wwhhoo llaasstt wwoorrkkeedd iinn tthhee ffiillmm ppllaanntt pprriioorr (t0o 11998800,,bbeettwweeeenn 11998800--11998869,, 11999900-- 11999988aanndd nneevveerr wwoorrkkeedd iinntthhee ffiillmm ppllaanntt wweerree 11..665566 ppppmm,,11..555511ppppmm.,01.778866 ppppmm aanndd 00..770000 ppppmm,,rreessppeeccttiivveellyy..OOFfccoouurrssee,,tthhiissiiss aallssoo aa rreefflleeccttiioonn oofftthhee nnuummbbeerr ooff yyeeaarrss wwoorrkkeedd iinntthhee cchheemmiiccaall ppllaanntt((t0o bbee pprreesseenntteedd llaatteerr iinn tthhiiss sseeccttiioonn)).. TThhaattsis,,tthhee eemmppllooyyeeeess wwhhoo wwoorrkkeedd iinntthhee ffiillmm ppllaanntt pprriioorr ttoo 11998800 hhaadd ssuubbsseeqquueennttllyy tthhee lloonnggeesstt ccoonnttiinnuuoouuss wwoorrkk hhiissttoorryy iinn cchheemmiiccaall ssiinnccee 11998800.. FFlluuoorroocchheemmiiccaall lleevveellss bbyy ccuurrrreennttjjoobb ccaatteeggoorryyaarree pprreesseenntteedd iinn TTaabbllee 77.. SSeevveerraall oobbsseerrvvaattiioonnss wweerree nnootteewwoorrtthhyy.. FFiirrsstt,,tthhee ddiissttrriibbuuttiioonn ooff hhiigghh--t1oo--llooww ggeeoommeettrriicc mmeeaann Vvaalluueess vvaarriieess bbyy ccuurrrreennttjjoobb ccaatteeggoorriieess.. CCeellll ooppeerraattoorrss hhaavvee tthhee hhiigghheesstt ggeeoommeettrriicc mmeeaann Sih iorochOrdee Palmer. OW 530.8308 +" Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00002233 3aMwAA1t0O005s004455e6 EpLoo3anMxs level of PFOS. The nextgroupare the chemical operators, maintenanc: and waPPsaatggeeeE2P2I44-0o01f0880556 level ofPFOS. The next group are the chemical operators, maintenanc!and waste ooppeerraattoorrss.. SSuuppeerrvviissoorr//mmggmmtt iiss nneexxtt,,ffoolllloowweedd bbyy tthhee ggrroouupp ccoonnssiissttiinngg ooffmmiillllooppeerraattoorrss,, eennggiinneeeerrlAaabb aanndd sseeccrreettaarryy.. FFoorrPPFFHHSS,,cceellll ooppeerraattoorrss hhaavvee tthhee hhiigghheesstt ggeeoommeettrriicc mmeeaann lleevveell.. TThhee nneexxtt hhiigghheesstt ggrroouupp aappppeeaarrss ttoobbee cchheemmiiccaall ooppeerraattoorrss,, wwaassttee )ppeerraattoorrss., ssuuppeerrvviissoorr//mmggmmtt aanndd mmaaiinntteennaannccee.. FFoorrPPOOAAAA,,cchheemmiiccaall ooppeerraattoorrss aappppeeaarr ttoo hhaavvee tthhee hiigghheesstt lleevveellss ffoolllloowweedd bbyy tthhee ggrroouupp ccoonnssiissttiinngg ooffcclelll ooppeerraattoorrss,,mmaaiinntteennaannccee,,mmiillll ooppeerraattoorrss aanndd wwaassttee ooppeerraattoorrss.. CChheemmiiccaall ooppeerraattoorrss aanndd mmaaiinntteennaannccee hhaavvee ssiiggnniiffiiccaannttllyy hhiigghheerr lleevveellss ooff MMS57700tthhaann aallll ootthheerr ccuurrrreennttjoobb ccaatteeggoorriieess.. CChheemmiiccaall aoppeerraattoorrss,, `mmaaiinmtteennaannccee aanndd mmiillll ooppeerraattoorrss hhaavvee tthhee hhiigghheesst.t ggeeoommeettrriicc mmeeaann vvaalluueess ffoorr PPFFOOSSAAAA.. PPFFOOSSAA aanndd MMS5S566 vvaalluueess wweerree ssiiggnniiffiiccaannttllyy hhiigghheerr ffoorr cchheemmiiccaall ooppeerraattoorrss tthhaann ffoorr mmosstt ootthheerrjjoobb ccaatteeggoorriieess. FFlluuoorroocchheemmiiccaall rraattiiooss((PPFFOOSS//PPFFHHSS,,PPFFOOSSI/PPOOAAAA., PPFFOOSSI/((PPFFOOSSSAAA++MMS5T7O0++BPFFOOSSAA++MMS5S566)),,MM5S7T0O/MMS5S566,,PPFFOOSSAAAA/IMM5SJ66 aanndd P'PFFOOSSAA//MM5S5566))aarree pprreesseenntteedd bbyy ccuurrrreennttjoobb ccaatteeggoorryy iinn TTaabbllee 88.. TThhee cceellll ooppeerraattoorrss hhaadd tthhee lloowweesstt PPFFOOSS//PPFFHHSS rraattiioo aanndd tthhee mmiillll ooppeerraattoorrss hhaadd tthhee lloowweesstt PPFFCOSS//PPOOAAAA rraattiioo,. "TThhee llaarrggeesstt PPFEOOSS//mmeettaabbaolliittee rraattiioo wwaass ffoorr tthhe cceellll ooppeerraattoorrss.. T"Taabblleess 99-1111 aarree iiddeennttiiccaall ttoo TTaabblleess77--99,,rreessppeeccttiivveellyy,,eexxcceepptt tthhaat tthhee eemmppllooyyeeeess'' lloonnggeessttjjoobb iiss aannaallyyzzeedd iinnsstteeaaddoofftthhee ccuurrrreennttjjoobb ccaatteeggoorryy.. CCeellll ooppeerartaotrsoaarrese nnoott iinncclluuddeedd aass tthheerree wwaass oonnllyy oonnee cceellll ooppeerraattoorr wwhho ssttaatteedd tthhiiss wwaass hhiiss lloonnggeessttjjoobb hheelldd.. TThhee hhiigghheessttPPFFOOSS,,PPFFHHSS aanndd PPOOAAAA lleevveellss wweerree oobbsseerrvveedd aammoonngg cchheemmiiccaall ooppeerraattoorrss. MMaaiinntteennaannccee aanndd cchheemmiiccaall ooppeerraattoorrss hhaadd hhiigghheerr MMS57700 aanndd PPFFOOSSAAAA lleovveelss.. OOvveerraallll,, rreessuullttss ddiidd nnoott vvaarryy ssuubbssttaannttiiaallllyy bbeettwweeeenn ccuurrrreennttjjoobb aanndd lloonnggeesstt ehelldd jjoobb.. TTaabbllee 1122iiss rreessttrriicctteedd ttoo oonnllyy tthhoossee cchheemmiiccaall eemmppllooyyeeeess wwhhoo ssttaitteedd oonn tthhee qquueessttiioonnnnaaiirree tthhaatt tthheeyy ccuurrrreennttllyy wwoorrkk iinn jjuusstt oonnee llooccaattiioonn((bbuuiillddiinngg)).. BSeeccaauussee bbuuiillddiinngg Sih iorochOrdee Palmer. OW 530.8308 +" Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00002244 3sMaAt1o0o0s5e0a4s5t7 .3M wllEP1-0006 Page 25 of 85 toni yr i ry rls, ds location is synonymous withjob category for cell operators,Buildings'/49 had the highest PFOS and PFHS levels. Building 3 and Building 4N represente3 the areas with Alten mpi tots ET ROSA Nich the highestPOAA levels although only one building,Building 1, had substantially lower POAA levels when compared to the other locations. M570,PFOSAA and M556 levels were highest in Building 3. Buildings 3 and 4MX(MX = mixer/extruder area)appeared 1t0o hhaavvee ccoommppaarraabbllee lleevveellss ooffPPFFOOSSAA.. AAmmoonngg tthhee 5 eemmppllooyyeeeess wwhhoo oonn yy wwoorrkkeedd iinn Building 4N,there was a wide range ofPFOSA levels. Because employees may currently work in only one building bu have had a past history of working in several buildings, we further restricted the analyses to only those employees who said they have only worked in one building throughout their employment. This restricted the number of subjects to just 21 individuals(17% of the random sample)with representation in these Buildings: 1,3and 4MX. Table 13 shows tthhaatt PPFFOOSS lleevveellss wweerree mmoorree tthhaenn 5S ttiimmeess hhiigghehreiirnn tthhee sseerraa ooff BBuuiillddiinngg 33 wwoorrkkeerrss tthhaann iinn the sera of Building 1 or Building 41VIX workers. PFHS levels were alriost 10 fold A higher. POAA levels were twice as high in sera of Building 3 workers compared to Dt 40 aren 5s Bin ir, Building4MX workers and more than 15times higher than Building 1 workers. M570 and M556 levels were 5 times higher in Building 3 workers than Buildings 1 or 4MX. PFOSAA and PFOSA levels were comparable between Building 3 and Building 4MX tent tg. workers and lowestin Building 1. SA ---- Tables 14 through 21 provide similar data analyses as the previous tables but now rn 171 orn gle heist ps, i represent the 187 total(random sample and volunteers)chemical participants. There eb fs ody i sl de were no substantial differences between the analyses ofthe random sample and of all itn. Sung on hie uiel cr es chemical participants. For example,among all chemical participants,mill operators were tthhee yyoouunnggeesstt eemmppllooyyeeeess((TTaabblleess 1144,, 1177));; mmoosstt ffeemmaallee eemmppllooyyeeeess wweerree ztihtheerr iinn tthhee SL gies vr Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00025 snore 3MA10050458 current and longest job category of chemical operators or engineer/lab mi2l3M EPI-0006 Page 26 of85 excluding katt, cry dp i FOS 7S sseeccrreettaarryy))((TTaabblleess 1155,,1188));;cceellll ooppeerraattoorrss hhaadd tthhee hhiigghheesstt PPFFOOSS aanndd PPFFIIiSS sseerruumm lleevveellss and engineer/lab, secretary and mill operators had the lowest PFOS and PFHS serum levels(Tables 16, 19); and chemical operators and maintenance workers had the highest lleevveellss ooff MM557700 aanndd tteennddeedd ttoo aallssoo hhaavvee tthhee hhiigghheesstt sseerruumm lleevveellss ooffPPFFOOSSAAAA,,PPFFOOSSAA and M556. Fluorochemical levels stratified by where employees only currently work ((TTaabbllee 2200)),,oorr hhaavvee oonnllyy eevveerr wwoorrkkeedd((TTaabbllee 2211)),,wweerree aallssoo ccoommppaarraabbllce wwiitthh tthhee rreessuullttss from the random sample. All chemical participants who have only worked in Building 1 had lower fluorocliemical levels than Building 3 workers for all seven luorochemicals ((TTaabbllee 2211)).. BBuuiillddiinngg 11 wwoorrkkeerrss hhaadd lloowweerr PPFFOOSS,,PPOOAAAA,,PPFFOOSSAAAA aai1dd PPFFOOSSAAlelevveellss than Building 4MX employees. PFHS, M556 and M570 levels were similar in Building 1 workers and Building 4MX workers. A series of multivariable analyses(data not shown)examining !ach fflluuoorroocchheemmiiccaall bbyy sseevveerraall iinnddeeppeennddeenntt vvaarriiaabblleess ((e..gg..,, aaggee,, bbooddyy mmaassss iinnddeexx,, ggeennddeerr,, cent etsty edi ry current job,longest-heldjob,whetheremployed only in the chemical )lant, years worked tg ees ey in the chemical plant)suggested there may be up to three important explanatory i variables. These were current(or longest)job, years worked within th,,- chemical plant and gender. retort ve te To better visualize the influence of years worked within chemi;al on serum fluorochen*al levels, we stratified the analyses by current job categories. In other w`woorrddss,,tthhee ddeeppeennddeenntt vvaarriiaabbllee ((ii..ce..,, ecaacchh ssppeecciiffiicc fflluuoorroocchheemmiiccaall))wwaass rreeggrreesssseedd oonn yyeeaarrss tensors pase ps Te sb worked in chemical foreach separatejob category. These linear regression analyses iri ------------ employed the untransformed as well as transformed(natural log)dependent variable. Analyses were conducted for the random sample(n = 126)as well as far all chemical SL gies vr Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 woos 3MA10050459 2881122..00026 EPLoo3s0Mne PageEP22I77-00105056 ppaarrttiicciippaannttss((nn == 118877)).PPrreesseenntteedd iinn AAppppeennddiixxEE aarree tthhee aannaallyysseess ffoorr ecaa,::hh fflluuoorrPooaccghheeemmiicocafall85 ffoorrtthhee rraannddoomm ssaammppllee((nn == 112266))aanndd tthheenn sseeppaarraatteellyy ffoorrcchheemmiiccaall ooppeerraattoorrss,,eennggiinnceeerr//llaabb,, `mmaaiinntteennaannccee,,mmiillll ooppeerraattoorrssaanndd ssuuppeerrvviissoorrss//mmggrmnt.. CCeellll ooppeerraattoorrss aanndd sseeccrreettaarriieess aarree nnoott pprreesseenntteedd bbeeccaauussee ooff tthheeiirr iinnssuuffffiicciieenntt ppooppuullaattiioonn.. FFrroomm tthhee ssccaatttteerrpplloottss aanndd mmooddeellss pprreesseenntteedd iinn AAppppeennddiixx EE,,tthhee ffoolllloowwiinngg wweerree oobbsseerrvveedd.. ((NNoottee::iinn AAppppeennddiicceessfflluuoorroocchheemmiiccaallss aarree pprreesseenntteedd iinn tthhe ffoolllloowwiinngg oorrddeerr PPFFOOSS,,PPFFHHSS,,PPOOAAAA,,PPFFOOSSAAAA,,MM557700,,PPFFOOSSAA aanndd MMS5S566.. FFoorr tthhee ssccaattteerrppllootss,,uuppppeerr aanndd lloowweerr9955%%ccoonnffiiddeennccee ccuurrvveessaarree pprroovviiddeeddoofftthhee ffiitteedd lliinnee.. FFiirrsstt,,ffoorr tthhe eennttirree rraannddoomm ssaammpple,,oonnllyy tthhee PPFFHHSS mmooddeell ffiit tthhee ddaattaa wweellll wwiitthh 2222 ppeerrcceenntt oofftthhee vvaarriiaattiioonn ooff P'PFFHHSS eexxppllaaiinneedd bbyy aann iinnccrreeaassee iinn yyeeaarrss wwoorrkkeedd iinn cchheemmiiccaall.. PPFFOOSS lleevveellss iinnccrreeaasseedd mmooddeessttllyy wwiitthh yyeeaarrss wwoorrkkeedd iinn cchheemmiiccaall aalltthhoouugghh tthhee vvaarriiaannccee eexxppllaaiinnesdd rreemmaaiinneedd ssmmaallll ((r=2.=1.01)0.). AAlltthhoouugghh iinntteerrcceeppttss mmaayy hhaavvee bbeeeenn ssiiggnniiffiiccaanntt foorr ootthheerr fflluuorroocchheemmiiccaall mmooddeellssffoorr tthhe eennttirree rraannddoomm ssaammppllee,,tthhe vvaarriiaannccee eexxppllaaiinneedd wwaass ccoonnssiisstteennttllyy qquuiittee ssmmaallll ((ii..e.,lleessss tthhaann 33 ppeerrcceenntt));;tthhuussssuucchh mmooddeellss hhaavvee mmiinniimmuumm pprreeddiiccttiioonn.. AAmmoonngg cchheemmiiccaall ooppeerraattoorrss tthhee mmosstt ssiiggnniiffiiccaanntt oobbsseerrvvaattiioonn wwaass tthhee ffiinnddiinngg ooffaa lliinneeaarr iinnccrreeaasseeooffPPFFHHSS lleevveellss wwiitthh iinnccrreeaassiinngg yyeeaarrss wwoorrkkeedd iinn cchheemmiiccaall.. TThhiirrttyy--ffoouurr ppeerrcceennttocfftthhee vvaarriiaattiioonn iinn PPFFHHSS wwaass eexxppllaaiinneedd.. TThheerree wweerree wweeaakkeerr ppoossiittiivvee lliinneeaarr aassssoocciiaattiioonns bbeettwweeeenn PPOOAAAA oorr PPFFOOSS aanndd yyeeaarrss wwoorrkkeedd iinn cchheemmiiccaall.. OOnn tthhee ootthheerr hhaanndd,,tthheerree aappppeeaarreedd ttoobbee aa ssuuggggeessttiioonn tthhaatt tthhee hhiigghheesstt lleevveellssoofftthhee fflluuoorroocchheemmiiccaall aannaallyytteess((PPFFOOSSAAAA,,MMS5T7O0,, PPFFOOSSAA aanndd MMS55566))wweerree mmoossttoofftteenn oobbsseerrvveedd aammoonngg cchheemmiiccaall ooppeerraattoerss wwiitthh jjuusstt oonnee oorr ttwwoo yyeeaarrssooffeexxppeerriieennccee.. AAmmoonngg tthhee eennggiinneeeerr//laabb ggrroouupp,,tthheerree wwaass aa wweeaakk aassssoocciiaattiioonn bbeettwweeeenn sseerruumm PPFFOOSS lleevveelslsaanndd yyeeaarrss wwoorrkkeedd iinn cchheemmiiccaall.. TThhee sstirroonnggeesstt aassssoocciiaattiioonn oobbsseerrvveedd aammoonngg mmaaiinntteennaannccee wwoorrkkeerrss wwaasstthhe lliinneeaarr iinnccrreeaassee ooffPPFFHHSS lleevveellss wwiitthh yyeeaarrss Wwoorrkkeedd iinn cchheemmiiccaall.. LLiikkeetthhee cchheemmiiccaall ooppeerraattoorrss,,aa ssiiggnniiffiiccaanntt aammoouumn ooff vvaarriiaattiioonn wwaass Sih iorochOrdee Palmer. OW 530.8308 +" Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00002277 3sMAAt1o0005s0e4a6z0 EPLO30aMSn explained (26 percent) although the data were sparse. Among the supervisorPiaPmagggmeeEt22P8I8-0o08f085056 explained(26 percent)although the data were sparse. Among the supervisor/mgmt ggrroouupp,,PPFFOOSS,,PPFFHHSS aanndd PPOOAAAA iinnccrreeaasseedd wwiitthh yyeeaarrss wwoorrkkeedd iinn cchheemmiiccaall.. AApppprrooxxiimmaatteellyy 115S ppeerrcceenntt oofftthhe vvaarriiaattiioonn wwaass eexxppllaaiinneedd iinn ecaacchh mmooddeell.. MMooddeell ffiitt wwaass ppoooorrffoorr tthhee mmiillll ooppeerraattoorrss bbeeccaauussee aallll bbuutt ttwwoo hhaadd wwoorrkkeedd ffoorr 55 yyeeaarrss oorr lleessss;;tthhuuss oonnllyy ssccaatttteerrpplloottss aarree pprreesseenntteedd((nnoott rreeggrreessssiioonn mmooddeellss)).. "The The nnaattuurraall lloogg ttrraannssffoorrmmaattiioonnss aarree pprreesseenntteedd iinn AAppppeennddiixx F F ffccrralalll cchheemmiiccaall eemmppllooyyeeeess((nn == 112266))iinn tthhee rraannddoomm ssaammppllee aass wweellll aass ffoorr tthhee ttwwoo ccuurrrreennttjjoobb ccaatteeggoorriieess wwiitthh tthhee mmoosstt nnuummbbeerrss((cchheemmiiccaall ooppeerraattoorrss aanndd eennggiinneceerr//llaabb)).. FFoorr tthhee eennttiirree rraannddoomm ssaammppllee,,aa wweeaakk aassssoocciiaattiioonn((r2==.0088))iiss oobbsseerrvveedd ffoorrPPFFOOSS aanndd yyeeaarrss wwoorrkkeedd iinn cchheemmiiccaall aanndd aa ssttrroonnggeerr aassssoocciiaattiioonn((r+Z==.2233))ffoorr PPFFHHSS.. FFoorr cchheemmiiccaall ooppeerraattoorrss tthhee ssttrroonnggeesstt aassssoocciiaattiioonn((rrz==.3344))iiss wwiitthh PPFFHHSS aanndd yyeeaarrss wwoorrkkeedd iinn cchheemmiiccaall.. AAlltthhoouugghh tthhee llaatttteerr aassssoocciiaattiioonn wwaass nnoott oobbsseerrvveedd aammoonng tthhee eennggiinneceerr//llaabb ccaatteeggoorryy wwiitthh tthh:e nnoonnttrraannssffoorrmmeedd vvaarriiaabbllee((sseeee AAppppeennddiixx EEJ),,tthhee nnaattuurraall lloogg ttrraannssffoorrmmaattiioonn ooffPPFFHHSS wwaass ssiiggnniiffiiccaannttllyy aassssoocciiaatteedd((rr2==.1.199))wwiitthh yyeeaarrss wwoorrkkeedd iinn cchheemmiiccaall((sseeee AAppppeennddiixx FF)).. PPrreesseenntteedd iinn AAppppeennddiixx GG aarree ssiimmiillaarr ssccaatttteerrpplloottss aanndd rreeggrreessssiioonn mmooddeellss ffoorraallll cchheemmiiccaall ppaarrttiicciippaannttss bbyy ccuurrrreennttjjoobb ccaatteeggoorryy.. TThheerree rreemmaaiinneedd aa ppoossiituivvee aassssoocciiaattiioonn bbeettwweeeenn PPFFHHSS oorr PPFFOOSS sseerruumm lleevveellss aanndd yyeeaarrss wwoorrkkeedd iinn cchheemmiiccaall,,wwiitthh tthhee ssttrroonnggeerr ooff tthheessee ttwwoo aassssoocciiaattiioonnssffoorrPPFFHHSS..BBeeccaauussee ooff mmoorree ssuubbjjeeccttss,,ssccaatttterrpplloortss arreeaallssoo nnooww sshhoowwnn ffoorr ccellll ooppeerraattoorrs.. TThheessee pplloottss ssuuggggeesstt,,aaggaaiinn,,aann iinnccrreeaassee iinn PPFFOOSS,,PPFFHHSS aanndd nnooww aallssooPPOOAAAA lleevveellss aammoonngg ccuurrrreenntt cceellll ooppeerraattoorrss wwiitthh yyeeaarrss wwoorrkkeedd iinn cchheemmiiccaall.. AAmmoonngg cchheemmiiccaall ooppeerraattoorrss tthhee ssttrroonnggeesstt aassssoocciiaattiioonn rreemmaaiinneedd wwiitthh PPFFHHSS,,wwiitthh wweeaakkeerr lliinneeaarr aassssoocciiaattiioonnss oobbsseerrvveeddffoorrPPFFOOSS aanndd PPOOAAAA wwiitthh yyeeaarrss wwoorrkkeedd iii1i cchheemmiiccaall. AAmmoonnggtthheeeennggiinneeeerr/llaabb ggrroouupp,,tthheerree rreemmaaiinneedd aa ppoossiittiivvee lliinneeaarr aassssoocciiaattiioonn bbeettwweeeenn eciitthheerr PPFFHHSS oorr PPFFOOSS wwiitthh yyeeaarrss wwoorrkkeedd iinn cchheemmiiccaall.. TThheerree wweerree ppoosssiittiivvee lliinneeaarr MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbiyyiv33eMVOrffodorrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee8nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00002288 3MA10050461 3MA10050461 EPLO3M0MG associations for PFOS, PFHS and POA with years worked in chemical amonPPgaaggbeeoEt2P2hI99-0ot01hf0e880556 associations for PFOS,PFHS and POAA with years worked in chemical among both the `mmaaiinntteennaannccee aanndd ssuuppeerrvviissoorri/mmggmmtt ggrroouuppss.. TTooooffeeww mmiillll ooppeerraattoorrss wwiitthh 5 oorr mmoorree wwoorrkk yyeeaarrss iinn cchheemmiiccaall wweerree ssaammpplleeddttoo ccoonndduucctt aa mmeeaanniinnggffuull aannaallyyssiiss.. TThhy ssccaattiteerrpplloott ddaattaa ddoo sshhooww aa wwiiddee rraannggee ooffssecrruumm PPOOAAAA lleevveellss aammoonngg mmiillll ooppeerraattoorrss wwiitthhjjuusstt oonne yyeeaarr ooff wwoorrkk eexxppeerriieennccee iinn cchheemmiiccaall.. T"Thhee ssccaatttteerrpplloottss iinn AAppppeennddiixx HH rreepprreesseenntt tthhee lloogg ttrraannssffoorrmmaattiioonnss ffoorr aallll cchheemmiiccaall ppaarrttiicciippaannttss aanndd tthhee ttwwoo mmoosstt nnuummeerroouussjjoobb ccaatteeggoorriieess::cchheemmiiccaall ooppeerraattoorrss aanndd eennggiinnceeerrl/llaabb.. AAggaaiinn,,tthhee ssccaatttteerrpplloottss ssuuggggeesstt aa ccoonnssiisstteennttllyy sstirroonngg ppooss ttiivvee aassssoocciiaattiioonn bbeettwweeeenn sseerruumm PPFFHHSS lleevveellss aanndd yyeeaarrss wwoorrkkeedd iinn cchheemmiiccaall aanndd aa leessssee aassssoocciiaattiioonn wwiitthh PPFFOOSS aanndd yyeeaarrss wwoorrkkeedd iinn cchheemmiiccaall. PPrreesseenntteedd ecaarrlliieerr iinn TTaabbllee66 wwaass tthhee oobbsseerrvvaattiioonn tthhaatt sseerruumm fflluuosrroocchheemmiiccaall lleevveellss wweerree lloowweerr aammoonngg ffeemmaallee wwoorrkkeerrss.. WWhheetthheerr tthhiiss wwaass dduuee ttoo aa ssmmaalllleerr pprrooppoorrttiioonn ooff ffeemmaallee wwoorrkkeerrss iinnjjoobb ccaatteeggoorriieess wwhheerree eexxppoossuurree wwoouulldd bbee tthhee hhiigghheesstt,, yyoouunnggeerrffeemmaallee wwoorrkkeerrss aanndd/oorrffeemmaallee eemmppllooyyeeeess wwiitthh lleessss wwoorrkk eexxppeerriieennccee iinn cchheemmiiccaall rreemmaaiinneedd ttoo bbee rreessoollvveedd.. TToo aaddddrreessss tthhiiss iissssuuee wwee ffooccuusseedd oonn tthhoossee ttwwoojjoobb ccaatteeggoorriieess tthhaatt hhaadd tthhee mmoosstt ffeemmaallee ssuubbjjeeccttss wwiitthhiinn tthhee rraannddoomm ssaammppllee aass wweellll aass aallll cchheemmiiccaall ppaarrttiicciippaannttss::cchheemmiiccaall ooppeerraattoorrss aanndd tthhee eennggiinneeeerr//llaabb ggrroouupp.. PPrreesseenntteedd iinn TTaabblleess 2222 aanndd 2233.. bbyy ggeennddeerr,,aarree tthhee ddeemmooggrraapphhiicc cchhaarraacctteerriissttiiccss aanndd sseerruumm fflluuoorroocchheemmiiccaall lleevveellss ffoorr tthhee rraannddoomm ssaammppllee ooff cchheemmiiccaall ooppeerraattoorrss aanndd tthhee eennggiinneeeerr//llaabb ggrroouupp.. FFeemmaallee eemmppllooyyeeeess hhaadd ssiiggnniiffiiccaannttllyy lloowweerr ggeeoommeettrriicc mmeeaann sseerruumm lleevveellss ooffPPFFOOSS,,PPFFHHSS aanndd PPOOAAAA.. MMuuhliivvaarriiaabbllee aannaallyysseess ooffcchheemmiiccaall ooppeerraattoorrssooffeeaacchh fflluuoorroocchheemmiiccaall lleevveell rreeggrersessesdoeondn ggeennddeerr,, yyeeaarrss wwoorrkkeedd iinn cchheemmiiccaall aanndd wwiitthh aanndd wwiitthhoouuttaaggeeaarreepprreesseenntteedd iinn AAppppenednidx II ffoorr tthhee rraannddoomm ssaammppllee.. FFoorr ppuurrppoosseessooff bbrreevviittyy,,oonnllyy tthhee ttrraannssffoorrmmeedd((nnaattuurraall lloogg))ddeeppeennddeenntt mmooddeellss aarree pprreesseenntteedd.. GGeennddeerr aappppeeaarreedd ttoo bbee tthhee bbeesstt pprreeddiiccttoorr ooffPPFFOOSS lleevveell((ii..!2..,,lloowweerr lleevveellss MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbtyyiv33eMMOrffodorrerIInnIssnppeePccattiiioomnneaavrnn.dd3CCMoo,ppyNyoii.nngg2a-ass04CC-oonn6ff3ii0ddee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00002299 3MA10050462 3MA10050462 er "3M mall EP1-0006 A AeI APage 30of85 among female chemical operators) with years worked in chemical not significantly ET Gent associated with PFOS. Gender was also significantly associated with 110AA levels on FORA fren lw dps ss ttn hic (lowerPOAA levels amongfemale workers)adjusting for years worked in chemical and FU age. Both gender and years worked in chemical appeared to be importint predictors of SA PFHS levels among chemical operators. Among the random sample of engineer/lab workers, gender was the most important predictor ofPFOS,PFHS,POAA and PFOSAA levels after adjusting for years worked in chemical and age(Appendix.). Data for nT chemical operators and the engineer/lab group from the all chemical participants showed comparable results(Appendices K and L). To further clarify this issue, regression analyses were stratified any gender as well as by job category. With male chemical operators as well as with the male engineer/lab rt teitegeomti oT group,there was a consistent association ofincreasing levels ofPFOS and PFHS(and POAA for chemical operators only) with increasing years worked, at least for the first sseevveerraallyyeeaarrssooffwwoorrkk..SSccaatttteerrpplloottss aarree ffoouunndd iinn AAppppeennddiixx MM.. MMoorree qquueessttiioonnaabbllee iiss. eon cto is ns pais cin. whether such an association remains linear or is polynomial(quadratic; over time. mor fe ceca perars heey scion so PAS ds Amongfemale chemical operators the only association observed wasforPFHS and years ote. Ses unin pend. Ne POS 6 FON cl worked. Scatterplots arefound in Appendix N. Neither PFOS orPOAA levels Teena rere oe appeared to increase with years worked in chemical among female chemical operators. he freemen ou fc ni ne 65 The datafor the female engineer/lab group are difficult to interpret since6ofthe9 cs lS workinchm, Ucit o cm(ne individuals had less than 5 years of work in chemical. Use ofan interaction term(gender ym hice nist mls ssn npr rien x years worked in chemical)in multivariable models was not an important predictorof fluorochemical levels. te tyar erscin re Cony Cpl amston Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00030 amstocsoes 3MA10050463 FFiillmm PPllaanntt EPLO33OMMS PPaaggeeEP331I1-oo0ff0880556 AAllttooggeetthheerr tthheerree wweerree 6600 ccuurrrreenntt eemmppllooyyeeeess wwhhoo rreessppoonnddeedd ttoo tthhee ffiillmm ppllaanntt rfaannddoomm ssaammpplliinngg.. AA ttoottaall ooff3366eemmppllooyyeeeess hhaadd wwoorrkkeedd oonnllyy iinntthhee ffillrm ppllaanntt((ii..e..,,'oonnllyy iinn tthhee ffiillmm ppllaanntt'rreeffeerrss ttoo ffiillmm ppllaanntt wwoorrkkeerrss wwiitthh nnoo kknnoowwnn eexxppeerriienecnec:oonn tthhee DD--11 mmaakkeerr oorr hhaavvee hhaadd nnoo pprreevviioouuss wwoorrkk eexxppeerriieennccee iinn tthhee cchheemmiiccaall ppllaannt)),,66 ffiillmm ppllaanntt eemmppllooyyeeeess wweerree kknnoowwnn ttoo hhaavvee wwoorrkkeedd oonn tthhee DD--11 mmaakkeerr aanndd 1188 eemmppllooyyeeeess hhaadd wwoorrkkeedd,,aat ssoommee. ttiimmee pprreevviioouussllyy,,iinn tthhee cchheemmiiccaall ppllaanntt bbuutt wweerree nnoott oonn tthhee DD--11 mmaakkeerr((TTaabbllee 2244)).. FFoorr aallll ffiillmm ppaarrttiicciippaannttss((nn == 7766,,rraannddoomm ssaammppllee aanndd vvoolluunntteeeerrss)),,aa ttoottaall ooff4499hhaadd wwoorrkkeedd oonnllyy iinn tthhee ffiillmm ppllaanntt,,77 wweerree kknnoowwnn ttoo hhaavvee wwoorrkkeedd oonn tthhee DD--11 mmaakkeerr aanndd 2200 hhaadd wwoorrkkeedd,,aatt ssoommee ttiimmee pprreevviioouussllyy,,iinn tthhee cchheemmiiccaall ppllaanntt.. AAmmoonngg tthhee 6600eemmppllooyyeeeess ooff tthhee rraannddoomm ssaammppllee,,tthheerree wweerree nnoo ssuubbssttaannttiiaall ddeemmooggrraapphhiicc ddiiffffeerreenncceess((TTaabbllee 2255))bbeettwweeeenn tthhee oonnllyy ffiilmm,,tthhee DD--1I mmaakkeerr aanndd pprriioorr cchheemmiiccaall hhiissttoorryy ggrroouuppss.. HHoowweevveerr,,tthheerree wweerree ssiiggnniiffiiccaanntt ddiiffffeerreenncceess min sseerruumm fflluuoorroocchheemmiiccaall lleevveellss aammoonngg tthheessee tthhrreeee ggrroouuppss ooffffiillmm ppllaanntt wwoorrkkeerrss.. TThhoossee eemmppllooyyeeeess wwhhoo hhaavvee oonnllyy wwoorrkkeedd iinn tthhee ffiillmm ppllaanntt((bbuutt nnoott oonn DD--II mmaakkeerr oorr pprreevviioouuss cchheemmiiccaall ppllaanntt hhiissttoorryy))hhaadd ssiiggnniiffiiccaannttllyy lloowweerr mmeeaann PPFFOOSS lleevveellss((TTaabbllee 2266)).. TThhee ggeeoommeettrriicc mmeeaann ooff PPFFOOSS ffoorr oonnllyy ffiillmm ppllaanntt wwoorrkkeerrss wwaass00..111100 ppppmm((9955%% CC1I00..009944--00..112219)))ccoommppaarreedd ttoo 00..228899 ppppmm((9955%% CC1I00..115599--00..552277))ffoorr eemmppllooyyeeeess kknnoowwnn ttoo hhaavveewwoorrkkeeddoonn tthhee DD--11 mmaakkeerr aanndd tthhee ggeeoommeettrriicc mmeeaann wwaass00..117788 ppppmm((00..113377--00..223333))ffoorrffiillmm ppllaanntt eemmppllooyyeeees.s wwiitthh pprriioorr hhiissttoorryy iinn cchheemmiiccaall.. AAsisimmiillaarr ssiiggnniiffiiccaanntt aassssoocciiaattiioonn,,aallbbeeiitt aatt aa lloowweerr ppppmm. lleevveell,,wwaass oobbsseerrvveeddffoorrPPOOAAAA.. TThhee oonnllyy ffiillmm ppllaanntt eemmppllooyyeeeess hhaadd ssiiggnniiffiiccaannttllyy lloowweerr PPFFHHSS lleevveellss wwhheenn ccoommppaarreedd ttooffiillmm ppllaanntt wwoorrkkeerrss wwiitthh aa pprreevviioouuss hhiissttoorryy iinn cchheemmiiccaall;; tthheeiirr PPFFHHSS lleevveellss wweerree nnoonnssiiggnniiffiiccaannttllyy lloowweerr tthhaann tthhoossee wwhhoo wwoorrkkeedd oonn tthhee DD--1I mmaakkeerr.. TThheerree wweerree nnoo ssiiggnniiffiiccaanntt ddiiffffeerreenncceessiinn sseerraa lleevveellss oofftthhee rreemmaaiinniinngg fflluuoorroocchheemmiiccaall Sih iorochOrdee Palmer. OW 530.8308 +" Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00003311 3SMwAA1t0o0os5o0i4s6s4 EPI003M0Mm6 levels among the three groupsof film employees. Interestingly, al film plant wPPoaarggeekEeP32rI20s-o10f0880556 levels among the three getups offilm employees. Interestingly, all film plant workers wwiitthh aa pprreevviioouuss hhiissttoorryy ooff hhaavviinngg wwoorrkkeedd iinn tthhee cchheemmiiccaall ppllaanntt hhaadd MMS5S566 vvaalluueess tthhaatt wweerree bbeellooww tthhee LLLLOOQQ.. WWee ddoo nnoottee tthhaatt tthhee DD--11 mmaakkeerr ggrroouupp hhaadd ccoommapaasraabbllee lleevveellss ooff MMS577001t0o tthhee oonnllyy ffiillmm oorr ffiillmm wwiitthh pprreevviioouuss hhiissttoorryy iinn cchheemmiiccaall ggrroouuppss((sseeee TTaabbllee 2266)).. WWee hhaadd hhyyppootthheessiizzeedd tthhee DD--11 mmaakkeerr ggrroouupp mmaayy hhaavvee hhaadd hhiigghheerr lleevveelhs bbeeccaauussee ooff tthheeiirr uussee ooff mmeetthhyyll FFOOSSEE aammiiddee wwhhiicchh mmaayy mmeettaabboolliizzee ttoo tthhee aannaallyyttee MM557700. PPrroovviiddeedd iinn TTaabbllee 2277 aarree rraattiiooss oofffflluuoorroocehheemmiiccaallss.. TThhee mmeeddiiaann rraattiiooss wweerree ccoommppaarraabbllee ffoorr tthheessee ggrroouuppssooffffiillmm ppllaanntt wwoorrkkeerrss iinn tthhee rraannddoomm ssaammppllee.. RReessttrriiccttiinngg tthhee aannaallyysseess ttoo ffiillmm eemmppllooyyeeeess wwiitthh nnoo DD--11 mmakaercckrrcchheeemmiirccaall ppllaanntt eexxppeerriieennccee,,tthheerree wweerree nnoo ssiiggnniiffiiccaanntt ddiiffffeerreenncceess bbyy aaggee ffoorr tthhee ffoouurr ccuurrrreennttjjoobb ccaatteeggoorriieess aannaallyyzzeedd::eennggiinnceeerr//llaabb,,ffiillmm pprroocceessssoorr,,mmaaiinntteennaannccee aanndd aaddmmiinniissttrraattiivvee((TTaabbllee 2288)).. AAlltthhoouugghh tthheeiirr sseerruumm lleevveellss wweerree ssuubbssttaannttiiaallllyy bbeellooww tthheeiirr ccoouunntteerrppaarrttss iinn cchheemmiiccaall,, mmaaiinntteennaannccee eemmppllooyyeeeess wwoorrkkiinngg iinn tthhee ffiillmm ppllaanntt hhaadd ssiiggnniiffiiccaannttllyy hhiigghheerr PPFFOOSS,, PPOOAAAA aanndd MMS57700lleevveellss tthhaann tthhee eennggiinneeeerr//llaabb ggrroouupp wwiitthhiinn tthhe ffiillmm ppllaanntt((TTaabbllee. 2299)),. EEnnggiinnceeerr//llaabb,,ffiillmm pprroocceessssoorrss aanndd aaddmmiinniissttrraattiivvee wwoorrkkeerrss hhaadd ccoommppaarraabbllee fflluuoorroocchheemmiiccaall sseerruumm lleevveellss.. MMeeddiiaann flluuoorroocchheemmiiccaall rraattiiooss wweerree ccoommppaarraabbllee aammoonngg. tthheesseejjoobb ccaatteeggoorriieessoofftthhee rraannddoomm ssaammpplleeooffffiillmm ppllaanntt wwoorrkkeerrss((TTaabbllee 3300)).. SSiimmiillaarr ffiinnddiinnggss wweerree oobbsseerrvveedd wwhheenn aallll ffiillmm ppllaanntt ppaarrttiicciippaannttss wweerree aannaallyyzzeedd ``oorr ddeemmooggrraapphhiiccs.s aanndd sseerruumm fflluuoorroocchheemmiiccaall lleevveellss((TTaabblleess 3311--3333)).. LLooccaatteedd iinn AAppppeennddiixx OOaarre ssccaatttteerrpplloottssoofftthhee oonnllyy ffiillmm ggrroouupp ffo.3rr ceaacchh fflluuoorroocchheemmiiccaall rreeggrreesssseedd oonnyyeeaarrsswwoorrkkeedd iinn ffiillmm.. BBeeccaauussee mmaaiinntteennaannccee wwoorrkkeerrss hhaadd hhiigghheerr lleevveellss,,oonn aavveerraaggee,,tthhaann tthhee ootthheerr tthhrreeeejjoobb ggrroouuppss aammoonngg tthhee oonnllyy ffiillmm eemmppllooyyeeeess,, tthheeyy aarree nnuummbbeerreedd oonn tthhee ggrraapphhss.. FFrroomm tthheessee aannaallyysseess tthheerre iissssoommee ssuuggggeessttiioonn tthhaatt PPFFOOSS aanndd PPOOAAAA lleevveellss mmaayy iinnccrreeaassee wwiitthhiinn tthhee ffiirrssttffeeww yyeeaarrss ooff wwoorrkkiinngg aatt tthhee DDeeccaattuurr Sih iorochOrdee Palmer. OW 530.8308 +" Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00003322 3sMuAn1o0o05s0o4e6s5 ml"3M EPI-0006 Page 33 of85 film plant and then subsequently plateau. However, unlike chemical workers, there is no nent conser EHS, Toe inn orem linear(or quadratic)association observed forPFHS. The remainingfluorochemicals enn sion ies odin i showed no association with years worked in film. DDIISSCCUUSSSSIIOONN The goal of this research effort was to quantify, based on random sampling, the relationship of employee serum levels of seven fluorochemicals at the Decatur chemical and film plants. In that regard, the data collected and analyzed present a convincing picture of significantly lower serum fluorochemical levels among employees who have only worked in the film plant when compared to those who are current chemical plant pres Foran on pont soc 5h ort employees. Forexample,comparing the geometric means for each fluc~rochemical ee tet pnts nh lo nly bcd in between chemical operators and those employees who only have worked in film,we nen or. PFOAIOAI0: PHS 580019, POAA observed the following ratios: PFOS(1.481/0.110),PFHS(0.428/0.015);POAA ARSE (1.887/0.052);PFOSAA (0.011/0.002); M570(0.229/0.022); and M556(0.044/0.003). en ce fo PEOSAA igs 0k priser These ratios,exceptforPFOSAA,suggest a 10-fold or greater differenze between chemical operators and film plant employees who work several hundred yards away from Building 33.. Thheese only ffilmm plantt wwoorrkers appear to hhaavve a geometric mmeeaann vvaalluuee ffoorr 1705 spiny es igre ep somes 7 00 PFOS that is approximately 3-4 times higher than the pooled geometric mean(0.029 op gs in os 55. os rs, hs ese ppm)from 64samples obtainedfrom 18 U.S.blood banks, thus,we suspect that on pes FOS ca iif rt gh mich onc occupationalexposure toPFOS occurs within the film plant although at much lower ts rn min lope king ech lo levels than among employees working atthe chemical plant. rrr ATY Among film plant employees we also established the fact that workers on the D-1 maker have serum PFOS levels approximately 3times higher than those who have never te tyar erscin re Cony Cpl amston Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00033 awstocsocs 3MA10050466 ilul3M EPI-0006 Page 34 of85 A worked on the D-I maker nor have worked in the chemical plant. Unexplained is the POAA levels of these workers on the D-1 maker as well as the levels observed among Wetter pes rene pn. Fc otherfilm plantemployees. We confirmed several hypotheses for the chemical plant employees. First, cell operators have the highest serum levels of PFOS and PFHS although their serum levels for other fluorochemical analytes were similar to other chemical employees who were seit prt m------ iinnvvoollvveedd wwiitthh tthhee cchheemmiiccaall rreeaaccttoorrss((ii..ee..,cchheemmiiccaall ooppeerraattoorrss aanndd mmaaiinnttennaannccee wwoorrkkeerrss)).. Second,chemical operators and maintenance workers had comparable serum fluorochemical levels. Besides their higher levels of PFOS and PFHS,:hey both had significantly higher levels of M570(the methyl FOSE alcohol metabolite)and to a lesser degree to PFOSAA which is the ethyl FOSE alcohol metabolite (as well as an FC product itself, FC-129). Chemical operators, but not maintenance workers, had higher levels of AAA PFOSA. Both chemical operators and maintenance workers had moderately higher levels I ---- of M556 than the otherjob categories. These data suggest that, beyond general plant- bbaasseedd eennvviirroonnmmeennttaall eexxppoossuurree ttoo PPOOSSFF aanndd PPHHSSFF((wwhhiicchh wwee aassssuummee ii:s; pprriimmaarriillyy JUthrough inhalation and conversion to PFOS and PFHS,respectively),the chemical retort er vies vor tr operators and maintenance workers have higherserum levels as a result oftheir J -- occupational exposure to the fluorochemical products. These occupational exposures etn Som, iC, Se 5 may be from the FC alcohols,FC amides,and FC acrylates. Because these Stet he pr en OS Se fluorochemicals have much lower vapor pressure than POSF and PHSF,these data may te ps se rots i ema i indicate that the exposure to these chemical products within the chemical plant is relatively limited to within Building 3 and Building 4N. Third, waste operators were retried es mols EC dE pec comparable tochemical operators forserum levels ofPFOS and PFHS but,like the cell rt eee ot ert i or operators,did not have higherlevels ofthe fluorochemical analytes.Fourth, mill SL gies vr Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00034 woo: 3MA10050467 EPLOG33OMMS PPaaggeeE3P3155-0o01f0880556 ooppeerraattoorrss wweerree ggeenneerraallllyy mmuucchhyyoouunnggeerreemmppllooyyeeeess aanndd tthheeiirr hhiigghheesstt fflluuoorroocchheemmiiccaall sseerruumm lleevveell wwaass ttoo PPOOAAAA.. YYeett,,tthhee mmiillll ooppeerraattoorrss''PPOOAAAA lleevveellss wweerree lloowweerr tthhaann tthhoossee. ooffcceellllooppeerraattoorrss,,cchheemmiiccaall ooppeerraattoorrss aanndd mmaaiinntteennaannccee wwoorrkkeerrss.. TThhiiss sstu.ggggeessttss tthheerree iiss ppllaanntt--bbaasseedd eexxppoossuurree ooffPPOOAAAA wweellll bbeeyyoonndd tthhee BBuuiillddiinngg44 aarreeaa wwhhiicchh mmaayy bbee dduuee ttoo tthhee: ffaacctt tthhaatt PPOOAAAA iiss aabbyy--pprroodduucctt oofftthhee eelleeccttrroollyyttiicc cceellll pprroodduuccttiioonn.. FFiinnaallllyy,,tthhee ddaattaa ssuuppppoorrtt tthhee hhyyppootthheessiiss tthhaatt tthhoossee iinnddiivviidduuaallss((ee..gg.,.,eennggiinneeeerrss aanndd sseeccrreett.ririieess)) wwhhoo aarree mmuucchh lleessss lliikkeellyy ttoo hhaavvee rroouuttiinnee ooccccuuppaattiioonnaall eexxppoossuurree wwiitthhiinn tthhee cchheermriiccaall ppllaanntt,, ddoo., iinnddeeeedd hhaavvee lloowweerr sseerruumm fflluuoorroocchheemmiiccaall lleevveellss.. EEmmppllooyyeeeess wwhhoo hhaavvee oonnllyy wwoorrkkeedd iinn BBuuiillddiinngg 1| wwhhiicchh iiss iimmmmeeddiiaatteellyy aaccrroossss tthhee wwaallkkwwaayy ffrroomm BBuuiillddiinngg 33,, ,lnaavvee sseerruumm fRluuoorroocchheemmiiccaall lleevveellss tthhaatt rraannggee bbeettwweeeenn 77((PPFFOOSS,.PPFFHHSS))aanndd 1155 ttiimmee:s:((PPFFOOSSAAAA)) lloowweerr tthhaann eemmppllooyyeeeess wwhhoo hhaavvee oonnllyy wwoorrkkeedd iinn BBuuiillddiinngg 33.. OOuurr aannaallyysseess ooff fflluuoorroocchheemmiiccaall lleevveellss iinn sseerruumm ffrroomm rraannddoommllyy ;seelleecctteedd eemmppllooyyeeeess ssttrreennggtthheenn tthhee rreeccoommmmeennddaattiioonnss tthhaatt wweerree rreecceennttllyy mmaaddee iinn aa DDeeccaattuurr iinndduussttrriiaall hhyyggiieennee aasssseessssmmeenntt aannaallyyssiiss[[LLooggaann,, 11999988]].. TThheerreeiiss aa ssttrroonngg ccoorrrreellaattiioonn bbeettwweeeenn tthhee hhiigghheerr eemmppllooyyeeeesseerruumm lleevveellss iinn tthhee pprreesseenntt ssttuuddyy aanndd aaiirr,,ssuurrffaaccee aanndd ppeerrssoonnaall mmoonniittoorriinngg mmeeaassuurreemmeennttss wwhhiicchh ooccccuurrrreedd dduurriinngg tthhee iinndduussttrriiaall hhyyggiieennee aasssseessssmmeenntt..iInn tthhee iinndduussttrriiaall hhyyggiieennee aasssseessssmmeenntt,, BBuuiillddinign33g hhaadd tthhee hhiigghheesstt aavveerraaggee aaiirrbboormnee ttoottaall fflluuoorroocchheemmiiccaalllleevveellsswwiitthh eeaacchh vvaalluuee ddeerriivveedd ffrroomm tthhee ttoottaall mmaassss ooff ddeetteecctteedd ttaarrggeett aannaallyytteess iinn eeaacchh ssaammppllee((PPOOSSF,,PPHHSSFF.,FFCC aammiiddeess,,FFCC ;atliccoohhoollss,,FFCC aaccrryyllaatteess))((sseeee bbeellooww)):: BB11llddggNNoo.. 343 4QOuutusiiddee asiirr *"mmgg//mm3 RReseultNss uol ts ooff Fluorochheemmiiccaall TTyube Samples Average* Air Saammpplleess _Low* N11o99.Samples 00.A.0v01e14r45a5ge* 00L..o00w00*00 [63160 11..66888844 0.1269 00.00007700 0.0047 313 0 000..001882666119 000...0550880407 HHiigghh** 003..8000665001813 030.855.2201156683 00.11224477 MSMuaabddjeeecAAtvvataoiillPaarbbollteeebcbiyyv33eMVOrffdoorrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppNyyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00003355 33MMAA1100005500446688 EPLO330MMS Surface wipe sampling was also conducted throughout the chemical plint (BuilPPdaaiggeneEg3P3sI66-0o101f.06280,556 (Buildings 1,2, Surface wipe sampling was also conducted throughout the chemical plant 33,,44,,1177,,3388,,4499,,5511 aanndd 5577)).. SSaammppllee rreessuullttss iinnddiiccaatteedd tthhaatt fflluuoorroocchheemiiccaallss wweerree ffoouunndd iinn nneeaarrllyy aallllssaammpplleesswwiitthh llaarrggee vvaarriiaattiioonnss iinn ccoonncceennttrraattiioonn.. BBuuiillddiingng33 hhaidd tthhee hhiigghheesstt ssuurrffaaccee fflluuoorroocchheemmiiccaall ccoonnttaammiinnaattiioonn wwiitthh tthhee aavveerraaggee ssuurrffaaccee ccoonncceennttrraattiioonn ggrreeaatteerr tthhaann 110000 uugg//110000ccm?m.2. AAllssoo,, mmeetthhyyll FFOOSSEE aallccoohhooll wwaass tthhee llaarrggeesstt ccoonnttrriibbuuttoorr ooff fflluuoorroocchheemmiiccaallss ffoouunndd tthhrroouugghhoouutt ssuurrffaaccee wwiippeess iinn BBuuiillddiinngg 33.. HHaanndd--wwiippee ssaammpplliinnggss iinnddiiccaatteedd tthhaatt eemmppllooyyeeeess wwhhoo hhaadd wwaasshheedd tthheeiirrhhaannddss hhaadd vveerryy llooww llee-vVeellssooff ffluuoorroocchheemmiiccaallss ddeetteecctteedd.. MMeetthhyyll FFOOSSEE aallccoohhooll aanndd PPOOAAAA wweerree tthhee ccoommppoouunnddss ffoouunndd mmoosstt oofftteenn oonn eemmppllooyyeeeess''hhaannddss..TThhuuss,,tthhee pprreesseenntt ssttuuddyy''ss sserraa fflluuoorroocchheemmiiccaall lleevveellss,, oobbsseerrvveedd bbyyjjoobb ccaatteeggoorriieess aanndd bbuuiillddiinngg llooccaattiioonnss,,ssttrroonnggllyy ssuuppppoorrtt tthhee rreeccoommmmeennddaattiioonsn.s bboommee ffrroomm iinndduussttrriiaall hhyyggiieennee aasssseessssmmeennttss.. TThheessee rreeccoommmmeennddaattiioonnss iirr-cclluuddee ssppeecciiffiicc eennggiinneeeerriinngg ccoonnttrroollss ttoo rreedduuccee iinnhhaallaattiioonn eexxppoossuurree,,aapppprroopprriiaattee ppeerrssoonnaall pprrootteeccttiivvee eeqquuiippmmeenntt ttoo pprreevveenntt oovveerreexxppoossuurree aanndd aapppprroopprriiaattee ppeerrssoonnaall hhyyggiieennee FFrraacctticceess aammoonngg eemmppllooyyeeeess ttoo rreemmoovvee sskkiinn ccoonncceennttrraattiioonnss.. FFoorr tthhee ffiirsstt ttiimmee wwee hhaavvee sshhoowwnn aa rreellaattiioonnsshhiippbbeettwweeeenn sseerruumm PPFHHSS lleevveellss aanndd tthhee nnuummbbeerr ooff yyeeaarrss wwoorrkkeedd iinn cchheemmiiccaall.. TThhiiss ffiinnddiinngg wwaass oobbsseerrvveedd aaccrroossss vvaarriioouuss ccuurrrreennttjjoobb ccaatteeggoorriieess wwiitthhiinn cchheemmiiccaall wwhhiicchh ssuuggggeessttssPPHHSFF,, dduuee ttootitss hhiigghh vvaappoorr pprreessssuurree,,iiss lliikkeellyy pprreesseenntt tthhrroouugghhoouutt tthhee cchheemmiiccaall ppllaanntt pprreemmiisseess.. TThhee `pphhaarrmmaaccookkiinneettiiccssooffPPFFHHSS aarree uunnkknnoowwnn,,aalltthhoouugghhdduueettoo tthhee sshhoorrtteerr cchhaaiinn lleennggtthh,,wwee ssuussppeecctttthhee bbiioollooggiiccaall hhaallff--lliiffee mmaayy bbee lleessss tthhaann PPFFOOSS.. WWee oobbsseerrvveedd oonnllyy aa mmooddeesstt aassssoocciiaattiioonn bbeettwweeeenn yyeeaarrss wwoorrkkeedd inn tthhee cchheemmiiccaall ppllaanntt aanndd sseerruumm PPFFOOSS,,aanndd ttoo aalleesssseerr eexxtteennttPPOOAAAA,,lleevveellss.. TThheessee aassssoocciiaattiioonnss aappppeaerattroo bbee mmoorree eevviiddeenntt aammoonngg eemmppllooyyeeeess wwiitthhiinn tthheiirr ffiirrsstt ffiivvee yyeeaarrss aass ddeemmocnnssttrraatteedd bbyy ssiiggnniiffiiccaanntt qquuaaddrraattiicc aassssoocciiaattiioonnss ffoouunndd wwiitthh bbootthh mmaallee cchheemmiiccaall ooppeerraattoorrss aanndd Sih iorochOrdee Palmer. OW 530.8308 +" Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00003366 3sMuAn1o0o05s0o4e6s9 EPLo03s0mMs Poge 70185 EPI-0006 Page 37 of85 eennggiinnceeerrss//llaabboorraattoorryy ppeerrssoonnnneell.. Like tthheeiirr mmaallee ccoouunntteerrppaarrtts,,ffeemmaallee cchheemmiiccaallooppeerraattoorrss aappppeeaarr {t0o hhaavvee iinnccrreeaasseedd Like EHS levels with yyeeaarrss wwoorrkkeedd.. HHoowweevveerr,,uunnlliikkee tthheeiifr mmaallee ccoouunntteerrppaarrttss,,tthheerree wwaassnnoo PFHS levels with apparent lliinneeaarr aassssoocciiaattiioonn bbeettsweeeeenn PPFFOOSS aanndd yyeeaarrss wwoorrkkeedd.. WWhheetthheerr tthhiiss iiss dduuee ttoo apparent Gifferent wwoorrkk pprraaccttiicceess,,eexxppoossuurree ppaattteerrnnss oorr pphhaarrmmaaccookkiinneettiiccss oonnccee aabbssoorrbbeedd,,rreemmaaiinnss different 10 be deterrmmiinneedd.. GGeennddeerr--rreellaatteedd ddiiffffeerreenncceess iinn tthhe ttooxxiiccookkiinneettiiccs ooffPPOOAAAA hhaavvee bbeeeenn to be dete reported foorr rraatss aalltthhoouugghh tthhee mmeecchhaanniissmm ooffeexxccrreettiioonn mmaayybbeessppeecciieess ddeeppeennddeennttssiinnccee reported f hese gender difffeerreenncceess wweerree nnoott oobbsseerrvveedd iinn mmiiccee,,rraabbbbiittss oorr ddooggss{(GGrriiff`itthth aanndd LLoonngg,, these gender dif 1980; HHaannhhiijjaarrvvii aanndd YYlliinneenn,, 11998888)).. TThhee hhaallff--lliiffee ooffPPOOAAAA wwaass eessttiimmaatteedd ttoo bbee 77 ttiimmeess 1980; hhiigghheerr((77 ddaayyss))iinn mmaallee rraatss tthhaann ffeemmaallee rraattss.. A limiittaattiioonn t0o tthhiiss ssttuuddyy ddeessiiggnn wwhhiicchh mmuusstt bbee ccoonnssiiddeerreedd iinn tthhee iinntteerrpprreettaattiioonn ooff A lim hthee ddaattaa wwaass oouurr iinnaabbiilliittyy ttoo mmoorree aaccccuurraatteellyy qquuaanntiiffyy aann eemmppllooyyeeee''ss wwoorrk hhiissttoorryy experience.. DDeeccaattuurr wwoorrkk hhiissttoorryy rreeccoorrddss pprroovviiddee ddeeppaarrttmmeenntt nnuummbbeerrss aannddjjoobb ttietlses bbuutt experience they ddoo nmoott pprroovviiddee iinnffoorrmmaattiioonn rreeggaarrddiinngg wwhheerree ssoommeeoonnee wwoorrkkeedd((ee..gg.,, gwhhaatt bbuuiillddiinngg(ss)) they or with wwhhaatt ssppeecciiffiicc fflluuoorroocchheemmiiccaallss)).. SSeellff--rreeppoorrtteedd wwoorrkk hhiissttoorryy iinnffoorrmmaattiioonn oabbtiaaiinneedd or with by qquueessttiioonnnnaaiirree wwass hhiigghhllyy ccoorrrreellaatteedd wwiitthh DDeeccaattuurr wwoorrkk hhiissttoorryy reeccoorrdd iinnffoormmaattiioonn;; by nevveerrtthheelleessss,,tthhee ssppeecciiffiicciittyy ooff wwhheerree ssoommeeoonnee wwoorrkkeedd aanndd wwiitthh wwhhaattcchheemmiiccaallss wwaass nnoott ne kKnnoowwnn.. BBeeccaauussee mmaannyy ooppeerraattiioonnss aarree iinn bbaattcchh mmooddee,,tthhee lliikkeelliihhoooodd ooffddeetteerrmmiinniinngg ssppeecciiffiicciittyyooffwwoorrkkllooaadd fflluuoorroocchheemmiiccaall eexxppoossuurree aammoonngg cchheemmiiccaall ooppeerraattoorrss iiss nnoott ppoossssiibbllee.. FFuurrtthheerrmmoorree,,ssuucchh rreeccoorrddss ddoo nnoott eexxiisstt bbaacckk iinn ttiimmee.. NNeevveerrtthheelleessss,,wwiitthh uussee ooff hthee eemmppllooyyeeeess ccuurrrreenntt((oorr lloonnggeesstt))jjoobb aalloonngg wwiitthh aaddddiittiioonnaall ssuurmrooggaattee vvaarriiaabbllee eexxppoossuurreess ((yyeeaarrss wwoorrkkeedd iinn cchheemmiiccaall,,bbuuiillddiinngg nnuummbbeerr))wwee wweerree aabbllee ttoo ccoommppaarree aanndd ccoonnttrraasstt ffluuoorroocchheemmiiccaall lleevveellss.. TThhee lleeaasstt pprreeddiiccttiivveeoofftthheessee tthhrreeee vvaarriiaabblleess(jjoobb ttyyppee,,bbuuiillddiinngg aanndd yyeeaarrss wwoorrkkeedd))wwaass yyeeaarrss wwoorrkkeedd wwiitthh tthhee eexxcceeppttiioonnooffPPFFHHSS wwhheerree aassttrroonngg lliinneeaarr Sih iorochOrdee Palmer. OW 530.8308 +" Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00003377 AEN 3MA10050470 ilul3M EP1-0006 Pagc 38 of 85 ets ee ends sh aassssoocciiaattiioonn eexxiisstteedd aaccrroossssjjoobb ccaatteeggoorriieess ffoorrPPFFHHSS wwiitthh yyeeaarrss wwoorrkkeedd.. We did not observe an association between hand-to-mouth usage )r hand etn ve es ed es i pt cleanliness(frequency of washing hands)and serum fluorochemical ]eve s. It is possible an association might have been masked because industrial hygiene had i-istituted an aggressive educational campaign several months prior to the collection of blood samples wet tmnt ta in this study;thus, current practices may not be indicative of past practices. Because the half-life ofPFOS is estimated to be 1000 days or more,such an associati:)n may not be discoverable with this study design. The serum levels observed in this study for PFOS and POAA are not different than those that have been previously reported for this study and other 31V, occupational `ppooppuullaattiioonnss[[OOllsseenn eett aal.l,., 11999988aa,, 11999988bb,, 11999999]1..OOllsseenneett aall.[[11999999]]hhaavvee nnoott aassssoocciiaatteedd. hepatic or lipid abnormalities with PFOS levels in the Decatur and Antwerp plant re ere os le 9 1 He populations that underwent voluntary medical surveillance in 1995 and 1997. Hepatic ie rer Sr rt i mPOA ll lipid or hormone levels have not been associated with serum POAA lev-;ls among3M A Cottage Grove male workers who have experienced higher serum fluoro,:hemical levels mn ee es oe De ps GB than those determined in the presentstudy for these Decatur employees!Gilliland and MMaannddeell 11999966;;OOllsseenn eett aall.. 11999988aa;; 11999988bb)).. Im, et ego as. In summary,the objective ofthis proposed research study was to characterize, emt, ein feo mi ROS FS, FAA via random sampling,the distribution ofemployee serum levels ofPFOS,PFHS,POAA, Fro STL FRO md MSS te SMDc hich fies Te PFOSAA,M570,PFOSA and M556 atthe3M Decaturchemical andfilm plants. The ddaattaa oobbttaaiinneedd ffrroomm tthhiiss eexxppoossuurree aasssseessssmmeenntt iinnvveessttiiggaattiioonn aarree. iimmppoortraannt ffoorr sseevveerraall rm. Fee ston eteinfeGk reasons. First,these data allow for a better understanding of the exposure distribution of em forte inh dt st ie serum fluorochemical levels in both the chemical and film plant employee populations. Second,these data may serve as future reference regarding human exposure assessment SL gies vr Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 amour 3MA10050471 2881122..00038 EPL003M0M6 forthe film as wela the chemical plant in the area of health studiieess aanndd cxposPPuaarggeeeEP33I99-0o01f0880556 exposure area of health stud for the film as well as the chemical plant in the reduction. Third. tthhee ddaattaa mmaayy bbee uusseedd ffoorr tthhee ccoonnssttrruuccttiioonn ooffaann eexxppoossuurree mmaattrriixx ffoorr tthhee Third, reduction. anticipated uuppddaattee oofftthhee rreettrroossppeeccttiivve.e ccoohhoorrtt mmoorrttaalliittyy ssttuuddyy oofftthhee DDeeccaattuurr eemmppllooyyeeee anticipated populatiioonn.. FFiinnaallllyy,tthhiss ssttuuddyy wwiillll aallllooww ffoorrtthhee ooppppoorrttuunniittyy ffoorr eemmppllooyyeeeess ttoo kknnooww tthheeirr populat own serum leevveellss ffoorr tthheessee sseevveenn fflluuoorroocchheemmiiccaallss aanndd eennccoouurraaggee ffuurrtthheerr pXr-araccttiicceess lleeaaddiinngg own serum l to. rreedduuccttiioonn iinn tthheeiirr sseerruumm fflluuoorroocchheemmiiccaall lleevveellss bbyy tthhee vvaarriieettyyooffeexxppoossuurree--rreedduuccttiioonn to a methooddss rreeccoommmmeennddeedd iinn tthhee DDeeccaattuurr iinndduussttrriiaall hhyyggiieennee eexxppoossuurree aasssseessssiinneenntt rreeppoorrtt meth [(LLooggaann,, 11999988]1.. Sohalto techs Ore aime +. 3. C204a30s Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00003399 3SMMAA1100003500447722 Epi00330MM6 PPaaggeeE4P4I00-0o01f0880556 RREEFFEERREENNCCEESS Griffith F, LLoonngJgJ.. AAnniimmaall ttooxxiicciittyy ssttuuddiieess wwiitthh aammmmoonniiuumm ppeerrfflluuoorroooocctt tnnooaattee.. AAmm Iinndd GHHryyifggfiAAtsshssFoo,cc 11998800:;4411::55776600558833.. HHpaeanrnfhhliiujjoaarrrovvoiicHHta,,nYYolliciinnaeecnnidMM.i.n tAAheppbrreooappgoolsseeedddossgppeeacciniedessraddtii. ffffIeenrr:eennBcceeeyiinnnetnthheeA,rreeSnnoaalllleeexxvccerrlnid:ttHiio,onncdoodsfsf.. n A,Solleveld H,e NNeeww DpeervfelluoopprmomoeecnntttassnoiiinncBBaiicooissdcciiienennctceheses:b:ettahhegeiilrreIIdmmoppglliiaccnaadttiirooanntss. ffIoonrr:LLBaaebbyoonrreaattoorryy AAnniimmaall SScciieenncceess. DDDooerrvdderrleeocchhtt:: MMaarrttiinnuuss NNiijjhhooffff.. 11998888::440099--441I22.. HHaannsseenn KK.. `Employees LaLtaabb3ooMrraaDtteoocrrayytuRRree.ppoorrSttt.::PAAannuaalll:yy3ssMiissoEonffviFFrCCossnmiiennnSSteearrluuLmmabSSoaarrmmaatpptolloreerysys..CCooJJlulunllngeec:cc,,tt1ee19d9d99F9F9.rr.oomm l Labo Employees at 3M Decatur. St. Paul:3M Environmenta L(LUoonggpaaunnblPPiWWs..he3d3rMMepDDoeercctaa)ttuuSrreFpFlltuueoomrrbooeccrhhee1mm5,iicc1aa9ll98II.nndduussttrriiaall HHyyggiieennee EExxppoossuurree AAsssseessssmmeenntt.. (Unpublished report.) September 15, 1998. GGJiiillplloiipllraaonntddeiFFnDDs,,anMMdaannchddoeellelstJJSeS.r.olSS:eerrauusmmtuppdeeyrrfolffuloocurcoouorpcaottaoincoontiacaallnacllcyoyiidieedxxaappnnooddsseehhddeeppmmaaetetniin.cc.eenAnAzzJJrmIieMmMses1,1,999966;:2266::556600-- l5i6p8oproteins and cholesterol: a study of occupationa 568. eOOpllissdeeennmGGioWWl,o,gGGiiiclllliiinllvaaennsddtiFFgDDa,t,iBBonuurrollfeerwwepMMroMMd,u,cBtBiuurvremishsoJJrMMm,,onMMeaassnnddiinenellmmeeJJSSnn,,wwMMiiaattnnhhddooeeccllccuuJJpIp1Laa1..ttiiAAoonnnnsa!l eexxppoossuurree etopippdeeerrmffillouulooorrogooiocccttiaannvnoeiiscctiaacgciaidtd.i.onJJ OoOfcccrceuuppproEEdnnuvvctMMiveeeddho119r999m88oaan;;e4400::661144--662222.. to OOplllssaeesnnmaGGcWWh,o,leBBcuuryrrsritisoskJJiMMn,i,nBBauunrrdlleehwwepMMatMMi,c,fMMuaanncntddieeolln JJiHnH..peAArrffnnlluueeoopprriiooddooeeccmmttiiaaoonnllooooiiggcciiaacccciiiinddnvvppeerrssoottddiiguguaaccttttiiiioooonnnnooff wpolraksemras.ch(o(l33eMMcyuusnntpopkuuibbnlliiinsshhaeendddrrheeepppoorarttt))i:;c1f19u99n98c8btb.i.on in pe workers. OOhlelpssaeetnnicGGaWWn,,d BBluiurpirmdissclJJiMnMi,,caMMlaacnnhddeeemllisJJtHHr,y,ZZeoosbbteellinLLRRf.l.uoSSreeorrcuuheemmmmippiceecarralfflllppuurroooorrddoouuooccccttttiaiaononnene ssuullffoonnaattee aanndd. eemmppllooyyeeeess.. J OhecpcauutippcEEannnvvd MMlieepiddd((c11li99n99i99c,,aliinnchpperrmeesissss))t..ry tests in fluoroch Occ Roacchh DDEE.. FFlluuoorroocchheemmiiccaall CCoonnttrrooll SSttuuddyy.. 33MM UUnnppuubblliisshheedd RReeppoorrtt.. 33.V.V1I CCoommppaannyy::SStt.. PRPaaouuall,, MMNN MMaayy 2255,, 11998822. `FSlScuchohurumomcaahnneLLmiMMca((l1199C88o22n)t).r.oLlLeeStttttueerdrytt.oo DDArrp..riFFlrraa29nn,kk UUbbeell((33MM 1982. MMeeddiiccaall DDiirreeccttoorr)) ccoonncceerrnniinngg Fluorochemical Control Study. April 29, 1982. VVinoollHllummmeearrnDD..SeQQruuuaanmntibittyaatLtiiCvv/eeMDDSee/tteeMrrSmm.iinnSaaattliitooLnnaookffePPFFCiOOtSSy,,::NNPPooFFrrOOtthhSSwwAAee,ss,ttPPBBFFiiOOooaaSSnnAaaAllAAyyt,t,iiccPPalOaO.lAA. AAJJuuaallnyyndd11P9P999FH99SH...S in Human Serum by LCIMS/MS. Salt Lake City Sih io roche Orde Palmer. OW530.8308 +" MMaaddee AAvvaaiillaabbllee bbyy 33MMffoorr IInnssppeeccttiioonn aanndd CCooppyiynigng aass ConfiCondfiedenr tial Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00004400 3aMMAA1T00005500447733 EPLO03MOMS PPaaggeeE4P31I1-0o01f0880556 AACCKKNNOOWWLLEEDDGGEEMMEENNTT `TThhee iinnvveessttiiggaattoorrss ggrreeaattllyy aapppprreecciiaattee tthhee ccoonnttrriibbuuttiioonnss ooff KKiimm YYoouunngg ttoo tthhiiss ffiinnaall rreeppoorrtt.. MSMuaabddjeeecAAtvvataoiillPaarbbollteeebcbyiyv33eMVOfrfodorrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00004411 33MMAA1100005500447744 3 2538 5 gg 2% 8&2 Z ds 28 28 aT 85 2=a S2f gsTFds $ER2z 3p2g%aczcciaets fF ggEegedc: : 2 gl [IE7 =~EILNElTEHHeS B5F R 8EFO FETFRB&REII F8PgBEIE5E3s5cyY RE2gf HI : I Hpoogss8E3s%E:3 3g MSuabdjeecAtvtaoiaPrbolteecbtyiv3eWOrodrIenrsIpnePctailomneavrn.d3CMo,pNyoi.ngC2a.s0C4o-n6f3id0e9ntial Information 28122..00042 1M EPI-0006 Page 42 of85 3 : 2 ee 8 228 TFH 2otr--ozs2eaos c-mva[m3es2F5mn Gweo-oslse 3 :E Bosl 2gHE 2 ig= Table 1. Random sample selection by Decatur departments with percent participation Dept Number Dept Name Employees with 090 location codes 7613 3M/Dyneon Related Decatur Total N Sample Size 112 30 2LI] 2 8 Q FaSE55E5S2 3$5 Ey CEeSF32 ffpifissieenisl FR EfEzzE85Ec 7620 7621 Decatur Bldg 2 Operations 25 10 Bldg 49 Operations 1 ffigni=i i:idi555e 7 mill ESllsazeszgasss Bf3 7630 Decatur Bldg 3 Operations 113 30 7641 Decatur Bldg 4N Operations 60 15 7609 Decatur SMD Maint-SA&C 54 15 37 6825 8038 7604 7605 7616 7617 7622 Mfg Servcices Process Eng 2 26 Process Instrumentation & CN 1 Supply Chain Resource Unit 1 Decatur SMD Chem Factory Adm. 4 Decatur SMD Chem Quality Ass 25 Decatur Chem Ship Rcv Whse 24 Decatur SMD Logistics 10 Decatur PCPD FF Admin 24 ae 5980 Decatur EHS&R 21 5 3 85888 8 Employees regardless of090 or 190 location 6853 Auto & Chem Mkts Eng 8(090) 5 6853 Auto & Chem Mkts Eng 6(190) 4290 Auto & Chem IT NPI/R&D 1 (190) 2 4294 Auto & Chem IT Mfg -- Quality/S 4(190) 4297 Auto & Chem IT CMG Mfg 6(190) alSs35e = 53 Waste water treatment employees 3 % 5984 Decatur Waste Treatment 6 6 2 Participated(%) Yes No 25(83) 7(70) 5(17) 5(30) 25(83) 13(87) 14(93) 23(88) 5(17) 2(13) 1 (7) 3(12) g5 23 5 (100) 4(80) o(o) 1 (20) 6(100) 0(0) Ea ~~Ti~~iId,/1E~ s gz MA10050475 SMuabdjeecAtvoaiParbolteecbtyiv3eMOfrodrerInIsnpePcatiiomneavrn.d3C.opNyoi.ngC2a-s0C4o-n6f3id0e9ntial Information 28122..00043 CC:I)vK iD m 0 > o v a iv om M 0 rn``,, 0 ~., EL rn CD -, Q & Sf45AZ3 E3 5 F - Eof 3 Table 1 (continued) HI Ey lk g 23 g8% 2 8 .0gd =2& 5 Dept Number Dept Name 83 Heatingplant employees 5982 Decatur Heating Plant Film plant employees All remaining 190 location Department codes Dyneon TOTAL Dyneon employees 12 dp SM EPI-0006 Page 43 of85 af = 1Lc gE 8 2 3= Total N Sample Size 10 4 Participated(%) Yes No 3(75) 1 (25) ! g ng 482 78 25 8 1025 232 32 a Sglgs 55(71) 6(75) 186(80) 23(29) 2(25) 46(20) zE2 0 3 v 0o' 9LV0900WAC MAT0050476 i8 2g 2c cggszeze & 8= dFreyeAvraibaioyby 3Sfobrnspecctaon anndsCoptyingSa oGnfbdental formation rCD- K 6 N CL cD CD 0 > rt ~ O N Q1 O 07 M CD CD O o E E -q o Qw a) o 3 v g: irl EPI-0006 Page 44 of85 3 i 32 3 : 2 3 = 3% g i] ff es gg i : 7] 2 eg 3 to sg i: :3 id .. i 3 Table 2. Number(and percent)ofrandom sample, volunteer and all participant chemical employees by demographic characteristics 3, 4 Jill Gender Female Male Only Worked In Chemical Yes No Current Job Cell Operator Chemical Operator Engineer/Lab Maintenance Mill Operator Secretary Supervisor/Mgmt Waste Operator 588g 2 =Es ] Sample(N = 126) = ag N (%) 24 (19) 102 (81) 67 (53) 59 (47) 5 (4) 47 (37) 23 (18) 11 (9) 13 (10) 4 (3) 18 (14) 5 (4) gg esseseze $3 "sRzovae Volunteers(N =61) N (%) 9 (15) 52 (85) 28 vozes-=o 33 (54) 28 (46) 4 (7) 17 (28) 14 (23) 6 (10) 11 (18) 1 (2) 8 (13) 0 (0) g% R=I8" gg ecggssese i All Participants(N = 187) N (%) 33 (18) 154 (82) 100 (53) 87 (47) 9 (5) 64 (34) 37 (20) 17 (9) 24 (13) 5 (3) 26 (14) 5 (3) 2 58 28122..00044 LLV0500WNC esgsszzses TT Jill 5 awatooso477 Longest Job Cell Operator 1 gist il Chemical Operator 5E 57 Engineer/Lab 21 Film Processor 3 Maintenance 14 Mill Operator 14 Secretary 6 =Es Supervisor/Mgmt 7 Waste Operator 3 "REmIze~~ (1) (45) (17) (2) (11) (11) (5) (6) (2) cgsszzees ~gEnen-we 2 (3) 20 (33) 10 (16) 2 (3) 6 (10) 12 (20) 1 (2) 8 (13) 0 (0) "RE"8R"~=2e =gsasgsas 3 (2) 77 (41) 31 (17) 5 (3) 20 (1 l) 26 (14) 7 (4) 15 (8) 3 (2) 28122..00045 8LI70900LV"C MMO0S0478 MSuabdjeecAtv1aoiaPrbolteecbtyiv3e OfrodrIenrsIpneactiiomn eavn.a3C,opNyoi.ng2.as04Co6n3fi0d8ential Information Cr-O Kv cD m ~a~ o v 0 CD m CD w O~ a0 , CD N E a -0 m 2L 0 CD D Zw nQ 0 CN)v(n 60 CO =h CD a) E 0 R 0P 33E3525 3S232s S5s2 32-32s 3E5s2s z3 Fs3 & 3 z S gife S gaLF2 = i S Table 2. (continued) Chew Gum Always/Frequently Sometimes Rarely/Never Chew 'lbbacco Yes No Smoke Cigarettes Yes No Hand to Mouth Contact Yes No Wash Hands No 5 8 3 s i = t Sample(N = 126) N (%) 22 (18) 32 (26) 70 (56) 19 (15) 105 (85) 41 (33) 82 (67) 84 (68) 40 (32) 1nI .V1 23 (8I j (19) gl Tl 2238g 2=&z8 #BE5 8a88 &a25 2T] Zl use 23 I 3% ER 1~1 EP1-0006 Page 45 of85 agll 4 a7r 8e 8 2888 BaEs 8g&g8 3288) zl | "lz es ex zz 92 us Volunteers(N = 16) N (%) 14 (23) 20 (33) 26 (43) 6 (10) 54 (90) 14 (23) 46 (77) 42 (70) 18 (30) i421 (70) 18 (30) | E z All Participants(N = 187) N (%) 36 (20) 52 (28) 96 (52) 25 (14) 159 (86) 55 (31) 128 (69) 126 (68) 58 (32) i43 fits) 41 (22) z Z| 2 ses sz =m 8% 3s | =k aSitteiooto Py roceSROgrrr1 paolmeSrv o31hnNoa2S.e04S63e05at fom 28122..00046 Crl-) Ka) S7m nco a D o iu ~o wa m m o w O ~ ELo m m -13m o m 3 a Zo 'sD N v o 6 3 La CL m D v 5 v 6Lb0C;006b'W ITD gE 3 2% 3M EPI-0006 Page 46 of85 533 EBE2 LE BOR io=| 3 FEo og 3 3 :i 8g 2: $=F $s8e2s2e8c3aTcEsMrRrEcEe @ $35ERIEB35% fzot =ig$7 82maNa2RTIoe 2 z| sIsasgogzoen g: j \8| BES288E28288C 1 $33508ERE8ET 2 d= JaAFRY=Iegae Table 3. Percentage ofemployees from the random sample,volunteers and all participants who responded that they currently work and ever worked in Decatur buildings/areas Lu _288222233ll82088gidl"5ds 5 3:u 3 5E1f4 :5 Currently Work in Buildings... 1 2/49 30S 3 NOS 4 N 4 Mill/Extruder 17 38/51 42 61 Film Wastewater Ever Worked in Buildings... 1 V49P 30S 3 NOS 4 N 4 Mill/Extruder 17 38/51 42 61 Film Wastewater Sample(N = 126) N (/a) 42 (33) 22 (17) 39 (31) 41 (33) 37 (29) 45 (36) 18 (14) 24 (19) 15 (12) 23 (18) 12 (10) 14 (11) Sample N (/o) Z| HRBRIINRALTS 52 (41) 33 (26) 68 (54) 72 (57) 64 (51) 80 (63) 22 (17) 36 (29) 29 (23) 25 (20) 41 (33) 19 (15) | Volunteer(N =61) N (%) 22 (36) 16 (26) 21 (34) 23 (38) 22 (36) 29 (48) 10 (16) 21 (34) 14 (23) 14 (23) 9 (15) 10 (16) i Volunteer N (/a) 25 (41) 14 (23) 30 (49) 31 (51) 30 (49) 43 (70) 9 (15) 21 (34) 18 (30) 12 (20) 19 (31) 7 (11) 2 Ez TEBIAIZLARG <z| RSR3IICRTRBE All Participants(N = 187) N 64 (34) 38 (20) 60 (32) 64 (34) 59 (32) 74 (40) 28 (15) 45 (24) 29 (16) 37 (20) 21 (I1) 24 (13) All Participants N (%) 77 (41) 47 (25) 98 (52) 103 (55) 94 (50) 123 (66) 17 (9) 57 (30) 47 (25) 37 (20) 60 (32) 26 (14) si. Ld 8288 8232 5 552, 83_E8 ES : 21+% 3s8e8a3c8a8g2e8ge8g8e2s2 J 2CR3A8AS8E2sE2G88R8T7| . JE 8 8 8 3 = 8s 2 2 1 7%: i g 8 2 & 8 2 BHN eE5F f88&8 Eg 8EC2I 2ogg3 MSuabdjeecAtvtaolParbotlebcyiv3e OfrodIenrsIpnePctailomnearvn.d3C,opNyoi.ngC2a.s0C4o.n6f3d0e9ntal formation C/)K v- Q m 0 o < -0 w o g D 0CD7 C Oo Q rn 0 ET D _0 -o m E a a ~ 0 z~ N cQ N i Ln A 0 O W to CD 0 3 v o' 1 M EPI-0006 Page 47 of85 3: Ef Z0f iiT : g#gf3z8F 523 2 f: i z A 2gLEE8 $ f8 z E 2s 1g 23 2i zi Table 4. Serum fluorochemical levels(ppm)ofrandom sample, volunteers and all participant chemical employees gE f8s2 =2 zFg 582 5 $5 3 s8s 83 ss os 4. 8 88 c 22Bg g 22 2 2g 5 z3 PFOS Random Sample Geometric Mean Mean Median Range 1.505 0.941 1.140 0.091 - 10.600 Volunteers Geometric Mean Mean Median Range fEs 1.259 0.758 0.877 0.052-4.940 i2j All Participants Geometric Mean Mean Median Range 853 % 1.424 0.877 0.994 0.052- 10.600 =EE= 83 858 88 gs$8C8f 5EE2 :3 PFHS 0.345 0.180 0.170 0.005- 1.880 0.272 0.122 0.125 0.001 - 1.590 0.321 0.159 0.167 0.001 - 1.880 POAA 1.536 0.899 1.300 0.021 -6.760 1.206 0.649 0.908 0.015- 4.640 1.429 0.808 1.200 0.015-6.760 53= gE & EE2s 38 8 33 82 %8 8 EEz E3 858 888=8 88 5 288 83 8 fff 8 I8 88 88 25 = z "= 8Ss 8Ss" 3 5 0s gz 8 2% 8 < 3EE8 E PFOSAA 0.023 0.008 0.008 0.001 -0.269 0.026 0.007 0.006 0.001 -0.234 0.024 0.008 0.008 0.001 -0.269 M570 PFOSA 2 0.150 0.062 0.081 a 0.013 0.067 0.008-0.992 0.012 0.0005-0.612 0.173 0.068 0.029 0.006 0.054 0.004-3.100 0.007 0.005-0.443 0.158 0.076 0.051 0.010 0.063 0.004-3.100 0.010 0.001 -0.612 Es Ligs 28122..00047 | 32 3% 2ig 33f3%e 311%% 3|3 fF :| g:$|8 |2 i33|%3 ||&% 32 : 3 gE 2- max) V.U.'),4 U.ULL U.ULb U.VUI - U.4Uo U.U41 U.UtU U.018 U.UUs - U.329 3 33 U.U48 0.022 U.023 0.001 -0.406 a. significantly different(p <.05)geometric mean than volunteers,student's t test [41:3Iixelfi l/YIE 3MAO050480 281122..00048 681709006t/W MAT0050481 SMuabdjeecAtv1aoiParbolteecbtyiv3e OfrodreIrnsIpneactiiomn eavn.a3C,opNyoi.ng2.as04Co6n3fi0d8ential Information CD M ~ Q { o v o - M CD < w Q o 5 E Cl) -U(D a ~ 0) w a o Z-0 cQ N n) CD n w~ o a CO m a o 3 3 AsuRsIf 1R2A.D8988 EE 88 idoiibf E8E3 e2z sg iif i 12 gs5 22 -M EPI-0006 Page 48 of85 Fpl BRR] z i7: ing%" i 5a gg da$2d8)g 3 2[3513H6 2 Z| ii$03089 v(=o.]% : i, v E i y 3k pmsl= en=33g3g 2OB2R OggR8E% OL ic fSegon dp Lnis b34, 2IgJ iz s.41 i21,1 F FIER E EIRTTET ER i a eevnecnes - THE OZR OER: gRgl3 sl.3 g csDs S9R8 28%5 2i%g 2 Is%3 WLeude %Fgosafl = 49 Table 5. Demographic characteristics ofcurrentjob categories ofrandom sample(N = 126)ofchemical employees Cell Operato? (N=5) Chemical Operator' (N=47) Engineer/ Lab` (N=23) Maintenance (N= 11) Mill Operator` (N= 13) Secretary (N=4) Age Mean SE(standard error) Median Range 3 45e 1.2 44 40-50 ined= a 13.4 68 & 42`'8'" 1.2 43 25-62 4leA 1.7 42 23-58 41' 9, 2.5 42 27-52 35`"`h 2.3 34 27-45 e 45e 4.2 45 42-49 wFaaeslt 12593S8E BMI Mean SE Median Range 25.8 1.5 25.0 22.1-30.0 2 28.3' 5.1 27.8 20.2-47.5 = 27.6 5.0 27.6 18.5-38.4 z 26.9 2.8 26.6 22.9-32.5 27.7 5.4 27.3 19.6-42.0 | 22.4'8 2.0 22.0 20.9-25.1 RRR Years Worked In Chemical Mean SE Median Range 23b.Qe 2.0 24 17-29 - II`ee 1.4 10 1 -31 - 15, 2.8 15 1 37 9fika 3.0 4 1-26 3.D.c.E&h 1.5 1 1 -21 15e 4.9 18 2-25 Gender* Female Male N(%) 1 (20) 4(80) N(%) 10(21) 37(79) N(%) 6(26) 17(74) 5 N(%) 0(0) 11 (100) N(%) 1 (8) 12(92) N 4(0) 0(0) Only Worked In' chemicx Yes No Hand to Mouth Contact Yes No Wash Hands Always Less frequently BF 3(60) 2(40) 3(60) 2(40) 5(100) 0(0) 23(49) 24(51 35 (76 11 (24) 40(87) 6(13) 14 (61) 9(39) 11 (50) 11 (50) l6(73) 6(27) 28 dl 6(55) 5 (45) 8(73) 3 (27) 10(91) I (9) 11 (85) 2(l5) 10(77) 3(23) l2(92) 1 (8) 1 (25) 3(75) 2(50) 2(50) 2(50) 2(50) if: $2.3 vel RRS ERE RRR Supervisor/ Mgmta (N= 18) 47b.c.4c 2.0 45 41 -57 29.5f 6.1 27.6 21.8-47.3 20"''d e 2.5 24 1-36 N(%) 2(11) 16(89) 9(50) 9(50) 12(67) 6(33) 13(72) 5(28) O EE R2E8 oo *Currentjob types significantly different, p <.05 chi square statistic (a-h)comparison for each currentjob category using student's t(p <.05) '" i29 3in2.%w BwUmR=L% Lxo3.a5l gsE=S =gz R3%OAEg Waste Operator (N=5) 5&cAe 3.7 50 49-52 25.5 3.2 25.8 21.8-30.1 14e 4.5 16 1 -27 N(%) 0(0) 5(100) 0(0) 5(100) 3(60) 2(40) 3(60) 2(40) 8 2 ss a9 3 tal 3 2 MSuabceecAtviaoiPaeblcokys3 OorrdeInIsnpePcatilonmaenaHChopyin6g2a.0C4o6n3f0i8dent nfomaton 2881122..00049 Cn R: r-- Q `D o v ~w o D rn ``,, p ~; QC o (D _% 0 vm O1 0. 0 CO ~;: n Z ~ ~ ~~ n `O N~ 60 ~ w R Z8b0500W ne -- f g s ZF 8 2 zEEZ| $: s| Iii EPI-0006 Page 49 of85 & 55 8 es ze gs: 43 2 I3sH 5z % gss doe zx {EE == 51igPog4i2&fE s5e. ==mx o333r3 E-s8 - gr | f i &o TEi 2z EL Ess ffEl g2r sF 8gz =om 388 3 i | foros oz gg I 3 Table 6. Mean,geometric mean and median ofserum fluorochemicals by demographic characteristics ofrandom sample(N = 126)of chemical employees Gender Female Male Mean 0.686 1.697 PFOS Geometric Mean Median 0.459 0.897* 0.412 1.310 E53338 fg.2 #32 s 3ig se o TEi om om i Hand To mouth Yes No 1.362 1.810 1.008 0.674 1.140 0.954 Wash hands Yes No 1.581 1.179 0.897 0.459 1.190 0.735 Worked only in chemicai Yes No 1.113 1.927 0.723 1.271 0.784 1.550 |$g3za2= 322%33 sEggEa t22H2 Mean 0.118 0.398 PFHS Geometric Mean Median 0.080 0.218* 0.082 0.223 0.278 0.474 0.173 0.185 0.168 0.181 0.360 0.259 0.188 0.136 0.176 0.126 0.247 0.456 0.126 0.270* . 0.141 0.306 5s28 EfIl 25 2333 23s8 Mean 0.691 1.735 POAA Geometric Mean Median 0.326 1.142* 0.245 1.000 1.504 1.602 0.963 0.637 1.355 1.210 mg oa 1.597 1.263 0.978 0.731 1.300 1.300 8g%m a5g2 OE5s 1.307 1.797 0.729 1.142* 1.060 1.590 ss ss =3 3 8g 352 EsHz 253 3sg _Eg3%g& 3g23z% 3g253r 3g23rm 3g2g= T g 832 53 13 1I] [(IdEs 2= BE-TERE E32E} Fi33t,E MaceviaFleesbtyi3iorr neerctBioanmaandiChopiying53a:5C4a5n3f0e8ntal information C/)WK cD m D o iv -0 w o g m m w a 0 -n D 5Cn -o m =-~' a 0 cD 4 =3 n z z 0 ,-~0< C~ C5a N N i Ln 6)o o Co aCD a~ 0S v 0 2 i 8" z3 $ Table 6. (continued) PFOSAA Gender Female Male Geometric Mean Mean Median 0.011 0.026 0.003 0.010 0.002 0.009 i Hand To Mouth Yes No 0.026 0.019 0.009 0.007 0.008 0.008 Wash hands Yes No 0.025 0.017 0.009 0.005 0.009 0.003 Z5 :Forked .;nly in chemical Yes No . 0.024 0.022 0.009 0.008 0.008 0.008 H i Hsg ggsz sHHz gosz EPI-0006 Page 50 of85 ) %E =g2| 54 :g8s gg|l &8258 gag2 s52 232 2gg = Ss gs 2% i 3j 3iz ESLz 228 gBzE 3ge g28 3 sz3g $83g 3g3g 3a2t 3 M570 Geometric Mean Mean Median PFOSA Geometric Mean Mean Median PI & M556 Geometric Mean Mean Median 5| sz g 238 0.077 0.168 0.053 0.089* 0.052 0.073 0.037 0.068 0.012 0.013 0.014 0.011 = Ss 0.025 0.058 0.014 0.025 0.013 0.028 528 g3t% as es i 0.153 0.139 0.085 0.079 0.637 0.081 0.050 0.080 0.012 0.013 0.012 0.011 oe ze So 0.054 0.048 0.022 0.026 0.021 0.030 0.162 0.893 0.088 0.055 0.672 0.632 0.063 0.045 0.013 0.009 0.013 0.009 o 28 Ss 0.059 0.020 0.026* 0.012 0.028 0.015 g2s8 0.142 0.160 0.075 0.088 0.063 0.074 0.059 0.065 0.012 0.014 5g3z 0.013 0.011 an ex 0.046 0.058 0.019 0.027 Sc 0.019 0.030 BE 28122..00050 Xo-ul exellIVIVIN o3 7 :2 RS * t test, p <.05 & 3C3387 "337s8 g"2$i.5fss tT: SMuatdeocAtvtaolPaobtlecbhyv3e1OfrodIensnpePctailomnearvn.dWChopyNoi.ng62a.s0G4e.n6f3i0d5ental Information 281122..005511 2 S39 $H2E)5 Re EEEP3io,By2e1 i rl EP1-0006 Page 51 of85 T Po ou farhBy ip fT S39| zigi8s7 Ife 3: Zz iz :i BEE Ce78 2 E E>EaodesuRrT Ta EBekd 1 "g7d8 38 58 5 Shi13 ghdis Table 7. 3 8 u| il 89 ZsFf 4ff d 3 34.4 LoE322833702 z Mean,range,geometric mean and 95% confidence interval ofgeometric mean ofserum fluorochemical levels by currentjob categories among random sample(N = 126)ofchemical employees Cell Operator' (N = 5) Chemical Operator' (N =47) Engineer/ Lab' (N = 23) Maintenances (N = 11) Mill Operator` (N = 13) Secretaryf (N=4) Supervisor/ Mgme (N = 18) Waste Operator" (N -5) E PFOS Mean Range G. Mean 95% C.I. 2.903 0.325-6.840 1.97Vf 0.732 - 5.304 1.781 0.471 -7.260 1.481`''e 6.h 1.250- 1.755 312 81 87 "EgEs 208 8;cE 8:% 0.634 0.095 -1.740 0.391"b-d&h 0.256 - 0.597 1.672 0.291 -4.060 1.299'e e'f 0.822-2.054 0.718 0.230-2.040 0.5890.0 0.419-0.828 0.497 0.220- 1.140 0.397'-b,dh 0.195 - 0.807 1.879 0.091 - 10.600 0.885` 0.480- 1.630 2.649 0.254 - 7.880 1.504'e e,f 0.493 -4.589 318 cEsTcE eTgiEsY 0 C7e8s78 E PFHS Mean Range G. Mean 95% C.I. 1.062 0.083- 1.880 0.697-""'.6 0.228 - 2.130 0.428 0.071 -1.860 0.308`-e,f 0.246-0.386 89535r3 CECT EF AY ES CC8E8R 2"3f= Eg5c 5; 0.171 0.005-0.905 0.078'.&b 0.046 - 0.134 0.237 0.023 - 0.790 0.153' 0.084 - 0.280 0.109 0.028 -- 0.374 0.074',b.&h 0.047-0.116 0.082 0.027 - 0.172 0.066`''6 0.031 -0.140 0.419 0.010- 1.420 0.215'e e.f 0.115-0.402 0.444 0.038- 1.210 0.232`` 0.069 - 0.775 355:BFT CgETcEy .s1s g3i2 Eal 3 ogBuf7 C"EgEE $3318 JoEyT SEgD ] gif nSpia &Y8388&7 OEE LE 81 87 EigE s R8i3f es Bpgcdx 28 gH zgeE 3sn.E3l= T"rfyF Aho85 2 POAA Mean Range G. Mean 95% C.I. 2.213 0.126 - 3.640 1.428c-f 0.422 - 4.833 2.252 0.150 - 6.760 1.887`''6 1.573 -2.265 0.376 0.035 - 2.320 0.208ab.d e,f.&h 0.134 -- 0.324 1.483 0.211 -4.680 1.095" c 0.670 --1.791 1.383 0.450 - 2.340 1.266`'''6 0.985 - 1.629 0.183 0.095 -- 2.611 0.172`'de.&h 0.113 -0.260 1.371 0.021 -4.540 0.637',``-f 0.310- 1.308 1.663 0.936 - 2.710 1.542e-f 1.052-2.259 8%5.82% sCg e IFJO o5go"z : T4E ofggg E[tEgEs ECs Ecg Baif Ec E5 0 gas oGnui gi_.,bi8i 3H.EHi83 E PFOSAA Mean Range G. Mean 95% C.I. -* g"i5z@ I"g3g 2 32 gE Cggr 82epiEfT 3Cg :tg 0.006 0.001 -0.016 0.003''Qe 0.001- 0.009 0.036 0.001- 0.269 0.011`,., 0.007-0.018 0.014 0.001 -0.073 0.0050-111, 0.003 - 0.010 EF 8% 33 OEE JB id 35% ae CRoETE 0.034 0.001 -0.083 0.017`., 0.007 - 0.043 0.020 0.004 - 0.038 0.015~` 0.010 - 0.024 0.002 0.001- 0.004 0.002""" 0.001- 0.003 0.011 0.001 -0.054 u.0ub 0.003 - 0.010 0.009 0.003-0.017 0.066 0.003 - 0.013 2 M570 Mean Range G. Mean 95% C.1. o gaas-- 5;gEgg I. 8 gl C3sios Bal2 aES9 C0% itaoe 0.035 0.024 - 0.056 0.033b.d 0.024-0.045 0.229 0.009 - 0.992 0.131'-e`-f6 0.094 - 0.182 0.074 0.008 - 0.410 0.049" 0.034 - 0.071 Zid iF &3 CEE 213 8: & aisCECE 0.268 0.038 - 0.701 0204a.c,e.f,6 0.124-0.335 0.045 0.025 - 0.115 0.042b.d 0.034 -- 0.051 0.039 0.010-0.072 0.0301.d 0.013 -0.071 0.122 0.010 - 0.553 0.064b.d 0.037 - 0.111 0.087 0.050 -0.159 0.079 0.052-0.12t ilS1SX011l,/1E, 3MMO0SD4E4 WSaidboelAvlaolParlootbeych OfrodrerInspePcatilomneavrndWChopNyoi.ng2a.s0C4o-n6f3id0e5ntial informa 28122..00052 CoK ~ v a D - 0 0 'D CD rn ~ O EL rn m lv a rn < w 0 Z I N CO 0oQ QO m 3 0 3 R o' 0 IS1iXiI1I,/1E, aWAT0OS04ES 5:33 &3 i: g"yEy:e sigs2 1r3y)e: 28Bo%E EE8 W$3.2z88 7 8 7"88 8.5 57 87 % 7% sis 81880 538 E"188% 32s: 3.33 roF4 &E Table 7. (continued) PFOSA Mean Flange G. Mean 95% C.I. 0.003 O.00l -0.011 0.002"` 0.001- 0.005 0.099 0.001 -0.487 0.0284`ds 0.017 - 0.048 0.017 0.001- 4.063 0.005"" 0.002 - 0.010 0.065 0.001 -0.569 0.0096 0.003 - 0.025 0.040 0.012 - 0.204 0.0264` 0.016-0.040 oidoaGkf412 2 LEEEE I7 E3 fTERgS3 8132 8"1E3y1e M556 Mean Range G. Mean 95% C.F. 0.014 0.003 - 0.028 0.011"1 0.005 - 0.218 0.074 0.001 -0.380 0.044 0.032 - 0.061 0.019 0.002-0.127 0.0101.1 0.006 - 0.015 0.115 0.016 - 0.406 0.013 0.002 -- 0.045 0.0744' ``- 8 0.0096.1 0.041 -0.135 0.006-0.015 : (a-h)comparisons for each currentjob category using student's t, p < 0.5 -3883]3= 0.031 0.009 -- 0.080 0.021 0.009 -- 0.054 0.015 0.003 - 0.030 0.0106, . 0.003 -0.031 SHEEE HEEs g:3 VI EPF-0006 Page 52 of85 2 g2 -f 2 of iEiIs &7 of sf oF E3718 "3FgE} 0.065 0.001 -0.612 0.0076 0.003 - 0.020 0.0381 0.002 - 0.161 0.012 0.003 -0-048 0.046 0.003 - 0.336 0.0156d 0.007 - 0.030 - 0.047 0.013 - 0.157 0.027 0.011 -0.068 aSitteiooto Py roceSROgrrr1 paolmeSrv o31hnNoa2S.e04S63e05at fom 28122..00053 U)K ~ v a y o o s rn ca <CD o 8- E m 2L a rn a a) w o Z-0 e? nrv v ~ C7 60 o Q co m o 3 ::I:31i~~iId,/1E~ [-- EPI-0006 Page 53 of85 &Sw- or. f FOoEgS3gl hSogcrd: aheRl3 twead= nAnoid4 aB3Tlg l3afgg E CI 5 2 :@ :g z oEglg issdp fBse] obsF] oEnsdl oGbas] oEoad] V g5 3.8 1.3 iz +8 LF ..% E3e: P3 OR38]% Red= BaT2 nefo nad$ allg old3 Table 8. Fiuorochemical ratios by currentjob categories for random sample(N = 126)ofchemical employees 22 53, S3.g5f4 y 2.:885g f5c.83p g $:Su8g 22S.-385 y Eedp 2g fair gfaltEer al PFOS/PFHS Mean Median Range PFOS/POAA Mean Median Range PFOS/Analyzes Mean Median Range M570/M556 Mean Median Range PFOSAA/M556 Mean Median Range PFOSA/M556 Mean Median Range 8 8 S s ~ = whe 2 Cell Operator' (N = 5) 3.0 de.h 3.3 1.5-3.9 1.5 ` 1.0 1.0-2.6 52.6 bh 56.1 4.9-93.3 3.5 2.8 2.0-7.5 0.4 0.3 0.1 - 1.3 0.4 0.1 0.04-1.2 a 2353 - i? " a a 30 - mad a 23 tal Chemical Operator" (N =47) Engineer/ Labe (N = 23) Maintenance (N = I]) Mill Operator` (N = 13) any< 5.5 d,` 5.2 1.1 - 14.8 0.9`(''g 0.9 0.3-3.1 7.40 4.7 1.3-61.8 3.7" 3.0 0.5-8.9 0.9` 0.2 0.03-8.5 Tsdg Bay2 Far3 [ml5 5.9 d,e 5.2 1.6-18.8 2.2 bale 1.7 0.7-4.4 7.4 a-' 3.9 0.8-36.8 5.8 b 5.7 1.9-14.4 1.1 ` 0.8 0.03-4.5 9.2',b,e,g 10.3 3.7-16.5 1.2 e.e.f 1.3 0.7-1.5 4.6 3,h 3.2 1.4-11.7 3.3 c,e 2.7 1.2-8.7 0.8` 0.1 0.01-3.1 - 8.5 a.b,g,h 8.3 4.3-14.9 0.5'.c.f.g 0.5 0.2-0.9 6.7a 4.8 2.5-20.5 5.8 b.d 4.3 1.2-21.3 2.4ad.6h 2.3 0.2-5.7 -. 3.0 0.3 0.03-30.7 ssdg 2.5 0.3 0.03-18.3 2 0.4` 0.1 0.02-2.7 7.6 d 2.1 0.8-52.3 3595 827SopRee ,ust3 aed= nol2 salZ iz Secretary( (N =4) 3 Supervisor/ Mgme (N = 18) Waste Operator" (N = 5) eS: "ve 6.1 5.8 4.8-8.3 5.0 d` 3.3 1.9-11.7 7.1 8 6.6 3.2-12.3 2 3= 0 Ade 2.5 b.d.e.h 2.0 1.7-4.4 1.8 ' b` 1.6 0.3-4.8 1.4 1.0 0.3-2.9 bet 224 6.79 6.9 3.2-9.7 16.7a 6.7 1.3-134.2 26.5` 9.8 0.8-99.4 and hag 3.2 3.2 2.2-4.3 5.3 4.2 1.6-9.5 3.3 3.4 1.0-5.3 = ~% Teg med s<z 0.2` 0.2 0.05-0.5 1.1 0 0.5 0.02-4.8 0.4` 0.3 0.1 - 1.1 of neg 2.5 2.7 0.9-3.7 4.7 0.3 0.02-64.1 2.6 0.3 0.03- 11.8 i$5I5g mReety"Ey wke=tlRg baxelfARg oa=mflR L o1037zSSnoseyogfRg EiB : 2 - - o 12 S xa 2 28122..00054 L8170900 MY C EON aSitteiooto Py roceSROgrrr1 paolmeSrv o31hnNoa2.Se04S63e05at fom (n K: r- v 7 CL U n D S< o rn cc 0 U < 0, N -0 CD 0 < A o Z-0 o cQ o ry y 0 A o D 0-11 m to E O v o fliers oFf 358,8z fie 550$,E8sd2 52s Pe EH] a88s g=ga 2 & Th ss zs ane i: 7 z22y2 Vl EPI-0006 Page 54 of85 z2 27 53 of Sca h $f:]A 373Ts HC32 S18385 575% gpl iBY TER ORSRL 2 z& PTDL an ae oe pe 3 gaged _,L53.,835%E3%38i.033f)y 5 328 GER i 2,38 2 Table 9. Age Mean SE Median Range BMI Mean SE Median Range Years Worked In Chemical Mean SE Median Range Gender Female Male Only Worked In Chemical* Yes No Hand to Mouth Contact Yes No Wash Hands Yes No 3HR Heed amla owneraz oo 2 Eye as ee ZEEE ATRn FRE g i 2T Demographic characteristics oflongestjob categories ofrandom sample(N = 126)ofchemical employees Chemical Operator' (N = 57) Engineer/ Lab (N = 21) Maintenance` (N = 14) Mill Operator (N = 14) Secretary` (N =6) BoBH a2eTor Zz 5 43 1.1 44 25-62 40 2.3 41 23-58 43 1.9 43 27-54 35 1.8 32 27-45 46 1.9 45 42-54 27.8 0.7 27.5 18-47 28.8 1.1 28.0 21-38 gEa&ns 27.2 0.7 26.7 23-33 27.3 1.4 26.9 20-42 24.2 1.4 23.9 21 30 sa Ben"Ta| 2ox8Co 28s E558 whes"1. voe otme wmen|# 28 58 ERTL. op 14 1.3 14 t-31 N % 8 (14) 49 (86) 12 2.7 8 1-37 N % 5 (24) 16 (76) 11 3.0 8 1-36 N % 0 (0) 14 (100) | 3a 1.4 1 1-21 N % 2 (14) 12 (86) 20 4.4 23 2-33 N % 6 (100) 0 (0) EEE 27 (47) 30 (53) 15 (71) 6 (29) 8 em 6 (43) 8 (57) 12 (86) 2 (14) 1 M) 3 (50) 38 on 39 (70) 17 (30) 47 (84) 9 (16) 11 (52) 10 (48) 15 (71) 6 (29) 83 go 9 (64) 5 (36) 86 (12) 2 (I4) 11 (79) 3 (21) 93 (13) 1 (7) 3 (50) 3 (50) 3 (50) 3 (50) | 3 51 35s] #7] Edam ] we en ee en Supervisor/ Mgmt! (N = 7) 49b,d 2.1 50 42-56 29.4 3.5 25.9 18-47 20.2 5.5 23 1-37 N % 2 (28) 5 (72) 4 (s71 3 (43) 5 (72) 2 (28) 6 (86) 1 (14) E88 3g f ae so| 3 iii3 zy 3 3 52 2 22 v :En *Significantly different percentage among longestjob categories,chi square,p <.05 (a-h)comparisons for each longestjob category using student's t, p <.05 #8 fg sg gg dL F$E3Y0 1nadBRa] EgeEg]t Waste Operator4 (N -3) 53b.d 2.3 52 49-57 26.9 2.4 25.8 23-32 1I.0 6.8 8 1-24 N % 0 (0) 3 (100) n (n) 3 (100) 3 (100) 0 (0) 2 (67) 1 (33) E5gdHz 3 an a5ees confoc zsP.a e8n 2 +35 38 8 8:8 3 2 8 & BPo. = g#0e]l E"T%7B%T oCstEosE f2p7 BtgY S8Spgfd czgc dgsg IR EEEEEER ERE 232 fe $BD5O ig 5 3% 3.5 53 i2rag5er $595 i=<5 & aSdeetAvialaFbelecbtyeiorCrIensrpiecPtaiomnearnd Chopyi6n3g.a94C5o5nf0i8dent Information 28122..00055 (Vi EPI-0006 Page 55 of85 2 3z E= 33 3g3 Sg5 Sg% Iz 3g% 33SE &3% gp<3 Sg% g os csiE Beods EzAiEe BE:E 8 SElOzFT%E4 E8g 30CEC8E2 ZiCE5E1 51CE8E1 C81e8:7 E f2 ouEfsi 8 $5155%0 Table 10. Mean,median,geometric mean and 95% confidence intervals ofgeometric mean ofserum fluorochemical levels by longestjob categories among random sample(N = 126)ofchemical employees g E ii3EO 5 if GL3s8E0 iPiI_b.Ty Es5i3EC S iE53O pys &53855 005 sy $38 PFOS Mean Range G. Mean 95% C.I. PFHS Mean Range G. Mean 95% C.I. POAA Mean Range G. Mean 95% C.I. PFOSAA Mean Range G. Mean 95% C.I. M570 Mean Range G. Mean 95% C.I. =38 5ep7lthhl%7 BE ByEC8E) sis &B738R7 "ECE 33.F2 2B.i5k eaETiChRBYon5C7pBrS CLF BZ 3;ET5E1 CSE0C8E] sys siz JEE1H8E1 3B7 E27 "ECE CECE Chemical Operator" (N = 57) Engineer/ Labb (N=21) 2% 3 Maintenance` (N=14) 2.088 0.338 - 7.880 1.697b.d.e.f 1.440 -1.998 0.520 0.095- 1.740 0.330x" 0 0.219-0.496 2.250 0.291 -10.600 1.49Ob.d.e.r 0.933 -2.379 0.543 0.073 -- 1.880 0.388bx,def 0.314-0.480 0.116 0.005 - 0.420 0.067'r 0.041 -0.110 0.297 0.023- 1.250 0.1768""' 0.101 -0.307 2.293 0.182 -6.760 1.972bcxf 1.694 - 2.295 0.287 0.035- 1.000 0.198a.e.d.8 0.134 - 0.295 1.667 0.211 -4.680 1.229a.b" 0.797- 1.900 18 BCIECEED 8 se B8Tu3z7 CECE 0.032 0.001- 0.269 0.01Ob.e 0.007-0.016 0.014 0.001 -0.073 0.005a 0d 0.027 - 0.010 g fySs SSs 0.029 0.001- 0.083 0.014be 0.007-0.031 2.3 BCIEEE 87fi8c%. CEC 0.213 0.009-0.992 0.120b.d.ef 0.089 - 0.161 0.060 0.008 - 0.164 0.046'0 0.033 - 0.064 s nihd 0.269 0.038 - 0.701 0.20060.f 0.126-0.315 2.3J 83% ggStiiS oga5 is9 Mill Operator (N=14) 0.735 0.230 - 2.040 0.609ass 0.441 -0.842 0.107 0.028 - 3.744 0.074x.0 0.048 - 0.112 1.383 0.450-2.340 1.274b0f 1.009- 1.609 0.019 0.004 - 0.038 0,014b'e 0.009 - 0.022 0.046 0.025 -0.115 0.043''0 0.035 -0.052 "o #7 3d3 =a L37EE37 2 BT Bd81 3o BBTed57 oEVad2o7 2 Secretary` (N=6) 0.388 0.129- 1.140 0.295"'-9 0.163 - 0.533 0.070 0.027-0.172 0.0573.c 0.033 - 0.097 0.143 0.053 - 0.261 0.124a0de 0.076 - 0.203 0.002 0.001 -0.004 0.001 a.e.d.f.8 0.001 -0.002 0.032 0.010 - 0.072 0.0258.0 0.014 - 0.046 of J8TLT a3= eS2 ST2 3E1%z 233 ef3 T8 s Supervisor/ Mgmtf (N = 7) 0.536 0.091 - 1.220 0.400'0.8 0.209 - 0.764 0.128 0.010 - 0.383 0.077a 0.030-0.193 0.407 0.021 - 1.790 0.177'.`.4.8 0.062 - 0.510 0.011 0.001 -0.019 0.0080 0.004-0.017 0.071 0.016 - 0.201 0.054'0 0.030 - 0.096 ,8 88 8 832 2 5 5 3 Waste Operator8 (N=3) 2.388 0.254-4.840 1.365b0f 0.245 - 7.600 0.256 0.0388 - 0.562 0.153 0.033 - 0.703 2.219 0.936-3.680 1.915b'e.f 0.881 -4.166 0.008 0.003 - 0.016 0.006 0.002 - 0.016 0.104 0.053 - 0.159 0.095 0.050 - 0.177 2 E:I:31i~~iId,/1E~ swtons4se gs EEiB g3 23 =3 83 = 5.8 833% 7 zS5s5 5%5 255 i5s g s:Fadips s15 e,sdp0i2S s gg MSuatdeocAtvtaolPaobtlecbhyv3e1OfrodIensnpePctailomnearvn.dWChopyNoi.ng62a.s0G4e.n6f3i0d5ental Information iv! EP1-0006 Page 56 of85 Table 10. (continued) Sg88 %5 7YE s2.i8 s213% 78 858 PFOSA Mean Range G. Mean 95% C.I. M556 Mean Range G. Mean 95% C.I. 0.088 0.001- 0.487 0.021"" 0.0126 - 0.0340 0.070 0.001- 0.380 0.039"d,e" 0.029-0.054 0.016 0.001 -0.063 0.004"d 0.002-0.009 0.014 0.002-0.039 0.009"' e,18 0.006-0.014 s 0.095 0.001 -0.612 0.010 0.003-0.028 0.117 0.015-0.406 0.069b,d,c,f 0.038-0.123 (a-h)comparisons for each currentjob category using student's t, p <.05 5 31g EY 3! IE I 3LS EsEr 0.042 0.012 - 0.204 0.028"' 0.018 - 0.044 0.013 0.002 - 0.045 0.010` 0.006-0.015 & =3 9 g g g 28 33 % cg g 0.024 0.009 - 0.080 0.017' 0.009 - 0.033 0.011 0.003 - 0.030 0.007"`8 0.003 - 0.017 Saf Bad 887138;7 S5I2 8Eh1 0.027 0.001 -0.173 0.00' 20. 0.004 - 0.012 0.019 0.003 -0.059 0.0110. 0.004-0.027 0.014 0.005 -0.027 0.012 0.005-0.029 0.067 0.001 -0.157 0.037"` 0.008-0.180 cg$s"2 g= 3 5. 24 31 E24 a 3s Fi 2 i 28122..00056 1. .11SX0111,/1E amatoosee F MoteARvastEby StoA r nspscCtOonRIsnPCoHgnS5ICAonLdens formation: 281122..0057 U K c D - 0 0g s (D ~0_.,9 rn w O rn cn -0 m :1 0 v Wa Z-O0 0 cQ ry N 6C 0n o a `0b, 0 ni 0O :~Z:31i~~iId,/1E~ SN gsmbampimb2imianbulc i 2 Z2 w 5 3s Sy Si.8y Be o8y Si.8s 22.840z 1 JPTOA IPI BN I, oz 3 3i) 2 . " gl & z: =fg 77s 3S 2 3 2 Sl 22 EPI-0006 Page 57 of85 F3? :ES SRg Sd #Rp edn Trg dSg 2: oeelilz 1.3 3 2 L.3" 5 gF odRE5l Yarng 8s]$3 sal mal3 ded end3 H5T050E7O Bad EexTtEECwLeIf TEREAT uA Il. . 3 f 2 sFf s3Te &n72 22}3 hel2 msl agg8 3 gPlEgsl el32 sl Ezaal Be)3 velg waggi 2 Bee] cat eT L.f 3.2 La7 nod ef 3 3 oe 3 PIT %eY Rol asl Bal onal Ball d Table 11. Ratio offluorochemical levels by longestjob categories among random sample(N = 126)ofchemical employees PFOS/PFHS Mean Median Range Chemical Operator' (N=57) 5,0cAg 4.9 1.1-14.8 Engineer/ Labb (N-21) 5.8'c d 4.8 1.9-18.8 Maintenance` (N= 14) 9.18 b'`'f 9.2 3.7-16.5 Mill Operator (N= 14) 8.88 b'`'f 8.3 4.3-14.9 Secretary` (N=6) 5.6 5.8 2.2-8.3 Supervisor/ Mgmtf (N=7) 6.0 3.9 3.0-11.7 PFOS/POAA Mean Median Range 1.Ob.e.f 0.9 0.3-2.9 2.08c'd'fg 1.7 0.3-4.4 1.3b'd'`'f 1.3 0.6-2.3 bx 0.5b.c.c.r 0.5 0.2-0.9 2.68'`'8 2.0 1.6-4.4 2.68'b.c.d.g 52.6 0.7-4.8 PFOS/Analytes Mean Median Range 13.4 5.4 1.3-99.4 5.9 3.9 0.8-16.8 5.3 3.8 1.4-11.7 a 6.6 4.8 2.5-20.5 6.0 5.5 3.2-9.7 5.5 3.3 1.3-17.8 . .1 M570/M556 Mean Median Range 3.8b,f 3.0 0.5-9.5 5.78` 4.5 1,9-14.4 3.5 3.1 1.2-8.7 2 5.6 4.2 1.2-21.3 3.7 3.9 2.2-5.8 6' .48 3.4 2.5-19.5 Ff0SAA/M5Na Mean Median Range 0.91 0.2 0.03-8.5 1.1 d 0.6 0.04-4.5 0.7d 0.1 0.01-3.1 S 2.38''b c'" 2.2 0.2-5.7 0.2d 0.2 0.05-0.5 1.4 1.2 0.02-3.7 PFOSA/M556 Mean Median Range 2.6' 0.3 0.03-30.7 2.2 0.3 0.03-18.3 0.5' d f 0.1 0.02-2.7 7.4c 2.1 0.8-52.3 - 2.6 2.7 0.9-3.7 9.28'c 0.1 0.02-64.1 ge g (a-g)comparisons for each longestjob category using student's t, p <.05 ..-= .1 215h2] weroe B217 Rgoagl ast3 bsT: oggg Waste Operators (N=3) 9.28 8.6 6.6-12.3 0.9b.e.f 1.0 0.3-1.3 22.2 13.9 0.8-51.9 3.2 3.0 1.0-5.5 0.2d 0.1 0.1-0.5 1.1 0.3 0.03-2.8 i3c 2 2. 2 2 9 3 em | 8 aSdeetAvialaFbelecbtyeiorCrIensrpiecPtaiomnearnd Chopyi6n3g.a94C5o5nf0i8dent Information 28122..00058 117SX011NE, s : CoK ~(T a cD a D - 0 0.-.. ,CD0 z rn OW EL CD m r' rn sy 0W Z o :' N Co .CA)0 o cW~ Q0 m a) o 3 R awatoosodst g a B ie o prp o erop eos FH i: -I EP1-0006 Page 58 of85 ELFE]H < 28 2@ % % 2 iHe EL se 8E5 E8 E8 E3%EE 8 <3 EE | "g s = *s "3 5: i] 3 5 i$z8. | E2338 32 2 fE3F3.g t2e 8 EBB 3 % 2 f & f E2f 38 82FE3% "85e13r317 gI7;et85y3; T85E7g Ea87 8f:rlEgd oBge:LtE8sS 38 4z G28 3o5k 02g3p G3F3 sigip #33sigisr s3k3 Agfp s338 Et f3e%"Si1p C8cpp cE$SE,oeESsgy CBCElg ot8Cz1g oss8:g8ot.sfg tS8f.g tsEhgi se5z5. 5%g 55& s%& 8%8 57= zyg 3d zt& os2 gt3 gs S%2 5E2R% FE Table 12. Mean,range,geometric mean and 95% confidence interval ofgeometric mean ofserum fluorochemicals among random sample(N = 126)ofchemical employees who currently only work in certain buildings(as listed) PFOS Mean Range Bldg. 1 (N=15) 0.768 0.109-2.190 BIdgs. 2/49 (N=7) 2.621 0.325-6.840 Bldg. 3 (N=22) 2.457 0.885 - 7.260 Bldg. 4MX (N=21) 0.607 0.23-1.620 Bldg. 4N (N=5) 2.000 1.440-2670 Waste water (N=4) 2.763 0.254 - 7.880 28 sl 20 fp27G8g S2g7$7d88%g E G. Mean 95% C.I. PFHS Mean Range 8 0.481 0.270 - 0.858 0.228 0.013 - 0.713 1.945 0.824-4.592 0.996 0.083- 1.880 2.135 1.693 - 2.693 0.568 0.151 - 1.860 0.525 0.364 - 0.757 0.101 0.028 - 0.374 1.937 1.369 : 1.378-2.723 0.136- 13.741 0.450 0.161 -0.832 0.386 0.038- 1.210 88 3gprSE 3o23olf S8%z"ogS2Eg7 G. Mean 95% C.I. POAA Mean Range i. 0.115 0.057 - 0.234 0.554 0.051 -2.700 0.709 0.262 -- 1.922 1.879 0.126 - 3.640 0.410 0.286 - 0.586 2.777 0.261 -6.760 0.069 0.039 - 0.121 1.303 0.450-2.110 0.397 0.192 - 0.821 2.088 1.300 - 2.860 0.177 0.018- 1.729 1.804 0.936 - 2.710 88 SRgI"ENomaRlp S0gE&TS7:f G. Mean 95% C.I. PFOSAA Mean Range on 0.240 0.119 - 0.487 0.013 a not -nnS4 1.251 0.412 - 3.802 0.005 0001-0016 2.128 1.467 - 3.087 0.055 0001-0160 1.188 0.865 -1.631 0.019 0AW-nmR 2.024 1.420 - 2.886 0.019 nn04-0n4't 1.677 0.815 -3.452 0.010 0nn';-0017 s:$ 3 S8gScp8Sg%p ztod 3EEdp = G. Mean 95% C.I. M570 Mean Range i 0.004 0.002 - 0.010 0.101 0.015 - 0.410 0.003 0.001 -0.008 0.028 0.010-0.056 0.023 0.012 - 0.043 0.382 0.063-0.992 0.014 0.007-0.026 0.037 0.025-0.053 0.011 0.003 - 0.048 0.099 0.054 - 0.205 0.007 0.002 - 0.031 0.091 0.050 - 0.159 8 wZlecE zoglcE sd Ef of8 3E G. Mean 95% C.I. 5s 0.071 0.044 - 0.115 0.023 0.013 - 0.043 0.308 0.224-0.423 0.036 0.031 -0.043 0.088 0.047 - 0.165 0.081 0.034 - 0.195 SWaidboelAvlaolParlootbeych OfrodrerInspePcatilomnevarndWChopyNoi.ng2a.s0C4o-n6f3id0e5ntial informa 281122..0059 X-1711 SX0111YIND, maroososez -cD~ a D - 0 0 CD rn ,Z rn w O rCnD _ -' E ~'0 m oL a rn za C7 z 0 n cQ ?' CO 0 o a QO m 3 0 3 R o' 0 if g2 id 3 LI 52 H 85 E83 33 8] o ivi EPI-0006 Page 59 of85 g2g, i Table 12. (continued) E 87 7R8%E5% A 35dPH PFOSA Mean Range 0.026 0.005 -0.161 13 55d3i1 0B G. Mean 95% C.I. M556 Mean Range 0.009 0.004-0.022 0.027 0.003 -0.127 o2f:2323 G. Mean 95% C.I. Years in chemical Mean 0.017 0.010-0.030 20 :8 58 : 8 3s 8g3 58 %g3f g%l 0.003 0.005 - 0.106 0.002 0.001 -0.005 0.012 0.003 - 0.028 0.009 0.004 - 0.021 24 0.102 0.003-0.569 0.036 0.018 - 0.072 0.119 0.024 - 0.380 0.092 0.066 - 0.129 10 $8.5 82 H 108 EE518; = 3.8 2.3 $$7288% 5 gl 58] - 82% 5 0.042 0.012 - 0.204 0.027 0.015 - 0.047 0.008 0.016 - 0.018 0.007 0.005 - 0.011 5 0.251 0.003 - 0.487 0.059 0.002 -1.595 0.076 0.026 - 0.175 0.056 0.019 - 0.163 13 0.007 0.002-0.011 0.006 0.002- 0.019 0.056 0.015 - 0.157 0.033 0.006 - 0.193 13 3aEPMM10006 EPPPaaIgg-ee06600006o0f88f55 TTaabbllee 1133.. oMMfeesaaennr,,urrmaannfggleeu,,oggreeoocohmmeeemttirrciiacclmmseefaaornntaahnnoddse99e55m%%plccoooynneffeiisddeeinnnccreeaiinntdneormvtasloaeomffpgrgleeeoovm(meNeatt=rrlii1cc2mm6)eeaann owwfhhsooessraauiimdd fttlhhueeoyyrhhoaacvvheeemooinncllayylswwfooorrrkkteehddosiiennooennmepeblbuouiyilelddeiisnngig/n/aarrraeenaadom sample(N = 126) BBllddgg6.) 1| BBollDddgg)..33 BBllddgg.. 4aMMXX os) (N=6) (N=7) (N=8) PPFFMOOSeSan 047 2561 0521 RaMRanenaggnee 00.11202.994--71417.70000 11.445520.0-5-6551.112200 00.2233000.-5-2001.883388 GG9..5M%MCeelaa.nn 95% C.I. PPFRHHMSSean RaRMnaenaggnee 01001.3430-0202797 0.114 -0.797 000o1.3n11-y7020 0.013 - 0.420 145223.22-99333619 1.453 - 3.619 0.15001.88-33155.860 0.151 - 1.860 034000.55-55044904 0.340 - 0.904 003008.00-66033152 0.038 -0.152 GG9.5.%MMCeeaalnn POA9A5% C.I. POMRAeaMAneaagnne Range 001008.00-66044223 0.018 - 0.223 00500..311-66044386 0.053 - 0.386 0.18005.5511199.450 0.185- 1.450 036336.0-022611760 0.366 - 6.760 003009.00-66044103 0.039 - 0.103 0.45110.001822.850 0.450- 1.850 9GG5..%MMCeelaaLnn PPFFMOO9eSS5aAA%AnAC.I. RaRManenaggnee 00005..321-2505294 0.053-0.294 00000.0100-0110003 0.001- 0.003 077223.0-033533351 0.773 - 5.351 000005.0-03030.0118 0.005 - 0.118 071115.0-0331%0476 0.719- 1.476 000008.00-22000037 0.008 - 0.037 G. Mean 99G5.5%%MCeCLa-1.nMM55M77e00an RaRManenaggnee 00000.0100-0110002 0.001 -0.002 00010.0508-8202201 0.015 - 0.201 000005.00-11066047 0.005 -0.047 006003.33-11088480 0.063 - 0.480 000008.00-110s5027 0.008 - 0.027 002006.00-44000053 0.026 - 0.053 GG9.5.%MMCeeaaLnn 95% C.I. PPFFMOOeSSAaAn RaRManenaggnee 00010.0805-5330159 0.018 -0.159 00000.900-22033.060 0.009 - 0.060 014005.22-77044520 0.145 - 0.520 000003..11-55088569 0.003 - 0.569 002008.0-044088081 0.028 - 0.081 000001.00-44033204 0.001 -0.204 9GG5..%MMCeelaaLnn 95% C.I. MM5sMs5e66an RaMneagne Range 00000.0901-1909037 0.009 - 0.037 00000.0302-2202585 0.003 - 0.585 00000.9.00-55055324 0.009 - 0.324 003003.00-99077213 0.033-0.213 001100-.000331408 0.011 -0.108 000400.-0001100019 0.004 - 0.019 GG95.% MMCeeLaa.nn ear9s5i%n cCh.Ie.mical Mean Years in chemical Mean 00000.0401-1404045 0.004-0.045 233 004002.0-07079.9150 0.042 - 0.150 i1ss 000500.-0010130334 0.005-0.034 11.66 MSMuaabddjeeecAAtvvataoiillPaarbbollteeecbbtyyiv33eMMOfrfodorrerIInnIssnppeePccattiiimooennraavnn.dd3CCMoo,ppyNyoii.nngg2a-ass04CC-oonn6ff3ii0ddee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00006600 3SMMAA11900005500449933 SMuabdjeecAtvtaolParbotlebciyv3e OfroIdnerspIencPtailomnearvn.d3C,opNyoi.ngC2a.s0C4o.n6f3d0e9ntal formation 2881122..006611 U K a y - 0 0s 6(D .9 rn 0 rn 0 cn -0 m oL ~ W Z0 - -0 O ry N ~ 0 o 0m o 3 R P i1:31i~~iId,/1E~ 3MAMO0SD4S4 55 a % | : EelT z 2 lFTeESnd2g z in|iE2 3 g1eent |g v . EPI-0006 Page 61 of85 3.3 i23 388a1 9 zTo 4Bi% 3 i _%% i 25 fog g2E iStSael 22 z D I33Rg ueld 3 d&g 3 E2I 38%=I a. z h:d 3= & pial bel 57F Ha. Table 14. Age,BMI and years worked in chemical among currentjob categories ofall participants(N = 187)in chemical Cell Operator' (N =9) Chemical Operator' (N =64) Engineer/ Lab` (N = 37) Maintenanced (N = 17) Mill Operator` (N = 24) Secretaryf (N = 5) Supervisor/ Mgmt9 (N = 26) < Baik Age SE Median Range 450 2.1 44 38-59 f 8.h 41 e 1.2 41 25-62 # 42e.s.h 1.8 43 23-58 41`0 1.5 42 27-52 34a b,e,d rs h 1.3 32 25-45 44e 1.3 44 42-49 48b e,d.e 1.2 49 33-59 g& mel = woom me = gzog Es nid g BMI Mean SE Median Range Reexsep 25.8 1.3 27.6 18--30 28.30 0.7 27.8 19-47 27.3 0.9 27.3 16-38 27.6 0.8 26.6 23-33 28.1' 1.1 26.9 20-43 22." 7b 0.8 23.0 21-25 28.9` 1.1 27.6 18-47 =5 Years Worked In Chemical Mean SE Median Range 19b.d,e 3.2 21 2-30 I OaX.e.g 1.1 10 1-31 15b.e8 2.2 14 1-37 i0a.c,s 2.6 3 1--30 2a,b. AQ,h 0.8 1 1-21 1 b` 3.9 20 2-25 21 b.d.e 2.1 24 1-36 1. = iRaUgaTl woos engy- i Re-D . AB3T2E]D men ARYa Lo As i T2%eel% une %-s7e iw 7a] Waste Operator' (N = 5) SQb`de 0.7 50 49-52 25.5 1.4 25.8 21.8-30.1 14e 4.5 16 1--27 1i3 ais2| 28 |= (a - h)comparisons for each currentjob category using student's t, p <.05 1 2330a LiA. ooEeTE pezIi] olf5 i%2g SMuabdjeecAtv1aoiaPrbolteecbtyiv3e OrfodreIrnsIpneactiiomn eavn.a3C,opyNoi.ng2a.s04Co6n3fi0d8ential Information 28122..00062 ~:~z~~~~1~~~E~ U) K cD a D - 0 0 cD ,Z rn 0 rn -0m ' a ~ w~ C-) o ry v ~ 0 60 o a C9 (D 3 o R o' IMA10050495 82CI 83 gz zs .|% sf = EF IX 3 z 8s8e gas2 gg Isfe | 4z 358 A5=% gipE aozms | 1f 3, =ss2z@z ooc838z 28 E56X8 57Eg2B5 ||32:G i 2=8 g2g g=g &E 2 ig |g 4s 53. 25 is.fd | 2|} 3I8 E BesEdpE s d0 z|g = sET g : fz zg 33.5d 5 g5783 i$ 3&3588g3g i3 . 3=3235 ii 42 i: EsQ i EPi-0006 Page 62of85 3.4 g2vo :ge5gY| 3sI 4f54g 2 P.E1E3 3z i3 g$s g8s g2s 8s Table 15. Number(and percentage)ofdemographic characteristics among currentjob categories ofall participants(N = 187)in chemical Cell Operator (N=9) Chemical Operator (N=64) Engineer/ Lab (N=37) Maintenance (N=17) Mill Operator (N=24) Secretary (N=5) Supervisor/ Mgmt (N=26) Waste Operator (N=5) 82 8% SxTR=S2e 83.% sz2 2OR8 8s Gender* Female Male 1 (1 l) 8(89) 12(19) 52(81) 9(24) 28(76) 0(0) 17(100) 3(13) 21 (87) 5(100) 0(0) 3(12) 23(88) 0(0) 5(100) Only Worked in Chemical* Yes No 5(55) 4(45) 30(47) 34(53) 22(60) 15(40) 10(59) 7(41) 22(92) 2(8) 1 (20) 4(80) 10(38) 16(62) 0(0) 5(100) 88 &3 aEz E2s 2g%s &O:i 8F3OEaS Hand to Mouth Contact Yes No 7(78) 2(22) 48(77) 14(23) 16(44) 20(56) 13(76) 4(24) 21 (88) 3(13) 3(60) 2(40) 15(58) 1 l (42) 3(60) 2(40) Wash Hands Always Less frequently 8(89) 1 (11) 53(85) 9(15) 23(64) 13(36) 15 (88) 2(12) 20(83) 4(17) 3(60) 2(40) 18(69) 8(31) 3(60) 2(40) * Significantly different(p <.05)proportions betweenjob categories,chi square test Io sid 8 gz sg 28122..000063 ::Z:31i~~iId,/1E~ -- WSaidboelAvlaolParlootbeych OfrodrerInspePcatilomneavrndWChopyNoi.ng2a.s0C4o-n6f3id0e5ntial informa U)K ~ v rn m aD - 0 0s rn ca 0 rn OQ~o rn _ cn -0 m oL a~. rn v W ~ 0 0 Z-0 o ~ C7~ N N ~ C7 60 oQ Q0 m 0 0 3 R o' 0 gisfBCHE ICEECE 2gFd VI EPI-0006 Page 63 of85 2 >5 587b:% BITg 313 i 2= 3Pi ooeusTogfo;pc 835 3 is Pole sT $38 g i 2ioe i3 27327) gi 5H2 EE :<2 z 0 P Ex m= i Poooopg1i8s : gz <8 ez i Ez i Bove B32o% Sf8y% Table 16. Mean,range,geometric mean and 95% confidence interval ofgeometric mean ofserum fluorochemical levels by currentjob categories among all participants(N = 187)ofchemical 2 E [GoE2 p3i5 sh gd3 TET g28 Gf 23 PFOS Mean Range G. Mean 95% C.I. PFHS Mean Range G. Mean 95% C.I. POAA Mean Range G. Mean 95% C.I. PFOSAA Mean Range Te$.h8 3 RL T"Z 37~8g FHAENE Bg &; SgS8%3 g(.283 8. 8: ~F3-33 Cell Operator' (N=9) 2.266 0.325 -6.840 1.643'e'd f 0.914 - 2.953 0.927 0.083 -1.880 0.664b,e d e.f g 0.346 -1.274 1.811 0.126 - 3.640 1.263`'18 0.619 - 2.576 0.009 0.001-0.01 8.3% TT =3573%g agiinc 8373% 2S7z% 2%gizY $385 3% pI EY LT EY "g"y FT":% ECS:z FA3T5 B335 238.33543 SE24F S3s2F gyilgi1z3 Chemical Operator' (N=64) Engineer/ Lab` (N =37) Maintenance (N = 17) 1.839 0.189-7.260 1.480`'`,8 1.253- 1.749 0.611 0.081 -1.740 0.390''b.d,g.h 0.282 - 0.540 1.772 0.291 -4.940 1.320`'e'f 0.904- 1.928 0.411 0.034 -1.860 0.292''`' d ef 0.239-0.357 0.148 0.005 - 0.905 0.075''b,d O 0.0500-0.111 0.309 0.023- 1.240 0.178'''d e 0.107 - 0.297 2.196 0.150-6.760 1.849`de,f,6 1.587 - 2.154 0.343 0.024-2.320 0 19$a.b.d.e.g,h 0.141 -0.277 1.512 0.211 -4.680 1.052`''9 0.691 - 1.602 0.042 U.UU f -- U.269 0.010 0.00i -0.073 0.037 6.Wi -U.i25 7% ICEEE sia 23 83 37Tt 37Ts S5so8o7ai%d;=2 gs . 0g3d0E z 3 Mill Operator` (N = 24) 0.625 0.025 - 2.040 0.501 a.b.48.h 0.374 - 0.672 0.082 0.001- 0.374 0.053''b.d.g.h 0.035-0.080 1.218 0.015 - 2.340 0.987`'19 0.668- 1.457 0.022 0.00 -6.049 Secretaryf (N = 5) Supervisor/ Mgmte (N = 26) Waste Operatorh (N=5) |g 0.451 0.220- 1.140 0.366x,', h 0.206 - 0.649 22 2= 1.732 0.091 - 10.600 0.842b`- -e 0.510- 1.388 pg 2.648 0.254 - 7.880 1.504e''ef 0.493-4.589 0.076 0.027-0.172 0.063"0.035 - 0.113 0.390 0.009- 1.420 0.180'1`'` 0.010 - 0.324 0.444 0.038- 1.210 0.232",e 0.069-0.775 0.167 0.095 - 0.261 O.l55a b,d,c.g h 0.106 - 0.226 a8 5 3& 1.289 0.021 -4.540 0.57 1 0.-Ax,f h 0.312- 1.043 . 1.663 0.936 - 2.710 1.542`''g 1.052 - 2.259 0.002 0.00i -0.004 3 0.009 U.00i -0.054 0.009 0.003- -0.0i6 Y CECEEE CECE gv33i% %83 .B8S 8%"ge8;e 8T1io8: oofsf;poBBrSg 8gf1f:pS8fECE C3048% 138.5 EB 3 sg 5.3 Bis piel 8 = 3C3SEy gEfg =TS 22 83537 aS&7gg 311g gis g7 IS 37 &S Ba3,82 3151 3"37%8 3 8 of iB 4 Sf di G. Mean 95% C.I. M570 Mean Range G. Mean 95% C.F. 0.003be 0.001- 0.008 0.045 0.012 - 0.169 0.032b,d 0.020 - 0.054 2g.33% Ed Eg 3czyg 0.014"'d 8 0.009 - 0.020 0.004b'e 0.002-0.005 0.284 0.009 - 3.100 0.143" x' , ,8 0.107 -0.192 0.064 0.004-0.410 0.041bd 0.030-0.056 2.38 psS%f.3Sd% 0.015b 0.007- 0.032 0.016" x 0.012-0.023 0.237 0.038-0.701 0.186'1'88''8 0.130- 0.267 0.044 0.023-0.115 0.041 b'd 0.036-0.047 OCEIEM @.% 2i9 E& ots od s$flsS8s d%i58 0Zadk "8 NE: 0.001 0.001 -0.002 0.005b 0.003 - 0.008 0.006 0.003 - 0.013 0.036 0.001 -0.072 0.029b,d 0.015 - 0.057 0.110 0.010 - 0.553 0.063bd 0.041 -0.096 0.087 0.050 - 0.159 0.079 0.052 - 0.121 28122..00064 /~:~Ti~~iId,/1E~ aMAT005047 MSuatdeocAtvtaolPaobtlecbhyv3e1OfrodIensnpePctailomnearvn.dWChopNyoi.ng62a.s0G4e.n6f3i0d5ental Information CoK ~ v rn m aD - 0 0s rn rn OQ~o cu _ ~Cn m oL :a. rn v Q W 0 0 z~ o ~ C7 CO N CO A C7 6)0 oQ Q0 m 0 : gd5h ioFyfE 2f 8:8 2% 87 Sg Sg SSsif.2 8 81 81 8 [ E8N4 31 z 3$< 3s38f:oifc zg 25 s 5) gL 81 Table 16. (continued) PFOSA Mean Range 0.006 0.0005- 0.015 G. Mean 95% C.I. 0.004 0.002- 0.009 0.088 0.001- 0.487 0.021" 0.013 - 0.033 0.011 0.066 0.001 -0.063 0.001 -0.569 0.003"'d' 0.002 - 0.005 0.012` 0.005-0.027 0.028 0.0005 - 0.204 0.017" 0.011 -0.025 g i BNiEg 513% 833:i 51 35E% Cid g M556 Mean Range G. Mean 95% C.I. 0.013 0.003 -0.035 0.01 Ob,d 0.006 - 0.017 0.074 0.001 -0.380 0.045'`'`'fg 0.034 - 0.059 0.024 0.002 - 0.033 0.010"a 0.007 - 0.014 (a-h)comparison for each currentjob category using student's t 885453533 cg S33 0.088 0.008 - 0.406 0.054''`''f'R 0.034 - 0.088 0.014 0.002-0.045 0.011 b,d 0.008-0.014 0 3 R o' 0 RTI EY 8E 7 57 f 37 5] oz S851887 E78i3: 5 "BE ~i EP1-0006 Page 64of85 85%81 i 3E]g 25. LEE Sg 3p 32 Ey 78 Ts 3 2 E,8 0.025 0.052 0.038 0.003-0.080 0.0005-0.612 0.002-0.161 0.014 0.004-0.042 0.007 0.003-0.015 0.012 0.003 - 0.048 0.015 0.003-0.030 0.0111-1 0.004 - 0.027 0.044 0.003 - 0.336 0.017b.d 0.010 - 0.029 0.047 0.014 - 0.157 0.027 0.011 -0.068 2.8 FE MSuabdjeecAtvtaoiaPrbolteecbtyiv3eWOrodrIenrsIpnePctailomneavrn.d3CMo,pNyoi.ngC2a.s0C4o-n6f3id0e9ntial Information 28122..00065 U)K a y - 0 0s 6(D ,9 CD O~ rn n -- a (D ~ z o Z-0 N CID co ~ 0 60 o a Q0 CD iv o 3 R o E:I:~Ti~~iId,/1E~ MA10050498 5 ped E h-oil- g2 2 oBsUoEnLlL 23Z 3 E EPI-0006 Page 65 of85 2 5a z3 J 3 E sE8 1.7 zmae 2 Ez&zz| -a,a 878]| 3 2 ig 5] t2.% ast % gsz E Ts "Tg| 3 3.3 2 2i in $2.8 3= 852]ioT3) : 2i 58i7e on.Y. = "dg 7% =2 g: g2 Table 17. Age,BMI and years worked in chemical by longestjob categories ofall participants(N = 187)in chemical if Bal RYRT =Sel 3$t:h58y 3317. 0a5]%. A2P2E8]%e kIAw %aatl2 Fi3g7 iFaU.;% Cell Operator' (N = 3) Chemical Operator (N = 77) Engineer/ Lab` (N = 31) Maintenances (N = 20) #8 2 $3f8rig11,3d5ria aiiyd z Age Mean SE Median Range BMI All rKV Mean SE Median Range zen 8SR)= zRmTaRl=a 43 2.5 45 38-46 24.8 3.4 27.0 18-29 42 s''' 1.0 44 25-62 28.0 0.6 27.5 18-47 41 `'B'' 2.0 41 23-58 28.0 0.9 27.7 21-38 gFO2R%D 43`r 1.5 43 27-54 27.7 0.7 26.7 23-33 5z 8& isl?2 =g Z nReU.hTlA4 Years Worked In Chemical Mean SE Median Range 13 6.7 11 2-25 13`'g 1.2 12 1-31 13`'9 2.3 8 1 -37 II`'f's 2.6 6 1-36 :z (a-h)comparison for each longest.job category using student's t, p <.05 = Mill Operator` (N = 26) 34''`'a,rs,h 1.4 32 25-51 28.1 1.1 26.9 20-43 2e,~.a,rr 0.8 1 1-21 Secretary (N = 7) 46` 1.7 44 42-54 24.1 1.2 23.4 21-30 20a` 3.7 20 2-33 5 RU- g aga : iSsedy YjHDeg iegszhl cRFaEAsELsT Supervisor/ Mgmta (N = 15) 49b'`'s` 1.7 50 33-59 28.3 1.9 27.1 16-47 22t"-d 3.3 26 1 -37 Waste Operator' (N = 3) 53''`'` 2.3 52 49-57 26.9 2.4 25.8 23-32 11 6.8 8 1-24 3 2 $38 2 SMuabdjeecAtv1aoiParbolteecbtyiv3e OrfodreIrnsIpneactiiomn eavn.a3C,opNyoi.ng2a.s04Co6n3fi0d8ential Information 281122..0066 v --~ a y - 0 0s rn ca CD O~ Qo rn 5 ---(aD 3 0' :3 z n 0 Z-0 0 n Z. C7 w Q0 CD a)' 5 3 R o' M 1. .11SX0111,/1E MAT0050468 fEfs 32d g 3 i :2 &2 of 2E fgggsgs om&c8a8 :2 2 se a 2 zs8 a8z5 3 H 5 2g g2 3 EY8 E3S2 &i gs VI EPI-0006 Page 66of85 Z 2fwd jfz g #2e2f 3ss g3xr ssee Z z F 52 BgyBqyd i 3 3 oo 3 Ex7| 88 55 23 %E 5 3 aga 2: gE8y| %SEsS :zSpol3z-%%9Ee.2E#s 8e5 3 % E 3 Table 18. Number(and percent)ofdemographic characteristics by longestjob categories ofall participant employees(N = 187)in chemical 28 Gender* Male Female Cell Operators (N = 3) N(%) 3(100) 0(0) Chemical Operator" (N = 77) N(%) 68(88) 9(12) Engineer/ Lab" (N = 31) N(%) 23(74) 8(26) 2s HgEsE Maintenances (N = 20) N(%) 20(100.00) 0(0,00) &z| #s= Mill Operator` (N = 26) N(%) 21 (81) 5(19) Secretary{ (N = 7) N(%) 0(0,00) 7(100,00) Supervisor/ Mgmtg (N = 15) N ON) l2(80) 3(20) Waste Operatorh (N =3) N(%) 3(100) 0(0) 8 a 52288 on ga2g gg 8$3s omg886 388s 8: Only Worked in Chemical* Yes No 1 (33) 2(67) 33(43) 44(57) 21 (68) 10(32) 10(50) 10(50) 24(92) 2(8) 3(43) 4(57) 7(47) 8(53) - 0(0.00) 3(100.00) < Hand to Mouth Contact* Yes No 3(100) 0(0) 56(75) 19(25) 14(45) 17(55) 14(70) 6(30) 22(85) 4(15) 4(57) 3(43) 6(40) 9(60) 3(100) 0(0) a3 av ig=ggs g8S=Fz7 3%= Wash hands Always Less Frequently 2(67) 1 (33) 63(84) 12(16) 20(65) I 1 (35) 17(85) 3(15) gg * Significantly different percentages by longestjob categories,chi square,p <.05 22(85) 4(15) 4(57) 3(43) 9(60) 6(40) 2(67) 1 (33) TES 33db] E2ge8s gogn g sz ggas 2% 2 g2 3 H3Y 47] g g2e 6E g5ss8g 2gsss a==3 FdreyeAvraibaiobyy 3 Sfobr nspecctaonanndsCoptyingSa oGnfbdental formation 28122..00067 rn ~ K tv rn m a D - 0 0 rn CD rn Oo 8(D _ cn -0 (D of a~. (D w~ ~n 0 Z o ~ n ~ N C) CN7 60 oQ Q0 'D 0 3 0 3 R o' 0 :~I~L~i~~iI~l,/1E~ -- 2 -)oh EP1-0006 Page 67 of85 Ed GEL Fif Bif E48 23% SIogRif E6l%e; B7I8E% E80E8 Etlist EpEy Don GEE Ai Fir rar Eid $s iF f E "3 E ] "gE UgrE oggTs8 ig Es 2 f5.s7 81fi3s7 g73381 :Poe Eth cE: 33.1 83; 8s siz 3g: zie LHg9 nEk tEgECEEEcCr ty fAg tEs oggm"Ee2 oginty8 iF2ie 3i EIRgEEEglELplBHa GEal Lgg=2O3iRlIEBI REYSEEgEfsRNBE?IRE3TI Table 19. Mean,range,geometric mean and 95% confidence interval ofgeometric mean ofserum fluorochemicals by longestjob categories among participants(N = 187)in chemical PFOS Mean Range G. Mean 95% C.I. PFHS Mean Range G. Mean 95% C.I. ETE C2E Ce Cell Operator' (N = 3) Chemical Operatorb (N = 77) Engineer/ LW (N = 31) Maintenance (N = 20) Mill Operator` (N = 26) 1.298 0.700-2.260 1.139`'' 0.571-2.274 2.008 0.093-7.880 1.638`'`'.& 1.385-1.936 0.486 0.081 - 1.740 0.313ab.de.&h 0.224-0.436 2.162 0.291 - 10.600 1.450`,`-g 0.988 -- 2.128 0.628 0.052 - 2.040 0.508b.c.d4h 0.386-0.669 0.762 0.381 - 1.200 0.686` -e~ g 0.358- 1.314 0.522 0.009- 1.880 0.3590'de.t9 0.292-0.441 0.106 1.005-0.420 0.061 ab,e 0.041 -0.091 0.340 0.023- 1.250 0.192ab.ae.'s 0.120-0.309 0.080 0.001 -0.374 0.0528-"-d 0.035-0.078 Secretary' (N = 7) Supervisor/ Mgmtg (N = 15) 0.370 0.129-- 1.140 0.291 ab.dh 0.176 - 0.480 0.740 0.091 -2.090 0.543"" 0.350-0.842 0.067 0.027 - 0,172 0.056ab.d 0.036-0.088 0.164 0.010-0.445 0.0958-11- 0.050-0.182 Waste Operatorh (N = 3) 2.388 0.254 - 4.840 1.365c' c, 0.245 - 7.600 0.256 0.038 -- 0.562 0.153 0.033 - 0.703 2 Cir Cgy Cid enw POAA Mean Range G. Mean 95% C.I. Bi CE1eIo8S7g 0.578 0.470 - 0.749 0.566 "0.428 - 0.749 2.231 0.052 - 6.760 1.863a`,dr,g 1.592 - 2.180 0.246 0.024- 1.000 0.170ab,de.h 0.124 -0.235 1.636 0.211 -4.680 1.147 ,`[8 0.780 - 1.686 1.203 0.015 -- 2.340 0.985b.c.rg 0.686- 1.413 0.138 0.053 --- 0.261 0.12 I ab.de.h 0.080 - 0.184 0.496 0.021 - 1.790 0.250b.d.e.h 0.131 -0.480 2.219 0.936 - 3.680 1.915` g 0.881 -4.166 E PFOSAA Mean Range G. Mean 95% C.I. =2 ORT ET 0.019 0.001 -0.051 0.006 0.001 -0.056 0.035 0.001 -0.269 0.01 1`f8 0.008 - 0.016 0.010 0.001 -0.073 0.004"" 0.002-0.006 5s7sipT c87p8 0.033 0.001 -0.125 0.014" 0.007 - 0.027 0.021 0.003 - 0.049 0.016`,!g 0.012-0.022 0.001 0.001 -0.004 0.001 bale 0.001 -0.002 0.007 0.001 -0.019 0.004,"l` 0.002 - 0.007 0.008 0.003 -0.016 0.006 0.002 -- 0.016 2 M570 Mean Range G. Mean 95% C.I. BR BI u7 0.064 0.001 -0.169 0.027", 0.004-0.164 0.259 0.009 - 3.100 0.1290"e e.te 0.099-0.169 0.050 0.004-0.164 0.036". 0.026-0.049 I.E 3;GE8E1 0.242 0.038 - 0.701 0.186a``'s 0.131 -0.263 0.045 0.023 - 0.115 0.042". 0.037 - 0.048 0.031 0.010 - 0.072 0.026b.d 0.015 - 0.042 0.067 0.013 - 0.201 0.051 b.d 0.035 - 0.076 0.104 0.053-0.159 0.094 0.050-O.i77 sf{ | s38 8 838 _z.z 8 & B gf o Lf or hEi Eoae iE Riiy tEi E LgEg Po. sis saz giz zi Eak FPoo8hE rTs E oTseigx mETEE sOlEaE sOlEgE FgtoofB]58h;riE&r: ornmagrl BlmiSIEI 8o31n8sy% h1Eug81 HH 32 3B7L8E7 L87E8E% Sg:E8 TT3L13E ETE CEE og g.8 Bi2ga g BEiTs CEEnsd _ gEiRa] g23E3 2 I "ETE Cy.: Hs PL BEog R 8 gE WSaidteioAvaioliParbloeebcyhe3MOfrodrIenrs1pepctaimonearvn.d3CopNyoi.ng03as04Co6n3f0i5dent Ifomatn 28122..00068 01 EPI-0006 Page 68 of85 PgLEi INPoLE o2S%5 e13d%onf39a3i7 Table 19. (continued) PFOSA Mean Range G. Mean 95% C.I. 0.008 0.001- 0.015 0.004 0.001 -- 0.031 0.079 0.001 -0.487 0.017`6 0.011 -0.026 0.011 0.001 -0.063 0.003b'd'` 0.002 - 0.006 . (gud EE15E7 0.087 0.001 -0.612 0.012`'6 0.005 - 0.029 0.029 0.010 - 0.204 0.017" 0.011 -0.025 0.021 0.003-0.080 0.0136 0.006 - 0.028 2 : FEE Ei 17y M556 Mean Range G. Mean 95% C.I. 0.0 i 3 0.003 - 0.035 0.006b'ah 0.001- 0.034 0.074 0.001 -0.380 0.042''"-f6 0.033-0.055 0.012 0.002 - 0.040 0.008bd,h 0.006 - 0.011 0.093 0.008 - 0.406 0.014 0.002 - 0.045 0.0542'"f'6 0.011'b d 0.034-0.086 0.008-0.014 (a-h)comparison for each longestjob category using student's t, p <.05 0.012 0.003-0.030 0.008b'ah 0.004 - 0.017 EEE PY 8E1E8 BE 0.021 0.001 -0.173 0.014 0.005 - 0.027 0.003b'" d 0.012 0.001 -0.007 0.005-0.029 0.019 0.003 - 0.059 0.013b'd 0.007 0.021 0.067 0.010-0.157 0.03" 78 0.008 - 0.180 ERE JF 1 : lowsX0111YIND, aMA100S0501 MacevialFeesbtyi3iorr neerctBioanmaandiChopyiing53a:5C4a5n3f0e8ntal information 2812..000069 U)K -~ a y - 0 0s rn o rn O o 8 Cn m O1 a rn < v W 0 Z-0 o g N CD N ~ C7 o w Q0 m o 3 R M !dil~i~~iId,/1E~ awatoos0s02 5= 8M7"3 h83 o2S3pz:5S3g Ss 3 8h i3: g 23 oF 5 53%37Bf8Tg fg373 g53g s3 F 2i% g8z=d ok iE fd. $23E8E38) i $8T;0.e3% 2 i=s c5 i 222 2k TEs )oL BPI-0006 Page 69of85 a7 3Ez, :{oe S$e2x5) 2$8222h is 5 $2 325288 5] 8 : 5 08 EZ of 3 32 03 s2e9 28%; 87ef 8#72 E1p Bp27 5B7r 2Ec% 8B%g 8BsEE;s Table 20. Mean,range,geometric mean and 95% confidence interval ofgeometric mean ofserum fluorochemicals ofall participants(N = 187)who currently work in only one building/area in chemical Bldg. 1 (N=23) Bldgs. 2/49 (N=12) Bldg. 3 (N=30) Bldg. 4MX (N=20) Bldg. 4N (N=5) Waste water (N=4) PFOS Mean Range 0.686 0.081 -2.190 2.257 0.325-6.840 2.426 0.189 - 7.260 0.556 0.052- 1.620 2.000 1.440 - 2.670 2.763 0.254 - 7.880 S 8 ER c s BE1735] 87 #38 24"833p 8 8F%s 373 G. Mean 95% C.I. PFHS Mean Range 0.438 0.281 -0.681 0.194 0.013-0.713 1.727 1.023 - 2.916 0.870 0.076- 1.880 2.000 1.544 - 2.590 0.567 0.139- 1.860 0.468 0.336 --- 0.653 0.079 0.001 -0.374 1.937 1.378 - 2.723 0.450 0.161 -0.832 1.369 0.136 - 13.741 0.386 0.038 -1.210 s8x 2 2C1E%C]E 2% 8%8 SLTT3Ep $ 533p 5I%p 2 2 E- 3 3 os& 5#s8 ff =f EELCERDECIECEE == gl3 8%3 8%3 SzTs od7gE SpCESsz & gz g3sg =A%p 584S 8Sf 8 BwD"2f1BYF 3273Bo8d%e 3s 8b i3isEib3p 3zg 32 GBg 32 oF G. Mean 95% C.I. POAA Mean Range 0.101 0.059-0.173 0.426 0.024 - 2.700 0.585 0.292- 1.171 1.807 0.126 - 3.640 0.417 0.309-0.561 2.665 0.261- 6.760 0.050 0.030 - 0.084 1.176 0.015 - 2.110 0.397 0.192 - 0.821 2.088 1.300 - 2.860 0.177 0.018- 1.729 1.804 0.936 -- 2.710 G. Mean 95% C.I. PFOSAA Mean Range 0.200 0.119 - 0.331 0.010 0001-0.054 1.247 0.631 -2.461 0.008 0.001 -0.051 2.111 1.587 -2.809 0.049 0.002 - 0.269 0.927 0.568 -1.515 0.021 0.002 - 0.049 2.024 1.420 - 2.886 0.019 0.004-0.043 1.677 0.815 - 3.452 0.010 0.003 -0.017 z3 Bi T"EBET 23g%fz83g% s3 =3 8% ECEECE gs2 af3 33CE3Eg &8 % sItg gIdg 38 8 8g%CEEaE3 s3gfoES&fg 33 ib ii ggd of G. Mean 95% C.I. M570 Mean Range 0.002 0.002-0.006 0.077 0.006-0.410 0.003 0.001 -0.007 0.043 0.010 - 0.169 0.020 0.012 - 0.034 0.481 0.063 - 3.100 0.015 0.010 - 0.024 0.040 0.024 - 0.613 0.011 0.003 - 0.048 0.099 0.054 -0.205 0.007 0.002 - 0.031 0.091 0.050 - 0.159 G. Mean 95% C.I. 0.050 0.033-0.075 0.031 0.018 - 0.052 0.348 0.260-0.465 0.039 0.035 -- 0.044 0.088 0.047 - 0.165 0.081 0.034 - 0.195 MSuabdjeecAtvoaiaPrbolteecbtyiv3eMOfrodrerInIsnpePcatiiomneavrn.d3C.opNyoi.ngC2a-s0C4o-n6f3id0e9ntial Information 2881122..00070 U)K cD a D 0 v rn CD CD w O CD 0 oL a CD ~a o -0 o n N v C)0 rn 0 oQ QO m 3 0 3 R o' 0 ~~il~i~~iI~l,/1E~ 3MAT0050503 ERE I 22.g 38g5 <5 2z 3: 5833 2oi%f] g2 E2 Table 20. (continued) PFOSA Mean Range 0.018 0.0005-0.161 89 33:9 88 pF d io5F z fof 2a G. Mean 95% C.I. M556 Mean Range 0.005 0.003 - 0.010 0.021 0.003 - 0.127 G. Mean 95% C.I. Years in chemical Mean 5;3 0.013 0.008-0.020 20 2 0.006 0.0005-0.021 0.003 0.002-0.006 0.013 0.003 - 0.347 0.010 0.006 - 0.017 19 0.109 0.003 - 0.569 0.037 0.020 - 0.066 0.121 0.024 - 0.380 0.095 0.073 -0.125 10 8&8 8 gs 85 87 85 = EglPRI2rE7 ozs7 :8d 3 z 3 tg Sg 82 34% 0.028 0.0005 - 0.204 0.017 0.010 - 0.028 0.251 0.003-0.487 0.059 0.002- 1.595 0.011 0.002-0.030 0.010 0.007 - 0.013 0.076 0.025 - 0.175 0.057 0.019-0.163 3 13 5 5 o& oe 5%7 8f7g 5f7 dET 7 %8&3 873%87 A -gz sEB a8 SE2E8 jiii EPi-0006 Page 70 of85 0.007 0.002-0.011 0.006 0.002- 0.019 0.055 0.015 - 0.157 0.033 0.006 - 0.193 13 2 WSaidboelAvaioliParbloetbeych3HrfioerrnspePcailamneavrn.dWChopyNoi.ngC2a.s0C4o-6n3f0d9enal nortan 2881122..0007711 e= v cD m ov o s rn CD 0,9 rn Oo E n -0 m 2 a rn 0 v 5 z W ~ C7 0 Z.- c 0 C7 CO ry N CD C7 o w ~+ Q0 N o 3 n~ R M i1il~i~~iId,/1E~ aMAt0050504 ii EPI-0006 Page 71 of85 3 gL] { 32 i & ooo 2:: #4 I 4 #8 2.3 3 i 8 = z #3] 8% gc 8S gs as 2 gd gs gf 3 PsTY Ee et31e8] 3e1t81s 3t1e3;r 5,tit8e. 813% te 5 82 it 2E 8 252 43di} oiF 93di o2R 33g 2 ofi338loF 3did 2 E iiz Table 21. Mean,range,geometric mean and 95% confidence interval ofgeometric mean for all participants(N = 187)who said they have only worke in one building/area in chemical g PFOS Mean Range G. Mean 95% C.I. PFHS Mean Range G. Mean 95% C.I. POAA Mean Range G. Mean 95% C.I. PFOSAA Mean Rang-, G. Mean 95% C.I. M570 Mean Range G. Mean Bldg. I (N = 11) 0.432 0.081 - 1.700 0.282 0.150-0.529 0.100 0.013-0.42 0.058 0.027-0.124 0.155 0.024 - 0.386 0.115 0.064 - 0.201 0.003 nnnl nnI+ 0.002 0.001 -0.003 0.062 0.02-0.201 0.041 fp 8D ff 7% rox os O"OBgEEyE O3EE IpEg fg R"OIEEEF S13 8.8 E"C2BT;EF 33 dz 203 $175e8] Bldg. 3 (N = 8) 2.693 1.450- 5.120 2.427 1.619-3.638 0.890 0.151- 1.860 0.578 0.236- 1.420 2.947 0.366 - 6.760 2.079 0.923 -4.681 0.027 AOe A 1 io 0.014 0.005 -0.036 0.308 0.03-0.480 0.270 Bldg.4 MX (N=17) 0.501 0.052 - 0.383 0.467 0.321 -0.681 0.053 0.01-0.152 0.045 0.026 - 0.076 0.987 0.015 - 1.850 0.817 0.467- 1.429 0.023 n nn' n non 0.017 0.011 -0.026 0.044 0.026-0.061 0.045 2 2 : 3g3c : :=E 3 Kil~i~~iI~l,/1E~ MA10050505 ig MSuabdjeecAtvtaoiaPrbolteecbtyiv3eWOrodrIenrsIpnePctailomneavrn.d3CMo,pNyoi.ngC2a.s0C4o-n6f3id0e9ntial Information 28122..00072 Co K ~ v u (D a D - 0 0 rn CD rn Go a rn _ m 2 :a. rn v w OL ~;:0 0 z-0 o ~ C)CO N N A C7 &0 oQ CD m 0 3 0 3 R o' 0 3385 =38 GE& Gad5 3 Table 21. (continued) z g 2 2 95% C.I. PFOSA Mean Range G. Mean 95% C.I. M556 Mean Range G. Mean 95% C.1. Years in chemical Mean I os IS 0.021 -0.080 0.158-0.462 0.035-0.057 0.013 0.0005-0.060 0.006 0.002-0.016 0.017 0.04-0.059 0.012 0.006-0.023 20 5 5.8 s SE 0.151 0.003 - 0.569 0.059 0.013 - 0.266 0.095 0.05-0.214 0.080 0.047 - 0.136 17 0.031 0.0005-0.204 0.018 0.009 - 0.036 0.013 0.06-0.022 0.014 0.009 - 0.021 1.3 i: Csl I87 T55Est e g s 2Ion$8 g3e.2e Sg Sg 3% sg =| Z Br og .8 g Et > itii EPI-0006 Page 72 of85 MSuatdeocAtvtaolPaobtlecbhyv3e1OfrodIensnpePctailomnearvn.dWChopNyoi.ng62a.s0G4e.n6f3i0d5ental Information 28122..00073 K cD m ov 0 rn CD 7 CD w O EQ o E% '0 2 a rn 0 o,a0) ~n0 aMA1005008 3$ RILERI3I8RA21ILHEl s8%s 12 ;M EPI-0006 Page 73 of85 If 3.% ZR. sil z [FEIB [5a & TF 8s7 FR. =D 3| i| 3 i: 2 Fe% @RL SED 3 q3 2z 2 2 23 2 Sg ze 22% g 3 d3] msg P8 a9 55 Table 22. Mean,median and range, by gender,ofchemical operators and engineer/lab for random sample by age,BMI and years worked in chemical Age Mean Median Range 5 Chemical Operators Female Male 41.3 40 28-61 42.4 44 25-62 Female 36.0 35 23-54 Engineer/Lab Male 42.7 43 27-58 R BMI Mean Median Range 26.9 27.4 22.0-32.7 a - 28.6 28.4 20.2-47.5 " 24.0 22.2 20.7-30.2 8 29.0 28.2 18.5-38.4 - 5, 3E__5 Years Worked In Chemical Mean Median Range . 9.6 10.5 3-20 2 11.4 10.0 1-31 =zsg" 9.6 1.3 1-33 a 16.5 15.0 1-37 IEE g . gy IE|E &yy $1zPog ii i E51 5.2 igs 3 eEB1273 8 FTE; 43 Et i:8 5.8.8 Bf 2/81 87 fg: 82 & 2 2 z2& 32.85zl 8257 .g57 g5f8 33 "sTg S"g 23 d: : MRadioAovaiParlootbeych3HrfeorrnspPecaalnmaenrd3C4o0pyHiongCaos.0Co4n8fi4d5ent infomation 28122..00074 3M EP1-0006 Page 74 of85 | EF -2 8a 8=o F5 8= eo8 F3 5= z 3EE 8 8% B"L5 E]% E"Dg AD% E3TE% EgE)g 22 iz HH Table 23. Mean,range,geometric mean and 95% confidence interval ofgeometric mean ofserum fluorochemicals by gender for random sample chemical plant employees whose currentjob waschemical operator or engineer/lab a PFOS Mean Range Chemical Operators Female(N = 10) Male(N = 37) 1.183 0.471 -2.380 1.943 0.490 - 7.260 Engineer/Lab Female(N =6) Male(N = 17) 0.167 0.101 -0.281 0.799 0.095 -1.740 838d% i 3o%k gi8d = G. Mean 95% C.I. PFHS Mean Range 1.051 * 0.764- 1.447 0.190* 0.071 -0.404 1.625 1.345- 1.962 0.492 0.134- 1.860 0.157* 0.115 -0.214 0.032 0.005 - 0.081 0.540 0.336 - 0.868 0.220 0.018 - 0.905 5.8 8.3 n87d 5872 2378573 87s CECE 88 88 &7 F087 #7 5 8 FE 3.5.2.3 3% 97 39 87 g8 23 -83 3 5 o23F i=.3F & G. Mean 95% C.I. POAA Mean Range 0.167* 0.119 - 0.235 1.342* 0.150 - 2.110 0.364 0.285-0.465 2.497 0.745 -6.760 0.023* 0.011 -0.048 0.103 0.035 -0.300 0.121 0.069 - 0.210 0.473 0.051 -2.320 og$833gs2k2. 5 = G. Mean 95% C.I. PFOSAA Mean Range 0.129* 0.701 - 1.818 0.012 0.001 -0.109 2.168 1.829 - 2.570 0.041 0.001 -0.269 0.078* 0.043 - 0.141 0.004 0.001 -0.018 0.295 0.186 - 0.468 0.017 0.001 -0.073 zg 58 2E878H1E EE 8 8: it E17 8 8 8.2 9 &% g8gg o2If%3 giidf = G. Mean 95% C.I. M570 Mean Range 0.006 0.002 - 0.016 0.114 0.029 - 0.357 0.013 0.008-0.022 - 0.260 0.009 - 0.992 0.002 0.001 -0.005 0.046 0.020 - 0.093 0.008 0.004 -- 0.084 0.084 0.008 - 0.410 % $i81 L&E7 8 % &7 i 8 53 Ig ES g g8 oiiRg G. Mean 95% C.I. 0.087 0.055 - 0.139 0.146 0.099 - 0.217 0.039 0.024 - 0.064 0.053 0.033 - 0.084 L~iL~i~~iId,/1E~ awAtoososor MSuabdjeecAtv1aoiaPrbolteecbtyiv3e OfrodrIenrsIpneactiiomn eavn.a3C,opNyoi.ng2.as04Co6n3fi0d8ential Information 28122..00075 ~:Iil~i~~iI~l,/1E~ 3MAT0050508 c`n' m ov o rn CD rn 0 Q o CD E 0 oL a rn 0 a0) ~n zs : o n~ CN) CvO 0 oQ cfl m 3 0 3 R 0o' & z2 E e48251}EcH%3 gsiii6:%S|y| g i 5 Table 23. (continued) PFOSA Mean Range G. Mean 95% C.I. M556 Mean Range G. Mean 95% C.I. * p < 0.05 is " 0.063 0.003 - 0.315 0.022 0.007 -0.062 0.041 0.007 - 0.118 0.027 0.014 - 0.050 =8 "8 a;"2 28 ga g8 Hn oy 8 8 8 3% 0.109 0.001 -0.487 0.030 0.016 -- 0.055 0.083 0.001- 0.380 0.050 0.035 -0.073 EPI-0006 Page 75 of85 2 gE z 5 2 =S 23 gs gs 5.g$ 8833 8 88 258 ES32 8% 0.017 0.0005 - 0.063 0.005 0.001 -0.024 0.010 0.003 - 0.02.7 0.007 0.004 - 0.014 0.017 0.0005 -0.060 0.004 0.002 - 0.010 0.022 0.002 - 0.127 0.010 0.006 - 0.019 BZ 5% ge 3EMPMm10006 PEPaaPg1ge-e07T0660oo6ff8855 T`Taabbllee 2244.. 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DDeemmooggrraapphhiicc cchhaarraacctteerriissttiiccssooffrraannddoomm ssaammppllee ooffffiillmm ppllaanntt eemmppllooyyeeeess bbyy ccuurrrreennttjjoobb work in chemical) c`caatteeggoorriieess wwhhoo hhaavvee wwoorrkkeedd oonnllyy iinn tthhee ffiillmm ppllaanntt((ii..ec..,,nnoott oonn tthhee DD--1I MMaakkeerr oorr pprriioorr work in chemical) AAMggeeean SSMMEeEedainan Median RRaannggee BBMMMIIean SMSMeEeEdainan RRMaaendngigeaen YYeeaarrss wwoorrkkeedd `Mean IInn ffiillmm Mean SSMMEeeEddiiaann RRaannggee GGeennddeerr FFeemmaallee MMaallee Contact HHaanndd ttoo Contact mmoouutthh YYeess NNoo `WWaasshh hhaannddss YYeess NNoo EnEnggiinneeeerr//LLaabb (NN==1010)) 44626 8 a2.8 48 2233--5588 22618.58 231.5 27.3 22116.6--3311.77 1144.38 1522.99 15 00.11--2299 22 (Q20o) 88 ((8800)) 8 8 2 2 (((Q828000o))) 88 ((8800)) 22 (Q20o) FFiillmm PPrroocceessssoorr (NN==1212)) 4"425 4a277.5 2277--5599 2881.646 22717..884 1188.00--4411.88 MaMianintteennaannccee (NN==7)7) 34005 03.3 10 3311--5511 181.757 251.8 '.9.5 224411--3322.99 AAddmmiinniissttrraattiivvee (NN==177)) 4a833 53.3 50 4400--555S 22912.52 22717..998 2244.44--4411.88 1144.11 1722.66 17 00.55--2299 44.66 333.44 3 00.`---1122 2200.44 2533.44 25 55--2288 22 (a17n) 1100 (8833)) 00 (0)) 77 ((11000)) 22 (29) 55 (m71m) rm 1100 ((8833)) 2 (17) 1100 (8833)) 22 (a17n) 4334 @((()4573N)) 66 ((8866)) 11 ((1144)) 4343 @ ((5571) (43) 44 (657N) 33 (@43)) MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbtyyiv33eMMOfrfoodrrIenrInsIspnpeePcctatiiloomnneaavrnn.dd3CC,ooppyNyoii.nnggC2aa-ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00080 3MA10050513 3MA10050513 3wEPMmL-0008 PEPaPaIgg-ee0880110o6off3855 TTaabbllee2299.. MsMeeeraaunnm,,lrraaunnoggreeo,,cggheeeooimmceeattrlriisccfmomreeraaannnaadnnoddm99s55a%%mpcclooeonnfffiieddmeepnnccleeoyiinnetteeesrrvvwaallhoooffhggaeevooemmeeottnrrliiyccwmmoeeraaknnedooff siinnetrthhueemfffiilllummorppollacannhtte(micii..cea.,lnnsoofttooronnrattnhhedeDoD-m-11saMMmapkleaerooofrrkeppmrripioelororywweoroerrskkwihocchhheeammviieccoaalnl)l)y worked it PPMFFeOOSSan RMRaaennaggnee G9G..5MM%eeCaaLnn 95% C.I. PPFFMHHeSSan RRMaaennaggnee GG9..5MM%eeCaaLnn 95% C.I. PPOMOAAeAAan RMRaaennaggnee GG9..5MM%eeCaaLnn 95% C.I. PPFFMOOeSSaAAnAA RMRaeanaggnee GG9..5MM%eeCaaLnn 95% C.I. MM55M77e00an RMRaaennaggnee GG9..%MMCeeaaLnn 95% C.I. MM5M55e66an RMRaaennaggnee GG9..5%MMCeeIaa.nn 95% C.I. EEnnggiinneeeerrl/LLaabb' (aN==1100)) 005500.-00099.77140 0.055-0.140 007400.-00099.331`16 0.074 - 0.116 000010.-0010160675 0.001- 0.075 000005.0-000099018 0.005-0.018 000006.0-030300055 0.006-0.055 001004.00-2202`03 0.014-0.036 000001.0-000022005 0.001 -0.005 000001.0-000022003 0.001 -0.003 000002.0-000066017 0.002 - 0.017 000004.0-0000550`07 0.004-0.007 000000.0100-0202 003 0.0001 -0.003 000001.0-0000110"603 0.001 -0.003 FFiillmm PPrroocceessssoorb (NN==1212)) 0003.02.1-120277250 0.032-0.250 007004..-1100066154 0.074-0.154 000004.0-010155047 0.004-0.047 0000o7.o-0n101017 0.007-0.017 000007.0-050555154 0.007 - 0.154 002004.0-044011068 0.024-0.068 000001.0-000022009 0.001 -0.009 000001.0-0000202 03 0.001 -0.003 000003.0-040488456 0.003 - 0.454 000004.0-010100022 0.004-0.022 000003.0-020299307 0.003-0.307 000002..-00000550811 0.002-0.011 MMaaiinntteennaannccee'` (N==77)) 013007..-1105599116 0.137 - 0.:16 013009.1-1505771'77 0.139-0.177 000001.00-1160634 0.001 -0134 0000o5.o-0n101026 0.005 - 0.(26 0002.00.0-09908828 0.021- 0.298 0030o-.o00n711232 0.038 - 0.132 000001.0-000022006 0.001 -0106 000001.0-000022003 0.001 -0103 000006.00-1180846 0.006-0146 0000[9,-0I01' 40824 0.009-0124 000001.00-0050516 0.001 -0116 000002.0-000044607 0.002-0.007 AAddmmiinniissttrraattiivvee' (NN==77)) 0050o4.-n101t1166 0.054-0.166 0.07007..-11000.44140 0.077 - 0.140 000006.0-010122033 0.006 - 0.033 000006.0-010100016 0.006 - 0.016 001007.0-030399063 0.017-0.063 002004.0-030355051 0.024-0.051 0.0000.100-00044006 0.001 -0.006 0.0000.200-00044006 0.002-0.006 000001.0-000055009 0.001 -0.009 0.0000.200-0004.4`007 0.002-0.007 0.0000..100-00022.003 0.001 -0.003 0.0000..200-00022003 0.002-0.003 ((a2--4d))ccoommppaarriissoonnss ffoorr ecaacchhccuurrrreennttjjoobb ccaatteeggoorryy uussiinngg ssttuuddeenntt''ss t MSMuaabddjeeecAAtvvafaoillaParbbollteeecbbtyyiv33eMVOrffodorrIenrIsnIspnpeePccattliimooennraavnn.dd3CCMoo,ppyNyoii.nnggC2aa:ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 3MA10050514 3MA10050514 22881122..00008811 3aEPMML0006 PEPPaaIgg-ee088022006off8855 TTaabbllee3300.. ReRaamttpiilooooyofefeffslluuwoohrroooccohhenemlmiyicchaaallvlleeevvweeollrsskbbeyydcciuunrrrfeeinnlttmjoaobnbdaanmmoootnnoggnrrtaahnneddDoo-ri1nn ssMaaammkppellreeooffffiillmm employees who only have worked in film and not on the D-1 Maker PPFEMOOeSSa/InPPFFHHSS MReaMMdeendiaginaeann Range EEnnggiinneceerr/lLLaabb (ONN ==1100)) 11373.500 11.88--766.151.66 FFiillmm PPrroocceessssoorr (NN-=1212)) 111332.080 44.991--222.989.00 MMaaiinntteennaannccee (N==17)) 22142626 44.3312-21120077.66 AAddmmiinniissttrraattiivvee (NN==77) 11110.41 55.111--011.646.55 PPMFFeOOaSS/nPPOOAAAA MReaMMdeendiaginaeann Range 434.000 11.33--390..022 333.222 11.22--366..233 222177 00.77--2551.77 323.800 22.222-244..822 PPMFEOOeSSa//AAnnnaallyytteess MeMMdeediainaann RaRannggee 111000.544 22.111--011.757.88 11040.300 00.22--433.131.22 777110 44.00--711011.66 11292.544 55.22--933.757.66 PPMFFeOOaSSAnAAA/MMS5S566 MReaMMdenediaginaeann Range 33I.6x6 00.55--111.414.00 000.757 00.0000033.-5-11.55 011533 00.11 --0555.11 222.131 00.55--244..344 MMM5S7eT00a/MnMS5S566 RMaMMeeneddagiineaann Range 2885.66 11.00--244.555.00 331.161 00.66--111.868.44 555669 00.44--511900.55 222.866 00.33--255..855 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbtyyiv33eMMOrffodorrerIInnIssnppPeeaccttiiimooennrvaa.nndd3CC,ooppyNyoii.nnggC2aa-ss0CC4oo-nn6ff3iid0de9ennttiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00008822 3MA10050515, 3MA10050515 3EMPMm10006 PEPaPaIgg-ee08803306o0ff8855 TTaabbllee3311.. DDDee1mmooMggarrkaaepprhhiioccrccfhhiaarmraaccpttleearrniitssttwiiicctssohofpfraaellvlliffoiiullsmmhppillsaatnnottryppaairnrttcichiiecpmiaipnctaasn(l(tNNs == 7766))bbyy oonnllyy ffiillmm ppllaanntt,, D-1 Maker or film plant with previous history in chemical AAggeeMean SMSMeEeEdainan RaRMaenndggieean AAlll (oNN==7766)) 4a510 23.4a5719.0 23-59 OOnnllyy FFiillmm (NN==4499)) 4"436 2-44535.96 23-59 DD--11 MMaakkeerr (N==77)) 1"412 301"-.7751.52 30 -55 FFoiifllmmchwwei/mhhiiicssattloorryy o(fNNc=h=e2m20i0c))al 4a7721 28-5s1t25.81 28-58 BBMMMIIean MSeSMEdEeianan RaRMaenndgigeaen 22803.53 18220707-..959418 18.0-41.8 0228..565 18220707-..969418 18.0-41.8 266L.s6 7-2%613.5.5517 21.7-31.7 22881.505 20202818-..0300 79 20.0-37.9 YYIneeaafrrislsmwwoorrkkeedd InSMfMEeielamann MeSMdeEdiiaann RaRnanggee 11414.244 11616..002 00.11--3366.00 11545.22 11717..004 00.11--3300 883.151 232..050 11--221 11424.566 11255..050 11--3366 GGeFenneddmeearrle FMMeaamllaeele 1166 (Q21n) 6600 ((7799)) 88 ((1166)) 4a1 s(h84) 22 (@29)) 5so(m71) 66 (G300)) 144 ((700)) CCuuErrnrrgeeinnnttejjeoorbb/Lab. FEFniigllimmnpperreoorcc/eeLssassboorr MMaaiinntteennaannccee AdAdmmiinniissttraattiivvee M1188 s(Q)24h) ng 34 (45) 11 (14) 1B3 a(n17) 12202 s(@)25n) 2808 (((14616)) 99 (818) 0o 6 o6(0) 611 (((81464))) 0[I](0) 668 (G(30o0))) 822 (((41000)) 4a (20) LoLnoEnngggeeissnttejjeoorbb/Lab. FEFinigllimmnpperreoorcc/eeLssassboorr MAadMimaniintnietsentnarananctceie:ve Administrative 13H84 a((s1580) 31182 2((65106)) 122 (a16e) u88 ((411966)) 2949 8 (49) (18) 88 ((166)) 0[6 IO3(]60)) 6 1 ((a81649)) 0[I(]0) 668 (G@3000))) 822 (((41000)) 4Fae(2)0) HcHoaannntddact1to0 mmoouutthh coYnYteaescst NNoo 442997 27 ((((6366464)))) 31316%3 3@(((72)137))) 25s 2 o((m 7219)) 12882 60(((464)000))) `WWaasshh hhaannddss NYYoeess No 66n55 a((g8866)) 11 (14) 4wo09 (a82)y) 9 (18) 077o10(O 10(000))) 1182 80(a9000) 2 (10) MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbtyyiv33eMMOfrfoodrrerIInnIssnppeePccattiiioomnneaavrnn.dd3CCMoo,ppyNyoii.nngg2a-ass04CC-oonn6ff3ii0ddee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00008833 3MA10050516 3MA10050516 3TMEPMLO0DS PEPPaaIgg-ee0880440.6o0f18855 TTaabbllee 3322.. PPFFMOOeSSan RRMaaennaggnee MfMleeuaaonnr,o,crrhaaennmggieec,,aggleesoofmmoeerttarrliilccfmmileemaapnnlaaannntddp99ar55ti%%ciccpooannnfftiieddmeepnnccleeoyiienntteeesrrvvbaayll oowfofrggkeeoohmmieestttorrriiycc:mmoeenaalynnofofiflsmseeprrluaunmmt, D-1 MtMlaaukkoeerrrocoohrrefmfiiilclmmalppsllfaanontrt awwliilttfhhipplrrmeepvvliiaoonuutssphhaiirsstttioocrriyypaiinnntccehhmeepmmliioccyaaelles by work history: only film plant,D-1 Only Film* D1 Maker hFFiiislltmomrwwyiiittnhhcpphrreeemvviiicooauulss O(nNNl=y=4F94i9l))m' D-(TM1N=M=a7k7)e)rb histor(oyN=in=2c02h0e)m)ical` 003200-.1012229964 0.032-0.264 012200-.3304497746 0.122 - 0.946 008000.20222.00692 0.080-0.692 9GG5..%MMCeelaa.nn 95% C.I. 010010.-.110111663b%c3 0.101 -0.133 0.16800.-2027.7949"461 0.168 - 0.461 014400-.11088255"3'8 0.144 - 0.238 PPFFMHHeSSan RRaMaennaggnee 000100-.000110667 0.001 -0.075 000500-.000220230 0.005 - 0.030 000700-.0003328810 0.007 - 0.210 G9G.5.%MMCeelaan.n 95% C.I. 00090o-.0o010n11c 4 0.009 - 0.014 00.001199 00.001122--00.003300 00.002244"' 00.001166--00.003366 PPMOOeAAaAA n RaRMaennaggnee 0.00600.-0005527798 0.006-0.298 002000-..1014426690 0.020-0.290 001200-..1114426620 0.012 -1.220 9GG5..%MMCeeLaan.n 95% C.I. 003010.-.0004400056%10 0.031- 0.051 005400-..101002992"'1 0.054 - 0.221 004900-..000771882""4 0.049-0.124 PPMFEOeOSSaAAnAA RaRMaennaggnee 9GG5..%MMCeeLaaLnn 95% C.I. 000100-..0000003320 0.001- 0.020 000020.-.0000004403 0.002-0.003 000100-..0000006622 0.001 -0.022 000200-..0000004409 0.002 - 0.009 0.001000..00.0006638 0.001 -0.038 0.00200-.00000.33005 0.002-0.005 MMs5M77e00an RaRMaennaggnee 000100-.0001148854 0.001- 0.454 0.00200-.0003.391964 0.002-0.164 000100-.0001107769 0.001 -0.069 9GG5..%MMCeeaalnn 95% C.I. 000050.-.0000007709 0.005-0.009 0.00500-.0001.150546 0.005 -0.046 000600-.0001100016 0.006-0.016 MM5sMs5e66an RaRMaennaggnee 000000.1.00-00099307 0.0001- 0.307 000100-.0000006615 0.001 -0.015 AAllllll vvaalluueess <<LLOOQQ 9GG5..%MMCeeaalnn 95% C.I. 000200-..0000003304 0.002-0.004 0.00200-.0000.044008 0.002 - 0.008 ((aa-cc))ccoommppaarriissoonn ffoorreeaacchh ccuurrrreennttjjoobb ccaatteeggoorryy uussiinngg ssttuuddeenntt''s t,, pp <<.0055 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbtyyiv33eMMOfrfodorrerIInnIssnppeePccattiiimooennraavnn.dd3CCMoo,ppyNyoii.nngg2a-ass04CC-oonn6ff3ii0ddee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00008844 3MA10050517 3MA10050517 3MEPMI-0006 EPPPaaIgg-ee0880550o6off8855 TTaabbllee3333.. MfMleeuaaonnr,o,crrhaaennmggieec,,aggleesoofmmoeerttarrliilccfmmileemaapnnlaaannntddp99ar55t%%iciccpooannnfftiieddmeennpccleeoyiiennteteesrrvvwaahlloooffogngeleooymmweeottrrrikiccedmmeeinaannfoiolfmfsspeelrarnuutmm (f(iil..ue..o.,rnnooocttheoomnnicttahheelsDDf--o11rMaMalalkkfeeirlromorprlwwanootrrpkkaeerddtippcrrieepvvaiinootuuessmllpyyliionnyccehheeesmmiwicchaaoll))only worked in film plant PPFFMOOeSSan RaRManenaggnee EEnnggii=nnee1ee2rr//)LLaabb'' (N = 12) 00..110088 00.005555--00.17700 FFiillmm =PPrr2ooc0cee)ssssoorr"" (N = 20) 003002.1-130333264 0.032-0.264 MMaaiiNnntt-ee8nnaa)nnccee'' (N = 8) 013007..-1106688257 0.137 - 0.237 AAddmmiinNnii=sstu9raa)ttiivvee? (N = 9) 005004..-1100088166 0.054 - 0.166 9GG5..%MMeeCaaLnn 95% C.I. 008002..-11000212027 0.082 - 0.127 0.0800.011.1141448 0.088-0.148 014030.-11066' 51859, 1 0.143 -0.191 008001..-11000315`29 0.081 -0.129 PPFEMHHeSSan RaRManenaggnee 00.001188 00..000011--00.007755 0.0.001166 00.000044--00.005522 00.001166 00.000011--000.03344 00.001122 00.000066--000.03333 9GG.5. %MMCeelaaLnn 95% C.I. 000006.0-010111012 0.006 - 0.012 000009.0-010122017 0.009-0.017 00[0x06.-0101023 0.006 - 0.023 000007..-0001100015 0.007 -- 0.015 PPOOMAAeAAan RaRMaennaggnee 0.00006..-00044.99188 0.006 - 0.188 000700.-00055.55154 0.007 - 0.154 002001..-0009925598 0.021- 0.298 0.01007.0-03037.7063 0.017-0.063 GG9..5%MMeeCaaLnn 95% C.I. 001007..-00303110054 0.017 - 0.054 00..004400 00.002277--00.006600 00..007722"8 00.00422--00.21244 00.003333 00.002255--000.04466 PPMFFeOOSSaAAnAA RaRManenaggnee 00..000022 00..000011--00.000055 0.00100..-00000.55020 0.001 -0.020 000001..-0000044017 0.001 -0.017 000001..-0000044006 0.001 -0.006 GG9..5%MMeeCaaLnn 95% C.I. 000001..-0000022003 0.001 -0.003 0.00020.-00000.33005 0.002-0.005 000001..-0000022005 0.001 -0.005 000002..-0000033005 0.002 - 0.005 MMs57M7e00an RaMRaennaggnee 000002..-0000066017 0.002-0.017 000002.0-030311454 0.002-0.454 000006..-0001177046 0.006 - 0.046 000001..-0000055009 0.001 -0.009 G9G.5.%MMCeelaaLnn 95% C.I. 0.00003..-00000.55007 0.003-0.007 000005.0-000088013 0.005 - 0.013 00.001144 00.000099--00.002222 00..000044 00.000022--00.000066 MM5SSM5e66an RaRMaennaggnee 000000..1000-0202007 0.0001 -0.007 0.00100.-00101939 07 0.001 -0.307 000001..-0000055016 0.001 - 0.016 000001..-0000033006 0.001 -0.006 GG9..5%MMeeCaalnn. 95% C.I. 00..000011"1 00..000011--00..000033 00..000044"3 00.000022--000.00066 00.001144 00.000022--00.000077 00..000022 00.000022--00.000033 ((aa-cc)) ccoommppaarriissoonnssffoorr eeaacchh ccuurrrreennttjjoobb ccaatteeggoorryy uussiinngg ssttuuddeenntt''ss{t,,pp <<.0055 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbtyyiv33eMMOfrfodorrerIInnIssnppeePccattiiimooennraavnn.dd3CCMoo,ppyNyoii.nngg2a-ass04CC-oonn6ff3ii0ddee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00008855 3MA10050518 3MA10050518 AAppppeennddiixx AA. DDeeccaattuurr PPllaanntt MMaappss AAPppappgeeenndd1iixx AA Page 1 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00008866 3MA10050519 3MA10050519 re rey JoAprpeenngdeiex A2 PFaegee 2 Crile ety 2= EL al | als SE Bo o y fg o Be i: ; 00 fBrf Slat] PROJP8.1 ---------------------- s Fer Ler al |, EL Sofa ET ffi EE f[y seeFol gel' EELxE fi aig 3 fo flx .1s qJrH Loh = 3 3 RL ha le LEN Ta me]| aad EER FL RpamsilBalg yt i Ee 2 5lge Li Ag B |g io= e Fe qT th Lf// ALL 5 BI| my l[5// : a f= D dei z : z< 3: inch = 470 feet - Peasy] |b m Ee dn :i 4 : Jeg =asd1e a hi 4. TA 4 EWaderAiaakbyb Stor speb cton ay ns CopyS2s Ceonti fomatn Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 awnronse 3MA10050520 22881122..00008877 saeperti Appendix A Page 3 3M Decatur Chemical Plant 3M Chemical {i " idi000 7u] tri Pi !/ 2 a B&B FL Li od 2 ' i Fo. v giPo o 8Te |1 x 8 fe oem eb]f "W- ."k Nt.4.11" 4. IS qjrH Jg!I | a[iiE] Ei id 8 gl |1|ilEEl ii Pl ER lee| i] fs fg pr Ha ned t %3 iPT Z-4 N w I M 43 2 qtkn ]i-g, Ra * ,J RNRIN." [Fin| lB 3H sn ii lE5o8 PCl Os Pl ! pill "f0 ei co T[=ow)iv] TV ! Gn HEHE + 0010'... | mE a bi Gi 3 hr s:b Es] yr. ik | Be [i] sour 'IS PUZ z Mace Avaiabl oy 3 or Inspection ana Copying a Confident nfomaton Made Available by 3M for Inspection and Copying as Confidential Information: Subect io Pecks Orde In Palme Hh 62.04 6308 Subject to Protective Order In Palmer v. 3M, No.C2-04-6309 22881122..00008888 aMto0sos21 3MA10050521 AAppppeenndidxiBBx SSttuuddyy QQuueessttiioonnnnaaiirree APApappgpeeenndd1iixx BB Page 1 SMMuaabddjeeecAAtvvataoiillPaarbbollteeebcbiyyv33eMVOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00008899 3MA10050522 3MA10050522 DECATUR EMPLOYEE QUESTIONNAIRiE DECATUR EMPLOYEE QUESTIONNAIRE APspaopgpeeenndd2iixx B3 Paae 2 TaTnhhaannkkinyyotouneffooarppppraaorrpttriicciiiapptaaettiibnnoggx.iinn this this research research study. study. PPlleeaasse rreessppoonndd tfoo eeaacchh qquueessttiioonn wwiithh eeiitthhereara sshhoortt aannsswweerr oorr an `x' in the appropriate box. NAME EEMMPPLLOOYYEEEE NNUUMMBBEERR, NAME 1. Have youeverworkedin tthheeCChheemmiiccaall Pllaanntt?? YYeess u O NNoo O 1. Have you everworked in iIf 2n0o,, pplleeaassee ggoo ttoo qquueessttiioonn 22 yes If 'yes' a. Howmany yearshaveyouworked in the chemical plant? Years=___ a. How many years have you worked in the chemical plant? Years= b. Whatyeardid you tart working in th chemical plant? Year=___ b. What year did you start working in the chemical plant? Year = 2. Please indicate if you haveeverworked in the following areas. Mark an i 1 boxes that applytoyou Please indicate if you have ever worked in the following areas. Mark an 'x' in all boxes that apply to you. O suidng1 Building 1 u 1 Buidings Buildings 3388 aanndd/oorr 5511 C0 Buuilididngsi22aannnddo/gorr4s499 u OI BBuuiildiinngg 4422((PaPckaagcinkgFaFCgCiiinneenrstgs)) 0 uic3 (iOSnCUOgSF ares) u O suin6g1 Building 3(OSCUOSF area) Building 61 OI Buiing 3 besides OSCUOarSeFa) Building 3(besides OSCUOSF area) C[FFiilmm PPllaantt al(all buildings) buildings) u O Bsuiludinig44nNNoogrnth 0 ui4miilloomniextrgucer u 00WaoWsattse(et(rBwe@uawuiatildtedierinnrggttssrr3e3eaa66ttmaamennenddntt57pp7)ll)aanntt E. Building 4 millroom/extruder u Other O Bsuiuldiinng 11g77 (FPlleoassse pspeeceif)y) 3. 3. Taihnnisknwkieinrnggheaabbofoouultltotwhhieenjjgooqbbuttehhsaatttiyoynoosu.uwwoorrkkedeffodortthhele lonogestnppeerrigioodd oeff tmismeewwhthiile employed employed aatt 33MM DDeeccaattuurr,, pplleeaassee answer the following questions. aa. JJdoobbitiittlee;: bb.. WWhheennddiiddyyoouuwwoorrkk thheerree:: FFrromom_(y(yeeaarn)tt)oo ((jyeeaanr)) c. AvAveerraaggee nnuummbbeerrooff hoouurrsspprerwweeeekkoonntthhiissjjoobb?? HHoouurrss== 4 When you worked oovveerrttiimmee,,wwhhaatt wwaass yyoouurruussuuaalljjoobbaassssiginmgenat?ment?_________ d. When you worked 4. PPleeaassee aannsswweerr tthhe following following qquueessttiioonnss rreeggaarrddiinnggyoyuourrucurrreennt jotobb. CuCurrernentt lplaanntt: CChheemmiiccaall u0 Ffiilmm u 0 Gurrjoebtnet: Current job title: `WWhhaatt yyeeaarr diidd you tat working you start working inthis current job: in this current job: Year= Year = om Other LOj SMMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbtyyiv33eMMOfrfoodrreIrnIsnIspnpePecactitimiooennr vaa.nndd3CC,ooppyyNoii.nnggC 2aa-ss0CC4oo-nn6ff3iid0de9ennttiaall Information Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00009900 3MA10050523 3MA10050523 AAPppappgeeenndd3iixx BB Page 3 AAvveerraaggee nnuummbbeerr ooff ohouurrssppeerrwweeeekk oonn When you work overtime, what is your tthhiiss joobb:: usual job Hours = Haousrss=ignment?___ _ __ _ _ When you work overtime, what is your usual job assignment? 5. PPlleeaassee iinnddiiccaattee iinn wwhhiicchh aarreeaa((ss)) yyoouu wwoorrkk iinn yyoouurr cCuurrreennttjjoobb..MMaarrkk aann 'x' iinn aallll bbooxxeess tthhaatt aappppllyy t1o0 yyoouu.. 0u Bsuiulidinngg11 u DO BBuiuldiingls33d88aianndndl/ogorr5s511 0u Buil2daindnlogr4s9. u DO Building42 ((PaPckaagcikngaFFCgCiinineenrrttgss)) Building 42 Buildings 2 and/or 49 u 0 BBuiludinig33k((OOSiSCCLnUIOOSgSFF aarreeaa)) u 0suBiuidlidinngg 6611 u Building 3(besidesOSCUOaSreFa) OSCUOSF area) u [J FFiillmmPPllaanntt((aalllbubuiillddiinnggss)) Building 3(besides u DO BBuiuldiindg44iNNnoortgthh u 0 su4 mii lloomn /extrg uder Building 4 millroom/extruder u 0 Bsuuilidningg 1177 u 0 WWaasstt(eewuwaiadttieenrrgttsrr3eea6attammneednntt57pp)llaanntt u O(POolteeh(aerBrsueilsdpiencgisfy36 and 57) -- (Please specify) 6. WWhihleaaittwwoolrrkk,,dedoo yyoouucchheeww gguumm?? 6. Ouawalawyayss uO ffrreeqquueennttlyy [uJ ssoommeettiimmeess u OJ rraarreellyy u [J nneevveerr 7. WWhilheaaittwwoolrrkk.,eddoo yyoouucchheewwltoobbaaccccoo?? Ou aa. sways always u 0 ffrreeqquueennttllyy OuJ ssoommeettiimmeess u [J rraarreellyy u [J nneevveerr 5. WWhhiilleeaattwwoorrkk,, ddoo yyoouu ssmmookkee cciiggaarreettteess?? DuOaamlwaayyss u DO frequenty frequently u OJ ssoommeettiimmeess u OJ rraarreellyy u [J nneevveerr 99.. HHooww ffrreeqquueennttllyyddooyyoouuwwaasshhyyoouurrhhaannddssbbeeffoorreeeaetatiinnggwwhhiilleeaattwwoorrkk?? MMaarrkkoonnllyy oonnee bbooxx.. Ouamalawyayss u 0 ffrreeqquueennttllyy u OJ ssoommeettiimmeess u (J rraarreellyy u CJ nneevveerr 1100._ WWhhaatt iissyyoouurrhheeiigghhtt?? 1111.. WWhhaatt iissyyoouurrwweeiigghhtt Feot= Feet = PPoouunndsd=s= Inches = Inches = MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00009911 3MA10050524 3MA10050524 APrpaopgpeeenndd1iixx C Page 1 Appendix C Appendix C DDiisstter`iiAbbmuutotiinoognnoCofhfeFFmlliuucooarrlooccEhhmeepmmliioccayallessesaa(nnNdd TT=hhee1ii2rr6)NNaaittnuutrraeallRLLaoonggdTTorrmaannSssaffmooprrlmmeaattiioonn Among Chemical Employees(N = 126)in the Random Sample SMMuaabddjeeecAAtvvataoiillPaarbbollteeecbbtyyiv33eMMOfrfodorreIrnIsnIspnpeePcctatilioomnneaavrnn.dd3CC,ooppyNyoii.nnggC2aa-ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00009022 3SMMAA1100005500552255 RCCahhneedmmiioccmaa)lSaPPmlaapnnltte PFOS oom Random Sample PFOS ppm I || n3 ||| E i 1 4) maximum maximum qqmueuadriittialene qunile median quartile minimum minimum CQluu1aa0nntt0ii0le%ess 99919010.0555.%%%0% 99977005..0050%%%% 57520505..0000%%%% 21215005..00%09%%0 0200..5055%%%% 0.0% Mean MMoommeennttss SMSStteddeaDEnervovr Mean SUULtppodppweeEerrrrr999or555%M%%eMMMaeeenaaannn LNNSouwmeWre9i5gh%tsMean Sum Weights 111000.666000000 17073..111638802770 311L..9a19232o852 0100..24411444s000 0000..012190101252 0091 0.091 0.091 11L.55e0044z77 0011..1716441832%%62 121116..2027202800098040 1260000 126.0000 126.0000 ShTTaepeissrttoflooWrriNNlookrmmWaallitTteyyst Shapir0o7-W4i3l9kWW9oW TesPPtr0r.oo0b0v<0aW0 0.734399 0.0000 APApappgpeeenndd2iixx C C Page 2 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbciyyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00009933 3SMMAA1T00005500552266 FRCCaahnhnededmooiormcmmoaaSsSlaiaPpmloamapnnnlette | In PFOS ppm i i |i | min QMu0e0s7 2300 maximum que nE7rss0ie% prL1e1oadaimts quartile Sein Soom aio median Same 0 oss quartile minimum pbrr0b0o%x a22 2mm6e minimum Quantiles 100.0" 99.5 97.5% 90.070 75.0% 50.0% 25.0% 10.0% 2.5% 0.5% 0.0% 2.3609 2.3609 1.9720 1.1415 0.6549 0.1310 -0.8215 -1.5388 -2.2793 -2.3936 2.3936 Womens Moments jo oes Mean Siber te] Std Dev Src an aos Std Error Mean Upper 05% Men as Upper95% Mean LER%: 55 Mien ors Lower95% Mean N 12000 N Sum Weighs Tao Sum Weights -0.0605 1.0263 0.0914 0.1204 -0.2415 126.0000 126.0000 Toto ormaiy Testfor Normality Strinw Tes Shapiro-Wilk W Test Ww Proven W Prob<W assis oow1 0.967746 0.0521 Popes AAppppeennddiixx CC Page 3 Made Avaiabie by 3W orInspection and Copying as Confidential Information: SSMuuabbdjjeeeccAttvttaooilPParrbooltteeeccbttyiivv3eeMOOrrfdodreerrInIIsnnpPePcaatllimomeneravrvn..d33CM,o,pNNyooi.n.gCC22a--s00C44o--n66f3i3d00e99ntial Information: 28122..00009944 aMATO0S0527 3MA1000550055227 CRhCaehnmedmiioccmaalSpaPmllaoanltte RanPdroims pomSample Dom = PFHS I |i Ha al i | 1C || C: }| | a.o [ maximum QQuu1aan0ntt0ii0lee%ss Las maximum 100.0% 5% 99.5% 90705%% 97.5% a111L1...73s788886886m60008500 qqmueuadrritiialene 97730550..0000%%%% 0000..3184277200700070 qe median quartile 52210550..0000%%%% 000o..o001r377s803s40 minimum 22015.3055.%.%0% 00.05%% 0000..000003135337474 00.00005544 minimum 0.0% 0.0054 SMMedeaaDnnev Moments Moments 0[0.33m445y500 USpSStttpdddeDEnrreorv9or5rM%MeeaMaennan 0000..400416317617677 SLLuNUNoopwmpweeerrWre999i555g%h%%tMMsMeeeaaannn 111222000666....0422000170004072000640 Sum Weights 126.0000 STohessttaffoorWpNiNoolrirkmmWaarllTitteoyys Shap omeW iro-Wilk W W TesPptr0ob0b0<a0W 0.729906 0.0000 APApappgpeeenndd4iixx C Page 4 MSMuaabddjeeecAAtvvataoiillPaarbbollteeecbbiyyiv33eMVOfrfodorreIrnIsnIspnpeePcctatilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee8nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00009955 3MA10050528 3MA10050528 FCCahrnedmeoimcmaaSl apPmllpaanltte RalnnPdoonmsSapmppmle In PFHS m ) i E h| maim QQuu1aan0nt0ii0lee%ss on maximum 909190970.55.5%%0%1/0 00o0..3665s33011333 aunile 99077050..050%%%% -0000.13.5160837007527 quartile edan 500% median ane 2l5o0os% quartile 75.030 50.090 25.01 --T2015..m870676o72150 -S2o.5o46n1 min 2201.5055%.%.%0% 00.05%% -3.4007 sm -4.3022 S522669 -5.2269 minimum 0.0% -5.2269 MSMeetaabnnev MWommeennttss -111.72711255s22 SSSUttipddpeEDBrreorv9or5r5MM%eeMaaennan ULpopveerr 05%9513f, MMeeaann 0c1L..li120o2m82se59 -1.94390976 LSNNouwmeWre9i5gh%tsMean 1112-226166..0009003000000070 Sum Weights 126.0000 ShShaToapespsiittroofo-oWrrWiiNNlookkrrWmmWWaalliTTltoeyysstPt rova ogW Pr0o2b3<0W2 0.975283 0.2302 APApappgpeeenndd5iixx C Page 5 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbiyyiv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee8nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00009966 3SMMAA1T00005500552299 RGCarhneemdmiioccmaallSaPPmlaapnnltte __Pompm Random Sample POAA ppm AAPppappgeeenn6ddiixx C Page 6 maximum maximum qqmueuadrritiailene qmuendiialne quartile minimum minimum QQuu1aa0nrt0il0lee%ss 99919097.0555.%%%0% 99077050..050%%%% 57525005..0000%%%% 122105050..%%00%% 0200..5055%%%% 0.0% 666.77766600000 653S..467636661010.080 2321...0043770322005050 0001.13.33288086601000 0000..000125.2501819414 00209 0.0209 0.0209 Mean MMoommeennttss SMSSiteddeaDEnervovr Mean SULUtpopdpwpeeeErrrrr999o5r55%%M%eMMMaeeenaaannn, LNSNouwmeWre9i5g%hsMean Sum Weights 111.535333656393 0011..1173913895090 121116..3073007000107087 1260000 126.0000 126.0000 ShTTapoeissrttoffooWrriNNlookrmmWaaltiTtyeyst Shapiroo-sWsilikWWeoW TesPPtrr<ooobv0<e0Wnl 0.875366 <0001 MSMuaabddjeeecAAtvvataoiillPaarbbollteeebcbiyyv33eMVOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppNyyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00009977 3SMMAA1T00005500553300 FCCahhnedmaiomcmaalSePPmliapnnltte Random Sample _m 7 PoMpmI| In POAA ppm _t t h maximum maximum qqmueuadnritiiallnee mqeudniialne quartile minimum minimum QQuu1aan0rt0ii0loe%ss 99919097.0555.%5%0% 99277005..0050%%%% 57520505..0000%%%% 12120505.0.%00%%% 00025..055%%%%n 0.0% 111.999111111000 1171..239730131100820 0001..2772622328814888 -20000..925956551210949 --2322..9890666585855050 650 -3.8680 -3.8680 Mean MMoommeennttss SMSSutiedddaEDDnreervvor Mean USULptpopdpweeEerrrrr99o955r56%%M%MeMMeaeaneannn LNNSouwmerWe9i5g%hsMean Sum Weights -0011.20150686151 0o01..11i21155s14158 1-20006.3.0132012057m103 1260000 126.0000 126.0000 ShTTaeopssittrfooo-rrWiNNolorkmmWaallitTtyeys Shapir0o%-W0i3l6kWW9W TesPPtr<ou0b0<b0W1 0.903769 <.0001 AAPppappgeeennd7diixx C Page 7 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbtyyiv33eMMOfrfoodrrerIInnIssnppeePccattiiioomnneaavrnn.dd3CCMoo,ppyNyoii.nngg2-aa0ss4CC-oonn6ff3ii0ddee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00009988 3SMHAA1t90o005s0e5s3t1 RCCahheenmmdiicocaalSl aPPmllapannltte PFOSAA pom Random Sample PFOSAA ppm 4lJ w . C iJ | os . J ~r r'I~ I ww ~J | ww -- =is J|f .N maximum maximum mqqueuadreitiialene qunile median quartile minima minimum CQlu1uaa0nn0tii0el%ess 99919907.0555.%%%0: 99977005..0050%%%% 57250550..0000%%%% 22115050..%000%%% 0200..0555%%%% 0.0% 000.222666900000 0000..011269463991310s150 000o..0o000z628s3801318212 00o0..0o00000o282707686 0.00112 oooooo 0.00112 000112 0.00112 0.00112 Mean MMoommeennttss SSSMtteuddabDEnererovr Mean SLUUtpopdpwpeeeErrrrr999o5r55%M%%eMMMaeeenaaannn SNLNouwmeWre9i5gh%tsMean Sum Weights 000.000322933633 0000..0000033300s393.56 120006..0000101360603033 1260000 126.00W 126.0000 `ShTTaoepssittrfofooWrriNNlookrrmmWaalliTlteyyst Shapir0o6-W0i0l7kWW8oW TesPPt0mr0bo0b<0eW0 0.600789 0.0000 APAppappgeeennddiixx C Page 8 SMMuaabddjeeecAAtvvataoiillPaarbbollteeebcbiyyv33eVMOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iid0dee9nnttiiaall Information: Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00009999 3SMMAA1t0o005s0e5s3z2 RCCahhneemdmiioccmaallSPPallamannptt InPrOSAA Random Sample PFOSAA ppm In | ' | E : I maximum maximum qqmueuadriittiolene qqmuueandriitiallnee mmiinniimmuumm QDuu1aa0nn0tti.il0oe%ss 99919097.0555.%%%0% 99070750..005%9%%E 75525005..0000%%%% 12210505.0.%00%%% 0200..055%55.%% 0.0% -111.333111333000 --21117..969300104435950 --S332.5.i577762e20119 --"5456..81880019188I6446 --`p66e..177t99944844 pe -6.7944 -6.7944 Mean MMoommeennttss SMSStteddeaEDnmevovr Mean LSUUotppwdppeeeErrrrr999o5r55%M%%eMMMaeeenaaannn LNNSoowmeWre9i5gh%tsMean Sum Weights -4L.a77s88911233 4001.5.11432350090002 1--255460..030503280840060 1260000 126.0000 126.0000 ShTTaepeissrttofoorWriNNlookrrmmWaaliiTtteyyst oomWo Shapiro-Wilk W W TesPPt<rr0oo0bb0<a1Ww 0.929527 <.0001 APAappgppeeenndd9iixx C Page 9 MSMuaabddjeeecAAtvvataoiillPaarbbollteeebbciyyv33eMVOfrfoodrrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00110000 3MA10050533 3MA10050533 v_sRRCCaahm nnreddmaioocmmmap lSSaaPpmmlaapprnllte tee m i M570 ppm -- || |i MH " ;Vl| C+ " | 4. La^en 1 1 - LJ moma uDuaJann0ti0i0ele%ss maximum sss 100.0% 000.959909222000000 00ssa 99.5% 97.5% 0.99200 v0a10i3s 0.69103 qmquueariittinlee 97570505..0000%%%% 00D0..1o149s91045e227s550 Gane median quartile 152221005055.0..0%000%%%%% 0.06685 0033 0.03773 o0009o65 0.02173 minimum o020s..055t%%% 0000..000000009888640050 minimum 0.0% 0.00840 SMMeteaannbe Vernrts Moments 000.111855600255 SSUSttpiddpdeEDErrerrv9oe5r5MM%eeMaaennan 0000..100188113666326 LUSxLNoopuwpwmeeerrWre999i555g%%%hsMMMeeeaaannn 120006..1011108170376036 112266.00000000 Sum Weights 126.0000 SShhTTaaepepsisirtrtoofo-oWrrWiiNNolkorkWrmWWamlaiTTtleeyssPtt ov ozsW Pr0o0b0<0W 0.712853 0.0000 APApoappgeeenndd1ii0xx C Page 10 SMMuaabddjeeecAAtvvataoiillPaarbbollteeecbbiyyiv33eMVOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iid0dee8nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00110011 3SMMAA1t0000s500853344 Choma part Chemical Plant anda Same Random Sample pep In M570 ppm |C | ||| =:1 l] i|i .4 -- .-- aaimem oOuOrFs 00080 maximum awe n0w253so0%r8 oL0os0ei0w08wr0 quartile pee median Sane 250% FH quartilc minum 2a05sl0o%a%r aSLpimostowy minimum Duantiles 100.0% 99.5% 97.5% 90.0% 75.0% 50.0% 25.090 10.0% 2.5% 0.5% 0.0% -0.0080 -0.0080 -0.3701 -0.8780 -1.6387 -2.7053 -3.2774 -3.8310 -4.6406 -4.7795 -4.7795 Moments Moments yen ass Mean Saber he Std Dev Sid Br Men dos Std Error Mean Upper 5% Mn 336 Upper95% Mean LAR: 55%vim i Lower95% Mean 1360000 N Sum weighs 3600 Sum Weights -2.5145 1.1167 0.0995 -2.3176 -2.7114 126.0000 126.0000 Tottor omy Test for Normality Shape Wik WTht Shapiro-Wilk W Test W Povan W Prob<W ossions oan 0.957094 0.0035 Page 11 AAppppeenndidxiCxC Page 11 MSMuaabddjeeecAAtvvlaaoillaParbbollteeecbbtyyiv33eMWOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo.nn6ff3iidd0ee9nnttiiaall Information Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00110022 MA10050535 3MA10050535 RGCahhneerdmmioccmaallSaPPmllaapnnltte PrOSA pom Random Sample PFOSA ppm | | sf 01 , " "1 ed |0 y e C) maximum maximum qqmueuadrriitiallnee qunile median quartilc minimum minimum QOuu1aann0tti0iie%ess 99919075.055.%%%0% 99270705..0005%%%% 57520505..0000%%%% 21215005..0%00%%%. 0200..05.5%5%.%% 0.0% 000.666111222000000 0000...24463771199284400880 0000..00025153616129285550 0000..00000010121226962959 0000..00000000001055250020 00.0000005500 0.00050 Mean MMoommeennttss SSSMtteeddaDDEnreervvor Mean SULUtppodppweeEesrrrr999o5r55%%M%eMMMaeeenaaannn LNSNouwmeWre9i5g%hsMean Sum Weights 00o.00s661s188 0000..0010181102604354 120006.,000001840212032 1260000 126.0000 126.0000 `ShTTaoepssittrfofoorrWiNNloorkmmmWaaliiTtteyyst Shapir0o5-W8i9l2kWW9oW TesPPtr0ro0ob0n<0eW0 0.580929 0.0000 APApappgpeeenndd1ii2xx C Page 12 MSMuaabddjeeecAAtvvataoiillPaarbbollteeebbciyyv33eMVOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00110033 3SMMAA1T00005500553356 RCGahhnaerdmiioccmaallSaPPmllaapnnltte in PFOSA' Random Sample In PFOSA .m | mmaaxxiimmuam qqmuuearidtutilnee qmeudiitaen quartile mmiinniimmuumm QQuu1ana0t0rif0ti%ess 999190970.55.50%%%%r 99017050..050%%%% 75520505..0000%%%%r 21215050..0%00%%% 0200..5055%%%% 0.0% -"000.344999111000 --"0007L..743a39551e170 -1.4620 ESr am -2.8787 --s645..7o490218e76176 --e7670..67600000809919 -777...666000000999 Mean MMoommeennttss SSSMtueuddabDEnererrvor Mean LSUoUtppwdppeeeErrrrr999o55r5%%M%eMMMaeeenaaannn LNSNouwmeWre9i5gh%tsMean Sum Weights -a413.5s305a14s05 0041..1019616099914340 1--264468..00609180996036 111222666..000000000000 `ShToaespsittrffoooWrriNNlkoormmWaallitTtyeyst Shapiro-Wilk W surWoW TesPptr0ro0ob0b<0aW2 0.946788 0.0002 AAPppappgeeenndd1ii3xx C Page 13 MSMuaabddjeeecAAtvvataoiillPaarbbollteeebcbyiyv33eMVOfrfodorrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00110044 3SMMAA1T900005500553377 CFRrCaahnnoeeddmsroiocmemeaSSlpaaPpormlmaapgnlnete M556 oom 4 ~ C ;D pt : G 2~ J. G %C "J y C -i CDS 1- C 60 awimn QuIa0n0i0o%s 040600 maximum [TR moEosrne oomae quartile hein S008 owas median Gane Box oo quartile moun a20so50o%%n oa0S00mo001se10 minimum Quantiles 100.0% 99.5% 97.5% 90.0% 75.0% 50.0% 25.0% 10.0% 2.5% 0.517o 0.0% 0.40600 0.40600 0.32165 0.15000 0.05995 0.02615 0.00765 0.00300 0.00175 0.00140 0.00140 Moments Moments Mean aosty Mean Saber oor) Std Dev Siro en pr Std Error Mean Diper95% Men aos Upper95% Mean Love 35% Mean ous Lower95% Mean N 1200000 N Sum Weighs 126000 Sum Weights 0.0519 0.0737 0.0066 0.0649 0.0389 126.0000 126.0000 Tot for ormaty Testfor Normality Shap WiW Tkot Shapiro-Wilk W Test W Sevan W Prob<W ass ooo 0.671484 0.0000 AAPpaopgpeeenndd1ii4xx C Page 14 MSMuaabddjeeecAAtvva{a0illaPabobltleeecbbiyyv33eMWOfrfoodrrerIInnIssnppeaPccaitiiloomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC 2aa.ss0CC4oo:nn6ff3iidd0ee9nnttiiaall Information Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00105 MA10050538 31VIA10050538 RCGahhneedmriioccmaallSaPlmlaapnnltte nse pom _ Random Sample In M556 ppm | I maximum maximum qqmueuadrritiialene quae median quartile minim minimum QQuu1aann0tsi0ile%ess 99919097.0555.%%%0% 99277005..0050%%%% 57520505..0000%%%% 22115050..0%00%%% 0200..3055%%9% 0.0% -000.059000111444 --""01L..s191039r19646 --r212..5e881195n57116 --a5435..086m74034113 --65653..7838104987317 6sm3 -6.5713 -6.5713 Mean MMoommeennttss SSSMtiedddaDDEnreervvor Mean SLUUtoppdvppeeeErrrrr99o9r5556%M%%eMMMaeeenaaannn )LNS\ouwmerWe9i5gh%tMsean Sum Weights 33Li.77996600 30o15..1n53265s13658 1--2i346..300506350655056 1260000 126.0000 126.0000 ShTTaoepssittroff.ooWrriNNlookrmmmWaaliiTtteyyst Shapirso-WeillkWWoW TesPPtr0ro0obiv<seWs 0.962731 0.0158 AAPppappgeeenndd1ii5xx C Page 15 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbciyyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00110066 3MA10050539 3MA10050539 APApappgpeeenndd1iixx DD Page 1 AAppppeennddiixx DD DDiissttrr`iiAbbmuuottinioognn FooifflFFmlluPuoloarrnootcchhEeemmmpiilccoaayllesseaasnndd(NTThh=eeii6rr0)NNaaittnuutrrhaaell RLLaoonggdoTTrrrraennSssaffmoorprmmlaaettiioonn Among Film Plant Employees(N =60)in the Random Sample SMMuaabddjeeecAAtvvataoiillPaarbbollteeecbbtyyiv33eMMOfrfodorrerIInnIssnppeePccattiiioomnneaavrnn.dd3CCMoo,ppyNyoii.nngg2a-ass04CC-oonn6ff3ii0ddee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00110077 3MA10050540 3MA10050540 Fim Pian RRaannFddiloommmPSlSaaanmmtppllee TT PFOS DDm 14 i aC9 -r I il :3 s :- | maximum maximum qqmueuadriittialene qunile median quartile minimum minimum OOuu1aan0ntt0ii0loe%ss 99919097.0555.%%%0% 99277050...0050%%%% 75S20505..000%0x%%% 22115050..0600%% 0002..0555%%%% 0.0% Men MMoommeennttss SSSMtteuddaDEDnemeovvr Mean SULUtpopdpwpeeeErrrrr999o5r55%%M%eMMMaeeenaaannn LNNSouwmeWre9i5gh%tsMean Sum Weights 000999444666000000 0000..82891714232665605050 0000..1222300718385255050 0000..00018683676792958080 0000..00002126353790923030 001500 0.01500 0.01500 00o..11m7417e8810 0000..0201101499700089880 60000..10123030303960693039 6000000 60.00000 60.00000 `ShTTaeopssittrfloooWrriNNlookrmmWaallitTteyyst Shapiroo6-sW2il6k0WW3oW TesPPtrr<oo0bv0<e0Wn1 0.682603 <.0001 AAPppappgeeenndd2iixx DD Page 2 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00110088 3MA10050541 31VIA10050541 RanFFdiilommmPPSllaaannmttple (npros Random Sample Ln PFOS DDrn 00 Yo ; "-4 0 -~ . maximum maximum qqmuueandriitiailnee qmuerdiialne quartile mmiinniimmuumm QOuu1aan0ntt0ii0loe5ss 99719095.055.%%90% 99277005..0050%%%% 75520505..0000%%9% 12210505.0.%00%9% 0200..05%55%.%% 0.0% -"`000.0005555855s5 --""0001..2220191596957s75 --1111..952589774611252 --22127..09440842420111 --S230..18719009100792 Sse -4.1997 -4.1997 Men MMoommeennttss SMSStteaddaDEDnmeeovvr Mean LUoSUptpwpdpeeeErrrrr99o05r55%%M%eMMMaeeenaaannn, LNSNouwmerWe9i5gh%tsMean Sum Weights -0116.99799966922222 0001..0.0688872779078798882 0-210..011870210s085078 000000 60.00000 60.00000 `ShTTaoepssittrfofoorrWiNNloorkmmWaallitTteyyst Sh apiro-Wilk W oorWoW TesPPtrorosbo<sbW 0.975227 0.4827 AAPppappgeeenndd3iixx DD. Page 3 MSMuaabddjeeecAAtvvataoiillPaarbbollteeebcbyiyv33eMVOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppNyyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00110099 3MA10050542 3MA10050542 RanFFdiilommmPPSllaaannmttple: rE) Random Sample PFHS oom 1 | i1S | {om a {ow d i 1 | O CD ok0 c mmaaxxiimmuumm qqmueuadriittialene qqmuueaidrnitiiallnee mmiinniimmuumm QQuu1aa0nnt0ii.l0ee%ss 999199705..055.%%%0% 999700..500x%%^ 757505.000%%% 52210550..0000%%%% 0221.0555.%%%0% 000..005%%% 000.222111000000000 000..121414606707000 000..000244666666000 0000..00000121716119698000 0000..00000000155736611558 0000..00000000111133331111 0.00131 Mean MMoommeennttss SMSSiiedddaEDDnmeeovvr Mean SUULtppodppweeEerrrsr99o9r555M%%%eMMMaeeenaaannn LNNSouwmerWe9i5gh%tsMean Sum Weights 00.0022225588 000.000033300595733 0000..00003103043056953273 55099...00010040060020 599..0000000000 ShTTaeopssittrfofoo-rrWNiNolorkmmmWaalliTtteyyst Shapir0o5-7W8i0lk7WW9oW TesPPtr0r.oo0b0b<0eW0 0.578079 0.0000 AAppppeennddiixx DD PPaaggee 44 MMaaddee AAvvaaiillaabbllee bbyy 33MVfofrorInInssppeeccttiioonn aanndd CCooppyyiinngg aass CCoonnffiiddeennttiiaall IInnffoorrmmaattiioonn:: SSuubbjjeecctt ttoo PPrrootteeccttiivvee OOrrddeerr IInn PPaallmmeervrv.. 33M,, NNoo..CC22--0044--66330099 22881122..00111100 33MMAA1100005500554433 RanFFdiilommmPPSllaaannmttple RLLannnPdPFoFHmHSSSpapmoppmml.e AAPppappgeeenndd5iixx DD Page 5 -i- maximum maximum qqmueaduritiaelne qunile median quartile mmiinniimmuumm QQuu1aan0rtt0ii0loe%ss 99919709..0555.5%0%% 99977005..0050%%%% 57520550..0000%%%% 22115050..%000%%% 0200..5055%%%% 0.0% -""11U.3s566e00s66 -2231..0056026620246 -3.0662 SSaent -3.6268 --"444..9194373366611552 --s665..6e163737m67717 "663m -6.6377 -6.6377 Mean MMoommeennttss SSMSittedddaEDDnmeeovvr Mean USULptpopdpweeeErrrrr99o555r5%%%MMeMMeaeeanaannn, LNNSouwmerWe9i5gh%tsMean Sum Weights -404.292656727858000 0040...01911225944250051810 5--4494..50501011606900052028 5900000 59.00000 59.00000 ShaTTpoeissrttoffoorWriNNlookrrmmWaaliiTtteyyst Shapirooo-WmiulskWW2oW TesPPtrr0oo5bb7<aMrW 0.977452 0.5773 MSMuaabddjeeecAAtvvataoiillPaarbbollteeebcbyiyv33eMVOfrfodorrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..001111 33MMAA1100005500554444 man Film Plant fea Random Sample oe POAA ppm =y =N]i| s~a - od ; a= ;1J ^ [H] i saa ~ moan Q0ui0s oamon maximum ie onNBiooearr iaaohmnieeee quartile Mw or ow median wn Ee ohm quartile mn BB0BEa3r odoobeomm minimum Quantiles 100.0% 99.5% 97.5% 90.0% 75.0% 50.0% 25.0% 10.0% 2.5% 0.5% 0.0% 0.29800 0.29800 0.27200 0.15400 0.10800 0.05520 0.02400 0.01560 0.00651 0.00598 0.00598 Moments Moments ven oust Mean Sr Sores Std Dev SB Somer Std Error Mean Trap iam fred Upper95% Mean om Sone Lower95% Mean soon N Somes Sooo Sum Weights 0.07084 0.06200 0.00807 0.08700 0.05469 59.00000 59.00000 J-- Test for Normality ShShapiro-Wilk W Test onsWooesno W Prob<W 0.843094 <.0001 Ee AAppppeendnidxiDxD Page 6 WSMaaiddboeelAAvvalaoillPaarbllooetbbeyyc3hMOfrfoodrrerIInnssppeePccattiiloomnneaavrnnddWCChooppyyNoii.nngg2aa.ss0CC4oo-nn6ff3iidd0ee5nnttiiaall informa Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00111122 aMaroososes 3MA10050545 faRnarndFFedioaloammmmSPrsSlaaaasnmratpinlee Ln POAA ppm | x-JC - || -3S - M || E mim ouI0n0t0e%s 120 maximum que ffim7i5rre0s% fT21ro9sess quartile fein Soon Zioes median ane 230% Shor quartile miimm 2a05os0o%%r hSpShirioanty minimum Quantiles 100.0% 99.5% 97.5% 90.0% 75.0% 50.0% 25.0% 10.0% 2.5% 0.5% 0.0% -1.2107 -1.2107 -1.3065 -1.8708 -2.2256 -2.8968 -3.7297 -4.1605 -5.0377 -5.1193 -5.1193 Moments Moments Mean oom Mean Saber pri Std Dev SiEner Mean pet Std Error Mean Upper 55 sn 278208 Upper95% Mean Lor 355 Mean Sasi Lower95%n Mean sna0000 N Sumweighs So0000 Sum Weights -3.02097 0.91335 0.11891 -2.78295 -3.25899 59.00000 59.00000 Testor oma Testfor Normality Shape ik WT Shapiro-Wilk W Test W Bova W Prob<W oom "asi 0.975823 0.5122 Page 7 AAppppeennddiixx DD Page 7 MSMuaabddjeeecAAtvvalaoillaParbbollteee cbbtyyiv33eMWOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo.nn6ff3iidd0ee9nnttiiaall Information Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00111133 MA10050546 31VIA10050546 RRPaanFnFFddOiilooSmmmmAPPASSllaaaapnnmmttopsmllee PFOSAA Dpm iu | |: | {oem | [|| - -4 | | Ct maximum maximum qqmueuadriittialnee qurile median quartile minioum minimum OQuu1aa0nn0tti.iJ0ee%ss 99919015.055.%%%0% 99270705..0005%%%% 75525050..0000%%%% 12210505.0.%00%%%, 0200s..055%%.% 0.0% Mean MMoommeennttss SSMStteuddaDDEnreemvvor Mean ULpoSUtppwdpeeeErrrrr999o5r55%%M%eMMMaeeenaaannn LNNSoowmerWe9i5gh%tsMean Sum Weights 000.000333777888000 0000..00002023969773785550 0000,.0000000024658387057 00o0..0l00000i12118220 0000..000W1101111112222 oz 0.00112 0.00112 0o0.000o00s53059747 0000..000000000s057i752224 50009..0000000005250453023 59.0000 59.00000 59.00000 SShhTTaaoeppssiittrrooff-oorWrWiiNNllookrkWmmoWaWaliitTTteyeyssPttrobar sieW 0.511689 00000 Prob<W 0.0000 AAPppappgeeenndd8iixx DD Page 8 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbciyyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00111144 3MA10050547 3MA10050547 [RRaarnnFFpddiilroommmmoPPSSllsaaaannnmmttppsllmee Ln PFOSAA pm -I: l | . |i | ||. ; |i mmm QuWa0rt0i0o%s 22758 maximum que 2079505s0%%a% IEsSE noasmw quartile ean S00% Sirs median Gale 250% om quartile minimam o02T5s0oo%%% Gorouroussus minimum Quantiles 100.0% 99.5% 97.5% 90.0% 75.0% 50.0% 25.0% 10.0% 2.5% 0.5% 0.0% -3.2754 -3.2754 -3.5529 -5.0593 -5.3247 -5.8781 -6.7944 -6.7944 -6.7944 -6.7944 -6.7944 Vaments Moments Men sossas Mean Saber oss Std Dev Sime Mean onion Std Error Mean Upper 5% Mean Sst Upper95% Mean Lover 95% Mean "ous Lower95% Mean x 500000 N Som weighs 5200000 Sum Weights -5.95844 0.84775 0.11037 -5.73751 -6.17936 59.00000 59.00000 Testor Normalty Testfor Normality Sapoik W Tet Shapiro-Wilk W Test W Pose W Prob<W oss col 0.843132 <.0001 APApappgpeeennddiixx D Page 9 MSMuaabddjeeecAAtvvataoiillPaarbbollteeecbbtyyiv33eMMOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CC,ooppNyyoii.nnggC2aa-ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00111155 3MAT0050548 3MA10050548 RanFFdiilommmPPSllaaannmtte. RanSMd5To7Om0Spapmpmppm le Cwo+ - || | |e i &B mmaaxxiimmuumm qqmuueaadrnitiiallnee qqmuueaadrnitiiallnee mmiinniimmuumm QQuu1aan0ntt0ii.le0se%.s 99019907..0555.%6%0% 99977005..0050%%%% 575050..000%%% 221550.000%%% 212.055.%0%% 000.055%%% 0.0% 000.444555444000000 0000...22405545181490903530 000..000141484202050 00..0000669900 000.000000244533122 000..000000121151212 000...000000000888000 0.00080 Mean MMoommeennttss MSSSttedddaDDBneeovvr Mean SUULtppodppweeEerrrrr99o9r555M%%%eMMMaeeenaaannn LNNSouwmerWe9i5gh%tsMean Sum Weights 00.002200224 000.000505979060121 0000...00003300554749468982 66000..000000040090090 6600..000000000 `STTheeassptitrffooo-rrWNNiolorkmmWaalitTtyeyst Shapir0o2-0W3i2lk0WW0oW TesPPtr0r.oo0b0b<0eW0 0.293209 0.0000 AAPppappgeeenndd1ii0xx DD Page 10 MMaaddee AAvvaaiillaabbllee bbyy 33MVffoorr IInnssppeeccttiioonn aanndd CCooppyyiinngg aass CCoonnffiiddeennttiiaall IInnffoorrmmaattiioonn:: SSuubbjjeecctt ttoo PPrrootteeccttiivvee OOrrddeerr IInn PPaallmmeervrv.. 33M,, NNoo..CC22--0044--66330099 22881122..00111166 33MMAA1100005500554499 RanFFdiilommmPPlSlaaannmttple La S70 pom Random Sample Ln M570 .m AAPppappgeeenndd1ii1xx DD Page 11 0 mmaaxxiimmuumm qqmueuadriittialene que median quartile minimum minimum QQuu1aan0ntt0ii0lee5ss 90019075.055.%%%0% 9907705.0.500%%%%n 57520505..0000%%%% 12210505.0.0%0%%%n 0200..0355%%%%.nn 0.0% -"000.777888999777 --"S010..m77387098670 --Zp34ra..a02s35i54e66 --ES54a..r49i47e37s49 --"T56e1..83893870771015 71300 -7.1309 -7.1309 Mean MMoommeennttss SMSStteddeaDEnvemvon Mean SUULtppodppweeeErrrrr999or555%M%%MeMMaeeenaaannn LNNSouwmeWre9i5g%hsMean Sum Weights -4417.19709868919292 s001..11i14402268l81119 0--5540.0.005808144306617076 000000 60.00000 60.00000 ShTTaeopssrttoff-ooWrriNNlookrmmWaalliiTteyyst Shapiroo-sWislk:WWoW TesPPtr0ro0ob2s<6eW3 0.948604 0.0263 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00111177 3MA10050550 3MA10050550 um ta Film Plant Random Samia Random Sample TT M556 ppm :| v .@ .4k momen Gu0a0n0e%s 0300 maximum que 0715s050s%5 0oSoa3ain0zs7isa0o: quartile ein 500% ouzso median ae 250% oazs0 quartile minimum o20s5f0ot%o%t oroomauoinit minimum Quantiles 100.0% 99.5% 97.5% 90.0%r 75.0% 50.0% 25.0%c 10.0% 2.5% 0.5% 0.0% 0.30700 0.30700 0.15407 0.00593 0.00250 0.00250 0.00250 0.00117 0.00021 0.00010 0.00010 Moms Moments Mean onic Mean Si Dev pre Std Dev Sid Bor en oman Sid Error Mean Upper 95% Nien 001s Upper95% Mean LEE 55% Men D000 Lower95%n Mean x pro N Sum Weighs press Sum Weights 0.00816 0.03932 0.00508 0.01832 -0.00200 60.00000 60.00000 Testor Nomaty Testfor Normality Shap Wik W Tht Shapiro-Wilk W Test W pana W Prob<W [I 0.162266 0.0000 AAppppeennddiixx DD PPaaggee 1122 MSMuaabddjeeecAAtvvaoaillaParbbollteeebbcyiyv33eMMOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo.ppyyNoii.nnggC2aa-ss0CC4oo-n6nf3ifd0ie9dnteinatl IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00111188 3MATO0S0851 31VIA10050551 RRaahnnFuddiiloomsmmmPspSSlaoaaarnmmoetpomllee Ln M556 ppm 1: \| . Ll _ T : :| :5 .LC . |\ -1D moma uWn00i0sF L150 maximum quite fp07ar500t% paSShonandiss quartile ean S00 Sos median aie 250% Sais quartile minimum r020i050d%%% SSS5ah371no03en0 minimum Quantiles 100.0% 99.5% 97.5% 90.01" 75.0 50.0% 25.0% 10.0% 2.5% 0.5% 0.0%n 1.1809 -1.1809 -2.7418 -5.1284 -5.9915 -5.9915 -5.9915 -6.7632 -8.6336 -9.2103 -9.2103 Womans Moments Mean so Mean SidDer a9s702 Std Dev Sud Boren 012367 Std Error Mean Upper 95% Nien Ses) Upper95% Mean Lover 5% Mean ome Lower95% Mean x pre N Sam Weighs om Sum Weights -5.93097 0.95792 0.12367 -5.68351 -6.17842 60.00000 60.00000 Testor Nomatty Testfor Normality Shap WwTet Shapiro-Wilk W Test Wana W Prob<W ossasni <oml 0.682874 <.0001 AAPppappgeeenndd1ii3xx D D Page 13 MSMuaabddjeeecAAtvvoaaillaParbbollteeebcbiyyv33eMMOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo.ppyNyoii.nnggC2aa-ss0CC4oo-n6nf3ifd0ie9dnetinatl IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00119 3MAT000852 3MA10050552 AAPpappgpeeenndd1iixx E& Page 1 AAppppeennddiixx EE SScc(aaYttttReeSrrppClloHottEss Maa)nnddfrorreeggrrreeassnssdiiooonnm eesqqauumaapttliiooenn(ssn ffoorr = fflluuoorroocchheemmiiccaallss bbyy 126) and for current jyyoeebaarrcssa\rwcXooorgrkrkieeedds ii(nnccchhheeemmimciiacclaall (YRSo`opCpeeHrraaEttoMorr)ss,,feoenrnggiirnnaeeneedrr//ollmaabbs,,ammmaapiilnnett(eennnaa=nncc1ee.2,6ss)uuappneedrrvvfioirssoocrrur//rmmeggnmmtttjaaonbndcammtiiellllogoorppieeerrsaa(ttcoohrrses)m)ical MMSuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00112200 3MA10050553 3MA10050553 mss Random Sample PFOS ppm By YRSCHEM ne | J 5Appendix E Page 2 | nn | 5 . Jt . n .. i l r i 10 15 20 25 30 35 40 1RSCHN onTerm tBer, Intercept YRSCHEM eo eomwreos,trotgJ Es,SoEsrTeprrnnSeHfuEo=m Source mT ham tim Model Linear Fit PFOSdfppm =0.89178 + 0.0478 YRSCHEM Summary of Fit RSquare 0.10868 RSquare Adj 0.100887 Root Mean Square Error 1.528756 Mean of Response 1.504686 Observations(or Sum Wgts) 126 Analysis of Variance DF Sum of Squares Mean Square 1 35.11712 35.1171 reF Ratio os15.0260 Error C Total 124 125 gSI mESSmeEnEEtoRTr Ememe Estimate OF 0.8917838 289.79964 324.91676 Parameter Estimates Std Error t Ratio 0.208682 4.27 2.3371 Prob>F 0.0002 Prob>ltl <.0001 Lower 95/* 0.4787397 0.0478029 0.012332 3.88 0.0002 0.0233943 ues Upper 95% 1.3048279 0.0722116 JteeARobeot yyerregpciionn onrsCCoopipnpg CorCtnetsr oman MadeAvailable by3M forInspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 281122..00112211 -- 3MA10050554 v en-- Random Sample PFHS ppm By YRSCHEM | ot AAppppeendnidxiExE Page 3 rA, T romTerm fratIntercept Drm, YRSCHEM Lra -t sess sr oree Linear Fit PFHSdfppm =0.11968 + 0.01757 YRSCHEM Si Summary of Fit sq sn RSquare 0.223991 mi oz RSquare Adj 0.2I7733 RroehnSoe-- Fi Root Mean Square Error 0.364103 ET ss% Mean ofResponse 0.344977 Sooe orSJ ECECRISSE ey ne Source Reeor Model B=g Tam Tim oom Error = JSwwoee3 EgSuuerweUauEEas woUoymn mSmmeifrnnt CTotal Observations(or Sum Wgts) Analysis of Variance DF Sum of Squares 1 4.744959 124 16.438777 125 21.183736 Estimate 0.1196844 Parameter Estimates Std Error t Ratio 0.049702 2.41 126 Mean Square 4.74496 0.13257 F Ratio 35.7919 Prob>F <.0001 Prob>ltl 0.0175 Lower 95% 0.02131 0.0175716 0.002937 5.98 <.0001 0.0117582 wm Upper 95% wm 0.2180589 cme 0.023385 Woadso Arvlaetibo bybtoriepacS ion anrCopingSas CSonianl formation Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00112222 -- 3MA10050555 r-- ole Random Sample POAA pm B YRSCHEM AAppppeendnidxiExE PPaaggee 44 . Lo Fm *.. "w Tt - . i,, 1, r. i f 1 1% 0 5 10 15 20 25 rsch'a1 TamTerm prIntercept Nn, YRSCHEM lro fl LESa isqemsEaornoWeE tevonerDdea arres inr saimnoa LJue= me Source 3 ` TE lm SE Model SE 7 EEE Error Ee, AJwDomEtEEm RS[ ZEEhuT-- TmR ETe Wroawrl vmoennfmea CTotal Linear Fit POAAppm = 1.29399+ 0.0189 YRSCHEM Summary of Fit RSquare 0.0246 RSquare Adj 0.016734 Root Mean Square Error 1.324636 Mean ofResponse 1.536271 Observations(or Sum Wgts) 126 Analysis of Variance DF Sum of Squares Mean Square 1 5.48740 5.48740 124 217.57785 1.75466 125 223.06524 F Ratio 3.1273 Prob>F 0.0794 Estimate 1.2939922 Parameter Estimates Std Error t Ratio 0.180819 7.16 Prob>jtl <.0001 Lower 95% 0.9360979 0.0188964 0.010685 1.77 0.0794 -0.002253 mie Upper 95% mE 1.6518866 ine 0.040046 Vito Avie ty Sor aprtea S ign s 8. Conan orm Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00112233 SAr0050556 31VIA10050556 PFOSRARaAanpndodoommmSBSayammYppAllSeeCHEM iw PFOSAA ppm By YRSCHEM 0 30 AAPpappgpeeenndd5iixx = E Page 5 0o2w0 Co E fEw 010 - L 0".0"0 H er -- o E CIEAE ACA) 0 10 Ee) 15 20 ASNEM 25 30 35 t0 MSooSudourerclcee EmECMroorodorerwl C Total TTIneotrmemrcept YRSCHEM Intercept YRSCHEM Lro fl PPFOSFAAdO fppmS==`00L.S.AiL00uni33ne2m2ea11aA rmr33F-ao-Fiiftrt00fF.0yi00t0006p 699YYRRpSSCCHmHEEMM RRRSqSqquuuaaarrreeeAg) Summary of Fit 00002.090353737363 R`RRMoSoeoqoatutnMaMoreefeaRaAenndsSSjpqquouanarsreeeEErrrroorr 00.0000.20203339288599933886 OOMbbessaeernrvvoaafttiiRooennsssp(ooonrrsSeSuumm WWagttss)) 126 0.023293 126 OF AAnaSlunymsioslaooSffqVViauarrwiieaassnnccee MemnSquae D4F1| Sum000o.10f080S087q74u220a9999r939e989s9 Mea000n.00S000q01u775a301r009e0 2s124 125 01957093 0.18840938 0.19570936 0.001519 F4F3RRa0at4ii4oo PP40r.r0o8o3b0b0>43eF4 0.0303 CEEOsstiiRmmaaRttse 000068 C.0321302 -0.000689 PPaaSrmGaemEelotorerrEEsstti(immaRatateesos 000S.t000d0E503r3rA24o1r t R266a.1t00i9:4o 0.000314 -2.19 PP<rro0bo>0blltll 0003 <.0001 0.0303 LoLOwo0e2wrIs9SrO5SE%%S 000112 0.0215985 0.001312 U0pU0pp4ep2r o69r651s0/9s0 0000067 0.0426619 -0.000067 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggCa2a.ss0CC4oo-nn6ffi3idd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00112244 3MA10050557 3MA10050557 MRRaanndo dooBmysSavarRmpm EpilGeeHEM a M570 pm B YRSCHEM 1 op| | SHgES ioeh .so . | oft DL. AA2po5pgeeen6dnigxi&xE Page 6 Co HA ACEAR FAFE AFM le r.-.. r-1 t-. . { . 1 1 , | werr~S:diu SVoSoouiucrecoe ECrrow Model Error C Total iVITTnRneotSrecmmrCceHepEt M YRSCHEM Fr nears Linear Fit MSTOppm= 0.17910 00223 YRSCHEM M570ppm =0.1791-0.00223 YRSCHEM SummaolrFyt Summary of Fit Rsqure oorress RSquare 0.017688 RoqueAd Gores RSquare Adj 0.009766 Root Mean Sauce Err alse Root Mean Square Error 0.185242 Mien Response aso Mean ofResponse 0.150471 Ovarations (or Sum Wes) 12 Observations(orSum Wgts) 126 Ansof vyasse Analysis of Variance wp Ls tug Te DF Sum of Squares Mean Square i oaiss "ooiels 20% 1 0.0766188 0.076619 1s Gl 00a pent 124 4.2550321 0.034315 is pre) oie 125 4.3316509 F Ratio 2.2328 Prob>F 0.1376 Gamma PSuanfee EimFaatlosa Poll Lowers Estimate Tn omsme 70 <ool iboswe 0.1791 om omiss 16 of ows -0.002233 Parameter Estimates Std Error t Ratio 0.025286 7.08 0.001494 -1.49 Prob>111 <.0001 0.1376 Lawer 95% 0.1290506 0.005191 Usperosw Upper 95% Ombre 0.2291494 bors 0.0007248 MSMuaabddjeeecAAtvvoaaiilaParbbollteeecbbtyyiv33eMMOfrfodorrerIInnIssnppeePccattiiioomnneaavrnn.dd3CC.ooppNyyoii.nnggC2aa-ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00125 MA10050558 3MA10050558 ProSFRAaaonrdmommySSaaYmnRpsBlieeCHEM PFOSA ppm By YRSCHEM 0171 w]050 goE 010 0!0 FT. . opt 0.10 Lo 0 Go Tim sar Re 5 10 15 20 25 10 3S wnISNRLt1 Pag7e AAppppeendnidxiExE Page 7 Source Source Vide Model Emr Error Cow C Total TomTerm Inert Intercept YRSCHEM YRSCHEM -- Low H PFOS=006AL73odw-sDOiOOKppm Linear Fit 3YRSCHEM PFOSAdfppm =0.06731-- 0.00043 YRSCHEM Smale Summary of Fit Roque otiers RSquare 0.00167:i Rue Ad "oness RSquare Adj -0.00639 Rook anSau Ere alleen Root Mean Square Error 0.11689:) MeanofResponse ages: MeanofResponse 0.06179:' Observation oe um Wet) ji Observations(orSum Wgts) 12o Arofavarasrce Analysis of Variance or "Sms Memswae Fra DF Sum of Squares Mean Square | dooms "Oot oom 1 0.0028424 0.002842 ns Teays oo owe 124 1.6943378 0.013664 1s Leman [rt 125 1.6971802 F Ratio 0.2080 Prob>F 0.6491 Emmoe PSaurErmoarr EsitRoalss Pui Lowrosw Estimate oGmoet o0isoss 42 <a oom 0.0673064 Doo mms ou oes oom -0.00043 Parameter Estimates Std Error t Ratio 0.015956 4.22 0.000943 -0.46 Prob>ltl <.0001 0.6491 Lower 95% 0.0357238 -0.002296 Uswosk Upper 950% oom 0.0988889 owmise 0.0014363 SMMuaabddjeeecAAtvv{aa0illaPabobltleee cbbiyyv33eMWOfrfodorrerIInnIssnppaePccaitilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo:nn6ff3iidd0ee9nnttiiaall Information Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00112266 3MA10050559 3MA10050559 reg roe Random Sample M556 ppm By YRSCHEM 0,110 i=ns Appendix E Page 6 0 ;D - E s .c FE2D ` PE "el . re meetis tf .1D s Bl 0 00 en : Sr D '5 2D 2c :G `RSC- N =,JW it oe BgoEmEE sca orSe=Erneo,rEaBeCo.nEETeEneEnRmeEsEmTm rr w"2 =pyoimom-=mewromne Term B Be, m SEBI E TTE Emn mEmE Intercept Linear Fit M556dfppm = 0.05953 -0.00059 YRSCHEM Summary of Fit RSquare 0.00791t; RSquare Adj -0.00m; Root Mean Square Error 0.07371(, Mean of Response 0.05194' Observations(or Sum Wgts) 12t, Source Model Error C Total Analysis of Variance DF Sum of Squares Mean Square 1 0.00537776 0.005378 124 0.67382941 0.005434 125 0.67920717 F Ratio 0.9896 Prob>F 0.3218 Estimate 0.0595259 Parameter Estimates Std Error t Ratio 0.010063 5.92 Prob>ltl <.0001 Lower 95% 0.0396089 YRSCHEM -0.000592 0.000595 -0.99 0.3218 -0.001769 er Upper 95% uEmEm 0.0794428 0.0005854 Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00127 3MA10050560 7C0Gfh8hRaepaomnnomiddcemoaoamlmBSSOySppaYaermAamapStrleCoersHsEM W PFOS ppm By YRSCHEM 1 m - sn . En . 1 2Bw y,1o es e . we s van 88 wa Page 9 AAppppeendnidxiExE Page 9 TYITnoRneitSrmerrmCeceHepttEM YRSCHEM ESorSMMuoooourdrreclclee Clout Error C Total Lun fi PPFOSdRfppmO==S1u1..m4S 41mLL16i6ain44rne66a+U ye+ra0F0oir.0t0F3p 3331122YYpRRSSCCmHHEEMM RRoaRRRSSoqqqrtuuuaaMerreeeeaAnAddSjquare Sruomrmaryof Fit 00o01..o0200c333609790s6964s0008s8485 MRMOeboeasoaentrnovMoafetfiaRRoneensssSppq(oouonasrsreeSeoEmrrWoirts) 1.237904 17811075 1.781106 Observations(or Sum Wgts) or A"nSsoofVsayraansca Analysis of Variance 47 Memswwo Frac DsFs11 %45 Sum of Squares ams 4.439524 73o3s9t7820 68.958297 Mean Square wn 4.43952 15201 1.53241 F Ratio ze 2.8971 p0o9w3r6 Prob>F 46 73.397820 0.0956 LEEsastiismnaastee 0PSPtaa2Sdrrd0aaEEmmr1ermeStotrreerrEEssttti(imRRnSaasatt0eeik6sos PP<rooObb>milltll LoLOwoSewsrrr99i5ss%s% OUBIS 1.4164581 0.0331178 00s 0.280181 0.019457 1705.06 1.70 oo <.0001 00007 0.8521458 0.0956 -0.006071 UU10p.p10p99ep878r00e0977re7I5O0sS%N4 0.0723065 MSMuaabddjeeecAAtvvaoaillaParbbollteeebbcyiyv33eMMOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo.ppyyNoii.nnggCa2a-ss0CC4oo-nn6fi3fd0ie9dnteinatl IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00112288 3MATO0S0861 3MA10050561 -- Random Sample RJounstois,n Chemical Operators PFHS ppm By YRSCHEM : || . | i E |i : "il ad 1 000 "' I , r I r 0 0 's n YFICHN I r I, 25 30 J5 ooepsti Appendix E Page 10 jemoBETerm Intercept YRSCHEM [SAJRosEEmeop,rr eTeatEa rrnouris ssiranSRoe2seas2 Source go am wesw Model maE 4 Tehmm dm Error =Lrw ri Linear Fit PFHSdfppm = 0.14813 + 0.0254 YRSCHEM Summary of Fit RSquare 0.342256 RSquare Adj 0.32764 Root Mean Square Error 0.333897 Mean ofResponse 0.427751 Observations(or Sum Wgtu) 47 Analysis of Variance DF Sum of Squares Mean Square 1 2.6145444 2.61054 45 5.0169158 0.11149 eaeF Ratio om 23.4157 a=ugProb>F C Total 46 REp.rance ST Estimate E Sam E SECUREE Sny E umes E me 0.148129 7.6274602 Parameter Estimates Std Error t Ratio 0.075573 1.96 Prob>Itl 0.0562 <.0001 Luwer 95% -0.004082 Upper 95% 0.3003395 0.0253956 0.005248 4.84 <.0001 0.0148254 0.0359659 SHaRteSalre orrpeecotr Coping sSorrtae er Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00129 anrcososes 3MA10050562 RandomSane Random Sample Chem Opers ChemicalOperators sougpm By vASGHEM POAA -m B YRSCHEM 5 z 100 w - 500 - oo5 90 i. - Rt . Fan Ca TT mg I 05 :: . 1 1 eds sas 10 15 wou03CHEM J' 1 20 25 I. 30 35 Sauca Source Viel Model foError Crom C Total TomTerm ment Intercept RSCHEM YRSCHEM En =Lim ii Linea Fe Linear Fit POAApp=M 173387 +DO4T02 YRSCHEM POAAppm= 1.73387+0.04702YRSCHEM SummoPaA Summary of Fit Rsquue oom? RSquare 0.09937 Rou Ady 003s RSquare Adj 0.079356 RootMen quaeEr 10s Root MeanSquare Error 1.342508 MeanofRespone si MeanofResponse 2.251574 Oeraion (ox Sum Wet) 0 Observations(orSum Wgts) 47 Anact viarasrcs Analysis of Variance or "melts MenSuwe FRaio DF Sum of Squares Mean Square | een ian ue 1 8.948633 8.94863 us Pre [rs 45 81.104760 1.80233 " prt oe 46 90.053393 F Ratio 4.9650 Prob>F 0.0309 Eiew [Sufmr r -- (Fai Pani Loweosk Estimate LB ONS ST <0 hie 1.7338672 donoist ome 2m aos osels 0.0470188 Parameter Estimates Std Error t Ratio 0.303857 5.71 0.021101 2.23 Prob>ltl <.0001 0.0309 Lower 95% 1.12187 0.0045187 AAPpaepgpeeendn1i1dxixE Page 11 Upporosw Upper 95% zien 2.3458643 0oesis 0.089519 MSMuaabddjeeecAAtvvalaoillaParbbollteeecbbtyyiv33eMWOfrfoodrrIenrInsIspnpeePcctatiiloomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo.nn6ff3iidd0ee9nnttiiaall Information Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00130 MA10050563 3MA10050563 PFCOhCSeRhARmaeaAimnpnicddocaoaomllmmOSOBpSypaeaemrmrYapapRtltloSoeerrCssHEM PFOSAA#m B YRSCHEM 0;) RAPppappgeeenndd1ii2xx EE Page 12 I | C 2) - 2Zz .n1]-- i : - HRC ----AA o co >i~rs ~ ti. ;',-r - ` . ~t-'~--rte-*-- ERE 0 S '0 1S 2J 2S 3J 3S wo `!nSCH:M SoSMuooudrerclcee EECMrroordroaerlt C Total TTIenoerrmmcept YIRntSerCceHptEM YRSCHEM jIg ii PRO=SL0.iL0ni4A ne9eaa4rr-FFiA 0itt.00p 118Yp RSCm HEM PFOSAAd Rsquire fpp m SummaofrFyt =0.0494 --0.00118 Summary of Fit YRSCHEM 0036.8 RRRRSoSSqoqqtuuuMaarrreeeeaAAnddSjquwre Error 0o0.0o0.0l5017346858:i1(.s948 MRMeOobeaosantenoMrofevfRaaRentesisSppoq(oonuonnasrssreeSeuErmroWrs) 0.057519 0036r7l 0.0364.7 Observations(or Sum Wgts) t.7 OF AAnaSluymrsiosiooSffyVoVauarraiia maansnccee MeanSaume DaF1| Sum000.o10f040S085q586u6700a844r155e188s Mea000n.00S000q053u563a6000r585e %45 46 0.15648269 0.14887811 0.15448269 0.003308 FR1a.R6ta9ti4ioo0 PP01rr.1oo69bb99>o47FF0 0.1997 ODEEsIstiSamWtatNoe 000UTI 0.0494028 -0.001177 PaPSrauarEmamemetotererr EEssttiimm(aaRttaeelsso 000S.t000d011E38r000r1oS:9r t R133a.3t77i099o 0.000904 -1.30 PPr0ro0bo>0b114l1 01997 0.0004 0.1997 LL0oow0wee3rr919552%% 0002995 0.0231822 -0.002998 U0pU0pp7epre5r96S53e3%k 0000642 0.0756233 0.0006442 MMSuaabddjeeecAAtvvaatoiillPaarbbollteeecbbtyyiv33eMMOfrfoodrrerIInnIssnppeePccattiiioomnneaavrnn.dd3CCMoo,ppyyNoii.nngg2a-ass04CC-oonn6ff3ii0ddee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00113311 3MA10050564 3MA10050564 ravcomsarsle Random Sample Cham comsrs Chemical Operators eS SEEM M570 ppm By YRSCHEM 50) w03) [ : + Eon : . w fo L TTo R das 0 $ f0 t5 onYRSCEN AAppppeendnidxiExE PPaaggee1133 Sauce Source Sit Model HorError Ca C Total woTerm Te Intercept Veschem YRSCHEM LffO 1[ [-- Linear Fit NSTppm= 0.3056 YoiRSCHEM M570ppm =0.30244 -- 0.00666 YRSCHEM Sra Summary of Fit Rs aonan RSquare 0.0710"1 Roar Ad Sosoes RSquare Adj 0.050428 Roo Mnsare Err an Root Mean Square Error 0.228411 Noho p= Mean ofResponse 0.229083 Onseraion to am Wes) Observations(or Sum Wgts) 47 Ana vanes Analysis of Variance or VERS emswe Fras DF Sum of Squares Mean Square f Ths Orne Sm 1 0.1796529 0.179653 H She oval peer 45 2.3481307 0.052181 dam Son 46 2.5277836 F Ratio 3.4429 Prob>F 0.0701 Camus FSurEor Esihse Pond Lowresx Estimate oS omiwm 38 wel obi 0.3024368 Goose Gow 1% oom booms -0.006662 Parameter Estimates Std Error t Ratio 0.051702 5.85 0.00359 -1.86 Prob>~tl <.0001 0.0701 Lower 95% 0.I983041 -0.013894 Ups Upper 95% Coos 0.4065696 aoowen 0.0005694 SMMuaabddjeeecAAtvvtaaoillPaarbboltleebcbiyyv33eMOfrfoIdornersInpIsenpcePtcatilioomnneaarvnn.dd3CC,ooppyNyoii.nnggC2aa.ss0CC4oo.nn6ff3idd0ee9nnttiaall formation Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 281122..00113322 amA1o0E0eS 3MA10050565 [--. Random Sample ChimesOsos Chemical Operators ert pem mrs PFOSA -m B YRSCHEM =0 3c w0 50 AAppppeendnidxiExE PPaaggee 1144 zo4 e -- Fadl . . TTT--_-- EE 000 . T 0 5 10 15 20 25 30 3S woYRSCHEM [. Source Voie Model EreError oat C Total TomTerre Inmenc Intercept rschin YRSCHEM bw Ft Ero01S5J 551A000d214pm Linear Fit YRSCHEM PFOSAdfppm =0.12291-- 0.00214 YRSCHEM Simm oiFe Summary of Fit Rue oasis RSquare 0.023165 Ropare A Sores RSquare Adj 0.0014:;7 Ron ea Sqr Err oisis Root Mean SquareError 0.1315:3 Nea Respone Son MeanofResponse 0.099349 Ohsrain to Sum Wes) a Observations(orSum Wgts) 47 Ang ofvaries Analysis of Variance or ME' wenswwe erase pF Sum of Squares Mean Square A 1i tr 1 0.01845661 0.018457 8 amsem come er 45 0.77830020 0.017296 ames on 46 0.79675681 F Ratio 1.0671 Prob>F 0.3071 Caiman GFtarrtRasy Pol Lowes Estimate oie owe 13 owe Commi 0.1229105 "ps oom 4m own owe -0.002135 Parameter Estimates Std Error t Ratio 0.029766 4.13 0.002067 -1.03 Prob>ltl 0.0002 0.3071 Lower 95% 0.0629591 -0.006299 Uppers Upper 950/6 owe 0.182862 ows 0.002028 SMMuaabddjeeecAAtvv1aaoiilaParbbollteeecbbtyyiv33eMO rffodorreIrnIsnIspnpeeaccttiiioomnn eaavnn.da3CC,ooppyNyoii.nngg2aa.ss0C4Coo6nnf3fii0dd8eennttiiaall Information Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 281122..00113333 aMAT00S0565 3MA10050566 ransomSarole Random Sample Chane opmmrs Chemical Operators w erie em M556m B YRSCHEM Fis AAppppeendnidxiExE Page 15 Fr .. Fad W TT TT 0 S SO 1S 20 waYRSUN sauce Source Sr Model ErrError Coa C Total Tom'Perm Ton intercept sche YRSCHEM MS=00-- S 95G26 2 m LinearFit YRSCHEM M556dfppm =0.09775 -- 0.00212 YRSCHEM prime Summary of Fit Rune oomus RSquare 0.069465 Rea Ag Ooms RSquare Adj 0.048786 Rove Sq Er Soria Root Mean SquareError 0.073484 NeatRepos Sores MeanofResponse 0.0744--8 Onn or sum We 3 Observations(or Sum Wgts) z 7 J-- Analysis of Variance or MERLE mse Frais DF Sum of Squares Mean Square Tube Dow sows 1 0.01813944 0.018139 uw om het 45 0.24299278 0.005400 Summ oa 46 0.26113221 F Ratio 3.3593 Prob>F 0.0734 Guna p SHEr-- RM Pon owas Estimate Com coun 3% com maw 0.097747 Soni Goss 4% oo dwoss -0.002117 Parameter Estimates Std Error t Ratio 0.016632 5.88 0.001155 -1.83 Prob>ltl <.0001 0.0734 Lower 95% 0.0642487 -0.004443 Upeosk Upper 95k omnes 0.1312453 coos 0.0002094 MSMuaabddjeeecAAtvvataoillPaarbboltleebbcyiyv33eMOfrfoIodrnerIsnpIsenpcePtcatiiloomnneaarvnn.dd3CC,ooppyyNoii.nnggCa2a.ss0CC4oo.nn6ffi3dd0ee9nnttiaall formation Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00113344 3MA0050567 3MA10050567 RRaaEnnnddgooimmnSoSaoamrmgapnllee w PPFFOOSSEpnpgpmiomBnBeyyerYY/LRRaSSbCCHHEEMM 1 AAPpappgpeeendn1i6dxi&xE Page 16 ; " T . . . . . . . r . . . . . . . Tu anE s E 5 1D 15 25 25 30 35 0 wo YRSCHEM SMoSouodurercclee EECMrroTrdoroerull C Total TTIenoremrmcept YRSCHEM Intercept YRSCHEM PPFOSR dfppOm==00S `..44S00LUui44nnd 44ome66aam+r+rF0aoF0if 0if.trt1.0Fy15i56lp644YYRRpSSCCHHmEEMM RRRSSsqqquuuaairreeeAd) Summary of Fit 000.101282034929363333 RRRMoSoeoqoatutnaMoMrefeeaaRAnnedSsSjqpquouarasrreee.EErrrroorr 0000..65503778324392246464143 ObMseearnvaotfiRoensspoonrsSeum Weis) 5 0.633961 23 Observations(or Sum Wgts) OF AAnSanluyasmiosloioffySVVmaasarriimiaasnnsccee MemnSwar D2F11 Sum o006f.899S288q48u6a686r696e60s93 Mea0O0n.3S9o9q8us78a65tr6)e7 221 22 79135572 6.9248903 7.9135572 0.329757 F2F9RRa9at8ii2oo PP20rr.0o9o9b9b8>8e0F2 0.0980 iEEsagttimmsaatee 00IS61 0.4044606 0.01564 PPaSarrWaaEmmmeeottreerrEEsstiimmUaaRtteoelsos 0O0S.t0L1d07ME80rI63r1oS39r It R22a1.t272i636o 0.009033 1.73 Pr0Pobb0>sli3t|l 00980 0.0343 0.0980 L0oLwo0ew3rsr90s5sS%% 000344 0.0330049 -0.003144 UOpU7ppIeprSer995sI9s'Ex0 00324 0.7759163 0.034424 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggCa2a.ss0CC4oo-nn6ffi3idd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00113355 3MA10050568 3MAII0050568 EHRSRaaEEnnnndggdpioonmoBnmemeeySerSraYia/mLmALpaapSbbllCeeHEM 1H PFHS ppm By YRSCHEM ] wD FD e hi AAappgppeeendn1i7dxiExE Page 17 Er w - D.?C I. D.DD DSSw10 : 1s5 m?0 n25 wo YR$CHLN Pat JnD 3s 5 MSooSuodruerclcee EMECronTrdoooerrull C Total TIToneermrmcept YYIRnRtSeSrCcCeHHptEEMM =LW fi PPFFHHSSdAffppppmm== 00`..L11Si0L0nui66ne55me77aam+r+roaF0F0ifi.r.ttF00y00t443399 YYRRSSCCHHEEMM RRSqqquuuaiarrreee Ag) Summary of Fit 000.000266051508,2029 MRRReooSaoqotutnaMMoreefeaRaAnendsSSjqpquouaanrrseeeEErrrroorr 000.01.07222030394093817739 OMObbessaeenrrvvoaafttiiRooennsssp(o(oonrrsSSeuumm WWgetss)) = 0.170933 .:3 OF AAnaSnluyasmiosloioffSyVVqaasruriieiaasnnsccee MemSaume D2F1I1 Sum of Squares oLgirsse 0.0777620 Mean Square c0o0mSe 0.077762 221 22 11L..i11991668113115664444 0.053255 FLFRRaaatieioo PP01rr.2o4o4b6b0>0e3F2 0.2403 01EEs0stii6mm5aut9se 00086 0.1065696 0.0043863 PaPraSarUamEmeMetotreerrEEssttii(mmaRattaeesos 0S.O0t0Od07TE01Ir7T3r88o6L1r t R1a11.t244i188o 0.00363 1.21 Pr0Por1bo>2bJst5lJ 000..212454020353 L0oLwo0ew2rs7r990556%% 0006 -0.042706 -0.003162 U0pU2pp5ep5ro8r94d55s%8x 0.0205518945S8 0.011935 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggCa2a.ss0CC4oo-nn6ffi3idd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00113366 3MA10050569 3MAII0050569 PORARaaEEnnnndgdgpoipnomnBmemeSeyeSardaYmiLmRapapShbllCeeHEM. Ww POAA ppm By YRSCHEM mi )) 5E . Eu]. -- JO HE DO) ERC10 1~ 2R0 EtiRE30AEA3; to wo YRS10, AAPpappgpeeendn1i8dxixE Page 18 TIYnIToRenetrSrmeomrCecepHpetEM YRSCHEM SMoSooudurrecclee EMECromTrdoooecrull C Total PPOOAAAAZpPpmTM==00..`31LS49iL9u0ni0ne7m7eaa++mrro0Fa0Fi.fi.trt00F00yi11t8855 YYRRSSCCHHEEMM RRSRSqSqquuuararreeeAG Summary of Fit 00".000000253313s29 MRRReooSaoqontutMaoMrefeeaaRAnnedSsSjqpquouanarrseeeEErrrroorr 0o0-.s075.2206s54727511l8772 MObesaenrvoaftiRoenssp(o(oonrrsSSeuomm WWagttss)) B 0.3762 78 33 Observations oDFF| AAnS"anlSuyumsamioos0ofiyo0fSSf1VqqVs3auua8raar9iriria6eean2ssnaccee MeMaen0n0SS1qq3uu8ar9re6e 2221 1 50p5..580r001133e998339y996662 027638 0.013896 0.276378 22 5.8178358 F0F0RRa5at0ii3oo PP00r.r8o0ob52w>04FF3 0.8247 03CEso5tii0mma9att6ee Ooi 0.3490696 0.0018542 PaPraSarumaEemretotererrEEssttiamItaRetaesiso 000S.t011d066E38r252r2o464r t R220a.t121i023o 0.008269 0.22 P0rPorbo0>bJo7tlJi 08247 0.0447 0.8247 L0oLwo0ewre0r99505%% -001SM2 0.0090046 -0.015342 UpUOppGepEreOr9Is5Ns%Tk 00150509 0.6891347 0.0190509 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbtyyiv33eMMOfrfoodrrerIInnIssnppeePccattiiioomnneaavrnn.dd3CCMoo,ppyyNoii.nngg2a-ass04CC-oonn6ff3ii0ddee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00113377 3MA10050570 3MA10050570 rosRRaaEpnnnagddoioonmemmeBesSSryaa/rmLmRa.ppSblleCe HEM fr PFOSAA m B YRSCHEM C; AAPppappgeeenndd1ii9xx & E Page 19 | Ed fo wo Ee C00 0E1C 0 wt5AonA20A C25A3ECC E35 ID YRZNW SoNSiouuocrsc!oe EnECMreorrdrooeralt C Total TTeeorrmment RSCHEM Intercept YRSCHEM I Lim ft POSAAfppm = L00iLi1nn7ee8aa9rr FF-iu0t00027 YRSCHEM PFOSAAdfppm RsRRqSuoquiwarreeeAdj SummaorlFyt = 0.01789 -- 0.00027 Summary of Fit YRSCHEM o"aosut 0.034722 RVoRRiSoocqowtutnaMMorfeaeRaneAndsSSjpqqouuanarsreee Eroroxr 00f-.000r1.109i916614e42774 OMbesaenrvofaRoensspo(onxsSeum Wes) 0.013949 23 Observations(or Sum Wgts) oDrF| AAnSMaluSyirmsDimosooofoifoSfaSqvwVuaoaiarrirsiasmeansssnccoe MeMaeonmSoqSueamrse FR07Ri5at5oiso 2a211 0.00029158 O00B09O7E5 0.00810598 0003s 0.000292 0.000386 0.7554 P3rosvF Prob>F 22 0.00839755 0.3946 oECsotiOmmuatee SPPOtaaGd0rraeauEmmlrEeerltotmlererrEEssttit(immRRaa2atatt5eeias3os PP0roob0o>I0ltI LLGoowweOrrs95ss/e6 Does 0.0178899 -0.000269 ows 0.006111 0.000309 052.93 -0.87 ome 0.0080 0.3946 000911 0.0051812 -0.000911 Uppwrssw Upper 95% 00S 0.0305987 0000S 0.0003741 MSMuaabddjeeecAAtvvataoiillPaarbbollteeecbbtyyiv33eMMOfrfodorrIenrIsnIspnpeePcctatilioomnneaavrnn.dd3CC,ooppyNyoii.nnggC2aa-ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00113388 3MA10050571 3MA10050571 S7R0RaaEEninnrdgdgioonBnmomeySeeSrraYa/iRmLmaapSinblCaeHEM = M570 ppm By YRSCHEM D SC we . G ..n i ge wrC_'0 s . -- wwC co TTRwoRn s J S 10 IS 1D 2S 'tISCHE1t s+sw JD JS 10 AAPpaopgpeeen2dn0idxixE Page 20 SNoSoouducrecoe Model fCoont Error C Total YTITIRnenotSreemmrrCcceHppttEM YRSCHEM Lim it MST0ppm M570ppm = = 00S.00u77LL44im7no7e-m0aa0r0a.arF00irlt00Fy00t044 YRSCHEM YRSCHEM RRRRRsoSSqoqqqutuuuMaaarreeeeeaAAnddjSjqua r Summary e Enc of Fit 00P-.0000.0r0000004i057s45::, OvRMMeoeeroaavtnnsMtoeifaoRRnneesssSppqo(ouonnarssreSeeuEmrrWores) 0.08786: Qanaos3:] 0.07406` Observations(or Sum Wgts) Anofaarasnco Analysis of Variance or| "SmDoorSowrasm:s DF Sum of Squares 21 MeMae0nm0SS0qqu0au0ro8e FF00Raa0t1oi0o 22211 0.00000754 pDaigrlieesns 0.16211665 00m 0.000008 0.007720 0.0010 Poosoer Prob>F 22 0.16212419 0.9754 oECvsutiiimmasstee SPPSotaaudrcuEaaErmrrmeorostortrenrEEssttitiimmRaFaaatatte7eiesso PPrlooObo>lmItsl -Looowewore9rm5s% Woon 0.0746991 o0m.0i2w73:3 a0 ose 2.73 -0.03 0.0125 0.9754 0009 0.0178643 -0.002917 -0.000043 0.001382 UU0pp0a0p.pne10or3ir291os855s3e9s%4 0.0028309 MSMuaabddjeeecAAtvvataoiillPaarbbollteeecbbtyyiv33eMMOfrfodorreIrnIsnIspnpeePcctatilioomnneaavrnn.dd3CC,ooppyNyoii.nnggC2aa-ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00113399 33MMAA1T00005500557722 Rar sanple Random Sample rama Engineer/Lab pros guns, vase PFOSA ppm By YRSCHEM TMC)3 Cw06 t - . fu F5 ad = " TIeN dEaeE e 16 15 20 ?$ 30 35 10 berli$tE;Y Aeppnendix Appendix E Page 21 Saco Source Soir Model EnError Coal C Total TomTerm Jen Intercept sche YRSCHEM =Lin R nnn Linear Fit PrOS=001A475C+ 0t001pSYRpSCHmEM PFOSAdfppm =0.01475+0.00015 YRSCHEM SmeoafFrs Summary of Fit Raum omnes RSquare 0.007656 Ria ag Sos RSquare Adj -0.0396 RonenSqrEre aon Root Mean SquareError 0.023047 NealReson ores Mean ofResponse 0.01689 Ota or Sm Wes) > Observations(or Sum Wgts) 23 Ansorvyrarscs Analysis of Variance or Eni wns rao DF Sum of Squares Mean Square To Toowbe "fooow own 1 0.00008605 0.000086 a dommes oowst per 21 0.01115404 0.000531 2 Gola fr 22 0.01124009 F Ratio 0.1620 Prob>F 0.6914 Cunae PSarEos EsTmaeRs PrN lows Estimate obi oni 3m doom 00m 0.0147485 on omme od Ogi mas 0.0001459 Parameter Estimates Std Error t Ratio 0.007169 2.06 0.000363 0.40 Prob>ltl 0.0523 0.6914 Lower 95% -0.000159 -0.000608 Upeose Upper 95% Obweses 0.0296564 000s 0.0008998 MSMuaabddjeeecAAtvvtaaoillPaarbobltleecbbtyyiv33eMOfrfondoresrIpnIsnepePccttiaonnmaavnn.dd3CC,ooppyNyiionnggC 2aa.ss0CC4oo.nn6ff3iidd0ee9nnttiiaall Information Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00140 3MAMO050573 3MA10050573 ssRsRaaEEonnnrdgdgiyoomnmmeeSeeSrtSaa/imLoleapnbleern ww M556 ppm By YRSCHEM wuw : i Tow --_ so Jeet TT ns ssw 0 5 10 1S 20 2S 70 3S 40 wo'IRSCNEk PAAapogppeee2nnd2idxixE Page 22 Sues Source Side Model EoError Chaat C Total TomTerm ep Intercept Viste YRSCHEM Gear ~'t Unourt Linear Fit MsS6dtopm =00I85 - 00001 YRSCHEM M556dfppm =0.0188 -- 0.00001 YRSCHEM SomaFa Summary of Fit Rsquie aceon RSquare 0.00004E Reqs Af "Sons: RSquare Adj -0.0475, Ro Mean Square Err dame: Root Mean Square Error 0.02742? Vian of Response Coit Mean ofResponse 0.018( Omervason or SumWat) x Observations(orSum Wgts) 2.-- Anofavarsa Analysis of Variance or "Mhiisam MemSuwe FR DF Sum of Squares Mean Square | "Towns ower ooo 1 0.00000073 0.000001 a oom oom por 21 0.01579191 0.000752 2 cosme ose 22 0.01579264 F Ratio 0.0010 Prob>F 0.9754 ume SPaurtmeetrer EsRtaoss Probl oweros Estimate obisnrs Goosss 23 looms Goole 0.0187973 "oes oom! 00 os 00 -0.000013 Parameter Estimates Std Error t Ratio 0.00853 2.20 0.000431 -0.03 Prob>ltl 0.0388 0.9754 _ower 95% 0.0010588 -0.00091 Upporosw Upper 95% Goes 0.0365359 owe 0.0008836 Made Avaiable by 3Mfor Inspection and Copying as Confidential Information Made Available by 3M for Inspection and Copying as Confidential Information: SSuubbjjeecctt ttoo PPrrootteeccttiivvee OOrrddeerr IInn PPaallmmeervrv.. 33MM,, NNoo.. CC22--0044--66330099 281122..014411 1 3SMMAr1i0c0i5o0s5z7d4 RRaaMnnaddnootmmaSnSaaanmmcppellee PPFFOOSS pMapipmpnmBtBeyynYYanRRcSSeCCHHEEMM. w . "= AAPppappgeeenndd2ii3xx E& Page 23 :w 5 wo Bon o8 ww SMoSouodurercclee EEmMCroroodoearlt C Total ITnTtoeermrmcept YRSCHEM Intercept YRSCHEM Lim it PP FOSdF fpprnO == 11S..33S u66LLii77mnn11ee33maa+f r+raoFF00ifir.t.t0F0yp i33228899YYp RRSSCCm HHEEMM RRsSRqqSuquuaaarrreeeAdj Summary of Fit 0o.o00m703s25s94a4 MRRReooSaoqotutnaMMoreefeaRaAnendsSSjqpquouaanrrseeeEErrrroorr 111.-6220754.250202229291444 ObMOsbeesarenrvvaoatftiiRooennsssp((ooonrrsSeSuumm WWegttss)) 1 1.672091 11 OF AAnaSnluymasiosliooSffyqVVuaasrariamiansncscoe MeanSauwe DF51i Sum o1f131S.91q150u057a728r850e065s5 Mean1LUS.Sq1Su0o0a7Sr88e0 09 10 15063061 13.955256 15.063061 1.55058 FF07Ra1at4oi4o PP0arr.oo7bb19>o4FF4 0.4199 13EEs7st1ii2mma5at5se COMES 1.3671255 0.0328884 PPaarSraGamEmeeottreerr EEssttii(mmAaaitmoeoss S000t.0d5532E280r09r77o111r t R220a.t686i353o 0.03891 0.85 PPr0roGbo>2bll6ll 0419 0.0276 0.4199 Il.ooOwweIerrI99S5S0%T% 00S 0.1891877 -0.055132 U2pU5pp4epr5o90r56s3%s 0120093 2.5450633 0.1209093 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggCa2a.ss0CC4oo-nn6ffi3idd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00114422 3MA10050575 3MA10050575 PEfSRaaNpMnnaoaddimonnomntmBSeaySnanYaamncmRpcpeSellCeeHEM PFHS m B YRSCHEM AAFppappgeeenndd2i4ixx E E Page 24 | I j . I r , r | "Tw Fa 11 15 20 wwYRS%H(N | : aI SSVooocudreace EnCEMroeordoraerlt C Total TITeonrmempt YRSCHEM Intercept YRSCHEM PPFHSFdfppHm==00SS..u11mLL32mi6i6dna77ne+ra+eyrao00Ff.r.ift0011t11p9944YYRRpSSCCHHmEEMM RRRSSsqqquuuaarrreee Ad Summary of Fit 00i.292661515552522 RMoRReoSoaqotutnaoMMrefeeaaRAnendsSSjpqqouunaarsreeeEErrrror ObMseearnvaotfiRoenspoonr sSeum Wet) 0.179502 0214058 0.214098 02750s 0.237455 Observations(or Sum Wgts) I I oDFF| AAnSSaluunymmsCioosliafooaSfSfoVaqViuiuaaalrwrriieeascessncoe MeMaeOnwSSlqouaweree F3FRRa7taioo 0991 00o0..5a415s148a2665l1541t918l716716 ois 0.146119 0.045838 PpS3rr.io1obo8v>7neF7 10 0.55865977 0.1078 oEEsotiiimmaatee P0SPataSr0drGaaEmESmrreerot:torererr EEsttmt(iamFRtaaaettl4esi2eos PPoroowb>elvtrl LLeoowoewrn9ee5sR% 00119444 0.1266974 0.0119444 0006 0.089528 0.00669 1791.42 1.79 ITE 0.1907 0.1078 00S 0.075832 0.003189 Upporos Upper 95/. 0s 0.3292263 000 0.0270783 MSMuaabddjeeecAAtvvataoiillPaarbbollteeecbbiyyiv33eMVOfrfodorreIrnIsnIspnpeePcctatilioomnneaavrnn.dd3CCMoo,ppNyyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee8nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00114433 3SMMAA11105007 005500557766 POARARaaVMnnaaddipmoonomBstmneySnSaaaaVnnmmRccppSeellCeeHEM. 0] POAA m B YRSCHEM S00 - i i40D - | FAAappgppee2endn5idxi&xE Page 25 < 2 00 - we1.00 of :iw O.DD -- HERECRE REE | 0 5 wi 10 1S 2D 2S 1 YRSCH1t1 SMoSooduuerrlcse EMECronTrdoooerlw C Total TIITYnoenRtremSemrcCpeHpttEM YRSCHEM =Lom 11 POAApp= POAAppm = 11.S.244u6LL6ii5m5nn11eemaa++rra00FoF.i.irf0tt02F2yi555555 YRSCHEM YRSCHEM RRRSSSqqquuaaurreeeAg Summary of Fit RoRSoqtuaMreeaAndSjquareErox 00-1.00030.09430697066760590936996 OMbRMesoeaeoarntnvoMaofetfaiRRnoeensSspqpo(uoonarsmrSeeeuEmrroWrats) 1.340539 Lissssis 1.483455 Observations(or Sum Wgts) 11 or AAna"lSnyusimsoaoofffVSVaiaarrriieaassnnc,e MemSaes 1DF Sum of0S6q6u7ar3e1s sess Mean Square FF0rR3aatmito 1915 11610661..86714673283417430305148 L908 0.66873 1.79704 PP0orr.soa3b7bs2>ee1Fr 10 16.842135 0.5569 LEGsutisnmeatse PoSPSatasurdrateaEmrmrseerotsotrererr EEssttitiFmmRaa2aatltt2eeise2os PProrobo>obltll LLaoowweeurr9ol5s%h o1.m2s46s5s11z1 opis 0.560567 20.6212 0s 0.0532 00.006291250916 0.0255527 0.041888 0.61 0.5569 0.069206 U0pU22.pp.e3p05re113r9416o65s111%3w 0.1203111 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbiyyiv33eMVOrffodorreIrnInsIspnpeePcctatiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggCa2a.ss0CC4oo-nn6ffi3idd0ee8nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00114444 3MA10050577 3MA10050577 PEOSARRAaaVMnnaipddiaomnoomtommenBnSySaaaannmVmccppReellSeeCHEM PFOSAA ppm By YRSCHEM wf AAPpappgpeeenndd2ii6xx E E Page 26 Zw Ted. 0.Oi :0w.w00 3 ns R4 58 a 0 5 wi 1D :7 20 25 30 Y3S HN SoSMuoourdrecclee EmECMrooordoaerll C Total YInTTIRneeotSrrmeemrCeceHppttEM YRSCHEM PPFROOSSAAAAddifpppprmm ==SL00ui.L.in00mn33ee44maa77rra---FFoirf0t0t..Fy00i00000066YYRRSSCCHHEEMM RRRsSRRoSSqqoqquu:uuaarrMrreeeeeaAAndYSjquareSEutmomary of Fit 00o.0r0l000o74s7::: 0-503.1113005.1 ObRMMsoeeeoaartnnvoaMotfefiaRRoneenssSppq(oouonnrassrSeeeuEmrroWrg) 0.03130; o03410n 0.03410( Observations (or Sum Wgts) 11 oDrF| AAnSa"luSnymsmDioosoafoioofSfSavqVquliaaaurosrimsneassencscoe MMeeam0n0SS0qa0u0sa0rn:e 10951 00Oo..oo000o00Re08Ee08I201T1479E188262 000090 0.000004 0.000980 10 0.00882198 FF00rRa0it4io2o PP00rr.9oa04bb09>o4sFF2 0.9495 Esinaw Estimate OMG 0.0346975 Doo -0.000064 [a -- Parameter Estimates SuEmr Pale Std Error t Ratio 0008 265 0.013089 2.65 00008 0m 0.000978 -0.07 Probl Prob>JtJ Ooi 0.0264 0545 0.9495 owrSh -ower 95% 0ODSOE 0.0050878 00026 -0.002276 UU0p.0Opp00oep6orsz4ei39idr005s7sr%s2 0.0021488 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbiyyiv33eMVOrffodorreIrnInsIspnpeePcctatiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee8nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00114455 3MA10050578 3MA10050578 Rand Sao Random Sample mana Maintenance ws70pn By pace M570ppm By YRSCHEM oT 0 a0 we050 Be {3 w || = w+TT S ww 10 ~S 20 wo1RiCAEu ss 25 30 AAZppappegen2dne7idxixE Page 27 Sous Source Voie Model PoError oat C Total TomTerm jrucIntercept VRackEM YRSCHEM lrej ~l Loos Ft Linear Fit MSToppm = 02607 500079YRSCHEM M570ppm=0.26076+0.00079 YRSCHEM Sma alFe Summary of Fit Rsquue acorns: RSquare 0.001745 RoweAd or: RSquare Adj -0.1091; Ro Mie SuseEre aon RootMean SquareError 0.20146E MeanofResponse 026801 MeanofResponse 0.268091 Shans or um Wi) n Observations(orSum Wgts) 11 Ansofvyersre Analysis of Variance or "Dim Mens Fra DF Sum of Squares Mean Square To "Town ome oom 1 0.00064018 0.000640 5 Glen ones pr 9 0.36530321 0.040589 0 alsa on 10 0.36594339 F Ratio 0.0158 Prob>F 0.9028 Cinge f SHE -- ia Pol erst Estimate oso omegw lo Gor doors 0.2607598 ums Oss ol asm 00s 0.0007906 Parameter Estimates Std Error t Ratio 0.084247 3.10 0.006295 0.13 Prob>JtJ 0.0128 0.9028 -ower 959/6 0.0701785 -0.01345 Ugerosn Upper 95% omoan 0.4513411 oom 0.0150317 MSMuaabddjeeecAAtvvaaiilaParbboilteeecbbtyyiv33eMWOrfoodrreIrnInsIspnpeePcctatiimoonneaarvnn.dd3CC4oo.ppyyNoii.nnggCa2a.ss0CC4oo-nn6ffi3idd0ee9nnttiiaall Information: Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00114466 MAT0050578 3MA10050579 PROSRRAaaMpVnnaaodditmonoBtmameSnynSaaaaYnnnmRcvpseSllCeeHEM. wT PFOSA ppm By YRSCHEM 60 | 04C AAPoaopgpeeen2dn8idxixE Page 28 Zi ~~ 1 0.20 ww ON TTT 0 a f0 a wow io t: 'f1r~tH[N io SoSVoouudcrecee Model ECorw Error C Total TITnoeermrmept IYnRteSrcceHptEM YRSCHEM -1 POSAdppm PFOSAdfppm = = S00..u00LJ 99im77n4e4ma34ra--oFi0rl0t.P0y00t0335511 YRSCHEM YRSCHEM RRSSRqqSquuusarreeeAdj Summary of Fit 00".o00o4e3s27s:4)3 RRRMoSeoqioountMaoMrfeeeRaaeAnnsdSSpjqqouunaasrreee EErrroorx -0.06251 0o09n% 0.174833 ObMseearvnaotfioRnesspo(onrsSeum Ws) n 0.064939 11 Observations(or Sum Wgts) OofFi AAnS"alunmymsoCiosasfoooStfqqVauuiiaarserieeacsssnoce MMeeaDmnSSoqwulmasree FForRaaitnioo 10951 0.01258420 moassesl 0.27509911 ose 0.012584 0.030567 0.4117 Pasrm Prob>F 10 0.28768331 0.5371 ooEspntiumeaste [-- Parameter Estimates oSuwEamosr iR1si3e Std Error t Ratio PomPbon>blistil -Ooowoweerer9ms5se%n Wooisos 0.0974427 -0.003505 Ome 0.073109 0.005463 06s1.33 -0.64 Os 0.2153 0.5371 00ises -0.067943 -0.015864 UoUpppepzrec9os5s%w 0oosssal 0.2628285 0.0088531 MSMuaabddjeeecAAtvvataoiillPaarbbollteeecbbtyyiv33eMMOfrfodorrIenrIsnIspnpeePcctatiiloomnneaavrnn.dd3CC,ooppyNyoii.nnggC2aa-ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00114477 3MA10050580 3MA10050580 ssRoRaapVMngnaadmdimonoBatmmnyeSnaSvaaannmAcncpSseilCearEM ww M556 ppm By YRSCHEM 0;0 ww . | E _ c se qr A0"20 PR 010 S-- n0 00 fe U3 05 uw 8a 10 1S 20 won'~StHEu d: x AAppppeendnidxiExE PPaaggee 2299 ESomSVMuoooeruddrrceeclee CErrroorat C Total YITITRneotnrSemmrCnceHpstEM YRSCHEM =Ln:7;i MMS5S566idtfppppmm ==S00u..m11m11UL00ian23rne66ay+r+eoF00t.00F00004488YYRRSSCCHHEEMM RRRooRRsoSSqqqwtuuuMaareirreaee nAAdSjqua Summary re ror of Fit 0aa-1.o0l00.oa01i9n10r17u9s912is32 ORMMoteeoeaatnrnoMvofetfaRoRennesssSppqo(ounonasrsSreeeuEmrroWre) 0.120441 otteir 0.1147 Observations(or Sum Wgts) AraofVyaranaco Analysis of Variance or1 "EDomwnoesn: |Mem0soumwse DF Sum of Squares 11 Mean Square FForRoaattlioo 0951 0.00023453 oomnmsom 0.13055477 ona 0.000235 0.014506 0.0162 p0o5o0r6 Prob>F 10 oEiGsultimemuartse 0.13078930 ParameterEsai Parameter Estimates OSGEenor Ra1i6a Std Error t Ratio PP0roobl>%litl 0.9016 Lloo0wwe0rr 9sms5gh% Oooies 0.1102627 oom 0.050364 013 0%0i6 2.19 0.0563 0.9016 000K -0.00367 -0.008035 0.0004785 0.003763 0.13 Upperssw Upper 95% 0m 0.2241958 000892I 0.0089921 Made Avalable by 3Mfor Inspection and Copying as Confident Information SSMuuabbdjjeeeccAttvttaooilPParrbooltteeeccbttyiivv3eeMOOrrfdodreerrInIIsnnpPePcaatllimomeneravrvn..d33CMMo,,pNNyooi.n.gCC22a--s00C44o--n66f3i3d00e99ntial Information: 2881122..00114488 10050581 3AM1A01000%50055881 0RSSSRauwanponedrdorosmovBmsmiSyosSaomYamdimRMpgpgSlrlmeCtetHEM a PFOS gm 8 YRSCHEM PAAappgppeee3nnd0idxixE Page 30 " Ei E7u Bs. < | "w tn- aEet8s. 10 won 15 20 `IPSCHEt 25 30 35 10 SMoSouodurreccee EnECMrooordoraerll C Total TYITIoRnentSermecmrCceeHppttEM YRSCHEM -Lro'1 PROSUppm PFOSdfppm = = -0S0..2u2Ln6i6m8en88ea8ma+r+raFo0F0itrf.1tF10y0t557788 YRSCHEM YRSCHEM RRSsRqqSuquaurarreeeAd) RRoSoqtuMareeaAndSjquar Summary eEros of Fit 00.011199577178801,) 203.61648720: MObRMesoeaeoarntnvoMaoftefiaRRoneenssSsppqoo(uonnarssreSeeuEmrrWoarts) 2.36682:: Lemon1: 1.87907:: Observatoirons(oArAnS"aulSymirsimWsogooitffasSVV)arareailmnasnccoe 1:> MemSawe Frain D1F11 Sum 8o2f922S260q.21u09a145r466e155s Mean Square oSlEes 22.0146 pF33r.R99oa21tv9i9E9o "16 17 esis 89.62951 111.64416 5.6018 006 Prob>F 0.0649 oECsoetimmsmatee PPSSLataurodraEasEmnmreeerottsorererrEEssttiti(mmaR0Rataatte2eislos PProrobom>blmtll LLoowwearrss9S5nt% O-I00.2S6T8I7E8S7 00S 1.218652 155-0.22 1.98 0069 0.8282 0.0649 0O0OTIT -2.8522 -0.007337 0.1057769 0.053358 U220pU.2p3p31e1p8r4e6869r525m0d75%s3 0.2188905 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbtyyiv33eMMOfrfoodrreIrnInsIspnpePecacttiiimooennrvaa.nndd3CC,ooppyyNoii.nnggC2aa-ss0CC4oo-nn6ff3iid0de9ennttiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00114499 3MAT0050552 3MA10050582 RSRaaunnpddooormmsSSoaarmmippgllmee w PPFHHSSSupermppvmBiBsyorYY/RRMSSgmCCtHHEEMM AAPpappgpeeenndd3ii1xx E& Page 31 E7 i " SiI' w- I 5 1D -- I , I' I` I' I , sn sone Is 20 2S 30 K 40 ow YRSDEW SMoSooudurercclee EEnMCroTordoorerull C Total TTIoenermrmcept YIRntSerCceHptEM YRSCHEM =LrW it PPFHSF dfppHm==00S .`.00S44LL6uii61A nn1m3ee3aa+m+rroa0FF0fiif0.trt01Fy1i883p355YYRp RSSCCHm HEEMM RSRRqSqquuuaiarrreeeAdj Summary of Fit 000..111499344600533)22 MRRReoSooaqotuntMaMroeefeaRaAenndsSSjpqqouunaasrreeeEErrtroorr 000a..44111444g3776775849 ObMseearnvaotfiRoensspoonrsSeum Wets) Sum Wgts) 15 0.418777 13 Observations (or OF AAnSanluyamsioslofoffySVVuasaarriamiansncscoe MemnSquae D1F16| Sum o002f.67S665q622u265a679r7262e333s Mea0noO.Ss6Uq6eu2aa6Tr72e2 "16 17 3a1sas6 2.7525963 3.4152686 0.172037 FF3R8Raa5tt1ii9oo PP30rr.0oo86bv57>o13FF9 0.0673 00EE4ss6tti1mm2sa8lt8ee 001832 0.0461288 0.018352 PaPraSarWamEmemetotreerr EEssttii(mrRaaattbeeoss 000S.t2O2d01IE33rS55r6Io63r t R00a1.t922i62o 0.009351 1.96 Pr0Poo8bb3>sl1lt7ll 000..080636117373 Lo0Lw4oe0wr69s6S50%% 000471 -0.406602 -0.001471 U0pU4pp9epre8r98d59s3%k 00NING 0.4988593 0.0381746 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggCa2a.ss0CC4oo-nn6ffi3idd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00115500 3MA10050583 3MA10050583 RSRauanpndedoromvmSsSaoamrmpgplmlete w PO SupiemBmnnyBsorYY/RRMSSgmCClHHEEMM w i0 n AAPppappgeeenndd3ii2xx EE Page 32 w :ww fo oon rnotAs sR D 2 15 20 7RSC0 25 30 J5 10 MSSoooduurercclee ErECMrroTrodoorerull C Total ITnTtoeerrmmcept YYIRnRtSeSCrcCHeHpEtEMM =YW ~i 'POAAppm = 0.L30iL8ni4en1eaa+rrF0Fii0tt5233 YRSCHEM RquPaOrAeAppm =0.SS3u0um8mm4a1mr+ya0oo.rff0FFy5ii2tt33 YRSCHE[M3 RRRRoSSqoqqutuuaaaMrrreeeeaAAnddSyjquareError: 000...11112722710038000-18788 `RMMOeboeasonaeotrnfvMoRaefteaiRsonenpsSsopq(onuonasrsSreeeuEmrrWoer s) 11.133.772007993::F8857 Observations(or Sum Wgts) ' 8 OF AAnaSnluymasiosliooSffyqVausararaiieansncscoe MeamSware 1D6F11 Sum2o5f55S.93q368u89a773r33e313s6 Mean5SlS.eaq32u82ga7rr3ese4 016 17 233511..393565131292636717 1.62275 F3FR3Raa1tii9oo PP03ro.0o3b8b1s7>9F2F9 0.0872 03EE0sst8iim4maa0lt4ee 000..003550228334220668554 PPaaSrrGaaEmmmaeottorerrEEssttii(mmFaaattteeess 000S.60t65d855E759r91r00o833r t R00a1.t484i727o 0.028718 1.82 PPr0ro6bo>4blt]6l 000..06084847262 LLoo-wwLee0rrS9s05s3%%6 0008S -1.082036 -0.008553 UUp1pppe6er9r9d85s0%3k 00..11.116339228008665553 MMaaddee AAvvaaiillaabbllee bbyy 33MVfofrorInIsnsppeeccttiioonn aanndd CCooppyyiinngg aass CCoonnffiiddeennttiiaall IInnffoorrmmaattiioonn:: SSuubbjjeecctt ttoo PPrrootteeccttiivvee OOrrddeerr IInn PPaallmmeervrv.. 33MM,, NNoo..CC22--0044--66330099 22881122..00115511 3MA10050584 3MA10050584 ProSaASSRuKaropsnecrdoreoovmminsSbySsoaadoAmrMpsngSllm,Ceet HEM PFOSAA ppm By YRSCHEM 0 D AAPppappegend3ne5idxi&xE Page 33 % 0C E C - i wd D 0) TI woaR AaE a 0 S 18 1S io 2S .0 3S 10 '0Sco SouSource Vode Model ErrError Tom C Total TomTerm nent Intercept VRschEm YRSCHEM ifm ii Lou Linear Fit POSAAdppm = 00059 0.0023 YRSCHEM PFOSAAdppm =0.00595+0.00023 YRSCHEM SamaofyFi Summary of Fit Rsquue cose RSquare 0.036903 RoqueAg om RSquare Adj -0.02:2 RootMenSq Err ones Root Mean Square Error 0.0129::7 NeanofRespone Sis Mean ofResponse 0.010556 erations on Sum Wet) Observations(or Sum Wgts) 8 Araya vararce Analysis of Variance or Bhim MemSuws Faso DF Sum of Squares Mean Square To Towown Doin oes 1 0.00010271 0.000103 cone owe er 16 0.00267372 0.000167 vo omen Ges 17 0.00277643 F Ratio 0.6146 Prob>F 0.4445 coins [ Sree -- Rat Pb Lowcssn Estimate ofissisy omess 0% Gam ooomes 0.0059463 Qos oo: O7 oss oocomws 0.0002285 Parameter Estimates Std Error I Ratio 0.006656 0.89 0.000291 0.78 Prob>Jtl 0.3849 0.4445 Lower 95% -0.008164 -0.000389 Upwos Upper 95% Goose 0.0200562 Gooosiy 0.0008463 Made Avalable by 3WforInspection and Copying as Confidential Information Made Available by 3M for Inspection and Copying as Confidential Information: SSuubbjjeecctt ttoo PPrrootteeccttiivvee OOrrddeerr IInn PPaallmmeervrv.. 33MM,, NNoo.. CC22--0044--66330099 2881122..00152 to0s0sas 3d MA1s 0050585 us `SSRRuuaappnneaddroroAmsmwSoS/aYramMiRmpggSplmmlCeiteHEM M570m B YRSCHEM = | wn : En . | g . -- Wl TS ua none wo APAappgppeeenndd3i4ixx & E Page 34 SoSMuoodurerclcee EnCEMroorodorerul C Total TYITIoRnentSermermrCcceeHpptEt M YRSCHEM =infi MSM5T7O0ppppmm== 00.0`0525SLL22uii92nn.9mee+aamr0r0Fo.aF.iif0t0rt00F3yi34411YYRRSSCCHHEEMM RRRSqSququauarrreec AJ Summary of Fit 000.000505009464686555 RRRMooSeoqoatutnMaMoreefcaRaAnendsSSjpqqouuanarsreeeBErororr 0000..111052500100555619185153 ObOMsbeesarevnravoatftiiRooennsssp((ooonrrsSSeuumm WWagstss)) 1 0.121594 13 oDFF| A AnaSluymrsoisiooSffi qVVuaaarrriisaeansnccee ood Sum of Squares MeMeaaonnoSSqmquuoaarsee FR1aR0a1tt1ii6o 11"661 03000..630328264522794971525708078587 00ess 0.022918 0.022655 PP01r.3ro02ba19>1s5F6 17 0.38539285 0.3295 oEEGsotSiimTmaamtt9oe PaPraSarwmaEemnetotererrEEsstti(immFaaattleeess SOtdOTEMrrOoEr t R0at&i7o PPOrro0boS>blBtlSl LLoo0wew1rr19985SS% ooouis 0.052294 0.0034129 000N93 0.077498 0.003393 100.67 1.01 0395 0.5095 0.3295 000378 -0.111995 -0.00378 U0pU2ppe1pr6o9sr5ss%2w 00I06062 0.2165826 0.0106062 MSMuaabddjeeecAAtvvataoiillPaarbbollteeecbbtyyiv33eMMOfrfoodrrerIInnIssnppeePccattiiioomnneaavrnn.dd3CCMoo,ppyyNoii.nngg2a-ass04CC-oonn6ff3ii0ddee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00115533 3MA10050586 3MA10050586 RSRauanpneddroovmsmoSSuaahmmippgllmeet w PPFFOOSSSAAupppepprmmvBiBysyoOYYMRRgSSmCtCHHEEMM 1 " | Eg0r10 -- <F~o03nD -- = :?D -- Lm . DID "ww sm"y u 0.00 -- I wown B85 0 5 1 - I - e P*71 1"r1 10 15 to 25 30 J5 to )RSIPHEA AAPppappgeeennd3dii5xx EE Page 35 MSSoooduuerrclcee ErECMrroTrodoorerull C Total ITnTeoerrmcmept YIYRnRtSeSCrcCHeHpEtEMM PPFFOOSSAAddfippppmm ==`-0L0.Si.L0nu0i3e3n3ma3e4r4amr+F+aoFi0if0trt..F00yi00t448833 YRSCHEM YRSCHEM RRRSqqquuuiiarrreeeAdj Summary of Fit 0oo.o1sn1s4s2ac124 MRRReoSoaoqotuntMaoMrefeeaRaAenndsSSpqjqouunaasrreeeEErrrroorr 000.00.0.61514448659820052662 ObOMsbeesarenrvvaoatftiiRooennsssp(o(oonrrsSSeuummWWagttss)) 1s 0,064622 18 OF A`naSAluynmsoiasloSolffqVyuVaaersrriieaiasnncscee MesnSquare FRatio 1D6F11 Sum000o.03f0454S555q858u303a838r808e232s Mea000n.00S0i2q4u5S2a8E1r3S9e9 PF22r.0Ro06ab6t3o3i11Fo n16 17 000..443005115335440113880553 0.022219 P00r.1o17b70>02F2 Esimalo PaPraSarGmaEmeemttreerrEEssttii(mmaAatsteeoss Probl LowerSS% 0-Q00E.0s0U4t3i83m2E3a68t77e S000t.0d0007E73r66r37o165r t -R00a14.t44i4s4o P0r0O.o6Ib6>66TI9t%24I L-0o00w10.e910r9629609058878%8 0.0048267 0.00336 1.44 0.1702 -0.002297 UpU0pp1ep2re9r93d51s%4k 00.000.111112999553001554 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbtyyiv33eMVOfrfoordreIrnInsIspnpeePcctatiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa-ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00115544 3MA10050587 3MA10050587 Ep--oEs--e,s Random Sample SupervisodMgmt M556 m B YRSCHEM Ee `ApAppepnednidxiExE Page 36 LTC)i0 .C D5 - . =. . 0 S 10 15 20 25 30 35 f0 ISCHff1 Ba, Term Intercept YRSCHEM =LW rt iESi EI aEtor seoEEoernSRrs--- g$huoomod: Source ET Model Team "im Error OcoEne meEEmEtEWOW rOWsE CTotal Linear Fit M556dfppm = -0.007 + 0.00261 YRSCHEM Summary of Fit RSquare 0.10532 RSquare Adj 0.049469 Root Mean Square Error 0.0843(2 Mean of Response 0.046 Observations(or Sum Wgts) 18 Analysis of Variance DF Sum of Squares Mean Square 1 0.01341369 0.013414 16 0.11387207 0.007117 17 0.12728576 F Ratio 1.8847 Prob>F 0.1887 Estimate -0.007018 0.002611 Parameter Estimates Std Error t Ratio 0.043437 -0.16 0.001902 1.37 Prob>lt, 0.8737 0.1887 Lower 95% -0.099101 -0.001421 ur Upper 95% WE 0.0850644 0.0066428 Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00115555 31VIA10050588 Randomsale Random Sample i orto Mill Operators prose by vaso PFOS ppm By YRSCHEM zEu w~.t~ TTT woYRSfNEI! AAHpopvReennSdgiixx & E Page 37 MSMuaabddjeeecAAtvvaaiilaParbboilteee cbbtyyiv33eMWOrfoodrreIrnInsIspnpeePcctatiimoonneaarvnn.dd3CC4oo.ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall Information: Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00115566 aMATO0S0589 31VIA10050589 RRMaainnlddOoopmmerSSaaatmmopprllsee ow PPFFHHSSMpilplpmpOmBpBeyyraYYtRRorSSsCCHHEEMM 1 4:, DJ: - | Ew | o i o CCCDTT LE 0 Ysri~EN APAppappgeeenndd3ii8xx EE Page 38 SMMuaabddjeeecAAtvvataoiillPaarbbollteeecbbtyyiv33eMVOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa-ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00115577 3MA10050590 3MA10050590 Random Sample Random Sample ik Operas Mill Operators TT POAA m B YRSCHEM 2 | 1 | C 00 v H " 2 ww ~BSCR[U Page 39 AAppppeennddiixx Page 39 EE MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbtyyiv33eMMOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CC,ooppyyNoii.nnggC2aa-ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00115588 3MAT0050591 3MA10050591 PrOSRARaAaMniinpldldoOoOompmmperBSSyaaaatmrVo.pyrRilsSoeCHEM | w PFOSAA.m B YRSCHEM i ||k |2 || ow TTT TT AA#piopheepned1i0nx & E Page 40 MSMuaabddjeeecAAtvvaoaillaParbbollteeebbciyyv33eMMOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo.ppyNyoii.nnggC2aa-ss0CC4oo-n6nf3ifd0ie9dnteinatl IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00159 3mAto0s0802 3MA10050592 M570RRaMaMpiipnnlmllddOOooppmmBeyerrSSaaYaattRmmoopSprrlslCseeHEM. w01? M570 ppm By YRSCHEM "010 0u0tB 2m " g00o t,,,i,.,.I.,.,I,...I..,r 8 wm 8 0 5 10 ?i wy Y?5CNJi AAPpappgpeeennd4d1iixx EE Page 41 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00116600 3MA10050593 31VIA10050593 RRaiannddOoopmmerSSaaatmmopprllsee PPFFOOSSAAMipll-oOmmp8eByraYtYoRRrSSs CCHHEEMM DwJno w E 2Em ' 1 w0 0o - - , $sS t8c naw 15 wa YE NEV AAPppappgeeennd4dii2xx EE Page 42 MMaaddee AAvvaaiillaabbllee bbyy 33MVffoorrInInssppeeccttiioonn aanndd CCooppyyiinngg aass CCoonnffiiddeennttiiaall IInnffoorrmmaattiioonn:: SSuubbjjeecctt ttoo PPrrootteeccttiivvee OOrrddeerr IInn PPaallmmeervrv.. 33MM,, NNoo..CC22--0044--66330099 22881122..00116611 331MVAI1A010005500559944 RRMaanniddOoopmmerSSaaatmmopprlslee MM5S5S6MppiplpmlmOBpByeyraYYtRRoSrSsCCHHEEMM 0.05 0.05 - 004 Ew E 0.0J w0.01 - w fs mow oB 8 G S w10n 15 2D 1S YRSiNfN Appendix APpapgeend4i3x EE Page 43 MMaaddee AAvvaaiillaabbllee bbyy 33MVffoorrInInssppeeccttiioonn aanndd CCooppyyiinngg aass CCoonnffiiddeennttiiaall IInnffoorrmmaattiioonn:: SSuubbjjeecctt ttoo PPrrootteeccttiivvee OOrrddeerr IInn PPaallmmeervrv.. 33MM,, NNoo..CC22--0044--66330099 22881122..00116622 33MMAA1100005500559955 APApappgpeeenndd1iixx F Page 1 AAppppeennddiixx FF SSccaaytettatesersrpplwloootrtskaaenndddirrneegcgrrheeessmssiiicooannlee(qquuYaaRttiiSooCnnHssEffooMrr)ffllfuuooorrraoolcclhhreeammniiccdaaollmss(s(nanamattpuulrreaall(lloo=gg tt1rr2aa6nn)ssaffnoorrdmmafatotriioovnn)o)bbyy years workeccduuirrnrreecnnhttejjmooibbcacclaa(tteeYoogRgriSieeCssH((cEchhMeemm)iifccoaarllaololppererraaanttdoororssmaasnnaddmpeenlnggeiin(n;r-s,=eerrf1/al2ab6b))) and for two SMMuaabddjeeecAAtvvataoiillPaarbbollteeecbbtyyiv33eMMOfrfodorreIrnIsnIspnpePecacttiiimooennrvaa.nndd3CC,ooppyNyoii.nnggC2aa-ss0CC4oo-nn6ff3iid0de9ennttiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00116633 3SMMAA1T10o00005s500559966 nersdairecnomoasn Random Sample In PFOS ppm By YRSCHEM AAppppeenndidxiFxF PPaaggee 22 Swit 1= o L. l: w{A h. . oa omTerm Ee Intercept eh YRSCHEM sue Source SiModel Error Cow C Total =L[W ii loFr=00oLo8wseyodnesiVapm Linear Fit sc In PFOSdfppm = -0.4008 + 0.02654 YRSCHEM Esq prt oss Summary of Fit RSquare RSRqSquuaarree AAddjj Ro aur re Root Mean Square Error Cont MMeeaannooffRReessppoonnssee or um We) Observations(or Sum Wgts) assis Analysis of Variance or MERELY DF Sum of Squares ' Sh 1 10.82508 mo mmn 124 120.82819 ew 125 131.65326 Comte S[ID--E Estimate Csuui dGanme 3in -0.400807 Parameter Estimates Std Error t Ratio 0.134748 -2.97 Gouna 000..000778442882222334 0-0.0.9.0806760105252S1 126 esame Mean Square EE 10.8251 om 0.9744 rrue F Ratio 11.1092 wr Prob>F ft0.0011 py Prob>JtJ Tooenl0.0035 oon Lower 95% cEoonm -0.667512 0.0265406 0.007963 3.33 0.0011 0.0107798 upp Upper 95% Th -0.134101 oan 0.0423014 Mace Avaiable oy 31or Inspection and Copyng a Carfcenta normaton Made Available by 3M for Inspection and Copying as Confidential Information: Subjects Poechie Order n Famer 30 No C2.04308 Subject to Protective Order In Palmer v. 3M, No.C2-04-6309 2881122..00116644 swatoososs? 3MA10050597 in PFEaRSnapndodomommBSySaamYmppRllSeeCHEM w In PFHS ppm By YRSCHEM RAN. andsinn i Ebawn F i "nt es 7 ce:oee at . am, r T I T I.I ,I,I, I , VSNL Ks oe 0 S 1C IS 2C n 3C 33 0 wa YRSCHEM PAAappgppeeendn3idxixF Page 3 SMoSooudurercclee EnEMCrooordoraerll C Total ITTnoerrcmmept YRSCHEM Intercept YRSCHEM =!W.1 IInnP PFHSF dfppmH==2S-42uS LL.0ii4mnn30ee3m2aa2rrf +a+FoFii0fr0ttF.0y05tp 5336666YYpRRSSCCm HHEEMM RSRRqSqquuuuuarrreecAdy Summary of Fit 000.22233306678839994 RRRMoSoeoqoatutnMaMreoefeaRaAenndsSSjpqqouunaasrreeeEErororr 011..A020737m022720s34393 ObOMsbeesarenvrvaoatftiiRooennsssp(o(oonrrsSeSuummWWagsm)) 126 -1.7152 126 OF AA naSlmysoil siooSffVqVaaury rieiaasnnccee MomSquao 1D4F1i Sum o1f4w4S4a2q.5zu26a5s3r6e4e4rs26 Mean Square aLsie 44.2564 12s124 125 186 81988 142.56346 186.81988 1.1497 sFFeRaatnoio 3PP<8r.ooo4obb9o>3F1F7 <.0001 2EG4sut0imm4mat8oe 0053664 -2.403248 0.053664 P0SPSatarudraEamEGmmroeorttororerrEEssttit(i-mmRalRaateatte@eiso2os 0008S 0.146366 0.008649 620 -16.42 6.20 PPrro<boo>bJ0tilJ <000I <.0001 <.0001 LLoo2wew6re090r55s% -020.%69S2W925 0.0365442 UU2ppp1pere19r35ds%s 0-02.710173853486 0.0707838 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbtyyiv33eMMOfrfoodrrerIInnIssnppeePccattiiioomnneaavrnn.dd3CCMoo,ppyyNoii.nngg2a-ass04CC-oonn6ff3ii0ddee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00116655 3MA10050598 3M A10050598 nfoaRnapndedoonmm SSaaTmmRpplAleeC EM in POAA ppm 8y YRSCHEM 2 PERRY J oE-- r -- _ a sEka r . JF SL : . Afoonpen Appendix F Page 4 wo RE 5 .E 0 1C S iE s isRE30NE35A)to ~scHa TomTerm nent Intercept Vestn YRSCHEM Sure Source Sie Model oy Error Shoal C Total =bwR Unot Linear Fit In POAApp =~ 30 + C0038 YRSCHEM In POAAppm =-0.2007+0.00738 YRSCHEM SamayaiFe Summary of Fit Rquue aooi:z RSquare RSRqSquuaarreeAAddjj 0.0042: 2 -00..000033:88 Root ean Square Er Lasers Root MeanSquareError 1.2568"7 Via of Resp alosts Mean ofResponse -0.10609 Onion or Sum We) Ye Observations(or Sum Wgts) 1.6 Anotavasatrca Analysis of variance oF BniSuane Memsawe Fra DF Sum of Squares Mean Square | She oles ose 1 0.83656 0.83656 1 wae sms par 124 195.88769 1.57974 1 19672625 vies 125 196.72425 F Ratio 0.5296 Prob>F 0.4682 Gunso [ Sut -- iP Pol Lowers Estimate Gaoess ous Lh coei osm -0.200686 done ooo om oss aoe 0.0073781 Parameter Estimates Std Error t Ratio 0.17157 -1.17 0.010139 0.73 Prob>lq 0.2444 0.4682 Lower 95% -0.540273 -0.01269 Upperosk Upper 95% owes 0.1389006 oomes 0.0274458 MSMuaabddjeeecAAtvvtaaoiilaParbbollteeecbbtyyiv33eMWOrfodorrIenrIsnIspnpeePcctatilioomnneaavrnn.dd3CCMoo,ppNyyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00166 aMATO0S05%9 3MA10050599 roJ lRandom Sample In PFOSAA ppm By YRSCHEM W wg LLL. eosAAppppeendnidxiFxF Page 5 wg TT I oeTenn fBoe, Intercept YRSCHEM =Lifa fi fEErrereEtrso,r eesn-- EseeErmorsssncsaaiomli:, oe Source EG Model CE TEE tam un Error EsnereeOEa ESEEEUEETD OmEp rwOeRebrEnu ed OueBeR CTotal Linear Fit In PFOSAAdfppm = -4.478 -- 0.02366 YRSCHEM Summary of Fit RSquare 0.03232 RSquare Adj 0.02451 Root Mean Square Error 1.44119:; Mean of Response 4.781: Observations(or Sum Wgts) 12(1 Analysis of Variance DF Sum of Squares Mean Square 1 8.60226 8.60226 124 257.55240 2.07704 125 266.15466 F Ratio 4.1416 Prob>F 0.0440 Estimate -4.477958 Parameter Estimates Std Error t Ratio 0.19673 -22.76 Prob>JtJ <.0001 Lower 95% -4.867344 Upper 95% -4.088572 -0.023659 0.011626 -2.04 0.0440 -0.04667 -0.000649 ie lt by Spon CogsCotta Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00116677 -- 3M A10050600 v[i--t.o Random Sample In M 570 ppm By YRSCHEM wpe 00: -- A] .* gFleey Jie oT -- T anh. -0,1 tot sn et -5 DD I ' t , { T t'i ' I ' I - HAFAEAC AE AP AFFAF D 5 10 15 N 25 30 35 10 wnYRS:HN sawn Linear Fit Insp = 2585 Se vRSCHEM In 570ppm = -2.353 -- 0.0126 YRSCHEM Emons Summary of Fit fro conser RSquare 0.01564 t Rote a Goorros RSquare Adj 0.00770? Rowan sau Br Vive: Root Mean Square Error 1.112421 Nemot hep pro] Mean ofResponse -2.5145 1 atom Wes) 5 Observations(orSum Wgts) 126 [ or AVrVsatSarRcn Wemamn Source So i Sm Men Model a a see Ge Error Sw ERE CTotal Analysis of Variance DF Sum of Squares Mean Square 1 2.43817 2.43817 124 153.44766 1.23748 125 155.88583 ZTomw [ SCre-- oomenr no Term Intercept sci Some owen ie YRSCHEM Parameter Estimates Estimate Std Error -2.353036 0.151851 -0.012596 0.008974 t Ratio -15.50 -1.40 FRaio F Ratio oe 1.9703 reer Prob>F peed 0.1629 Peo Prob>Itl al <.0001 aim 0.1629 Page's `ApAppepnednidxiFxF Page 6 MadoAvalabl by 31fo Inspection andCopyingas Genfidental Information SSMuuabbdjjeeeccAttvtatooilPParrbooltteeeccbttyiivv3eeMOOrrfoddreerrInIIsnnpePPcaatllimomeneravrvn..d33CM,o,pyNNoio.n.gCC22a--s00C44o--n66f3i3d00e99ntial Information: 28122..00116688 aMA100S0601 3M A10000550066001 1PERORaaSnnpdAdooommmSBSayammVgpRliSeeCHEM In PFOSA ppm By YRSCHEM 000 fo te wa a EE Ae -1a .00 met : -?.D0 Zo Ji or i EE AL s -m 1.00 t -- le -3 D0 EIwIeCIEAEAE D 5 16 15 20 2: 3D 35 Q `ISCH N AAPpappgpeeendn7idxixF Page 7 SoSMuoourdrcecele EmECMroorrdoearlt C Total TTIoenremmrept YRSCHEM Intercept YRSCHEM IInn PFFOOSSAAddifppppmm==SL-4u4Li..imn1n13ae3m6a6sr33aFoF---ifrtt0F0.yt00.11770011YYRRSSCCHHEEMM RsRRSqqquuuuarreeeAl) Summary of Fit 0oo.oo0o0sm9es8s4rs6 MRRReoSoaoqotnutaMoMrefeeaRanAendsSSjpqqouunaarsreeeEErrrroorr 0.0018t 1 L"aassuss 1.899215 MObesaernvoatfiRoensspoonrsSeum Wg) Wgts) 126 4.35445 126 Observations(or Sum ay ofVs rs Analysis of Variance oF "SumoiSoues MemSaun Frio DF Sum of Squares Mean Square 1 Sires es 1a 1 4.44768 4.44768 4 4726998 prey 124 447.26998 3.60702 ns sums 026% 125 451.71766 F Ratio 12331 Prob>F 0,2690 EoimaioPP|aarraamemStaaeerEEEsmsitemiamatteess(Fale Estimate oD0o6n -4.13633 Std Error ooossR 0.259252 t Ratio 1L58u3 -15.95 -0.017012 0.01532 -1.11 Lowers Lower 95% dew -4.649466 00uBe -0.047336 Upporssn Upper 95% D608 -3.623194 003 0.0133113 Made Available by 3MforInspection and Copying as Confidential Information Subject to Protective Order In Palmevr. 3, No. C2-04-6309 Made Available by 3M for Inspection and Copying as Confidential Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 Information: 2881122..00169 3MA10050602 3MA10050602 oJ le Random Sample 1n M556 ppm By YRSCHEM -1,00 - am 4% Che - 1 i aa : os AAppppeenndidxiFxF Page 8 I as -rE E00 y EM " Tas man -100 0 I , r .,.,.r.,,, i 10 1S 10 15 30 31J t0 YRSC4[it =Irej fi onTerm joaIntercept Em. YRSCHEM pSTmsMEpvoEoeonNarecoerTmEEs wssoeeononnmm2ms Source Linear Fit In M556dfppm = -3.6365 -0.01244 YRSCHEM Summary of Fit RSquare 0.010235 RSquare Adj 0.002254 Root Mean Square Error 1.362297 Mcan of Response -3,79603 Observations(or Sum Wgts) 125 Analysis of Variance DF Sum of Squares Mean Square omF Ratio Model 1 2.38002 2.38002 1.2824 Error C Total 124 125 cur Estimate fdmEs -3.636469 230.12586 232.50588 ---- Parameter Estimates EE Std Error t Ratio SEEEERR 0.18596 -19.56 1.85585 Prob>F ryProb>Itl eOwRw<.0001 0.2.596 wr Lower 95% mWmE -4.004539 -0.012445 0.010989 -1.13 0.2596 -0.034196 pe Upper 95% IumBe -3.268399 0.0093062 Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00117700 3M A10050603 Jupnt, Random Sample IEEChemical Operators In PFOS ppm By YRSCHEM Bs AAppppeenndidxiFxF Page 9 - wnTerm jrIntercept em. YRSCHEM brn R reopS s sPoe p LinearFit RE sce In PFOSdfppm =0.25621 +0.0124 YRSCHEM Summary of Fit o=e, cjios RSquare 0.038311 RSquare Adj 0.01694 EinAtenete da RootMeanSquareError 0.58910 sm Mean ofResponse 0.392725 ewe Observations(or Sum Wgts) 47 wmee or -- UIedEmm seneam roemn Source Model E ELEL Error nEw wo CTotal Analysis of Variance DF Sum of Squares Mean Square 1 0.622261 0.622261 45 15.620109 0.347114 46 16.242370 F Ratio 1.7927 Prob>F 0.1873 omctEssSs SSaG EpnTaEoD Es Momun omoens Estimate SER 0.2562063 Parameter Estimates Std Error t Ratio 0.133348 1.92 Prob>ftl 0.0610 Lower 95% -0.01237 0.0123988 0.00926 1.34 0.1873 -0.006253 rumnn Upper 95% 0.524783 0.0310501 Wate Aaa by Sr spin ans Copying a Corral maton SSMuuabbdjjeeeccAttvtatooilPParrbooltteeeccbttyiivv3eeMOOrrfoddreerrInIIsnnpePPcaatlilmomenreavrvn..d33CMMo,,pNyNoio.n.gCC22a--s00C44o--n66f3i3d00e99ntial Information: 2881122..00117711 - 3sMAo1u00s50604 ChReRamanindcdaoolmmSOSpaaommrpptlloeres IInn PFS pgm Chemical PFHS ppm By YRSCHEM Operators By YRSCHEM ws = " : } as, LE Ep - AAPppappgeeennd1dii0xx FF Page 10 BY ys 8 6 on oB 8S sn SMoSouodurercclee ErECMrroroodoerrul C Total Tom IYnITRenetSrrecmrCecHepptEt M YRSCHEM =a =:-Wfi In PFH=S1.LU7inn1esA7aa6r+rFitf 0t.049p1 YRpSCHmEM In PFHSdfppm Rsquure SummaofrFyit = -1.7176 + 0.0491 Summary of Fit YRSCHEM 0345573 RRSoRRqSSouqqtuuaaaMrrreeeeaAAnddSjjquareError 00O0..333033411580053:375i3 M`ROMeboeasoaentrnvMooaeftfaiRRoneenssSsppqooournrassSreeeuEmrroWrt) 0.640812 L1740 -1.17704 Observations(or Sum Wgts) 41 OF AAnSanluymasiosllooSffyqVVuaasrariieiaasnnscceo MewnSquare aDsF11 Sum o1f998S..4q777u558a888r000e005s88 Mean9o0S.4rq71u5t08a60ro18e "45 46 28236813 18.478805 28.236813 0.41064 2FR37Raa6t2ii9o 2PP3<rr.0oo70bv60>o21FF9 <,0001 7EE0sst7iimm6ast9se 0049092 -1.717649 0.0490992 PPaaSrrUaaEmmemetotererr EEssttii(mmRaatotelesos 000S.10t14d045E050r07r33o288r t-11R141a.8t58i14o4 0.010072 4.87 PP<rou0b0>bl0tsll <0 <.0001 <.0001 LoL2woe0wr0r99957S7%% OOB8IZ8 -2.00977 0.0288128 UlpUppeaprosr9o5ss%w 0063S -1.425527 0.0693855 MMaaddee AAvvaaiillaabbllee bbyy 33MVffoorr IInnssppeeccttiioonn aanndd CCooppyyiinngg aass CCoonnffiiddeennttiiaall IInnffoorrmmaattiioonn:: SSuubbjjeecctt ttoo PPrrootteecctiivvee OOrrddeerr IInn PPaallmmeervrv.. 33MM,, NNoo.. CC22-.0044--66330099 22881122..00117722 3MA10050605 3MA10050605 Craemmesn Random Sample re Chemical Operators In POAA ppm By YRSCHEM Le 2 : 200 " ErON - ee oh AAppppeendnidxiFxF Page 11 = a TTI 0 5 t0 15 20 25 30 3 woISCHIli -Term ae Intercept i: YRSCHEM soe Source ovModel JoError EE C Total =lraR oroAssamsf=o0isSi8t Linear Fit scm In POAAppm = 0.51048 + 0.01132 YRSCHEM Sn Summary of Fit Rs acer: RSquare 0.027722 a iii] RSquare Adj 0.00611( Eee Ere Fre Root Mean Square Error 0.63568E [ro on Mean ofResponse 0.635094 fs or-- A Observations(or Sum Wgts) 47 wg Analysis of Variance or TAIT swe Fre DF Sum of Squares Mean Square : Sq Medn Loe 1 0.518477 0.518477 | em Toe um 45 18.184368 0.404097 4d 46 18.702845 F Ratio 1.2831 Prob>F 0.2633 OE.--.-- . SI, Estimate oSefnn Ebemm V0M%E RMwE ghmaen mGomes 0.5104788 Parameter Estimates Std Error t Ratio 0.143878 3.55 Prob>JtJ 0.0009 -ower 95% 0.2206941 Upper 95% 0.8002634 0.0113177 0.009992 1.13 0.2633 -0.008806 0.0314418 Mado Avaialo by 3H fornspecan and Copying as Confident infomation Made Available by 3M for Inspection and Copying as Confidential Information: Rio Protech rer Palmer 340 Ho Co.04845 Subject to Protective Order In Palmer v. 3M, No.C2-04-6309 28122..00117733 A 3MA10050606 SeEI pEee, Random Sample Chemical Operators In PFOSAA.m B YRSCHEM wh +. . wrS .* fu -- -- Font `ApAppepnednidxiFxF Page 12 Taw .. . . : . =70 15 2D 25 30 jS 1RSNIL -Term Wm Intercept YRSCHEM =lreufi poLinear Fit = -- In PFOSAAdfppm =14.2679-0.01959 YRSCHEM Summary of Fit BEEeE eazy RSquare 0.0132f 1 Eeee RSquare Adj -0.00867 par Root Mean Square Error 1.603004 vmmeoo eCRaEeE Source OG TTIEEER Model Mean of Response Observations(or Sum Wgts) Analysis of Variance DF Sum of Squares 1 1.55397 -4.4836 47 ewnm Mean Square Em1.55397 F Ratio 0.6047 Error C Total 45 46 arnEstimate Sn -4.267867 115.63304 117.18701 J DEE Parameter Estimates Std Error t Ratio SEW 0.362816 -11.76 2.56962 Prob>F re Pob>ltl OW mR <.0001 0.4408 Lower 95% -4.9986I4 -0.019594 0.025I96 -0.78 0.4408 -0.07034 one Upper 95% omm -3.537119 0.0311532 Made Available by 3iM for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00117744 3MA10050607 J Random Sample grass Chemical Operators I WHEE, In M570 ppm By YRSCHEM a PRA i SS J or Appendix F Page 13 - 5 . 10 15 20 ti 10 i5 '~RSCHEi Term Intercept YRSCHEM =trea ft po Linear Fit wom Esc In 570ppm = -1.6206 -- 0.03729 YRSCHEM er RSRqSquuaarree. Summary of Fit 00..009922;:88 =, Some RSquare Adj 0.072006 EEN ee oi Root Mean Square Error 1.109871 Ei tet Mean ofResponse -2.031:2 2 2 Observations(or Sum Wgts) 47 reo J TEE Analysis of Variance Source DF Sum of Squares Mean Square F Ratio Model 1 5.628506 5.62851 4.5693 Error C Total 45 46 frmnm rEEennEeErRtoEEn Estimate 55.431655 61.060161 Parameter Estimates Std Error t Ratio 1.23181 Prob>F 0.0380 ee Prob>ItJ Lower 95% -1.620635 0.251203 -6.45 <.0001 -2.126582 -0.03729 0.017445 -2.14 0.0380 -0.072425 we Upper 95% -1.114688 -0.002154 Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00175 3M A10050608 [-- Random Sample Print Chemical Operators norman Baie In PFOSA ppm By YRSCHEM ws. wd . oo oT -- 2Ef,T% awd -~ : Te 1m + HAF Ar ArArArar D $ 1C 1S ?D 2S 30 35 wo~PSCHEII HE AAppppeendnidxiFxF Page 14 somTerm Tae Intercept sche YRSCHEM [ Source VoModel [Error Coa C Total =,m Ii InPFOSn3eS1n4At00d217pm= Linear Fit YRSCHEM In PFOSAdfppm = -3.2174 -- 0.03217 YRSCHEM ya Summary of Fit Rsque ao RSquare 0.026974 Epa Ad Soest RSquare Adj 0.0053:11 Ron enSureErr toon Root Mean Square Error 1.832508 NeiRego SS Mean ofResponse -3.5711)7 SoooSam Wg) a Observations(or Sum Wgts) 47 Reofsvaora Analysis of Variance or Moneta vemsams Fran DF Sum of Squares Mean Square f iri 1 4.18951 4.18951 4 sie wa ret 45 151.12876 3.35842 8 i5s3iaae Sm 46 155.31826 F Ratio 1.2475 Prob>F 0.2700 Ewe FCaahmoeteEsiialisn Pool Lowes Estimate ST Chew The Tam Toma -3.217438 Dunin comws au ome dom -0.032172 Parameter Estimates Std Error t Ratio 0.414782 -7.76 0.028805 -1.12 Prob>JtJ <.0001 0.2700 Lower 95% -4.052848 -0.090187 Upmrosn Upper 95% Twos -2.382028 oosees 0.0258433 MSMuaabddjeeecAAtvvataoillPaarbboltleebbcyiyv33eMOfrfoIodrnersInpIsenpcePtcatiiloomnneaarvnn.dd3CC,ooppyyNoii.nnggC2aa.ss0CC4oo.nn6ff3idd0ee9nnttiaall formation Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00117766 3MA0050609 3M A10050609 -- Random Sample chamenos: Chemical Operators ep rsa In M556 ppm By YRSCHEM AAppppeendnidxiFxF PPaaggee 1155 mL Nl te --_-- fof RI " i HAFAE AwroAn F AF AF ar: sous Source SrModel iError ErC Total TomTerm nmIntercept freYRSCHEM Inset = 2n7a7n0003YR1SC4H1 LinearFit EM In M556dfppm = -2.7767 -- 0.03141 YRSCHEM SimaFor Summary of Fit Rsque oosne RSquare 0.065942 KearAl Sons RSquare Adj 0.045185 Roo i Sau Er tin Root Mean Square Error 1-12121,5 VeoResor SES Mean ofResponse -3-122.113 Ofcom or sum Wes) 5 Observations(orSum Wgts) x.7 Ana otvatace Analysis of Variance op Upp Cla DF Sum of Squares Mean Square : Swe NEE ne 1 3.993849 3.99385 G5 sme wn ses 45 56.572602 1.25717 haus one 46 60.566451 F Ratio 3.1769 P rob>F 0.0814 Gmwe FSutrrstEnRasw pool Lowes Estimate Pir i RC -2.776667 Goin Oop Lm om oor -0.031412 Parameter Estimates Std Error t Ratio 0.253775 -10.94 0.017623 -1.78 Prob>lq <.0001 0.0814 Lower 95% -3.287794 -0.066907 Upersex Upper 95% vv -2.265539 ous 0.0040837 MSMuaabddjeeecAAtvvataoillPaarbboltleebbciyyv33eMOfrfoIodrnersInpIsenpcePtcatiiloomnneaarvnn.dd3CC,ooppyyNoii.nnggC2aa.ss0CC4oo.nn6ff3idd0ee9nnttiaall Ifnofromrmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00117777 aMAI0050610 3MA10050610 EE-- Random Sample EEnnggiinneeeerr/iLiaabb In PFOS ppm By YRSCHEM er Appendix F Page 16 Ee] 25 + = LrW R J =Linear Fit i5= En In PFOSdfppm = 1.4007+ 0.03146 YRSCHEM - Summary of Fit Bhte. uIm RSquare 0.170302 =E RSquare Adj 0.130793 =wZRFe E EiEEmf"EBTerEEE=wm5 mmmygommm Term Source Model Error C Total Root Mean Square Error Mean of Response Observations(or Sum Wgts) Analysis of Variance DF Sum of Squares 1 4.001539 21 19.495151 22 23.496691 Estimate Parameter Estimates Std Error t Ratio 0.963504 -0.93898 23 Mean Square 4.00154 0.92834 F Ratio 4.3104 Prob>F 0.0503 Prob>tq Lower 95% Upper 95% Intercept -1.40069 0.299699 -4.67 0.0001 -2.023942 -0.777437 YRSCHEM 0.0314649 0.015155 2.08 0.0503 -0.000052 0.0629819 Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00178 3MA10050611 In PFRHRaSaEEpnnnndoggdiiomonnmmeeBSeoySrraa/iYmmLaabRpp.blSleCeHEM w In PFHS v ppm By YRSCHEM i Pe . bEd IF EZuh7 : : 2 wd, P38 D 5 10 t5 ?mD os25 Ee) rkSCH l 88 30 35 AAPpappgpeeend1ni7dxiFxF Page 17 SMoSouodurercclee ECErMroTordoorerull C Total TTIneotremmrcept YRSCHEM Intercept YRSCHEM IInn PPFFHHSSddffppppmm==`-33LS.L.i1ui1n7n7em4e4aa55mrr++FoaFiif00trt..Fy00i48t227755 YYRRSSCCHHEEMM RRSsRqSququuuarrreeeAdj Summary of Fit 00..011.991225886.0166 RMoRReSooaqotutnaMMoreefcaaRAnendSsSjqpquouararsreeeE.Errrroorr 1120.22.51113375334010155 OOMbbesseaernrvvaoatftiiRooennsssp(o(oonrrsSSeuummWWegsts)) 3 -2.547: 1 : 3 OF AAnaSlnuymsioaslooSffiqVVauarairiieaasninccee MesnSwuare D2F1| Sum30of797.S313q848u66a300r07e787s7 Mean Square 7n386n08 7.38608 221 22 38300386 30.914308 38.300386 1.47211 FRSR0aa1tii3o Pe50r.0ow03b16s>70F3 0.0360 SEss1tii7mma5tue 00427483 -3.174495 0.0427483 PaPSradarEmammeeottorerr EEssttiRinmaaaltooess 0O0S.tO3dI37E07r3S0r9oS9r t Ratio B2A2I -8.41 0.019085 2.24 PP<roo0b>lW11ll11 000 <.0001 0.0360 LLo3oww9es5r 9993554%% OO030G0I -3.959334 0.0030601 UU2ppp3pe8re99r65a5%7s 0.084366 -2.389657 0.0824366 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00117799 3MA10050612 3MA10050612 RRaannddoommSSaammppllee Ergneoanh EngineedLab 0= In POApmB:y YRSCHEM In POAA ppm By YRSCHEM a"n E . : y go Sand | Eann d{7 am . a5 3 nwn o Es Page 16 AAppppeenndidxiFxF Page 1B NESmoaSMeooududrcreecele CEroroar l C Total IYTInTRneotreSerrrenrCceHtptEM YRSCHEM =Lrea 4 1In POnAApPpm==O1S-81u.2LL8im3i2An35nem5a+ef raa0oFA0rrif0t-F1y0o71.4p7242YYpRRSSCCmHHEEMM RRsRRRoSSoqqqqtuuuuMaarerreeeeaAnAfdSjq)uareSrumomrary of Fit 00ooL..o000oui04mm27s3370st502s52 ORMMboeeeoaartnnvMoaofesfaoRRnneesssSppq(oouonnarssrSeeeuEmrroWris) 1.079651 "se4s -1.56794 or o"SahoosifSVmiaannscee Observations(or Sum Wgts) Analysis of Variance 23 Memsweo Frm DF |1 2221 Sum225o2wf4711S.r.20q42m6u720sa861315re776e81717s Mean Square 267 1.22617 Vises 1.16565 F Ratio ost 1.0519 p03a16r7 Prob>F 22 25.704738 0.3167 dEEsestimsmeaetee PoaSSPtaaddrwmEaEmarmnertotrrearEEsxti(titmPRsaaaottelseioos PP<rooobb>mlJltlJ LooLwoeworr9om5s%k ooaie oOisR -1.823526 0 0.335826 103-5.43 Ode <.0001 Gorn -2.521909 .0174I76 0.016982 1.03 0.3167 -0.017899 Upporss Upper 95% rise -1.125143 oosi 0.0527339 MSMuaabddjeeecAAtvvoaaillaParbbollteeebcbiyyv33eMMOfrfodorrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo.ppyyNoii.nnggC2aa-ss0CC4oo-nn6f3ifd0ie9dnetinatl IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00118800 3MA10050613 3M A10050613 nProsRRakaEEnAnnrdgdoisoomnommeeneesSrrBaay/immLaapRpnbllSeecHEM EeIn PFOSAA ppm By YRSCHEM -2.50 -J DD - -a3Da--d nde ------------------------------------------------------------ Eo ~~ FFFLaaTilenndTl-- in n-- na | 0 S 10 'S ?0 75 3C 35 wour5CH:d Page 19 AAppppeendnidxiFxF Page 19 ESVnoSMoueoourdirreccrlee Com Error C Total TomTerm mere Intercept YRSCHEM YRSCHEM =JW i InFFOS=U5Ane1a5rAF-it00d036Ipm Linear Fit 7 YRSCHEM In PFOSAAdfppm = -5.15 -- 0.00367 YRSCHEM SennaFa Summary of Fit Rsqure omizie RSquare 0.0012_4 RousAd "ois RSquare Adj -0.046.3 Root ianSquare aor Tiss Root Mean Square Error 1.44825 Meanof Response San Mean ofResponse -5.2038 Oervton orSum Wg) EH Observations(or Sum Wgts) : 3 AaofVas rarcn Analysis of Variance or "BhotSumm MemSwme Frac DF Sum of Squares Mean Square i rm Ds oo 1 0.054411 0.05441 a 0is995 m6 pont 21 44.045995 2.09743 2 "lois fr 22 44.100406 F Ratio 0.0259 Prob>F 0.8736 Emus PSaurfarmoortr SaiPnatlese Publ Lowers Estimate Sie Om le <n ames -5.149964 Sones oom ols osms oosion -0.003669 Parameter Estimates Std Error t Ratio 0.450479 -11.43 0.02278 -0.16 Prob>IIJ <.0001 0.8736 Lower 95% -6.086779 -0.051043 Upporssw Upper 95% amie -4.213149 oowmu 0.0437044 MSMuaabddjeeecAAtvvaoaiilaParbbollteeecbbtyyiv33eMMOfrfoodrrerIInnIssnppeePccattiiioomnneaavrnn.dd3CC.ooppyyNoii.nnggC2aa-ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 281122..00118811 MAT00S0614 3MA10050614 LnMSTRR0aapEEnpnnndgmdgoiionmnmeeSeBySerara/mYimLpaaRplbblSeeC.HEM Ln M570ppm By YRSCHEM -2r.00e-d : PAAappgppeeen2dn0idxiFxF Page 20 ww sn H5 EE ER 0 5 10 ed15 YFSCH[V 2) 25 30 3: LM It TTInoetremmrcept YIYRnRtSeSrCcCHeHpEtEMM SMoSouodurercclee ErCEMmroTrodoorerult C Total In $70pprm = 3.L0i5Ln9ie8naera+rF0Fi.it0t0297 YRSCHEM RquIrn 5e70ppm =-3S`.u0Sm5um98am+rmy0oa.off0r0FFyi2it97 YRSCHEM0002026 RRRRoSSqoqqutuuuMaarrreeeeaAAnddSjjquareError 00.9-0010.0.5020640435527555 MObRMesoeaeoartnnvMoaoeftfRiaRoenenssSsppqoo(unonarssreSeeuErmroWrs) 0.915631 ECTEHl -3.01612 Observations(or Sum Wgts) 23 OF A`naSAluynmsoiasloSoiffqVyuVaaarsrriiaeiansncscee MeanSgure D2F11 Sum1o7f00.S.06q030u356a572r741e479s7 Mea000n.0S083q3u57a734r47e7 221 22 1711776..46641016992661695 0.838391 F0F0RRa4at2ii6oo PP00rr.8oo03bb48>o21FF6 0.8384 3E0Ess5ti9imm7aa6lt2ee 000297 -3.059762 0.0029739 PaPraSarWamEmemetotererrEEssttiimm(aaRttaeeisso 000S.t202d0184E448r84r00o299r -t01R070a.t247i14o 0.014402 0.21 Pr<Por0bo0>bI0otlIlI OSE <.0001 0.8384 L3oLwo6ew5re0r995551%% 00297 -3.652051 -0.026977 UpU2ppe4pr6o9r05907/%9 0039252 -2.467473 0.0329252 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbtyyiv33eMVOfrfoordreIrnInsIspnpeePcctatiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggCa2a-ss0CC4oo-nn6ffi3idd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00118822 3MA10050615 31VIA10050615 J Random Sample ronees Engineer/Lab In PFOSA ..m B YRSCHEM ant . FE -10) - Da ov AAppppeendnidxiFxF Page 21 -8 C0 0 5 r[ i 5 13 lS 2C 15CR61 I iI I i ZS 3C 3S rrTerm Ee, intercept YRSCHEM =Liter fi rossF po Linear Fit SE ons sr In PFOSAdfppm = -5.5202+ 0.00865 YRSCHEM RA Summary of Fit on . RSquare 0.004124 fEe ne pr RSquare Adj -0.0433 i Root Mean Square Error 1.864648 i 53 Mean ofResponse -5.39325 LEE 3 Observations(or Sum Wgts) 23 groor JuEE er oo Source TEE wee ou Model EZ Tam tam um Error Be, 4 gm = CTotal Analysis of Variance DF Sum of Squares Mean Square 1 0.302390 0.30239 21 73.015154 3.47691 22 73.317544 F Ratio 0.0870 Prob>F 0.7710 I ---- . Estimate -5.520173 SEE OTE OWE ODE IE 0.0086496 Parameter Estimates Std Error t Ratio 0.58 -9.52 0.02933 0.29 Prob>JtJ <.0001 0.7710 Lower 95% -6.726339 -0.052345 Upper 95% 4.314007 0.0696438 Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00118833 3MA10050616 1nsRsRa8aEEnnnpdgdoniomonmgmeSBeySraea/mvLmnpaApbllSeeCHEM Ts In M556..m -B YRSCHEM 2 i a FL Fal Sannl dT ` cam . "5 I' I' +t' I' I' I' Tins as ss 5 !D is i0 IS 30 33 wen YRS:H11 Page22 AAppppeendnidxiFxF Page 22 SMSoooduuercale EECMrrorrdrooeralt C Total IYnITTRneeotSrremmrCccepHpttEM YRSCHEM =.reail I1n Mn55M6dSfppSm ==64S-7U4pu.Ln9i7me9nr9ae31ma1rra-oF+Fifrt00tF..y00t0997733YYRRSSCCHHEEMM RSRRqSsququuuaurreeeAdj Summary of Fit 0c0.00o1330s275 RRRMMOooSbeeoqoeaatutrnnaMvoMroaefefeiaRaoRAennnedsSsSjppqqoouonnarssreSeeEuErmrrrooWrrs) -0.03397 ri 1.174741 Lisso5n -4.65037 Observations(or Sum Wgts) 23 DoFr| AAnS"aluSnymmsioosiofs0oSSff3aqv8Vuyua2aarr4mria6eeas2nsnsccoe MMeeamnDSSqwaueasree FF0Raaatmoio 222111 2500853..89368808023234666222 Er 0.38246 1.38002 0.2771 Porsobo>nF 22 29.362824 0.6041 LEEs0stim0maa1tee 0SPPtaSadru3raEEamrmsermootarrear EEssttitiMDmmRaamAattteee?isso PP<roub>b0JtlJ LLSooweewr9eo5s% O0OTITS -4.793115 0.0097276 007s 0.365404 0.018478 05 -13.12 0.53 0d <.0001 0.6041 00899 -5.553008 -0.028699 UUappppoearrm9o5sm%w 0ouEIss -4.033222 0.0481544 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbtyyiv33eMMOfrfoodrreIrnInsIspnpeePcctatiiloomnneaavrnn.dd3CC,ooppyyNoii.nnggC2aa-ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00118844 3MA10050817 3MA10050617 AApppappgeeenndd1iixx GG Page 1 AAppppeennddiixx GG chemicaSSlcc(aaYtttReerSrppClloHottEssMaa)nnddfrroeerggarrleelsscsshiieoonnmieecqqauulaattpiiaoornntsiscffiooprranfftllsuuo(onrro=occh1he8em7mi)cmfaiolcrsacblbu.sr;ryyeeenaatrrssjowwboocrrakkteeeddgoiirnnies (cell ooppceehrreaattmooirrscs,,acclhh(eeYmmiiRccSaaCllHooEppMeerr)aafttooorrrsas,l,leecnnhggeiinmneieecer/a/lllaapbba,,rtmmiaaciiinnptatenetnnsaa(nnnccee=,,1mmii8ll7ll)oofppoeerrrcaauttroorrressnatannjddobssuucppateeerrgvvoiirssiooerrsi/(mmcggemlmtlt)) MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00118855 3MA10050618 3MA10050618 presses All Participants rods hen . PFOS ppm By YRSCHEM fo el AAppppeendnidxiGxG Page 2 a Eten pyle ES wo 10 15 ,C 25 3D 35 0 1R$O N TomTerm Te Intercept fe YRSCHEM dooce Source SoModel Foo w Error C Total ors Linear Fit osm 0st obs YRSCHEM PFOSdfppm =0.87788+0.04433YRSCHEM pi Summary of Fit sq amen RSquare 0.109673 fowagh sioas RSquare Adj 0.10486 Roc Er fads Root Mean Square Error 1.424349 Venere an Mean ofResponse 1.424443 frotlon or 0] Observations(or Sum Wgts) 187 osetia Analysis of Variance orToSRTRNEImEER wemsnen roa OF Sum of Squares Mean Square En ah 1 46.23325 46.2333 wes Gomer 185 375.32259 2.0288 we Sn 186 421.55584 F Ratio 22.7888 Prob>F <.0001 corse sSasHEaEmDs eon uns Estimate oChim Sohewm s4em malm mCoomso 0.8778797 Parameter Estimates Std Error t Ratio 0.154783 5.67 Prob>ltl <.0001 Lower 95% 0.5725098 0.0443319 0.009287 4.77 <.0001 0.0260105 tens Upper 950k mes 1.1832495 own 0.0626534 Mace Avaiable oy 31or Inspection and Copyng a Carfcenta normaton Made Available by 3M for Inspection and Copying as Confidential Information: Subjects Poechie Order n Famer 30 No C2.04308 Subject to Protective Order In Palmer v. 3M, No.C2-04-6309 2881122..00118866 swtons0619 3M A10050619 rr. All Participants = PioPFHS ppm By YRSCHEM AAppppeendnidxiGxG PPaaggee 33 Ew c Do.e El. ih. is Crwo T 1RSC0 _ .rm Frs01i5o10 pS001o394vmRSC= Linear Fit HEM PFHSdfppm = 0.12463 + 0.01594 YRSCHEM a Summary of Fit Rsqure vain RSquare 0.210847 Roneaa Seon RSquare Adj 0.206581 fre fod Root Mean Square Error 0.347846 [rSotiosa Wes) Sni Mean ofResponse 0.321211 Observations(or Sum Wgts) soe or -- "AUE-- NS" Source So : Sn Model i Ww pwas Error mW Ee CTotal Analysis of Variance DF Sum of Squares 1 5.980711 185 22.384463 186 28.365174 Tn Conse sEuanEniTsH Term Ten oie SoEm WR Intercept in Sin ome Tm YRSCHEM Estimate 0.1246314 0.0159447 Parameter Estimates Std Error t Ratio 0.0378 3.30 0.002268 7.03 187 sume Mean Square SE 5.98071 omw 0.12100 rae F Ratio be 49.4286 ber Prob>F a <.0001 pont Prob>JtJ Tm 0.0012 She <.0001 mos Lower 95% Swen J.0500558 owes ).0114703 upaosn Upper 95% Chen 0.1992071 aon 0.020419 WSMaaiddboeelAAvvalaoillPaarbllooetbbeyyc3hMOfrfoodrrerIInnssppeePccattiiloomnneaavrnnddWCChooppyyNoii.nngg2aa.ss0CC4oo-nn6ff3iidd0ee5nnttiiaall informa Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00118877 amaroosoez 3MA10050620 PORAnAalpl poPaamrBrtsiyccipVpaaRnnStssCHEM r} POAA ppm By F YRSCHEM a - su sT0mdLfu T yr e ""f=orne. g Tin wEoAE x Ee AAPpappgpeeennd4idxi6xG Page 4 ESMSMroooouododreecolle ECroroart C Total IYTInTRneotSeremmrCrceHpttEM YRSCHEM Lau ri POAAgp POAAppm = = 11S.220u0Ln88im00ne59ema+srao00Fe.ifr0t01F1y7i78888 YRSCHEM YRSCHEM RRsSRqqSquuurarreeeAdj Summary of Fit 0r0.00e12497m6191 RMOoRRMehSoeosaqoaetutnrnaMvMoroeaefefiaaRRAonneednSssSjsqppquoo(uaonnarrssreeeSeEoErrmrrWooirrgs) 0.019439 1266529 1.266529 Las7t 1.42851 or A"SnimaootivSaiqrieassnce Observations(orSum Wgts) Analysis of Variance 187 MemSwew halo 1D85F1i 11865 Sum239o20f694S6777q..255u75717a5169r79666e0066s060 Mean Square hs 7.51900 100 1.60410 F Ratio ses 4.6874 Poowoe Prob>F 186 304.27666 0.0317 LEEsButimmBsatee OSPptaSaLdruraEaEEmrmmeroRaotrererrEEssitti(mmRFtBaaaett7leis8eos PPr<roobo>nbltlll LLooowwesrr9ss5S%h QOmws 1.2080941 0.o1o3o7m6s3s3 2;8.78 2.17 OOM <.0001 0.0317 NOSES 0.9365598 0.0015867 0.017878 0.008258 U1LpU.0pp4a0e7pMrm9eI96reG25sS08s/sS46 0.0341694 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbtyyiv33eMMOfrfoodrreIrnInsIspnpePecactitiimooennr ava.nndd3CC,ooppyyNoii.nnggC2aa-ss0CC4oo-nn6ff3iid0de9ennttiaall Information Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00118888 3MA10050621 3MA10050621 wrancouns All Participants PIpic PFOSAA --m B YRSCHEM =t:0 w r{Ean 010 " T foa e Sr J00 10 1s 20 25 30 J I woIFS:-HEW og AAppppeendnidxiGxG Page 5 TomTerm Zn Intercept fs YRSCHEM --" Source Sr Model osError Tha C Total pure PP FOSF AAdO fppS m==0A 0..L00i33nA 44e66a3r3-Fd --i0t0..00f 0000884p 4 YYRRp SSCCHHm EEMM pairs Summary of Fit Re ooszsos RSquare 0.052504 Koa Ag oie RSquare Adj 0.047383 rie -- psi Root Mean Square Error 0.04017 NeufRegone aoa Mean ofResponse 0.024293 Onan Sam We) i Observations(or Sum Wgts) 187 Anat Vatrce Analysis of Variance or CUES Lo DF Sum of Squares Mean Square To They Oona 1 0.01654217 0.016542 ww opume omen has 185 0.29852064 0.001614 dw een oo 186 0.31506281 F Ratio 10.2516 Prob>F 0.0016 rms nSamr SATS pu lowes Estimate obs omg rm wo Sowome 0.0346317 "owes Goais : ome omis -0.000839 Parameter Estimates Std Error t Ratio 0.004365 7.93 0.000262 -3.20 Prob>JtJ <_0001 0.0016 Lower 95% ).0260196 -0.001355 Uperese Upper 95% ohn 0.0432438 owen -0.000322 MSMuaatddeoecAAtvvataoillPaaobbtlleecbbhyyv33eM1OffroodrIenInsnsppeePcctatiiloomnneaarvnn.ddWCChooppyyNoii.nngg62aa.ss0CG4oe.nn6ff3iid0de5ennttiaall Information Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00118899 amatoosoezz 3MA10050622 M57A0AtlplpmpPaarstBysicciVppAaaSnntCssHEM. M570 -pm. B YRSCHEM " APAappgppeeenndd6iixx G G Page 6 2 w ton H ESETEE SE] ES D 5 1D wo 15 2D AR CHEF 25 30 3: f MSooSoudurercclee EnECMroTordoorerull C Total ITTneoerrmmcept YRSCHEM Intercept YRSCHEM MMS57700ppppmm ==00.`.11S88L58nui22nemea---amr0r0.oa.FF0i0ifrtt00F22yi44t77YYRRSSCCHHEEMM RRRSqqquuuauarrreee Adj Summary of Fit 000.00008099144499377 MRRReoSooaqotutnaMMoreefeaRaAnendsSSjqpquouaanrrseeeEErrrroorr 0000..1202580873431899405534773 OMbseearnvaotfiRoenssp(oonrsSeum Wets) 1 0.157804 Observations(or Sum Wgts) 187 OF AAnaSnluymasiosllooSffyqVVauasrwriieiaasnnsccee MeanSaure 1D5511 Sum o1f004S..9q111u466a338r0042e215s5 Mea0O0n.0S1r8q40u3g6a03r2s2e5 186185 186 15059866 14.916841 15.059866 0.080632 FF1RRa7attimioo Pro1r.o1o78bb7i>3osF8 0.1845 0EE1ss8ttii8mm2aa0tt4ee 000466 0.188204 -0.002466 PPaaSrraWamEmeemttreerrEEssttii(mmRaaattleeoss 000S.t000d300E0r888r51So7r t R166a.3t11i300o 0.001851 -1.33 P<rPor0bo0>blo0tflll OIBS <.0001 0.1845 L0oLwo1ewr7e9r5s%% 00061 0.1273257 -0.006118 U0pU2ppep9re0r9o85S2%% 000IEeS 0.2490822 0.0011868 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattliioomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00119900 3MA10050623 3MA10050623 PFOSAAAapll ppPaamrrtiBiyccoipuVanAnttSssCHEM Im PFOSA ppm By YRSCHEM C ;C APAppappgeeenndd7iixx G G Page 7 0 5C -- Si 01|.0)NTES 5 n0 onw15oo2n)on25 ASCHID 1h0 oJ5 w+O SMooSuodurerclcee EEMCmroTrdoroerull C Total YITnITRoneetSrrmemrcCceeHppEt M YRSCHEM =~t1 P~FOSPAdfRppmO==`00S..S00LL55uii33nAn9m9e1aa1msr---aFdFoi0if0rtt0.Fy00ft0002222pYYRRSpSCCHHmEEMM RRsRSSqqquuuarrreeeAd) Summary of Fit 000.0000000045181656 MORebRRMosSoeaoeqoartnutnvMaMoaroetefefiaaRRoAnneendsSsSsjpqpqou(ouonanarsrsreeeSeuEEmrrroWors) -0.00489 oma 0.107249 005126376 0.051246 Observations(or Sum Wgts) 187 DorF1 AAnS"aluSnymusimosOafooooSfifoqVlVSuiaoauardgrmaasesnsnssccae MMeea0annS0Sqau0uaw%ree FR0a0Rt9ati5ioso 1181885651 0.0010985 2203631 2.1279346 00lSR 0.001098 0.011502 P00rP.7ro05ob9w7>5o6F5F 186 2.1290331 0.7576 0EE0setiiHnmaa0tse P0PSataSrdr0adaEmEmreSermttorererrEEssttitiRmmRa4aaattt6eoeis3os P<b0 Prob>JtJ LolwDoe0wrBr9l95eSS%% 0D.o05o3z90i9s9 00.00011066595 043.613 <0.7005071 00019 ).0309165 -0.000216 0.000699 -0.31 0.7576 -0.001596 UpU0ppep0remr9es5sn%h OOS 0.0769033 0.0011635 SMMuaabddjeeecAAtvvataoiillPaarbbollteeecbbiyyiv33eMVOrffdoorreIrnIsnIspnpeePcctatilioomnneaarvnn.dd3CCMoo,ppyNyoii.nnggC 2aa.ss0CC4oo-nn6ff3iidd0ee8nnttiiaall Information Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00119911 3MA10050624 3MA10050624 S56AAploalmpPaarrtBiiycciYppRaannStsCs HEM 0m5I m M556 ppm By YRSCHEM i gm 20" J - BT rPee 0Te5 uID nw15ou1nD s15 wn 30 35 + YRSCHN PAAapogppeeendnidxi6xG Page 8 TomTerm nce Intercept YRSCHEM YRSCHEM Soo Source VioModel Eror Error Clout C Total ='I= It J MSS=0t05L48do1a0Fn0ii005z3 pm Linear Fit YRSCHEM M556dfppm =0.05481 -0.00053 YRSCHE-M Summaorfy Summary of Fit Rsquure oooniss RSquare 0.007159 RSqureAd amine RSquarc Adj 0.001763 RootMeanSquareEra 0072s Root Mean Square Error 0.07024 MeanofResponse oon Mean ofResponse 0.048273 Observations (or SumWat) is Observations(or Sum Wgts) 186 AnsofVayrarsca Analysis of Variance or "Simos Memswwe Fro DF Sum of Squares Mean Square 1 Dens Oomsi 1oaen 1 0.00654604 0.006546 18 0m ma Puet 184 0.90780250 0.004934 i ose 0230 185 0.91434853 F Ratio 1.3268 Prob>F 0.2509 Conus PSaurEarmeotrer SetMmaatkeso PobI lowers Estimate ousmies OOMeT 1S <001 OG 0.0548148 Dosn omnes lls 02% Omid -0.000528 Parameter Estimates Std Error t Ratio 0.007667 7.15 0.000459 -1.15 Prob>ltl <.0001 0.2509 lower 95% 0.039688 -0.001434 Usperss Upper 95% Obgwels 0.0699416 ooeer 0.0003767 MSMuaabddjeeecAAtvvaoaillaParbbollteeebbcyiyv33eMMOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo.ppyyNoii.nnggC2aa-ss0CC4oo-nn6f3ifd0ie9dnteinatl IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00119922 3MAT00S0625 3MA10050625 -- res All Participants Cell Operators PFOS ppm By YRSCHEM tsAAppppeendnidxiGxG Page 9 : _ En . - w 5= Lrw [I B}ee, aEgeTn--oBO owra o.aoE.rTtTEeeT EEeEEEo eyvea0a-sm croomn Inert Term Intercept SBE ET SE YRSCHEM Source Model Error C Total Linear Fit PFOSdfppm =0.41242+0.09869 YRSCHEM Summary of Fit RSquarc RSquare Adj Root Mean Square Error Mean ofResponse Observations(or Sum Wgts) 0.2341f 0.12477 1.814422.26555, S Analysis of Variance 1F Sum of Squares Mean Square 1 7.0469I3 7.04691 7 23.044960 3.29214 8 30.091872 F Ratio 2.1405 Prob>F 0.1869 odin Estimate 0.4124178 0.0986878 Leis 03 Parameter Estimates Std Error t Ratio 1.4036I2 0.29 0.067453 1.46 om Prob>Jt+ 0.7774 0.1869 owes L over 95% -2.906623 -0.060815 oeuonThem Upper 95% 3.7314586 0.2581907 Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00193 3MA10050626 pir All Participants efre m Cell Operators PFHS ..m B YRSCHEM AAppppeenndidxiGxG PPaaggee 1100 2 = 0".w3C . , - ,1 , T . D 5 13 15 20 25 3J MUD wrSource izModel yoError amTerm on Intercept 2 YRSCHEM C Total Lrw Ft rt Linear Fit sion 005 Bs vas PFHSdfppm =-0.0673+0.05293 YRSCHEM sige a osmon Summaryof Fit RSquare RRSSqquuaarreeAAddjj EE etn Root Mean Square Error RmTm ven Mean ofResponse ofxeio; 0.573083 00..551122009955 0.464481 0.926611 Observations(or Sum Wgts) opictvases Analysis of Variance on SEE we om DF Sum of Squares pt ooaFmmER en 3 1 2.0272533 ammo one 7 1.5101985 1 be fr 8 3.5374519 sy mLarEsnEtn omy wr Estimate oe EE EW mm -0.067334 GE mel an ome Shen 0.052932 Parameter Estimates Std Error t Ratio 0.359316 -0.19 0.017268 3.07 9 Mean Square 2.02725 0.21574 F Ratio 9.3966 Prob>F 0.0182 Prob>ltl 0.8567 0.0182 Lower 95% -0.916987 0.0121003 ww Upper 95% mE 0.7823194 fhm 0.0937637 MT ite sR itiotyBStoA r apRtaEn CopyingT5 GSonna oman Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00119944 San 3MA10050627 POACAACloeillptlPpaaoCOmbrrpptiyeoirccriaTpaptaaaRonrnrEtssssCHEM w POAA ppm By YRSCHEM J f_ on -- 22 . - |{ I [ " TT 0 S w . aa a 1D 1S 2D 25 3D 35 wo 1RS:HEY =LEM Q PPOOAAAAppppTMm == 00.S125Uu57L7oi5m9no44emaa++rrao00FF.ifr0tt0F68y22r6688YYRRSSCCHHEEMM RsRRSqSqquuuarrreee Ad) RoRSoqtuMarieeAndSjq u a re Summary ror of Fit 0oo.0s04.ms323o34s141ui813s93 MRMOeobeoeantrnvMooaeffiRaRoenesnsSpspqoo(unonarssreSeeoEmrroWrs) 0.980819 1810356S 1.810556 Observations(or Sum Wgts) 9 SNoSooudurrecse DorF1 AaAnSsa"luSymmsioosrfosoSSffqeavVuauaearrmirienaeasnnsccee MMeeamnSSSquuemaree EvECMrorerdooreralt 72'1 4.946633 fpirvveir 6.734042 06201 4.94663 0.96201 C Total 8 11.680674 ITTneoerrmmept PaPasorECmasamtoeseittmmeaeeterseEEssttiamtaOSSteiesrdsHEmrrEeor ttRh0aat3io4o YIRntSerCceHptEM oes 0.257943 0.0826835 oes 0.758747 0.036463 2710.34 2.27 YRSCHEM Fs F Ratio sim 5.1420 Probf Prob>F 0577 0.0577 Prosi Prob>1q 0709 0.7439 osm 0.0577 AAPppappgeeenndd1i1ixx G Page 11 MSMuaabddjeeecAAtvvaatoiillPaarbbollteee cbbtyyiv33eMMOfrfoodrreIrnInsIspnpeePcctatiiloomnneaavrnn.dd3CC,ooppyyNoii.nnggC2aa-ss0CC4oo-nn6ff3iidd0ee9nnttiiaall Information Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00119955 3MA10050628 3MA10050628 A`AlGlol tPPOaarptteiirccapitpaoanrntstss fr PPFFOOSSAAAACelplpopmOpmBeBryaytYVorRRsSSCCHHEEMM w |Em > w S03 mos mos xs won ;= R PPFFOSOAASdAfpApdm==f`0L0.pSi.0L0nui3p3en00mae3m3arm11rFoaF--~iift0rt0.F.y0i00t0111122 YYRRSSCCHHEEMM ReRRqSququuiiarrreeeAdj Summary of Fit 0o0.a34131s58a34232119 RMoRReSooaqotutnaMMoreefeaaRAnnedSsSjqpquouararsreee.EErnroorr 00o0..0o03013r9352s43263t319 OMObbesseaernrvvaoatftiiRooennsssp(o(oonrrsSSeuumm WWegitss)) 9 0.009223 9 Source oF AAn"anlSyuasimsloooiffySVVaqasrruiieiaasnnsccee MenSaums EMrSMorooduoderreclle DF711 Su0m000.o00f001S002q09u961a182r254e59s94 Mea0o0n.0oS00oq00u0w1a918r131e3 Cow Error C Total 878 000218103 0.00126844 0.00218103 0.000181 Tom PPaarraEamsmeietmteaerireEEssttiimmaattSeeissdEror 1Rato IYnITRenetrSrecmrCeceHpptEt M Estimate O00O1S3 0.0303118 Std Error O000035 0.010413 t R222a.2t99i611o YRSCHEM -0.001123 0.0005 -2.24 FF5R0Raa3tt6ii2oo PP050rr..0oo005bb539o>967FF72 PPr0or0b2>ol2tb6l 0097 0.0226 0.0597 AAPppappgeeenndd1ii2xx GG Page 12 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbciyyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00119966 3SMMAAA11T00005500662299 Apa All Participants Conoperans Cell Operators Aroma vESSHEM M570 ppm By YRSCHEM AAppppeendnidxiGxG PPaaggee 1133 go.v De ;"N HAN E; EP AFAR FBFE RF wo sous Source Voie Model ErrError Soa C Total TomTerm nent Intercept rach YRSCHEM =LMFI a Linear Fit MSToppm = 0.0876 000314 YRSCHEM M570ppm =0.10376-- 0.00314 YRSCHEM Sry IF Summary of Fit Rque assoc RSquare 0.38073E Ropar: ag 020268 RSquare Adj 0.292269 Rowan SqrEre Oates RootMean Square Error 0.04068E Nnof Repose frost Mean ofResponse 0.044833 Ova onSum Wi) S Observations(or Sum Wgts) 9 AnsofVyaness Analysis of Variance or MES Mensa Fro DF Sum of Squares Mean Square To SCs "oon sam 1 0.00712436 0.007124 3 onsen odes ear 7 0.01158772 0.001655 Po cow oer 8 0.01871208 F Ratio 4.3037 Prob>F 0.0767 Cumas [ amy -- Re Pol owrson Estimate olor own 3% cam open 0.1037558 "oobi ois am ome oss -0.003138 Parameter Estimates Std Error t Ratio 0.031474 3.30 0.001513 -2.07 Prob>111 0.0132 0.0767 -ower 95% 0.02933 -0.006715 Umperost Upper 95% obwm 0.1781816 ooo 0.0004388 Made Avaiabie by 3W orInspection and Copying as Confidential Information: SSMuuabbdjjeeeccAttvttaooilPParrbooltteeeccbttyiivv3eeMOOrrfdodreerrInIIsnnpePPcaatllimomeneravrvn..d33CMMo,,pNyNoio.n.gCC22a--s00C44o--n66f3i3d00e99ntial Information: 28122..00119977 3SMMAA1I0R0N5I000633)0 prosCnAACalerlllPPlaaOOrrpptieeicrcrpaiatpatYaonoanrtrtssssscHEM. PFOSA ppm By YRSCHEM D2 AAPppappgeeenndd1ii4xx G G Page 14 : a, "0.3 N Vim e Eo> ns D 5 ID wo15 IRSDN 2D 25 3s0 os35 SMoSouodurercclee EECMmroTordoorerall C Total ITnTtoeerrmmcept YRSCHEM Intercept YRSCHEM PPFOFSAOdfpSpm=A="00Ld.S.i0L0nu1i1ine00mea00am2r2pr-oa--FFifi0rtp0F..ty000.m00022 YYRRSSCCHHEEMM, RRSqqquuuuarreeeAd) Summary of Fit 000..011355122788800299 MRRReoSoaoqotutnaMMoreefeaRaAenndsSSjpqquouanarsreeeEErrrroorr 0000..000000034641727795984942 ObMseearnvaotfiRoensspo(onrseSum Wes) i 0.006259 Observations(or Sum Wgts) 9 OF AAnaSlunysmicsaoioffSVVqayaruriiaaaasnnccee MeanSquwe DF711 Sum000o.00f000S000q010u06a220r958e008s22 Mea0nO0.0S0o0q00u0o0a02ro23e9 87 8 000018990 0.00016088 0.00018990 0.000023 F1FR2PaR6ta2it6oo PP01rr.2oo2bb96>o28FF6 0.2982 00EsIsOtmi0mIaa%t4e 0002 0.0100194 -0.0002 Pa0PSSr0tadadr0maEE3merm7ertote9ererrEEssttt(iimRmR2aaatat7oeio0sso 00018 0.003709 0.000178 Liz2.70 -1.12 PPr0uo0bb>0l116]1 02982 0.0306 0.2982 LL0oow0we0err19945S8%% 000062 0.0012498 -0.000622 UpU0ppOeprIer9Ss5TeY%x 0000212 0.018789 0.0002212 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00119988 3MA10050631 3MA10050631 Apancoms All Participants Corpomors Cell Operators se om by YRSCHEM M556 ppm By YRSCHEM m004 0w03 No oo M 00? " + 001 r--,- - oe TIN D00 TT aw8a ws 0 ~11 S 10 1, 20 25 YliSCHEI Es lrta R Ms=S001Jr6e 36-00d0025pYRSCm Linear Fit HEM M556dfppm = 0.01826 -- 0.00025 YRSCHEM SimuPlt Summary of Fit Rque aos RSquare oman ous RSquare Adj 0.0478: -0.0882: Root enSueEre ooliss Root Mean Square Error 0.01154. MnofResponse Soran Mean ofResponse Oervaons or Sum Wes) : Observations(or Sum Wgts) 0.01347F, c. sauna or A"rDhctavoarwasrca MemSges Source Hoe 1 "Toooosits ooown Model Eno 7 ommsy coon Error Chom oom CTotal Analysis of Variance DF Sum of Squares Mean Square 1 0A0004686 0.000047 7 0.00093337 0.000133 8 0.00098024 Tom [ Chim--Sagroc Rao Term nore ooleer oon 20 Intercept rschem Gworss Ooms 0% YRSCHEM Parameter Estimates Estimate Std Error 0.0182567 0.008933 -0.000254 0.000429 t Ratio 2.04 -0.59 Fri F Ratio oss 0.3515 pwr Prob>F os7is 0.5719 Poboll Prob>ltl 000s 0.0803 0s 0.5719 Page 15 AAppppeendnidxiGxG Page 15 Made Avalable by 3WforInspection and Copying as Confidential Information SSMuuabbdjjeeeccAttvtatooilPParrbooltteeeccbttyiivv3eeMOOrrfoddreerrInIIsnnpePPcaatlilmomenreavrvn..d33CMMo,,pyNNoio.n.gCC22a--s00C44o--n66f3i3d00e99ntial Information: 22881122..00119999 a1 3AMMAA10000t50063322 PrrCOhSaeiAplmmplpiPacemaarrBtltiyiOpccpiwVepprrRamanaSttsosCorrHssEM PFOS ppm By YRSCHEM i . B00 1.03 s6w0. . . fo " . AAPppappgeeenndd1i6ixx G Page 16 0A 1.|10t0 Te w Sns RI ai s I wo 0 25 30 YRiCHll1 VTTIRneotrSremmrcccpeHpttEM YRSCHEM VsSoaouusrcscee TCEMororrdrooeralt C Total =lreaii: PFOSalppm PFOSdfppm = = 1S.A4SLL5Iii1iCn0neS5ame++raoF001irl.m0tF0337t76655 RSRRqSsuqqauuarurreeeAdy Summary of Fit OeNRReRMrSooeavoqoantutanMaoMiorafeefoaRaReAnnnesdSssSpjqpqououonanrasrsreeSeeuEEmrrrWorer s) Observations(or Sum Wgts) or Amneoalfvtairisasnce Analysis of Variance DF |1 @a62 Sum o5f7S77.q.30u3a636r97e5%5s0 19074.4003442755 63 104.40425 LiEEssxtiiiomssatitsse oPSPStaadrrsnamEmreeerrttoererrEEssttiIiRmmRaaeaatttleweilsso coves 1.4510518 coms: 0.237545 am6.11 2.17 0.0376538 0.017352 YRSCHEM YRSCHEM 00o0..op000r75eo505sc55ss89ts66 1.25103 153906p2y 1.839062 64 MemSame Mean Square a% 7.36950 156508 1.56508 pF44F.o7Rr7ana00tt8it8o7o 003 Prob>F 0.0339 Poll Prob>Itl cool <.0001 0m 0.0339 1L0u-.wo3o9weov7eroor6s92mn0Se5s6ers%6 0.002967 Upperssn Upper 95% roms 1.925897 odes 0.0723406 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbtyyiv33eMMOfrfoodrreIrnIsnIspnpeePcctatiiloomnneaavrnn.dd3CC,ooppyyNoii.nnggC2aa-ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00220000 3SMMAA11100005500663333 CheAArlrlicPPaaarsltiOipccieppraaanntttossrs Ww PEFHHCShSepmppipmcmalBByOypVYeRrRaSStCCoHrHEsEMM. AAPppappgeeenndd1ii7xx G G Page 17 1 . El. on vsHy om fn oB 8s wo MSooSuodurerclcee ErECMrroorodoerarll C Total TTIneotremmrcept IYnRteSrcCeHptEM YRSCHEM PPFHFSdfHppmS==00dS..L11iu77Lfn9i9m1no14ea4mpa+r+raFoF00ipirf..tt00Fy22im22t4477 YRSCHEM YRSCHEM RRSqqquuuarreeeAd) Summary of Fit 000.22278824383404565 MRRReoSoaoqotutnaMMoreefeaRaAnendsSSjqpquouaanrrseeeEErrrroorr 0000..343221276062474810103536 ObOMsbeesarenrvvaoatftiiRooennsssp((ooonrrsSeSuumm WWgattss)) o 0.410705 64 OF AAnaSnluymasiosllooSffyqVVauasrraiaimansncscoe MemSaume D@FI1 Sum o226f.66S620q245u486a628r818e8933s Mean220S.16q60u026a405r655e9 @62 63 92305102 6.6058219 9.2305102 0.10655 2F F6RRaat4tioo 2PP4prr.oo6bve3>o4F4F <.0001 OIEE9sstIii4mma4at7oe 0024713 0.1791447 0.0224713 PPaaSrrGaaEmmemetotererr EEssttii(mmaRattaeesos 000S.t000d066E411r929r7o179r t Ratio 248%2.89 0.004527 4.96 PPr0robo0>bJ0tlJ <00Ol 0.0053 <.0001 LL0oow0we5sr29s5S52%% 00B2l 0.0552502 0.013421 U0pU3pp0epr3or90935s1%k 00ST 0.3030391 0.0315217 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00220011 3MA10050634 3MA10050634 PoCGnhreApelmomliiaPmccaaraBlctsiyOcOpeipYeparaRansrSttasoCrrHssEM Tw POAA ppm By YRSCHEM : ww - o Ls F w 1, ae 1s ATF [I - w LAERCACAE AE AEE Ee AAppppeendnidxiGxG PPaaggee 1188 souca Source Soe Model EreError Tow C Total TomTerm nent Intercept Vestn YRSCHEM Ira Fl PO=A 1714U5A6n+aD:OpNET4Pm Linear Fit YRSCHEM POAAppm = 1.71456 t 0.04674 YRSCHEM Samara Summary of Fit Rque alos: RSquare 0.10198; Raq Aly domo: RSquare Adj RRoooottMMeeaannSSqquuaarreeEErrrroorr 011...022866790995880-23- NiamofRespons Tis Mean ofResponse 2.196234 Obervaons orSum Wet) o Observations(or Sum Wgts) 64 Anotavaras Analysis of Variance or "Shots Mensa Fra QF Sum of Squares Mean Square | far rir 1 11.35666 11.3567 @ 599717 [rig 62 99.99717 1.6129 a fii Soin 63 111.35384 F Ratio 7.0413 Prob>F 0.0101 Eman [ Enoo-- VRB Pub lowers Estimate le ome Ta <0 maw 1.7145638 ous oasls 265 aol Gases 0.0467429 Parameter Estimates Std Error t Ratio 0.241143 7.11 0.017615 2.65 Prob>JtJ <.0001 0.0101 1 _ower 95% 1.2325247 0.0115305 Upowosw Upper 95% Fim 2.1966029 dows 0.0819552 MSMuaabddjeeecAAtvvalaoillaParbbollteeecbbtyyi v33eMWOfrfoodrreIrnInsIspnpeePcctatiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo.nn6ff3iidd0ee9nnttiiaall Information Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00220022 MA10050635 3MA10050635 GhAaAtlmlcPPaaarrlitOicpcieippraaanntttsosrs w PPFFOOSSChAAeAAmifpcomamlBOBypeYrYaRRtESoCrCsHHEEMM. 0.) APpapgeend1i9x td G Page 19 wd. . Em oe w)0) C5 ons ono8rt 10 woni5 ASCHN 20 25 8s 30 35 MSSoooudurercclee ECErMroorTdoorerult C Total TIToneenmrncept YRSCHEM Intercept YRSCHEM =im R PPFOSFAAdOfppSm==`0AL0.S.i0L0nui55neA5m5ea88amr4r4-oaFdF--ifi0rtt0F0.yi00f011336p6YYRRpSSCCHHmEEMM RsRRqSququuuaurreeeAd) Summary of Fit 000.000244622822488188 MRRReoSoaoqotuntaMMoreefeRaaAenndsSSjpqquouanarsreeeEErrrroorr c000..0o005259u692829s49717 ObOMsbeesarenvrvaoatftiiRooennsssp((ooonrrsSSeuumm WWgetss)) 6 0.041812 64 OF AAnSanluymasoisllooSffyqVVauasrariiiwaasnnsccee MemmSuae FRato D@F11 Su0m002o.0f100S0799q696u22a955r881e88s Mea000n.0S000q03u995a61sr26e6 PF22r.7Ro73ab3t7a7i6r6o &62 63 02276257 0.2I799991 0.22762579 0.003516 P0r1o0b3>1F 0.1031 Esta PPSaardraaEmmmeettxeerrEEssttiimm(aRatatelesos Provsl] Lower95% 000.E00s500t5i38m6S3a5t1e2 000S.t00d010E1r82Sr5o29r t 1R44a6.t99i5%6o Prob>ltl <O0I <.0001 L0Oo0.w00e3Br30930E258S%2 -0.001361 0.000822 -1.65 0.1031 0.003005 U0Uppp0epre7r9o5Ms%w 0000263 0.0783421 0.0002833 MSMuaabddjeeecAAtvvataoiillPaarbbollteeebcbiyyv33eMVOfrfodorrerIInnIssnppeePccattliioomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00220033 3MA10050636 3MA10050636 S7GChhepA0alpmmliimaPcacarllntbyiOpcpgiYeepRrarsanSattCsorHsEM EE] M570 ppm By YRSCHEM = ge 9 JA " Tm ins e mos oa 10 weia5r 7) tS 3D 3> ASCHN Page 20 AAppppeendnidxiGxG Page 20 SMooSouduerrlce EErCMroordroaerlt C Total YITTtnReotrrSemmreCcneHpttEM YRSCHEM =Lrw It Linear Linear Fit MS70ppm = 037266. 000856YRSCHEM M570ppm =0.37266 -- 0.00856 YRSCHEM SummaofrFyi Summary of Fit RSqure ooo RSquare 0.031978 RSquaeAd) 0016364 RSquare Adj RRoooott MMeeaannSSqquuaarreeEErrrroorr 0.016364 00..443311440044 MeanofResponse o2mis2 Mean ofResponse 0.28442 Observations or Sum Wes) o Observations(orSum Wgts) 64 AnofaVarsnc Analysis of Variance oF "SumofSeumss MemSaws Fra DF Sum of Squares Mean Square i smn oT 20m 1 0.381171 0.381171 @ USER 01860 Pur 62 11.538802 0.186110 & 1915573 ois 63 11.919973 F Ratio 2.0481 Prob>F 0.1574 Esinuo [ SEmor -- (Palo Pb lowers Estimate 0366 O0BSIS 455 <00l 00915 0.3726642 00856 00098 43 OI 000s -0.008563 Parameter Estimates Std Error t Ratio 0.081915 4.55 0.005984 -1.43 Prob>JtJ <.0001 0.1574 lower 95% 0.208919 -0.020525 UU0pp5ppiea6rri9o058s%Sw 000m 0.5364095 0.0033979 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbiyyiv33eMVOrffodorreIrnInsIspnpeePcctatiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee8nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00220044 3MA10050637 3MA1005063 PROCCShrAeaAAlmmtliipPccaapaaorrmllBtiOiOypccpiegepYraraaRanntttSsosorCrsHs EM PFOSA ppm By YRSCHEM C ;0 wC {eC . 1ti ~OJC .. s 37m?7 - : . r E-- rr 300 Sl R--8 mon a 0 S t0 wi1S ASUN t0 2S JO 35 PAAappgppeeen2dn1idxiGxG Page 21 sMooSoduuecrlcee ECEMmroordorearll C Total YITTnRneoteSrmemrCnceHtptEM YRSCHEM PPFROOSSAdAfdpfppmp==m0S0..u11LL00imi88nne66ma83erao--al=frr00it.0Fy0i00119988YYRRSSCCHHEEMM RRSsRqSquqauuarereeAq Summary of Fit 0o0.o00i1e08s3zs2y3 RMoRRMOeSoboeaqosatutennMarMooreveffeiaRaRoAennensdSsSspjpqqoouonunarssrSreeeuEEmrrroWorrs) 0.002489 ors 0.132746 oosson 0.088272 Observations(or Sum Wgts) 64 oF AAn"alSyunsimsooofffaSVrwareeismnascncee MemSaare |DF Sum oom of Squares 000% Mean Square FFLRirastaieo 6@a21 011L..0200209902533509402090 002 0.020392 0.017622 Pp01rr.2o1ob65b>72FF2 63 1.1129329 0.2862 0IEE0sstSimSmmEatIee 0PSPt0aoSdrr2UoaE2Emmr0aermtot6rreerr EEsntiti(mmRaR4aata3ttelie1soos PPrro<boO>bMItIll L0oLwo0ewre6r9d5sS%% 00181 0.1086821 -0.001981 OOIMI 0.025206 0.001841 1084.31 -1.08 02 <.0001 0.2862 0006 0.0582964 -0.005661 U00pU.01pp10ep55are90lr90es665ss77%dw8 0.0016999 MSMuaabddjeeecAAtvvataoiillPaarbbollteeecbbtyyiv33eMMOfrfodorreIrnIsnIspnpePecactitimioeonnr vaa.nndd3CC,ooppyyNoii.nnggC2aa-ss0CC4oo-nn6ff3iid0de9ennttiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00220055 3MA10050638 3MA10050638 ChAeAlmllicPPaaarlrtOiipcpieaprnaantttsosrs wT MS555C8h6epmpipocmmalBByyOpYYeRRrSaStCCoHrHEsEMM, PAAappgppeee2ndn2idxiGxG Page 22 i co. oH HEREC AE EAE] we SMoSooudurercclen ECEMmroorodorerwl C Total InTTieoerrmmcept YRSCHEM Intercept YRSCHEM MSS=06.L0i9Lni7nd e0e3aarr-F0Fifi0tt02p 22YRpSCHmEM RSqMu5r5e6dfppm = 0SS.u0um9m7m0a3mry--ao0ofr.f0FFy0iit2t22 YRSCHEoMomss2 RRRRoSSqoqqutuuMaairreeeeaAAnddS)jquareError 0000..000057577272565594953332 M`RMOeboeasoaentnrvMooaefftRaiReonensssSppqooounnrassSreeeuEnrrWorets) 0.072643 007416o7 0.074167 Observations(or Sum Wgts) 64 oF A An"alSyun smiosoioSffaqVVuaaarrriassansnccoe MesnSquwe dF11 Sum000o.03f022S251q557u50a964r481e113s3 Mea00n0.00S020q255u55a529r914e4 &62 63 035277094 0.32717681 0.35277094 0.005277 FF4r5Ra0iti1oo PP40r.r0o83bo51>0b41F 0-0314 00EEss9tti0mi3amt3ae 000219 0.0970334 -0.002219 PPSaarGraEammmoeottraerrEEsstti(immRaatateeoss 000S.0t00d01E013r70r39o83r t 2R77a2.t00i033o 0.001008 -2.20 P<rPoob>b0JstlJ 0034 <.0001 0.0314 i0oL0wo6ewr4s96S05S7%% 00023 o.0694607 -0-004233 UU0p.pp2ep4re690r56s%2 0000205 0.1246062 -0.000205 MMaaddee AAvvaaiillaabbllee bbyy 33MVffoorr IInnssppeeccttiioonn aanndd CCooppyyiinngg aass CCoonnffiiddeennttiiaall IInnffoorrmmaattiioonn:: SSuubbjjeecctt ttoo PPrrootteecctiivvee OOrrddeerr IInn PPaallmmeervrv.. 33MM,, NNoo.. CC22-.0044--66330099 22881122..00220066 3MA10050639 3MA10050639 rms All Participants rpoorsesa Engineer/Lab PFOS ..m B YRSCHEM 1" | oT : wT AAppppeendnidxiGxG Page 23 a wr 0.00 ' I' I l I r' r' I' I 0 5 t0 15 20 25 Jo J5 i. YRSiHN someSource SoModel EESS Error Tometne Term Intercept YRSCHEM C Total J Linear Fit rosa 03655 opis SCH PFOSdfppm =0.36243+0.01624 YRSCHEM Summary of Fit aque ouses RSquare 0.158643 ma oi RSquare Adj 0.134604 Ewe Ercr Shot Root Mean Square Error 0.504597 frosted Sinem Mean ofResponse 0.611027 ST mvs 5 Observations(or Sum Wgts) 37 J Analysis of Variance or EEN sews ame D Sum of Squares Mean Square ToS ee On 1 1.680348 1.68035 A me NE a 35 8.911651 0.25462 od 36 10.591999 F Ratio 6.5995 Prob>F 0.0146 come pSaESconEan owe Estimate oComan Sihmeem T3e Tbeel Tomaany 0.3624261 Parameter Estimates Std Error t Ratio 0.127461 2.84 Prob>lt! 0.0074 Lower 95% D.1036677 0.016237 0.00632 2.57 0.0146 0.0034058 pene Upper 95% VEN 0.6211844 eae 0.0290681 WBadoiAvlaFlaotbeyh31CfroreepaFciaomn aanSCopoying5a3s0o4ri30a8nal formation Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00220077 awAtoososio 3M A10050640 apap All Participants reer Engineer/Lab rvs pom ByvaScrEM PFHS ppm By YRSCHEM w)D w)81 " HY Lo: : -- -- OCR HAC= E AEEEE AEragr 10 woi5 n YKKlan Pope 24 AAppppeendnidxiGxG Page 24 sauce Source Noe Model EneError Eat C Total TomTerm ent Intercept TRschEM YRSCHEM = = lrej Q Lori Linear Fit PRStm = 008186 + 0001 YRSCHEM PFHSdfppm =0.08056+0.00441 YRSCHEM Sma iF Summary of Fit Roque oonoas RSquare 0.091924 Eso AG Goss RSquare Adj 0.065975 Root eanSueEre Geen Root Mean Square Error 0.186981 NiamofResponse Gls: Mean ofResponse 0.14805? Otsrvons ox Sum Wee) Ss Observations(orSum Wgts) 3-1 Anottvrrsea Anatysis of Variance or MER wmsaen Fao DF Sum of Squares Mean Square t Ge Ome Sh 1 0.1238708 0.123871 5 lus ood rer 35 1.2236624 0.034962 % Jie Soon 36 1.3475332 F Ratio 3.5430 Prob>F 0.0681 Curae [ SaEnor -- iM Pub lewerssx Estimate oso own In oom oom 0.0805558 Goons oma Is cowl ooo 0.0044085 Parameter Estimates Std Error t Ratio 0.047231 1.71 0.002342 1.88 Prob>tl 0.0970 0.0681 Lower 95% -0.015328 -0.000346 Upperosn Upper 95% ohens 0.1764397 oomien 0.0091631 MSMuaabddjeeecAAtvva1aoiilaParbbollteeecbbtyyiv33eMOrffoodrreIrnInsIspnpeeaccttiiioomnn aeavnn.da3CC,ooppyyNoii.nngg2aa.ss0C4Coo6nnf3fii0dde8ennttiiaall Information Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00220088 3MAT0050841 3MA10050641 POAgAAElErplnnpgPmgiaanrnBrtoeyieiocrrciY/piaRLaaannSntbsCs HEM 0 POAAppm By YRSCHEM 3 J: PAAappgppeeen2dn5idxixG Page 25 ? 00 Ein B3ud . . 0 0.50 - 7 E EEC E AC it I ` I I' I ' I' I r I EA D 5 t0 15 worYFICHEW TomTerm orgs Intercept YRSCHEM YRSCHEM SMoSoouducrecee Model EnCororError C Total =Lreafi ~POAAPPm POAAppm = = 00.S3300m3nL3i44nne44ea+as+r00oFer0.ilt00yF02i25577YYRRSSCCHHEEMM RRRqsoRRuSSqoqqsutuuraaMrrreeeeeaAAnddSj)qu are Summary Err o f Fit 0o-o.00c00.4o00m5s2s282st75sr..:1s44 MRMeOobeasoanctnroMvofaefiRaRoenenssSppqoo(unonarssreeSeuEmrroWrs) 0.4509: o3an6>i 0.34276: Observatoirons(orAAnSaMulSnymisimWsogaootlffsSvV)iaaarreiinaassnnccee 3 MemSwwe Frio 3DsF11 %35 Sum of Squares Ooi 0.0420387 TTihse8siss 7.1165096 Mean Square oowms 0.042039 0mm 0.203329 F Ratio aves 0.2068 Pooers Prob>F 36 7.1585483 0.6521 0EE3sstii0nmao%tee SPSPtaaodrrElaaEmmrMeerstoRtreerrEEssttti(mmRR2aaatat6ieio6oss PP0rrobo0>bJ6tlJ LLOoowweerrm9S5S%k SSR 0.3034436 OMS 0.113902 20.4656 06S 0.0116 00S 0.0722111 0.0025682 0.005648 0.45 0.6521 -0.008898 Upporosw Upper 95% Ose 0.534676 0OloMe 0.0140344 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbtyyiv33eMMOfrfoodrreIrnInsIspnpePecactitiimooennrava.nndd3CC,ooppyyNoii.nnggC2aa-ss0CC4oo-nn6ff3iid0de9ennttiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00220099 3MA10050642 3M A10050642 -- pris All Participants ron re Engineer/Lab PFOSAA ppm By YRSCHEM DH w J J; o 0 D6 fnBa0g.03 0.A01 r-- . -- Z 0".w00 ~`T ~ti ~~r ,~r=a T{+L i 9 5 'C 1S iD 2S 3D ~~ IJ YRi%Ha Ee AAppppeendnidxiGxG Page 26 eoTerm =Be, Intercept YRSCHEM rosSStaHosprmscs Linear Fit m PFOSAAdfppm = 0.01271 -- 0.0002 YRSCHEM Summary of Fit rr om RSquare 0.026565 se ome RSquare Adj -0.00125 Ele pr Root Mean Square Error 0.016393 Sr = Mean ofResponse 0.009642 Observations(or Sum Wgts) 31 o goor J UE Le a Source BOT CERRE weno coe Model Tamm aw um Error Ep ime wr CTotal Analysis of Variance DF Sum of Squares Mean Square 1 0.00025666 0.000257 35 0.00940502 0.000269 36 0.00966167 F Ratio 0.9551 Prob>F 0.3351 JI SsrneEmeanEmes Estimate ouDm REE nOeWn mOEmR wOEeS 0.0127146 Parameter Estimates Std Error t Ratio 0.004141 3.07 Prob>lq 0.0041 Lower 95% 0.0043085 Upper 95% 0.0211207 -0.000201 0.000205 -0.98 0.3351 -0.000618 0.0002162 Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00221100 3M A10050643 AAElllnlPPgaanrretticeciripnpaaanntbtss MMS57700 pEpnppgmminBBey yerYY/RRLaSSbCCHHEEMM. 015 010 02.)35 Dw.10 gn015 HE0.20 RE Fw0.15 : 0w.10 o we . . .. Te DoO d - tt 0.00 0B51 o 10 B.15or s .m20I o,B2o 55r R3C N m 35 owI AoSCNadi AAPpappgpeeendn2i7dxiGxG Page 27 SMoSooudurerclcee ErCEMTrorrodooeurrlt C Total TTIonetrmemrcept YIYRnRtSeSCrcCHeHpEtEMM -Limn MS70ppm = 0.06LL6i0in7neae0raF.Fir080016YRSCHEM RequMi5r7e0ppm =0.SS0u6um6m0ma7m-rya0o.orff0F0Fyi0At16 YRSCHEM0.000864 RRSRRoqSSouqqtuuaaarMrreeeeaAAndSdjqjuare Error 00-0.00007.2050012781766668.84 MObRMesoeaeoarntnvoMaoftefiaRRoneenssSsppq(oouonrarsSrseeeuEmrroWrts) 000..00066733555163615756 Observations(or Sum Wgts) 37 OF AAnSanluymasioslolofSfyVqVauasrriiieiaasnnsccee MeanSquae 3D5Fli Sum000.o.10f0900S700q411u877a200r088e211s Mea000n.00S000q00u5011a677r211e 333%56 000...111999777664558222880222 0.005642 FF00Ra3at0ti3o PP0ru.o0bb3s>0FF3 00.38662299 00EE6as6tti0mm7sa1tt3oe 0-0.000.06060000171616443 PPaaSrrWaaEmmeeottreerrEEssttiimtmaRatatolesos 000S.00t00d1108E899r98r77o144r t 0R33a4.t44i738o 0.000941 -0.17 Pr0Por0bo>b0Jotl4J| 000..808606212949 loL0wo0e2wrIo9SrS53I%%O 0-0.000.2007005257017449 U0pU1pp0ep4ro5r99o50s7%w 000..001000114775449660474 MMaaddee AAvvaaiillaabbllee bbyy 33MVfofrorInIsnsppeeccttiioonn aanndd CCooppyyiinngg aass CCoonnffiiddeennttiiaall IInnffoorrmmaattiioonn:: SSuubbjjeecctt ttoo PPrrootteeccttiivvee OOrrddeerr IInn PPaallmmeervrv.. 33M,, NNoo..CC22--0044--66330099 22881122..00221111 33MMAA1100005500664444 -- All Participants roomyen Engineer/Lab PFOSA ppm By YRSCHEM D.D9 DoDeE q{" ie . . E -- w - -- Err 0.00 --Jr7 T r 88F ~ T-, , f T,1~ D 5 'D 15 20 2S 30 3S +, aYRSCROA wy AAppppeendnidxiGxG Page 28 nTerm a Intercept EN, YRSCHEM rgr ESsJ eqoE,meeP tEO cRnovEI ErEY wos2syooi2mn]= Source be r Tim um Model YBoe, 4Fecem Tomer Error Linear Fit PFOSAdfppm = 0.01025 + 0.00007 YRSCHEM Summary of Fit RSquare 0.002597 RSquare Adj -0.0259 Root Mean Square Error 0.019338 Mean of Response 0.011372 Observations(or Sum Wgts) 37 Analysis of Variance DF Sum of Squares Mean Square 1 0.00003408 0.000034 35 0.01308800 0.000374 omeF Ratio 0.0911 ceotuProb>F C Total 36 sis Estimate JGEuEn 0.0102528 0.01312208 -- TE--D Parameter Estimates Std Error t Ratio SoEmE UiEh 0.004885 2.10 wn Prob>ItJ WWNE0.0431 0.7645 vom Lower 95% ghpem 0.0003365 0.0000731 0.000242 0.30 0.7645 -0.000419 Yelk Upper 95% gm 0.0201692 moe 0.0005649 MT ite sR itiotyBStoA r apRtaEn CopyingT5 GSonna oman Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00221122 sntonscess 3MA10050645 [rr All Participants Sei Engineer/Lab ess ney vrs M556 ppm By YRSCHEM =J;5 www'0 a Ji u . C'S wi-- 2 C'D D CS CT 0 t " 4 1 D S '1T r 1 = 1 , i r aa it 1~ iD tS 3D 35 tIV wo"1SCHEV Page28 AAppppeendnidxiGxG Page 29 TemTerm Tmt Intercept sche YRSCHEM SouSource ShiModel JError Sa C Total =Lau ri MsS00i3a3u1dt00o00 m= Linear Fit YRSCHEM M556dfppm = 0.03151 -- 0.00049 YRSCHEM Soar oF Summary of Fit Rg oor: RSquare 0.01335_ Ro Ad "Sorat RSquare Adj -0.01484 Ron etnSueErr onsen Root Mean Square Error 0.056294 NetRee Soran: Mean ofResponse 0.02407E Otmevaion oxSum We) i Observations(or Sum Wgts) 3, React Vara Analysis of Variance or VERA saan rai DF Sum of Squares Mean Square To "Toone "own oa 1 0.00150111 0.001501 % one ome mer 35 0.1I091707 0.003169 $0 Slam Cn 36 0.11241818 F Ratio 0.4737 Prob>F 0.4958 [I e Puno t Cons Estimate obi om Th Go comes 0.0315087 Tooss oowos o ob Coos -0.000485 Parameter Estimates Std Error t Ratio 0.01422 2.22 0.000705 -0.69 Prob>jtj 0.0333 0.4958 -ower 95% 0.0026409 -0.001917 oomoenms tipper 95% 0.0603766 0.0009462 MSMuaabddjeeecAAtvvtaaoillPaarbboltleebcbiyyv33eMOfrfoIodrnersInpIsenpcePtcatiiloomnneaarvnn.dd3CC,ooppyyNoii.nnggC2aa.ss0CC4oo.nn6ff3idd0ee9nnttiaall formation Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00221133 ama1o0m0848 3M A10050646 P08AMlMVblPaaPoiraanirmBnttaeiycncnaiapYpnnRanccneSetssCHEM ww PFOS m = YRSCHEM w- mw PAAappgppeeen3dn0idxixG Page 30 ne } " TS . uwso 8s as SboSooudurrece EnEMCrooTrdoroerlw C Total ITTnoeermmpt YIRntSerCceHptEM YRSCHEM Lim ri PROSifppr=m PFOSdfppm = 1LS.L0uiL03i9nmn0o3e5ma++ra90FoF0ii0rf.tt0F70y76e659955 YRSCHEM YRSCHEM RRRRRSoSSSqoqqqtuuuuMaaurrreeeeeAnAddSjjquareSEummmrary of Fit 00001..2233208338328281611608958+4( MObRMesoeeaoartnnvoMaotfefiaRRoenensssSppqoo(unonaxssreeeuEmrroWret) 1.203104 L779i 1.772294 Observations(or Sum Wgts) 1, op AAnA alynsisoaol ffVVaiarriiaasd nnccee en D1F15i Sum2To11of07sS.q028u2i8a4z8r2ee419s Mean Square l1o7w5e 10.8242 F Ratio pamol 7.4781 115 2512.57131183801 1.4475 Poroo1bs>sF 16 32.536130 0.0154 LEC0sotbi0mraa4tse P0PSSataru3draaEEmmmremertmtorererrEEssttiti(mmRRa2aatmtt6eleis2aos PPr0oobb>0lliq -Oooiwwoeerar9w95iSs%% Ooase 1.0390494 0.0769454 omsis 0.396284 0.028138 2732.62 2.73 00S 0.0192 0.0154 O0ITIE 0.1943936 0.0169718 UpporSSh Upper 950/6 ses 1.8837052 OLeNdl 0.1369191 MMSuaabddjeeecAAtvvaatoiillPaarbbollteeecbbiyyiv33eMVOrffodorreIrnInsIspnpeePcctatiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggCa2a.ss0CC4oo-nn6ffi3idd0ee8nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00221144 3MA10050647 3MA10050647 PEHSAAplMlMlpaaPPmiiaatnBrrottiyneiccaniinYappcnaRaocnnSt.etssCHEM TM PFHS nom By YRSCHEM 1[) AAPpappgpeeennd3d1iixx G G Page 31 _ } -- :000 Ss 05 r i mks 8s 10 15 ? wow { 1 CH11+ T i 15 !0 35 SMoSooudurercclee ErECMrroTrodoorerult C Total TInToeermrcmept YRSCHEM Intercept YRSCHEM PPFHSF dfppHm== 00S S..L00iu77Lni22med n55ae77mar++raoFF0f 0iifr..tt00Fy22i44tp8522YYRp RSSCCHm HEEMM RRRSqqquuuurarreeeAdj Summary of Fit 0o0.5s52s511i65s32s15 MRRReoSoaoqotutnaMMoreefeRaaAenndsSSjpqqouunaisrreee EErrrroorr 0000..23524024717506055353515 ObMseearnvaotfiRoenssp(oonrsSeumWWegsts)) n 0.309053 17 Observations(or Sum OF AAnaSlunymsiosoisoSffqVVayuarraiimaassnnccoe MemSque D1Fs11 Sum o011f.91S121q255u595a934r355e577s3 Mean011S.01q162u215a505r948e4 1615 16 20414810 0.9155453 2.0414810 0.06104 1F8FR4Ra4at7ti0oo 1PP80r.r0o4bo04>7b6F0 0.0006 ooEEsmstSti6mmaEst2ee 00248165 0A725662 0.0248165 PPaaSrrGaaEmmneeotorerrEEsstti(immRaatateeoss 000S.t000d88E01r13r87o66r t R004a.t288i99o 0.005778 4.29 PPrOuobb>ssjt]j 00006 0.3866 0.0006 l.0ooww1esr0r9S05S8%% 0OIS0L -0.100882 0.012501 U0pU2pp4ep6ro0r91954S%9% 0037132 0.2460149 0.037132 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00221155 3MA10050648 3MA10050648 PorkrAplMVplpaaaPimrranBriattcneiycpnaiauYnpnnaRccnisSetssCHEM TM POAA ppm By YRSCHEM w $ we 2 Zw - I" w Tn sons ss wa Pag3e2 AAppppereindidxiGxG Page 32 Suse Source Nios Model EnerError Coat C Total TomTerm Ines Intercept YRSCHEM YRSCHEM POA 0525G8Z o8o+n0e0P r6146m= Linear Fit YRSCHEM POAAppm =0.92588 +0.06146 YRSCHEM SommoeFrt Summary of Fit Rsqure ozs RSquare 0.221317 RqureAd D1epune RSquare Adj 0.169404 RootMean SquareErr 127601 Root Mean Square Error 1.272661 MeanofRepose 151529 Mean ofResponse 1.511529 Otservation (or Sum Wes) 0 Observations(orSum Wgts) 17 AnsofVayrarsco Analysis of Variance or "mows Mewar Rao DF Sum of Squares Mean Square | 6505100 oousio sae 1 6.905100 6.90510 15 20295008 Totosr promt 15 24.295008 1.61967 1 51200108 00567 16 31.200108 F Ratio 4.2633 Prob>F 0.0567 Cunae ParSaamEertrerCatiRnaatees Pub lowergse Estimate Ossie Oalols 221 002 Gwen 0.9258836 Ooi omver 206 00s 000SE 0.0614567 Parameter Estimates Std Error t Ratio 0.419195 2.21 0.029764 2.06 Prob>ltl 0.0432 0.0567 Lower 95% ).0323938 -0.001984 Upporgsw Upper 95% 1m 1.8193733 OaeT 0.1248977 MSMuaabddjeeecAAtvvaoaillaParbbollteeebbcyiyv33eMMOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo.ppyyNoii.nnggC2aa-ss0CC4oo-nn6f3ifd0ie9dnteinatl IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00221166 MAT0050649 3M A10050649 apap All Participants nn Maintenanoe srosatomorascren PFOSAA ppm By YRSCHEM 0 to 0m.2q-* m 0.10 d i. ~~ Ew TT TTT Rs DOD ? r o S to is 20 25 30 3 wo'fIS61HBI rTpopesndi6x Appendix G Page 33 oe Souroe foModel EroError Ea C Total TomTerre friIntercept sctm YRSCHEM J Unear Fit Pros 008 0009s YRSCHEM PFOSAAdfppm=0.04575--0.00095 YRSCHEM ary oF Summary of Fit RRopnead paesesd RSquare pai fre RSquarc Adj es fis Root Mean Square Error hoon We) 7 Mean ofResponse Observations(or Sum Wgts) 0.064237 0.001853 0.040022 0.036697 17 or -- ERTLEN vesaws ra Analysisof Variance [Sma Mtmen oe DF Sum of Squares Mean Square Loh em rer I 0.00164936 0.001649 I fend 15 0.02402685 0.001602 16 0.02567621 F Ratio 1.0297 Prob>F 0.3263 Ccuoemmse SR vMaErEE tUsWS pToNy om"hnoense Estimate UI me am omm omwe 0.0457483 -0.00095 Parameter Estimates Std Error t Ratio 0.013183 3.47 0.000936 -1.01 Prob>Jt) 0.0034 0.3263 ...ower 95% 0.01765 -0.002945 pres Upper 95% owe 0.0738465 omiom 0.0010453 Sibello Prtechss Order Palmer. IWh No C2--.048--308 -- Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00217 3aMMAA1100005500665500 Apancoms All Participants Vane Maintenance wwwe wero py RSE M570.@ m B YRSCHEM fo J . Bwoel T wtAERC D .0 wiRoS CAC20 EAEI ?~ :0 RE! 3S rRScfu AAFpooppeeendn3idxixG Page 34 somo Source Soir Model ErrError oa C Total TomTerm Tan Intercept fen YRSCHEM fr Linear Fit Sopp = 021068 + OT YRSCHEM M570ppm =0.21068+0.00273 YRSCHEM Samra Summary of Fit Rsqure aoe RSquare KearAf aos RSquarc Adj Ron MnSquareErr prem Root Mean Square Error NOensoeRneoorrSeumWg) prW Mean ofResponse Observations (or Sum Wgts) 0.03116 -0.03343 0.168111 0.236706 17 Reactvars Analysis of Variance or MTEoRm wemtsownmeer Eoraan DF Sum of Squares Mean Square wm oom Pur 1 0.01363420 0.013634 15 0.42392181 0.028261 i men wn 16 0.43755601 F Ratio 0.4824 Prob>F 0.4979 ocoSne cSj hets -- hiSam pcooonn egowwenss Estimate 0.2106824 GN Own os oem ows 0.0027309 Parameter Estimates Std Error t Ratio 0.055373 3.80 0.003932 0.69 Prob>ltl 0.0017 0.4979 -ower 95% 0.0926575 -0.005649 Upuos Upper 95% ono 0.3287074 oon 0.01111II SMMaauddeeeAAvvtaaillPaabbelleecbbkyys33i1MCfforIornesInpIsenpceptctiaioomnn eaavnn.dd4CC0oopnpyiynoigCng2aa0ss4CC8oon3nff0ide8erntaiall inforInformation: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00221188 3aMMAA1100005500665511 PROSAMAlprVMlapapPiaiamnrratBtsneiyccnaiapnpYnacacRnneetSssCHEM wT PFOSA ..m B YRSCHEM be 2 w _ AC -- . . U) -- 1 o )CC Ia - I 1 I .'I Cons 0 > 10 Is wou ISCHEN aE as I . r. I 20 25 30 IS Ira F1 PPFOSEAdfOppm S==0S00L.u50iAL95nim9ne3e3a7ma7dr+ra+FoF0iif0rt.tF.l0y0a00.0066p9)YYRRpSSCCHHmEEMM RsRRSSqqquuuuarreeeAd) RRoSoqtuMarecaAndSjq u a re Summary Error of F it 00o.o00o06a2s15s8 0-.01.4056830917 RMMOobeesoaaetnrnvoMoafetfaiRRoenenssSppqoouonnarssrSeeeuEmrrWoir s) 0.149807 fren 0.065944 Observations(or Sum Wgts) 17 SMoSouodurerclcee DorF1 RAn"alSyiasimsoooiffsVSVaaarrmiiyeaansnccee Coos Sum of Squares MMeeam0n 0SS0qu8umaTreIe EmEMCrooordoearll 111155 0.00087072 0O337n500e82 0.33663010 oomMz 0.000871 0.022442 C Total 16 0.33750082 TTIoneemrrmeept Ppoaar0EEarsommtiaeeirmtmaraeottlreeEEssti|immaaoSSttteoddssEEorrroorr t(RRa1at2io0o YIRntSerCceHptEM 0000601 00004 020 0.0593671 0.049344 1.20 0.0006901 0.003504 0.20 YRSCHEM FF0Ra0atoSio PP0or.sro0ibo3s>8fsF8 0.8465 PPr0ro2bo4>bl7tl6l 0846S 0.2476 0.8465 AAPpappgpeeen3nd5idxiGxG Page 35 Suet Pecks Cre In pamev.40noC2048308 MMaaddee AAvvaaillaabbllee bbyy 33MV ffoorrInIsnsppeeccttiioonn and and CCooppyiynig ng as as Confidental Confidential Infor Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00221199 3awMAAt1o0o0s500e65522 -- All Participants Le Maintenance is crm M556ppm By YRSCHEM ---- Appendix G oe Page 36 0,; - ii al ws JE COC' TTT Ae S to 1S to 2S 3o J" wnISCG TomTerm Zn Intercept ch YRSCHEM ;,iw fi SrroffRNsrrqer s umiroee)esT tqcuesn=eEp 0s 0aeJ US nott LyvabtAosaocn teYRSsCHhEoMaS"aoinSomanotsreWs Fomm Source Yo 4 Nom oomu Pur Model EA No aha fr Error OocNoemSin OSSoeEMueSSnmE EsmaeGnssh pSGeEymNi lVdooiomemows CTotal Linear Fit M556dfppm = 0.07814 + 0.001 YRSCHEM Summary of Fit RSquare 0.011725 RSquare Adj -0.05416 Root Mean Square Error Mean of Response Observations (or Sum Wgts) 0.101656 0.0877 17 Analysis of Variance DF Sum of Squares Mean Square 1 0.00183898 0.001839 15 0.15500978 0.010334 16 0.15684876 F Ratio 0.1780 Prob>F 0.6791 Estimate 0.0781426 Parameter Estimates Std Error t Ratio 0.033484 2.33 Prob>Iq 0.0339 l ower 95% 0.0067735 0.0010029 0.002377 0.42 0.6791 -0.004065 twos Upper 95% Shean 0.1495118 Does 0.0060704 Wado Avalalo by for Inspection and Copying as Confidential informa S`MSuaubbdjjeeeccAttvttaooilPParrbooltteeeccbttyiivv3eeMOOrrfdodreerrInIIsnnpPePcaatllimomeneravrvn..d33C4Mo,,pNNyooi.n.gCC22a--s00C44o--n66f3i3d00e99ntial Information: 28122..00220 3SMMAA1100008500665533 ProSSsuepAplppleaoarPramvvrBirtasiyaocrraiTsap/HaisnMgEtgnsGmttHEM 0 PFOS so m B YRSCHEM wo : " fo Em = mw = 3 Si2 nTuT s io is ?a ?s Jo J5 to wa1R5N N Pag3e7 AAppppeenndidxiGxG Page 37 SENaSMmioouuodrrcesclee Coat Error C Total IYnTTIRneotSeremmrCrceHtpEt M YRSCHEM Lira "t PrO=0S7-- 15t4. f009ppm Linear Fit 4YRSCHEM PFOSdfppm = -0.2184 + 0.094 YRSCHEM "SumaofrFyi Summary of Fit Rsqure o10us88 RSquare 0.194588 RousAd 0161029 RSquare Adj 0.161029 Roo:Mean SquareEro 20708 Root Mean Square Frror 2.073295 MeanofResponse iT Mean ofResponse 1.732181 Ohiervaions orSum Wits) 2% Observations(or Sum Wgts) 26 ArofaVarasnca Analysis of Variance or "Emon MemSuwe Frio DF Sum of Squares Mean Square T 2450474 pyr I 24.92474 24.9247 2 10316526 i0% por 24 103.16526 4.2986 3 12809000 fro 25 128.09000 F Ratio 5.7984 Prob>F 0.0241 Comse PSaurEmreolreEstiimFaatelse Pobll Lowers Estimate O36 Oo 024 Ome aomon -0.218386 pans: oowo 241 Omal oom 0.0940032 Parameter Estimates Std Error t Ratio 0.906363 -0.24 0.039038 2.41 Prob>ltl 0.8116 0.0241 Lcwer 95% -1089012 00134332 Upperosw Upper 95% les 1.6522407 our 0.1745732 M`MSaaudbdjeeecAAtvvataoiillPaarbbollteeecbbtyyiv33eMMOfrfodorreIrnIsnIspnpeePcctatilioomnneaavrnn.dd3CC4oo,ppNyyoii.nnggC2aa-ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 281122..00222211 3SMMAA1100005800665544 P15SSuAuAplppleomPrPavaarrirtsBvyiiococriVpnspRa/ainMnGtggsEsmttHEM IE PFHS.m B YRSCHEM PAAappgppee3ennd8idxiGxG Page 38 Ero . = Dr w - In 1 l T 1 1 Tia ada ;0 15 2: 25 Jo 35 to wo Ypscii;A SMoSouodruercle ECEMrroordroaerll C Total IYnITTReneotrSrmecmrCecepHpttEM YRSCHEM =u>raft~ PPFHSFdfppHm==00SS..00u4LL4i4omUn88ae6mar++racF0F0fiilr0.ttF01yt166.p6633YYRpRSSCCHmHEEMM RSRRqSsququauarrreeeAJ Summary of Fit RRSooqtuMaereaAndSjquareEnon 000.1118585010717161 00.317581216156 MROMeboeasoactnrnvoMaoefdfiaRRoenenssSppqoouonnarssrSeeeuEmrrWors) 0.378289 0389124 0.389914 Observations(or Sum Wgts) 26 DorF| AAnSa"luSnyimsmiosoOaofiorSffSqVaVbuiaaaarroririeaesassnsnccee MMeeamonSmSqueuarare:e FFsRaaatosio 22zs41 0.7799725 S"2H1E04E9 3.4344674 0IBI8 0.779972 0.143103 P5[Pr.ro4ob=5b>0oF4F 25 4.2144399 0.0283 OGCEWsotGinSmaaItsRe SPPOtaaSdlrrGa6EeEmSrmemrItotr3rearEEssitmt(imaRR0ataatt2oeiso1so PPrOoobb7>l18Il1 LoLdwoewrser9o5ss%k Doss 0.0448618 29 oon 0.165373 7123 230.27 2.33 os 0.7885 0.0283 oso -0.296449 00019294 0.0166 0.00 Upperss Upper 95% 0366 0.3861726 oo 0.0313297 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbtyyiv33eMMOfrfoodrreIrnInsIspnpePecactitiimooennr ava.nndd3CC,ooppyNyoii.nnggC2aa-ss0CC4oo-nn6ff3iid0de9ennttiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00222222 33MMAA1100005500665555 SuAAplrlenPPaiirsctoiprcaispMnaitngtsnst Supervisors/Mgmt w POA ppm By YRSCHEM POAA am B YRSCHEM w : = "' ." pt - f 0 C '- [ 1 I 1- 1 I HEE EERE C i 10 1: 20 2S :0 3, f wo nSCHy PAAappgppeeen3nd9idxiGxG Page 39 SMooSuodurerclcae EmCEMroTordoorerull C Total TTIoneermrmcept YRSCHEM Intercept YRSCHEM "POAAPPTM = 0.L1i7Ln6i7en6aera+rF0Fi.itt05352YRSCHEM POAAp Rsqure p m = `SummoafrFyt. 0.17876 + 0.05352 Summary of Fit Y RS CH EM 0.19309 RoRRRSSSoqqqtuuuuaMarrreeeeaAnAgdSjquareError 000L...i111s966a03020601000s999 MeROMboeasoanetrnvMooaefftRaiReonesnsSsppq(oouonnarssreSeeuEmrroWres) 1.184218 128924 1.2894 Observations(or Sum Wgts) 26 OF AAn`anlSyuasmiosloloffSyVqVaausrraiiieaasnnsccee MemSauae D2F1| Sum o3f8.8S.6.q500u688a9003r885e00s00 Mean Square sLo0s2o7 8.08080 224 25 a17373s 33.656935 41.737735 1.40237 FFsRRaeattizioo Pp5orr.ooz7bb6s>o2FF2 0.0245 OIEEgsstiTim6msalttsse 00SI247 0.1787618 0.0535247 PPaSarrUaaEmmmeeottreerrEsEsttii(mmaRattaeesos Std Error OO0s9e 0.517694 t R020a.t343i505o 0.022298 2.40 PP0rroo7bb>3sIlt9lJ 0024s 0.7329 0.0245 LNoLwoEewsrsvr9Se5Sw%% NOOTSOS -0.889697 X1.007505 UpUlp2pe4prmo292r50s0% 0099544 1.2472201 0.0995444 MSMuaabddjeeecAAtvvataoiillPaarbbollteeebbciyyv33eMVOfrfodorrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00222233 33MMAA1100005500665566 Emoeee Ali Participants Supervisors/Mgmt PFOSAA ppm By YRSCHEM C ,S i =Appendix G Page 40 0 0+ i )0? - "0.30 0 =r ~ i HE 5 10 1S 20 25 J0 35 iO )VCHN -iw '1 wr=BBS--i -aheeefe EnTnoEE o eBfBvwmEy2En om Source Model Error C Total o eBranmGEEi EEERELEwm mmBm BwEmS Term Intercept YRSCHEM Linear Fit PFOSAAdfppm = 0.00564 + 0.00016 YRSCHEM Summary of Fit RSquare 0.023751 RSquare Adj -0.01693 Root Mean Square Error 0.011408 Mean of Response 0.009045 Observations(or Sum Wgts) 26 Analysis of Variance DF Sum of Squares Mean Square 1 0.00007599 0.000076 24 0.00312335 0.000130 25 0.00319934 F Ratio 0.5839 Prob>F 0.4522 Estimate 0.0056392 0.0001641 Parameter Estimates Std Error t Ratio 0.004987 1.13 0.000215 0.76 Prob>ltl 0.2693 0.4522 Lower 95% .0.004654 0.000279 Upper 95% 0.0159319 0.0006075 `SMSuaubbdjjeeeccAttvttaooilPParrbooltteeeccbttyiivv3eeMOOrrfdodreerrInIIsnnpPePcaatllimomeneravrvn..d33C4Mo,,pNNyoio.n.gCC22a--s00C44o--n66f3i3d00e99ntial Information: 28122..00224 3SMMAA1100008500665577 ASuAlpllePPraavrriitscioiciprpasanintgtsmst wsM5T70S0,uppeprmviBsyorYYsRR/MSSgCCmHHt EEMM " : AAppppeennddiixx GG PPaaggee 4411 -|A Fos ows BosA oKnG ws MSooSoduurercclee EECrMroTordooerrull C Total TITnoteemrrmcept YIYRnRtSeSrCcCeHHptEEMM MS70ppm = 0.03L7ni2en8ea+ar0rF.Fi0itt0349 YRSCHEM RSquMi5r7e0ppm =0.S`0u3Sm7um28amr+my0oao.ffr0F0Fyi3tt49 YRSCHEM0.081466 `RRRRSSSoqqqouuutaMaarrreeccanAAdSdjqjuareError 000..000484313141969464 0.127205 M`ROMeboeasoaentrnovMoafetfRaiReonenssSsppq(oouonnarsrsSeeeuEmrrWorgts) 000...11102097972728088%58 Observations(or Sum Wgts) 26 OF AAnanlSyuasmioslofoffySVqVasaurriaiiamansnsccee MeanSquire D2F1I Su0m0003.o3f0483S844q344u443a93r464e616s Mea000n.00S0l3q364u414a484r413e3 EF2254 04002..3428278293749393060717 0.016181 FF21Raa2t8ti6o P20Pr..ro11ob52b>7o85FF6 0.1575 00EEss7ttii2mm8aatt3ee 000..000003337442997448553 `PSPaaWrrGaaEmmeeottreerrEEssttiRimmaaatteoess. 000S.00t00dS52ES53r66r90o59r t R00a1.t646i767o 0.002395 1.46 PPr0ro5bb0s>l9lt0yl 00..O15IS50T79S50 Lo0Lwo0ew7re7r94S59S3%% -400)0..00017071444449993 U0pU1pp5pe2er0r94S50s%2% 000..010005882440334779882 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbtyyiv33eMVOfrofrodreIrnInsIspnpeePcctatiiloomnneavarnn.dd3CC,ooppyNyoii.nnggC2aa-ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00222255 33MMAA1100005500665588 parsons All Participants Sponsor Supervisom/Mgmt PrOSoKm By YRRCHEM PFOSA ppm By YRSCHEM moil . 0 60 Eo 3i . el0.10 - ww : 0n innwowAnaE ow 0 F ." T ' r '1 5 10 15 3 15 WSCFN , T J0 35 40 AAPpappgpeeenn4d2idxiGxG Page 42 souce NORRavRsosqaPnrouuvMatreiFeoaoRArenndsSsjOpqou(aono =rrsSeSe"0ESuG0mrumAL1Ws omr6ooeim9fsSda)aaao0nturrs 0Fsiey0stn3a3p3YRpSMCeHmmEo00oSM10oa23ssw662772ee0562937% Fao Source Mood | Codes OG 1953 Model Err 2 Oana 00s PvE Error Coat = rived so CTotal Tom Cums [ SaErer -- iRale Poli Lowerssn Term oe ol olssws 03 ois ows Intercept YRSCHEM Qos Ooms 140 ONS OOS YRSCHEM Linear Fit PFOSAdfppm = -0.0169 +0.00333 YRSCHEM Summary of Fit RSquare 0.075283 RSquare Adj 0.036753 Root Mean Square Error 0.126709 Mean ofResponse 0.052267 Observations(or Sum Wgts) 26 Analysis of Variance DF Sum of Squares Mean Square 1 0.03137008 0.031370 24 0.38532631 0.016055 25 0.41669639 F Ratio 1.9539 Prob>F 0.1750 Estimate -0.016933 0.0033349 Parameter Estimates Std Error t Ratio 0.055392 -0.31 0.002386 1.40 Prob>Itl 0.7625 0.1750 Lower 95% -0.131256 -0.001589 UoUpopppeoramr9oe5sn%w 000m 0.0973903 0.008259 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbtyyiv33eMMOfrfoodrreIrnInsIspnpeePcctatiiloomnneaavrnn.dd3CC,ooppyNyoii.nnggC2aa-ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00222266 33MMAA1100005500665599 sa pucours All Participants Stroman Supervisors/Mgmt = ssn iy vASChEn M556 ppm By YRSCHEM = o - r fro-- g Appendix G Page 43 ETTrAe aaa wo souce Source Vode Model Err Error hot C Total TomTerm neers Intercept eschim YRSCHEM -- Linear Fit ssitppm = OORT + 00235YRSCHEM M556dfppm =-0.0067+0.00235 YRSCHEM Samar iF Summary of Fit Rsqure oui RSquare 0.101017 Ropare dj Sain RSqunre Adj 0.061931 Ron ian Sq Err Sonne Root Mean Square Error 0.072994 NimotRespons Sort MeanofResponse 0.04378 Oto ou Wg) % Observations(or Sum Wp) 25 Anaof airrsea Analysis of Variance or MURUAGRT eosqas Fhao OF Sum of Squares Mean Square To STumn "oom asks 1 0.01377030 0.013770 5 ome omen reer 23 0.12254662 0.005328 3 Cie ie 24 0.13631692 F Ratio 2.5845 Prob>F 0.1216 cuirse PSuasmmeortrEstitmataes Pool Lucas Estimate wom om at lowal oom -0.006656 Sumas amie ie oie owes 0.0023503 Parameter Estimates Std Error t Ratio 0.034603 -0.19 0.001462 1.61 Prob>ltl 0.8491 0.1216 Lnwar 95% 0.078239 0.000674 Upperosk Upper 95% Ooms 0.0649258 ows 0.0053745 MSMuaabddjeeecAAtvva1aoiilaParbbollteeecbbtyyiv33eMOrffoodrreIrnInsIspnpeeaccttiiioomnn aeavnn.da3CC,ooppyNyoii.nngg2aa.ss0C4Coo6nnf3fii0dde8ennttiiaall Information Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 281122..00222277 33MMAAT100005500666600 PEOSAAMaltiplptlmlPPaOOarpprtBeeyiirrcpaaiYatptAnaoonrStrtsssCsHEW. PFOS ppm By YRSCHEM I OD 2EI0no -- w0 0o HEEwa 0 I s it YRSCHEU TEEE 7 AAPppappgeeenndd4ii4xx G6 Page 44 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00222288 3MA10050661 3MA10050661 pr AAiMlriollpPlpaaOpnrmBpetieriycrcapaiYiaptoRanornrtStssssCHEM ww PFHS ppm By YRSCHEM iND -- E we0.20 Z 010 :0 JO . li oo i I 1 I EEE EE 0 5 i0 1; 2) wo YRSCHEN AAPppappgeeennd4dii5xx GG Page 45 SMMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbiyyiv33eMVOfrfoodrrIenrInsIspnpeePcctatiiloomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee8nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00222299 3MA10050662 3MA10050662 ipartcpms All Participants i Cpmriors Mill Operators go POAA m B YRSCWEM " || ls I|w EEE EEE | wa ArPpaopgpeeennd4di6ixx G Page 46 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbtyyiv33eMMOfrfoodrrIenrInsIspnpeePcctatiiloomnneaavrnn.dd3CC,ooppyNyoii.nnggC2aa-ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00230 3MA10050863 3MA10050663 PEOSAAAAiMlrillplPpaapOprrpmatiericrBcaypaiiaptoVanornrtRtssssSCHEM = PFOSAA ppm By YRSCHEM 0 GS 0P E C.OJ r- Zw < 0.07 001 :ww . 0c0 71 w8u 3 7 as 0 I I I I S 10 15 N 75 IRSCH-51 AAPppappgeeenndd4ii7xx GG Page 47 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbiyyiv33eMVOfrfoodrreIrnInsIspnpeePcctatiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee8nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00223311 3MA10050664 31VIA10050664 MS70ppm AAMVliillllPPBaaOOrypprteetirrccYaaiptptaRaoonnSrrttssCssHEM w M570*m B YRSCHEM " iZou wm w v1 3 8 soa .on ww AAPppappgeeennd4dii8xx GG Page 48 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00223322 3MA10050665 3MA10050665 PFOSAAAMMliilpllplPmPaOOarpprBteeiiyrrccaaipttpYaaoonRnrrttsSsssCHEM PFOSA ppm By YRSCHEM )?5 w)2C - osVS C- - C C 7 Zo0.10 0.05 r. "wODD - I Ts D 5 i I i 8 5B 10 15 i0 25 wo ASCHN AArppappgeeenndd4ii5xx GG Page 49 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbciyyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00223333 3MA10050666 3MA10050666 AAMllilPaOprptaeirccaitpaaonrstss MSSppm By YRSCHEM Mill Operators M556 ppm By YRSCHEM w0 Cj 001 wuD 03 - e 'n D C2 2I i 0 | :w0.00 , I 1 1 1 | 5% or 8 0 j 10 15 2C 25 wo YHSCH(N AAPppappgeeenndd5ii0xx GG Page 50 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00223344 3MA10050667 31VIA10050667 AAPpappgpeeenndd1iixx HB Page I AAppppeennddiixx HH SSccaatttteerrpplloottss aanndd rreeggrreessssiioonn years worked in chemical eeqquuaattiioonnss ffoorr fflluuoorroocchheemmiiccaallss (YRSCHEM) for all chemical ((nnaattuurraall lloogg participants ttrraannssffoorrmmaattiioonn)) bbyy (n = 187) and for years workt`etwdwooinccuucrrhrreeemnnittcjjaoolbb(ccYaattReeSggooCrriiHeeEss(M(cc)hhfeeommrcciialaalllcoohppeeemrriaacttaoolrrsspaaarnntddiceeinnpggaiinnnteesez(rrn/ll=aabb1))S7)and for MSMuaabddjeeecAAtvvataoiillPaarbbollteeebcbiyyv33eMVOfrfodorrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00223355 3SMwaAt1100005500666688 opeaAlulpPaaprromBtsisyciopYaannAtsSsCHEM In PFHS ppm By YRSCHEM gol Ue .. I OD W 0.03D L wd-1 DD 20-? CD ry nehtad amyth ZEA E Ze dh. 3.00 -1.00 C 5.0D -60D -1I.00 0H+ F5 A10ACw1SIaCAEARIF35ar 1..3XV SourSource Vode Model EnoError Clow C Total TomTerm nerIntercept VRSCHEM YRSCHEM Ertrafi Looe i Linear Fit In PFRSafo=pm 25311 + 005519 YRSCHEM InPFHSdfppm=-2.5211 +0.05519 YRSCHEM SomayFai Summary of Fit Rsque ozesEr RSquare 0.226387 RsqureAd 0222208 RSquare Adj 0.222205 RootMeanSquare Err Tiss Root Mean Square Error 1.150356 Meno Resporse Hass Mean ofResponse -1.84074 Oeraons (or Som Wes) 157 Observations(orSum Wgts) 187 AnofgVaain Analysis of Variance or "Emon MenSwae Frio DF Sum of Squares Mean Square | reds els sai 1 71.64131 71.6413 155 2aisiei0 In pr 185 244.81410 1.3233 156 Siedssil oon 186 316.45541 F Ratio 54.1376 Prob>F <.0001 Gna pSaurarmoosEsti(mFaatekse Pol lows Estimate SS olsom oh coo coms -2.52111 Oosslss Coors 736 <O0 Goins 0.055185 Parameter Estimates Std Error t Ratio 0.125008 -20.17 0.0075 7.36 Prob>ltl <.0001 <.0001 Loner 95% -.767738 0.040388 Page 3 AAppppeendnidxiHxH Page 3 Upersst Upper 95% saan -2.274482 oGemezl 0.0699821 Made Avalable by 3Mfor Inspection and Copying as Confident Information SSMuuabbdjjeeeccAttvttaooilPParrbooltteeeccbttyiivv3eeMOOrrfoddreerrInIIsnnpPePcaatllimomeneravrvn..d33CMMo,,pNNyooi.n.gCC22a--s00C44o--n66f3i3d00e99ntial Information: 2881122..00223366 10050665 3d MA1s 0050669 InPOAAsAlal PpaapromBtsiycciopYamnRtsSsCHEM 0 In -- POAA ppm By YRSCHEM 1 JOBS dAeL t LpeSn Sa v l= Er3g Ew, fsLoonetetir od . ao Ji yo. an J i, I I i, [ , r . i Tins aE aE D 5 10 15 20 25 JD J5 40 wonYRSCHEM APApaopgpeeenn4didxi#x11 Page 4 SouSource ModeModel EnoError Coat C Total YITITRneontSrememrCcreHpttEM YRSCHEM =[in R I1n POAnAppP m ==-S-L00Ouo.3L3ie2m2n88sem9asAr++aFFo00irif0t.Fy00tA09.94433YYpRRSSCCp HHEEMM RRsSRSqqquuuarereeAG Summary of Fit RRSooqtuMaercanASdqjuareEnor 00001..0200009006111638737686323232 MOebRMssoeeonartnovMaofefiRaoRenensssSppqo(ournxassSreeeu)m'errWorg) 1.291882 "0212a66 -0.21266 Observations(or Sum Wgts) oF M"SuamoeifsSvwaermsnsce Analysis of Variance 187 MemSwan Fao 1D5F511 11586 5 Sum of Squares tom 2.09272 3S01807855706%5 308.75765 Mean Square an 2.09272 Toss 1.66896 F Ratio 12% 1.2539 p02o68e3 Prob>F 186 310.85036 0.2643 oGEsutiammsatee OPSPtaaSdrMruaafEmrmrSereoottrrenr EEsstmtiiamR2tmaatot%eeisso PPOrrobo>mbItlj LLow0weer6ro93s5t% Coals -0.328943 Oman 0.140388 Liz-2.34 1.12 0st 0.0202 0.2643 000s -0.605913 -3.007186 0.0094318 0.008423 Upporss Upper 95% osm -0.051973 00609 0.0260493 SMMuaabddjeeecAAtvvataoiillPaarbbollteeecbbtyyiv33eMMOfrofdorreIrnIsnIpsnpePecactitimioeonrn vaa.nndd3CC,ooppyNyoii.nnggC2aa-ss0CC4oo-nn6ff3ii0dde9ennttiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00223377 3MA10050670 3MA10050670 i AREr-- All Participants w nTi nrOSr AApo. m By vaSCHEM In PFOSAA ppm By YRSCHEM Page's AAppppeendnidxiHxH Page 5 ER CREE Tdwoneda Ae TomTerm nen Intercept sche YRSCHEM souSource Vie Model EnaError Co C Total ,rm rt InPROSAAI = 4[4--107-0Y0RS3C3HE4 Linear Fit M In PFOSAAdfppm = -4.4107 -- 0.03347 YRSCHEM man iF Summary of Fit Rqure oss RSquare 0.06056 RousAG aossas RSquare Adj 0.055482 RooMean SquareErr Vaan Root Mean Square Error 1.486622 Nan of Repose Li Mean ofResponse -4.82337 Orato or Sum We) fH Observations(or Sum Wgts) 187 AgofVrs arcn Analysis of Variance or Enea. Memsqwn FRaio QF Sum of Squares Mean Square | dss hss lows 1 26.35653 26.3565 8 rie To00 Pow 185 408.85842 2.2100 1s 53am fr 186 435.21495 F Ratio 11.9258 Prob>F 0.0007 Caras FSumtortrEstiimRaateksy Pabl Lowessn Estimate Shoe Diem De om mas -4.410692 Dom ome 545 oom ows -0.033472 Parameter Estimates Std Error t Ratio 0.16155 -27.30 0.009693 -3.45 Prob>ltl <.0001 0.0007 Lower 95% -4.729413 -).052595 Upperosx Lipper 95% doom 4.091972 oom -0.01435 Made Avaiable by 3W orInspection and Copying as Confidential Information SSMuuabbdjjeeeccAttvtalooilPParrbooltteeeccbttyiivv3eeMOOrrfoddreerrInIIsnnpePPcaatlilmomenreavrvn..d33CMMo,,pyNNoio.n.gCC22a-.s00C44o--n66f3i3d00e99ntial Information: 28122..00223388 MAI0050671 3M A1000055006871 eJe All Participants In M570ppm By YRSCHEM wif von Edi eT AAppppeendnidxiHxH PPaaggee 66 Pf omoBEt No BM m itl 'i1SCN[N -Tenn Be, Intercept YRSCHEM Source Model Error C Total SO Linear Fit SR In 570ppm =-2.4506 -- 0.00984 YRSCHEM irr, or Summaryof Fit ER, sae RSquare 0.009202 fe RSquare Adj 0.003846 Root Mean Square Error 1.151312 x mTsEEe MeanofResponse Observations(or Sum Wgts) Analysis of Variance DF Sum of Squares -2.57193 wer187 Mean Square neF Ratio 1 2.27743 2.27743 1.7181 185 186 or ErEeEr Estimate Samm -2.450623 245.22096 247.49839 Parameter Estimates Std Error t Ratio 0.125112 -19.59 1.32552 Prob>F pin Prob>ltl W OER <.0001 0.1916 Lower 95% -2.697456 -0.009839 0.007506 -1.31 0.1916 -0.024649 es Upper 95% .20379 0.0049701 Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 281122..00223399 3MA10050672 InPFOAAlSrlppAPoaarmrtiiBcciyppaaYnntRssSCHEM In PFOSA ppm By YRSCHEM D 00 of wi. Ll -1 DO r ~. r Eh I gi -2 DO . wd Lae -3.00 6066 !ft-o ffe - 1.00 .. 3Lo JE A% i Sop Ji Il el -`-6.00 ot TL -LOD . . eee ae -6.00 inswia8 nse 0 1 . i' 1. 1 , 1' I' 1 5 10 15 20 25 30 35 ID YRSCH 1 AAPppappegen7ednidxiixH Page 7 SMoSouodurerclcee EEnMCrooordoraerll C Total YnTITRnoertSnemcrnCceHptEM YRSCHEM =Lin [I InPROSAdippr =L4Li.i4nn0ee3as5rFF-iitt001431 YRSCHEM In PFOSAdfppm Rsque SummaorfFyt = -4.4035 -0.01431 Summary of Fit YRSCHEM ooor67s `RRRRSSSoqqoqutuuMaarrreeeeaAAnddSj)quare Eror 0.007678 0f0r3e1es 0.002314 MORMeboseaoeartnnvMoaoeftfiaRRoneenssSsppqoo(uonnarssrSeeeuEmrrWoret) 1.834221 Sifstto -4.57987 Observations(or Sum Wgts) 187 porF1 AAna"lSnysiimsaoooffiVVSaiaruriimaassnnccee Sum of 3159 Squares MMeeaannsSSqqiuuaasrweo 11i5t8ss51 4.81599 easa2773s 622.40775 360 4.81599 3.36437 186 627.22374 FRLRaaatosio Pp01rr.2oo43bw33o>11rF5 0.2331 Camas Estimate SAE -4.403463 Doss -0.014308 PaPSrauarEmammeeottererr EEssttiFimmaaaltteeess c0o1lms Std Error 0.199323 1 Ratio 2422000 -22.09 0.011959 -1.20 PP<ruoobb>0llltil 0zBl <.0001 0.2331 Lowwros% Lower95% Ames -4.796706 a0 -0.037902 UpUoppeplre9er5sn%s 000ssss 4.01022 0.0092855 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbiyyiv33eMVOrffoodrrIenrInsIspnpeePcctatiiloomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee8nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00224400 3MA10050673 3MAII0050673 shor son All Participants In M556 ppm By YRSCHEM -1 N -200 - A A -3 C0 EiE V- 2-4 00 .n =ee a es Appendix H Page 8 wnTerm Lam Intercept fe YRSCHEM oy Source hoModel HorError Tow C Total T=T RAE T e| 0 5 10 15 20 25 30 35 i 11'SCHi V ==] =Ltv it rs Linear Fit In stom=3born YRSCHEM In M556dfppm =-3.7337--0.00771 waa Summary of Fit Rae oo RSquare Eg Soom RSquare Adj unten oun Root Mean Square Error Le fr Mean ofResponse Seaton oom We) Ts Observations(orSum Wgts) YRSCHEM 0.00447 -0.00094 1.298323 -3.82913 186 Aras taro Analysis of Variance IUD wenn tom DF Sum of Squares Mean Square : Tom "Uwe owe 1 1.39270 1.39270 wo singe less beer 184 310.15820 1.68564 ds ime fed 185 311.55090 F Ratio 0.8262 Prob>F 0.3646 fo E pEm S oy rors Estimate Se Suen Tha Toe -3.733702 Gone Goous dei ase oomn -0.007709 Parameter Estimates Std Error t Ratio 0.141718 -26.35 0.008481 -0.91 Prob>ItI <.0001 0.3646 Lower 95% -4013306 -0024441 parte Upper 95% Then -3.454098 comes 0.0090235 SWMaaiddteeioAAvvaiaoliilPaarbblloeeebbcyyh3e3MMOfrfodorrIenrIsn1sppeepcctatiimoonneaarvnn.dd3CCooppyNyoii.nngg0a3ass04CCoo6nn3fif0di5ednetinatl Ifomatn Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 281122..024411 VE 3MA10050674 rE wruneoms All Participants neCf aaSyn Chemical Operators In PFOS ppm By YFISCHEM SD oe1 VC Je Za - . i Bet AAppppeenndidxiHxH Page 9 -1 Dv .-1 SD [REAPAwCoACAFAFar 0 10 1S ?D ?5 :o ~s YPSUN TomTerm ToRmSceen Intercept == =LfW F1 soe S[ RKaoeosoeeeorarE haeesEStEsrT a[ RenLvaarEtae-- s smoffSrineriveeaasdn me Source So : Thm Mem Om Model Hor a mum own ee Error a6 BEE Sie CTotal Linear Fit In PFOSdfppm =0.19093 +0.01954 YRSCHEM Summary of Fit RSquare 0.067842 RSquare Adj 0.052807 Root Mean Square Error 0.663197 OObMbseseaernrvvaoatftiiRooennsssp(o(oonrrsSSeuumm WWgittss)) 0.392284 6"4 Analysis of Variance OF Sum of Squares Mean Square 1 1.984648 1.98465 62 27.269497 0.43983 63 29.254145 F Ratio 4.5123 Prob>F 0.0376 coo SSEaIrum py owrisn Estimate oChoote oonmee dVnR Uonhmhe Tahweimn 0.1909269 Parameter Estimates Std Error t Ratio 0.125927 1.52 Prob>ltl 0.1346 Lower 95% -0.060798 YRSCHEM 0.0195403 0.009199 2.12 0.0376 0.0011521 uporisn Upper 95% Sha 0.4426522 om 0.0379285 Mace Avaiabl oy 3 or Inspection ana Copying a Confident nfomaton Made Available by 3M for Inspection and Copying as Confidential Information: Subect io Pecks Orde In Palme Hh 62.04 6308 Subjectto Protective Order In Palmer v. 3M, No.C2-04-6309 2881122..00224422 aMto050675 3MA10050675 InPCECNrheSAAolmonlmippPceaaamrlntiOBOccppypieeparVraaannAtttsSsoorrCssHEM In PFHSppm By YRSCHEM go B i [A E 3E a Te fal ash aVs on 8 nnds 4 10 woISn 2D 25 30 35 45CH1u AFApappgpeeendn1i0dxi1xH Page 10 SMSoooduuerrlcse EnCEMrooordorearll C Total TITYInoenRtrremScmrceCepHpttEM YRSCHEM IInnPPFHSFdfppHm ==`1-SS1Ln.u2i7ne26mde8a2ma2r++aoFr0if0irtF0.yi044.88p2299YYRpRSSCCHmHEEMM RRSsRqSqquuuiarrreeeAd Summary of Fit 0002.272838044555199 ROboRRMMsSoeeoeqoaartutnvnaMaMooretefefiaaRRoAnenendSssSjqppqou(ouonanarsrsreeeSeuEEmrrrrWooreris) 000"..712702701331000065566416 o -1,23054 Observations(or Sum Wgts) 64 or AAn"alSnyisimsoaooiffVSVaiqarratimaassnnce MenSawe Fra D@F1| Sum30o12f42.S.71q122u228a20r09e005s77 Mean Square 200122s0 12.1220 22PF48r.Ra66aw66ts3i5r6o 62 soe 30.472595 0.4915 P<roo0b0>1F 63 42.594602 <.0001 EGLstuiTnmaEate PaOSPStraLudraEDaEmmmrIoeorEottrrerr Ecsttmt(i1amRF2taaa9ettleis8eos PP<rr0ob0o>0Iblh LL9owoerwa95s% o-p1.i72g8z18 0094 0.133118 497 -12.98 <<.O0000I1 -10.o9a9s4s2s7s9 0.0482922 0.009724 4.97 <000 0.028854 Uppers Upper 950% les -1.462081 00670 0.0677304 SMMuaabddjeeecAAtvvataoiillPaarbbollteeecbbiyyiv33eMVOrffdoorreIrnIsnIspnpeePcctatilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee8nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00224433 3MA10050676 3MA10050676 --- All Participants aP rmras Chemical Operators In POAA ppm By YRSCHEM sEeega Appendix H Page 11 10 'FAW omTerm je Intercept [cM YRSCHEM =lrn 11 ee Linear Fit wr<0 ornss asg c In POAAppm =0.45333+0.01564 YRSCHEM Sa Summary of Fit sqm oven RSquare 0.051828 Rt oo RSquare Adj 0.036535 Eee sas Root Mean Square Error 0.612605 Rs sei Mean ofResponse 0.614523 EE ws a Observations(or Sum Wgts) 64 eo BeTLE oe ee Source EET TEE am ES Model Ea ARS Ra Error Fw 8 EEE fr CTotal Analysis of Variance OF Sum of Squares Mean Square 1 1.271823 1.27182 62 23.267630 0.37528 63 24539453 F Ratio 3.3890 Prob>F 0.0704 cme SrEpEmCcOTsE oy loin Estimate OJ BE SHE WR Wm mE 0.4533333 Parameter Estimates Std Error t Ratio 0.116321 3.90 Prob>Itl 0.0002 Lower 95% 0.220811 0.0156424 0.008497 1.84 0.0704 -0.001343 umnm Upper 95% 0.6858555 0.0326278 WSaadae lAevBaebtyo3 CforrepcFanersn 3CopyingCa204o5r5t05nta format Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00224444 sutososr? 3MA10050677 aparece All Participants nprcO ommenR oBsyovmars s Chemical Operators In PFOSAA ppm By YRSCHEM Jo. | AAppppeenndidxiHxH PPaaggee 1122 + eer 5 LH wo ITis T?5 fA0 45COEM 18 5 3. 0 15 sauce Source Si Model ErrError Era C Total TomTerm Ji Intercept TRSYRSCHEM =Lm 11 nat Linear Fit InPROSAdm =S055 002268 YRSCHEM In PFOSAAdfppm =-4.0532 --0.02268 YRSCHEM Soman airs Summary of Fit rsa aon RSquare 0.016184 Roa Ad Soo RSquare Adj 0.000316 Rootian square Ere Verols RootMean Square Error 1.619017 Ven of Resor nner MeanofResponse -4.28694 Onsen om Wes) " Observations(or Sum Wgts) 64 Anofavrrsce Analysis of Variance or ME wensuwe Fao DF Sum of Squares Mean Square i Sm EE ow 1 2.67335 2.67335 @ sis gam rer 62 162.51531 2.62121 fr fd 63 165.18867 F Ratio 1.0199 Prob>F 0.3165 fume PSarHtsEsiRmateos Pub lowssn Estimate Sm Chm bh Swe Were 4.053244 Doom ome To ones come -0.022679 Parameter Estimates Std Error t Ratio 0.307418 -13.18 0.022456 -1.01 Prob>ItI <.0001 0.3165 Lower 95% -4.667764 -(.067569 Uppwes Upper 95% Then -3.438725 oom 0.0222112 Subject 1o Protective Order In aimev. 3, No. 2.046308 MMaaddee AAvvaaiillaabbllee bbyy 33MV ffoorr IInnssppeeccttiioonn aanndd CCooppyyiinngg aass CCoonnffiiddeennttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00224455 33MMAA1100005500667788 CheAAmllcPPaaarlrtOsicpcpeiparanantttsosrs i 0 In MMC5Sh77e00mppipocammlBBOyypeYYrARaStSCoCrHHsEEMM, 1 AAPpappgpeeenndd1ii3xx H H Page 13 = ss wos | 888s to w's.5 to >s :c ;s `ISCHI.N MSSoooudurercclee ECEnMroroodoerrwl C Total TTIoneemrrmcept YRSCHEM Intercept YRSCHEM =m Wo'i 10 570ppm = 1.L5i0Lni0ne9ea-arr0FF0iit4316YRSCHEM RsquIanr5e70ppm =-S1`.uS5m0um0a9mr--my0oa.off0rF4Fyi3tt16 YRSCHEM01079 RoRRRSSSoqqqtuuuaaMarrreeeeaAAdndjSjquare Enor 001.0010.93912920898796921619 ObRMMsoeeeoaartnvnoaMorfefiaRRoneensssSppq(oouonnarssrSeeeuEmrrWoerts) 1.139966 "Loseos -1.94564 Observations(or Sum Wgts) 64 ODFF1 6@@2I 63 CLEEsSst0ii0mmBaa6tnSe 01 -1.500868 -0.043162 AAnSalnuymsioasfooSffseVVauariariiwaasnsnccee Sum8o0f9o5S.7eq6u08sa32r38e29s2 0283710 80.570389 90.253710 PPaaSrrdaaEmmmeeottreor EEssttiRimmaaatlteelss 000S.2t020d161E64r4r525o66r It -2R66a79.t9i333o 0.015812 -2.73 MeMaenmsSSqaauaumree 129952 9.68332 1.29952 F2F4RR5aat1ti8oo PP70rr.0oo40bb58o>12FF4 0.0082 PPr<uo0bb0>0lslq 00R <.0001 0.0082 LoLwo1ew9rr%99S5SS%T% COME -1.933557 -(.074769 UU1ppp0pe6r8e91r57s%9 -010.016811S79 -0.011555 MSMuaabddjeeecAAtvvataoiillPaarbbollteeebcbyiyv33eMVOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppNyyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00224466 3MA10050679 3MA10050679 LnSmT All Participants Chemical Operators In PFOSA - *m 8 YRSCHEM wd See | fsa oim--" | mhoy. i] -LT Ps = + wy AAppppeendnidxiHxH Page 14 i.Term 2Em., Intercept YRSCHEM ---= Itm r'1 Linear Fit FAL tSoEeEa eeetnma sdze: Source Model g=o o80 Tam Em LE Error osorm SBsa EErmSeEEOeW mOnW wOTm=Ee CTotall In PFOSAdfppm = -3.4933 -- 0.03575 YRSCHEM Summary of Fit RSquare 0.030317 RSquare Adj 0.014677 Root Mean Square Error 1.851004 Mean ofResponse -3.8617 Observations(or Sum Wgts) 64 Analysis of Variance DF Sum of Squares Mean Square 1 6.64144 6.64144 62 212.42545 3.42622 63 219.06689 F Ratio 1.9384 Prob>F 0.1688 Estimate -3.49335 Parameter Estimates Std Error t Ratio 0.351467 -9.94 Prob>111 <.0001 Lower 950/9 -x.195923 -0.035745 0.025674 -1.39 0.1688 -0.087068 Tuohn Upper 95% -2.790777 0.0155766 si vat tr nipcion and Cong a Corral Hornet Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00224477 swstcososm 3MA10050680 prAll Participants cramsomar Chemical Operators SiSpem er vRSErEU In M556 ppm By YRSCHEM d= | Page15 AAppppeendnidxiHxH Page 15 sauce Source SsModel ErrError oa C Total TomTerra TeIntercept sce YRSCHEM >,E TIe TER 10 wins 70 YRSCHEM ==Lm Q Io stdpm 2-- 00003Y0RS1CH2 LinearFit EM In M556dfppm = -2.7891 -- 0.03042 YRSCHEM Samra Summary of Fit Rg oosrs RSquare 0.063375 Karead peed RSquare Adj 0.048268 Roo insare ror Larios Root Mean Square Error 1.070608 Nena Rese Sosa OOMbbseseaernrvavotafitoiRnoesnssp((ooonrrsSSeuumm WWggttss)) -3.10248 6LL4] Ana vasaca Analysis of Variance or Me dems Fro aF Sum of Squares Mean Square ' me be 1 4.808428 4.80843 a docs Liew reer 62 71.064468 1.14620 8 fre on 63 75.8728% F Ratio 4.1951 Prob>F 0.0448 Ewe PSuaEn iRmas pun Lows Estimate Sow omms 7 mel hi -2.789057 Gowas Coowss 30 os oo -0.030415 Parameter Estimates Std Error t Ratio 0.203286 -13.72 0.01485 -2.05 Prob>ItI <.0001 0.0448 Lower 95% -3.19542 -0.0601 Uperosn Upper 951/16 Swe -2.382693 oma -0.000731 SMMuaabddjeeecAAtvvtaaoillPaarbboltleebcbiyyv33eMOfrfoIdornersInpIsenpcePtcatilioomnneaarvnn.dd3CC,ooppyNyoii.nnggC2aa.ss0CC4oo.nn6ff3idd0ee9nnttiaall formation Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 281122..00224488 aMAI0050681 3MA10050681 HI =m 2 in PFAOAStEEllnnppgPgpaiarmrnrtoecieBeicrypri/apiYLanaanRtbbtsSsCHEM In PFOS ppm By YRSCHEM : Ti| [= re 2Ea7u ) . w AAPpappgpeeenndd1ii6xx H H Page 16 PS i 0 5wiso 2B C o830B8 25 35 YRSCH[M MSoSooduuercclee EECMmroTordoonerult C Total InTTteoerrmmcept YRSCHEM intercept YRSCHEM Er Lrw r1 IInn PPFFOOSSddifppppmm ==`-L11Si.L.n5ui52ne2m1e1a2a2mrr++oaFi0if0t.rt.F0y0i33t779944YYRRSSCCHHEEMM RSRRqSququuaaarrreeeAd) Summary of Fit 000.222255800933677199 MRRReooSaoqotutnaMMoreefeaRaAenndsSSjpqqouunaasrreeeEErrrroorr 000"..80288289585489800603144 ObMseearnvaotfiRoenssp(oonrseSum Weis) Observations(or Sum Wgts) n -0.94033 37 OF AAnaSnluymsaiosfoyoSffqVVsauarariiieaasnnsccee MemSeuue 3D5F1| Sum o2f99.S..4q116u772a22617r55e822s6 Mean901S.77q18u27a267r7Ss5e 333656 635438 27.462686 36.635438 0.78465 1FR1R6aa9t0oi3o 1PPo1rr.ol6ob9b>e0eF3 0.0016 lEEssltiimmeaatee 009363 -1.521161 0.0379363 PPaaSrraWamEmeemttroerr EEssttii(mmRaaattbeeoss 000S.t22d022E33r795r5o84r t -R663a8.t4i802o0 0.011095 3.42 PPr<uo0bb0>sI0tl]J 00l6 <.0001 0.0016 LLoo1vw9ee7rr8994550%%3 OJISA -1.975403 0.)154116 UpU1ppep0re6r9o65s9%% 00606 -1.06692 0.060461 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggCa2a.ss0CC4oo-nn6ffi3idd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00224499 3MA10050682 31VIA10050682 warm All Participants ih Engineer/Lab rr nn In PFHS ppm By YRSCHEM end AAppppeendnidxiBxH Page 17 # . 1 | fw ---- Eo | gr Source foModel JError Soa C Total TomTerm Fl Intercept LiveYRSCHEM wa D 5 1D 15 20 25 JD 35 tRSXV == =L(W:t In=33p -- 0 05r 02 o Linear Fit YRSCHEM in PFHSdfppm = -3.3667+0.05024 YRSCHEM ena Summary of Fit Rsqoe aasisss RSquare 0.291558 remy bid RSquare Adj 0.271317 TE ms Vises Root Mean Square Error 1.056855 Frodo 55 Mean ofResponse -2.5975 mw 5 Observations(or Sum Wgts) 37 -- Analysis of Variance ou UE wen En OF Sum of Squares Mean Square ' To Mie ARS 1 16.088669 16.0887 5 ome WT 35 39.092987 1.1169 Boum a 36 55.181656 F Ratio 14.4042 Prob>F 0.0006 py p DEES OIT ty mon Estimate cShne oShoeme mTee Sdweew cSohmeesr -3.366746 Parameter Estimates Std Error t Ratio 0.266961 -12.61 Prob>ltl <.0001 Lower 95/6 -3.908703 0.0502418 0.013238 3.80 0.0006 0.0233675 pwn Upper 95% Dake -2.824789 come 0.0771161 ate oy SR gro Sona Se Seat fom Made Available by 3M for Inspection and Copying as Confidential Information: Sitio to Proce Orr 1 palmerv 31h No 2.046305 Subject to Protective Order In Palmer v. 3M, No.C2-04-6309 28122..00225500 -- 31VIA10050683 wsorers All Participants Engineer/Lab In POAA ppm By YRSCHEM Font AAppppeendnidxiHxH Page 18 == an . iTerm Intercept YRSCHEM oEo -- EERaErEEoseJ T25n E r escanwrcaea5i Source Linear Fit In POAAppm = -2.0155 + 0.02576 YRSCHEM Summary of Fit RSquare 0.107494 RSquare Adj 0.081994 Root Mean Square Error 1.001589 Mean of Response -1.62112 Observations(or Sum Wgts) 37 Anatysis of Variance DF Sum of Squares Mean Square F Ratio Model 1 4.228818 4.22882 4.2154 Error C Total 35 ne36 aEnEoEn 35.111285 39.340103 Parameter Estimates 1.00318 Prob>F 0.0476 Estimate Std Error t Ratio Prob>ltl Lower 950% -2.015494 0.253001 -7.97 <.0001 -2.52911 0.0257581 0.012546 2.05 0.0476 0.0002892 ns Upper 950/0 -1.501878 0.0512271 Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 281122..00225511 3MA10050684 inPFOSAAAEEltAlnngpPPgiapanrntormeieocBcrripy/piaLaaannYnbtsRsSCHEM -in PFOSAA m 9 YRSCHEM PAAappgppeeend1ni9dxi1xH Page 19 E So < 'l. Er = -63 I -100 qe -- | Ts.. 0S n ins 10 1S 20 ?S wo Y1S$HIN as 30 3S SoSMoouudrrecle CEMEfomrodooerll C Total IYnITTnReeotrrmSemcrCceeHppttEM YRSCHEM Swi =LwX fI IInn PPFROOSSAAAAddffppppmmS==5u-L.5nim.5an5e4am4ar2r2a2F2oFtifr---tF00yi..0000774455 YYRRSSCCHHEEMM RRSSRqqSuquauuarreeeAdj Summary of Fit 00.000"0505044211399 MRRReOMobSoeaosqoanetutnrMoavMroefaeeftaRaiRAennoedsSnsSqjsppquoouaonnrarssreSeeeuEEmrrroWorreis) 1"1.33s-6602e2.1103s32223 -5.65628 Observations(or Sum Wgts) 37 DoFF| AAnSa"luSnymusimoseafo0oiSff3sqv5Vuiqaa3raur8iriea5easns3snccs.e MeMaenmOSSsqauoasrsee 335651 e66s40429..9339533939011816657553 18550 0.35385 1.85540 36 65.293017 FR01Raa0tii7o PP00r.6ro16bo95>0v0F7 0.6650 SEEscStoinmOaatoe -D5o.5o4r2s20i1 -0.007451 PPeaSrrGaaEmmmeeottrerr EEssttii(mmRaatateesis Std Error o0OM 0.344074 t-d1R0e6al4.t1il41o 0.017062 -0.44 PP<rrob0o>blltll 060 <.0001 0.6650 L6oLwo2ewr0r90o5s0%% 00208 -6240704 -0042088 UApUppepsrar9de5s%n 002nise 4.843697 0.027186 SMMuaabddjeeecAAtvvataoiillPaarbbollteeecbbiyyiv33eMVOrffdoorreIrnIsnIspnpeePcctatilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee8nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00225522 3MA10050685 3MA10050685 pancsans All Participants ermeaerias Engineer/Lab f nBn yYASCIEM In M570ppm By YRSCHEM - a-t I'D - fF PeiX300 - i "ly w]. | c 4 R -5.DD HAFRrarAFBFaA! D 5 10 15 20 25 30 5 wowYRSDEN Pag2e0 AAppppeendnidxiHxH Page 20 Sauna Source Sie Model ErError Show C Total TumTerm Imeee Intercept RsCHem YRSCHEM =,in 14 fr. Linear Fit In ST0ppm = 33088 + C0073YRSCHEM In 570ppm =-3.3086+0.00738 YRSCHEM SomayFae Summary of Fit Rue aoiosss RSquare 0.010486 RqureAl "Dorms RSquare Adj -0.01779 Root eanSause Br aera? Root Mean Square Error 0.967617 VimofResponse Toss Mean ofResponse -3.19558 evaons (or Sum Wet) 5 Observations(orSum Wgts) 37 naoftvasasrca Analysis of Variance or Vn Memsawe Frio DF Sum of Squares Mean Square | mss ose os 1 0.347256 0.347256 5 Digws mam Pewe 35 32.769885 0.936282 % Sina fr 36 33.117141 F Ratio 0.3709 Prob>F 0.5465 Gime G[ af-- ni Pan Lowssk Estimate Sows om Ds com Swmew -3.308597 Goma Ooi: os oss oom 0.0073812 Parameter Estimates Std Error t Ratio 0.24442 -13.54 0.01212 0.61 Prob>ltl <.0001 0.5465 Lower 95% -3804792 -0017224 Upperosh Upper 95% Faas -2.812402 oo 0.0319863 SMMuaabddjeeecAAtvvtaaoiilaParbbollteeecbbtyyi v33eMWOrfodorreIrnIsnIspnpeePcctatilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall Information Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 281122..00225533 MA10050686 3MAII0050686 Aparscpans All Participants ramos Engineer/Lab w]emest . en _1i In PFOSA ppm By YRSCNEM ad i pol | perm nf " i" TT Ad wa Souco Source VioModel poy Error Croat C 'Total TITIYneRontreSmemrCcpeHptEt M YRSCHEM =rLW :1 InPFOS=5G3Ao60sds+0f008opm Linear Fit 6 YRSCHEM In PFOSAdfppm =-5.8688+0.0086 YRSCNEM Summary oF Summary of Fit Rsque oousaez RSquare 0.005342 RSqureAd ous RSquare Adj -0.02308 Root MeanSqrErr ise97 RootMean Square Error 1.583297 NinfResponse Sm Mean ofResponse -5.7372 Onsrvatons or Sum Wigs) (4 Observations(orSum Wgts) 37 Ansof Vyansco Analysis of Variance or "Timosamm MemSuwe Rao DF Sum of Squares Mean Square i 0311s bers ors 1 0.471187 0.47119 5 7739006 L506 pow 35 87.739016 2.50683 % $5310205 en 36 88.210203 F Ratio 0.1880 Prob>F 0.6673 Eimaa PaGraaEmreotrer EstiRmaattees Probl Lowssn Estimate Same oes ee col ewes -5.868846 Goomsssl ool: 041 on Coles 0.0085981 Parameter Estimates Std Error t Ratio 0.39994 -14.67 0.019832 0.43 Prob>111 <.0001 0.6673 Lower 95% -6.680763 -0.031663 PAhapogppeeen2dn1idxixH Page 21 U-pSUc5pp.ooep0res5ur96wso95s2me%w9 0.048859 MSMuaabddjeeecAAtvvaoaiilaParbbollteeecbbtyyiv33eMMOfrfoodrrerIInnIssnppeePccattiiioomnneaavrnn.dd3CC.ooppyyNoii.nnggCa2a-ss0CC4oo-nn6ffi3idd0ee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00225544 aMAt0050687 31VIA10050687 at paiopans All Participants py Engineer/Lab mETwssspmgvesren In M556 ppm By YRSCHEM PAAappgppeeen2dn2isxixH Page 22 | gmf1, st | Fol | fle] M in . | E 00 a :Jen . -690 - ' i I I T 1 I TT rE 0 5 .0 t5 20 25 J0 35 wrYRSCNEN Sour Source Voie Model RoError Chow C Total TomTerre ruc Intercept YRSCHEM YRSCHEM =Eraa I'I I Loew it Linear Fit In MS=S73e8 0p .0076p 3YRSCmHEM In M556dfppm =-4.7368+0.00765 YRSCHEM Summa oF Summary of Fit Rsque oom RSquare 0.00737 frome 00m RSquare Adj -0.02099 Root ean Sause Err Loaiza Root Mean Square Error 1.198158 MeanofRespome elses Mean ofResponse -4.61966 Otiervaion or Sum Wet) ] Observations(orSum Wgts) 37 Aes ofvarares Analysisof Variance or "nSiSaem Mesure Frio DF Sum of Squares Mean Square | ase oan oo 1 0.373036 0.37304 i s02isi las per 35 50.245432 1.43558 % "Daisies Sone 36 50.618468 F Ratio 0.2598 Prob>F 0.6134 1 Parra Estimates Estimate ST Omi Uses com os 4.736793 Guess O0isies ost oes om 0.0076503 Parameter Estimates Std Error t Ratio 0.302654 -15.65 0.015008 0.51 Prob>iq <.0001 0.6134 Lower 95%1 -5.35121 -0022817 Upper 95% ims 4.122375 ooenn 0.0381178 MSMuaabddjeeecAAtvvalaoillaParbbollteeecbbtyyiv33eMWOfrfoodrrIenrInsIspnpeePcctatiiloomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo.nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00255 3MA10050685 3MA10050688 rcaJ--asec All Participants In PFOS ppm By YRSCHEM c: - AEE lot - [I =] T esR Appendix H Page 2 Toomnen Term Intercept YRSCHEM " TTwo T, = qm -2m0) -A : . . 403 -- t , T , I , I , 1 , 1 , 1 , 0 S 10 1S 20 2S JO JS YRSCHpi C=] Linear Fit [RSS 1 -- In PFOSdfppm =-0.493 +0.02935 YRSCIiEM ---- Summary of Fit wpe aor RSquare 0.0981-8 om fe RSquare Adj 0.093304 ferrin id Root Mean Square Error 1.00299 Ne ee ve a2 Mean ofResponse -0.131:3 ome or J ERI--E sun rao Source fo : IST MSE erie Model oe w meben es ret Error I aaprnne ] tsE p eaemSmm mTWeBNpTShoodSherpermset CTotal Observations(or Sum Wgts) Analysis of Variance OF Sum of Squares 1 20.25968 185 186.09638 186 206.35607 Estimate -0.493042 0.0293465 Parameter Estimates Std Error t Ratio 0.108991 4.52 0.006539 4.49 11.7 Mean Square 20.2597 1.0059 F Ratio 20.1403 Prob>F <.0001 Prob>ltl <.0001 <.0001 Lower 95% -0.708069 0.0164454 pon Upper 95% When -0.278015 ode 0.0422476 Le V e Available by 3M for Inspection and Copying as Confidential Information: `SSuubbjjeecctt ttoo PPrrootteeccttiivvee OOrrddeerr IInn PPaallmmeerr vv.. 33MM,, NNoo.. CC22--0044--66330099 28122..00256 ---- 3MA10050689 005 Appennddiixx I1 PPaaggee 11 Appendix I RReeggrreeTessgssriieoosnnsioooffnfleluRRquouaaorarnnotoddcichooohenemmmmoisisfcacaaammflllppulloooeennrcocggucueerhrnnreeddemneenitrrtc.,jajlooyyeebboaacncrrhhssgeewewmmnooiidrrcceakkarlleeddaoonppiideennrrccayahhettaeoeorrmrmssisic(cw(ananoll=r=kaaen4n477ddd)):a:ianggeec:;hfefomolillcloaowwleedd bbyy regression equation of fluorochemical on gender and years worked in chemical: SMMuaabddjeeecAAtvvoaaiilaParbbollteeecbbtyyiv33eMMOfrfodorrerIInnIssnppeePccattiiioomnneaavrnn.dd3CC.ooppyNyoii.nnggC2aa-ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 281122..00225577 3MAT005060 3MA10050690 ChRReaamnnicddaoolmmOSSpaaommrppalloeers Chemical Operators SIiunnmPPmFFaOOrSSy ppofpomFmit RRRSSqqquuauaarrreee Ad Summary of Fit MRRReooSaoqotutnaMoMreefeRaaAenndsSSjpqqouuaanrrseeeEErrrroorr OMObbessaeenrrvvoaafttiiRooennsssp(o(oonrrsSeSuumm WWagttss)) 00.011622133911785833 0000..350507672515759520705989 a 0.392725 47 SMoSouodurerclcee EnCEMrooordoraerll C Total OF AannaSlauymesiosslooSffqVVuaarariimaasnnccee MeanSawwe OaF33 Sum o1f222S.0q000u000a02r279e99s9 Mean Square 0O6sBr66 0.666766 43 46 16202370 14.242071 16.242370 0.331211 LSoaSuocurkrcoceefFit PuPTLouartrceaeklEEorErfrrrFoooirrrt T0MMo9aat7xxa9lRR6ESSrqqror 0.9796 OF SLLuaamcckkolooflSFFqiiuttaws MemnSuare O4aF12 Sum o11f033S3.9q931u110a028r224e239s3 Mea0n0o.1S3x6q35u9e9a22rs78e4 52 10a.233012804m9 0.165924 43 14.242071 ITonerermrmept GGIYnEERtNeNSrDDcCEeEHpRRtE([MFF--MM)] AGE YRSCHEM AGE PPaarr0aam0EmEes4wottit6eimo3rmaa3EEits7seettii|mmaattee0sSsS4tWd1E2Er4ror4or8r t RR0aatt1ieo 00.0-0000249.062240883818311272 0000..0114100192228418484282 -2002.0.8102512 00096 0.0092881 0.0029634 00l0319 0.010914 0.010819 0270.85 0.27 S`oSGuoEurrNccDoeER GYERNSDCEHREM AGE YRSCHEM AGE Nan DF EEffffeccttSTTueemssottiSquaes Nparm[1TIo OF 1 Sum oo1Lf.2aS3q5siu5sa3%er6ee2ns7 11[I 1 1 oguss 0.2398607 0.0248502 FaFRoRaatliioo 040o..00m7927a24012 0.0750 F2F0RRa0atii0oo PP20r..ao01bn12>36F1F3 0.1263 F F2RR0aatuii8oo Pp20r.r3o0o8b4b3>4s3F8 0.3833 PPr0ro9bo1>vl0to9l 0000..309091499093593 0785S 0.3995 0.7855 PP0rro0bo>3bF 0000..7330899459995553 0.7855 PAPAappapgpgeeeenn2dd2iixx I1 SMMuaabddjeeecAAtvvataoiillPaarbbollteeebcbiyyv33eMVOrffdoorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00225588 3MA10050691 3MA10050691 MSSoooudurercclee ErECMrroroodorerwl C Total LSoaSuocurkrccoeefFit TPPLouuatrrcaeeklEEoErmfmroFooinrrt T0MMo8aat1xxa2lRR2ESSrqqror 0.8122 TITneotrmemrcept VIGGnREEtNNeSrDDCcEEeHRpRt[E(FMF-NMf)l YRSCHEM SSGoouEurrNccDeeER YGRESNCDHEERM YRSCHEM ChRReaamnincddaoolmmOSSpaearmmapptlloeers Chemical Operators SI1unnmPPmFFaOOrSSy ppofppmFmit RRRSSSqqquuuaaarrreee AQ) Summary of Fit RRMRSooeoqoatutnaMMoreefeaRaAenndsSSjpqqouunaasrreee Error Error OMbesaernvoaftiRoenssp(ooonrrsSeSuumm WWgtts)) Observations oF AAnnaSalluyymssioissfooSffqVVuaaarriieaasnnccee DwF22 Sum o1f114S.29q967u76a559r442e481s8 644 46 16202370 14.266921 16.242370 OF SLLuaacsmkkoaolrfSFiutaws D22iF%6t Sum o11f151S...q202u151a0559r998e3%5s6 "18 44 11348..202665660999228115 00.011822111666922733 0000..33506968991024672295887 a 0.392725 47 MeMaeOnnSSoqaumuamsree 00,392847274284 0.324248 MeMaeonnSSsqquuamaree 016919 0.431382 0.169499 F0FRR4aat6tioo PP30rr.0o0o8b4v7>67oF2 0.0577 F2F5RRa4at5ti0oo PP20rr.2o5ob24v>51oF0 0.0221 oEElsetSii7mm0astSee 0-00002..110205072977899045459 0.0109494 |PPaarrSaaGmmEeertteeorrrEEssttiimmaaRtteeasso 0O0S.t11dL03E18r4E9r8o32r t R211a0.t11i80o0 000STE 0.101793 0.008978 122 -2.04 1.22 Npam DF EEffffeecttSTTueemssottfSquies Nparm DF 11a 1 1 Sum of Squares oLuEsT 1.3531877 1 1 0.4822506 PP0roob2>lw2tl 0000..20029747761112 0.2291 FaFRRaamttioo Lem 4.1733 1.4873 LL0ooww1esrr69S5S8%% --000040..411012336700398S987 -0.007145 P0Prro0obb>aoFF 029 0.0471 0.2291 AAPppappgeeenndd3iixx I1 Page 3 UpU0ppeprear9S5ms%k 000.2-"40093..0100870039228878 0.0290438 SMMuaabddjeeecAAtvvataoiillPaarbbollteeebcbiyyv33eMVOrffdoorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00225599 3MA10050692 3MA10050692 ChRReraamnneddcaoolmmOSSpaaermmapptlloeers Chemical Operators `IISnnuPPmFEmaHHrSSy ppofpomFmit RRRSSSqqquuuaaarrreee Ag) Summary of Fit RRRMoSoeoqoatutnaMMoreefeaRaAenndsSSjpqqouunaasrreee EErrrroorr OOMbbessaeenrrvvoaafttiiRooennsssp(ooonrrsSSeuumm WWgatts)) 0040..444377499377233 000"..3L554I884T443I55400038552 a -1.17704 47 MSSoooudurercclee ECnEMrooorduorenrlt C Total OF AAnnSalauymisiosslooSffaVVuaaarrimaanenccoe MemSuare PHOF33 Sum o111f322S.65q594u406a670r065e53s0 Mean40aS.s3q5i1u1sa56sr3sse5 p44s63 28236813 14.690763 28.236813 0.34165 SoSLuoarucrckcoeefFit TPL[ uoaruceklEoErfrrFooirrt 0TMMo9aat8xxa8lRR4ESSrqaror 0.9884 OF SLLuaaccmkkoooffiFFSiittuas MemmSaumre O4a1F2 Sum o11f044S3.3q326u682a215r596e6588s Mea000n.1S336q5u100a390r08e7 52 43 11044..636929080717696353 0.164098 TTIneotremmrcept Y`IGRGnEEtSeNNCrDDcHeEEpRREt([MFF--MM)] AGEYRSCHEM AGE PPaarraammEeesttieemrraEEtssettiimmaatteesSs uro LE8sti7ma8te 0S4t1d8E8rr5o4r t aRRadatisto --o0100..843647r97078084317 O00.Oo.4ll11I008G48uS499S94 --343432..343436 000088 0.047003 -0.000586 00098 0.011085 0.010988 0054.24 -0.05 SoGSuoEurNrccDaeER YGYAREGRSENSCDCHEHEREMM AGE Narn OF EEfcfetctSTuToemsstot.iSquawes Nparm1L[i oaOF1 Sum o33Gf.7lS7q6z8u61ea10ar9e580s0 11roa11 Oooo719 6.1426340 0.0009719 1F1FR0Raa2tli2oo 1110717..0990077829928552 0.0028 1FF2R1ra6taiso 1PP<3rr0.o2o0b10b>61eF5 <.0001 FF2r1R3aat4it7o PP02rr.3o1o7b3b0>47eF7 0.3707 PP<rrooobbo>sdlltl]l 0<00..000000000I011818 00.90507071 0.9577 P0rP0ro0ob1b>8fF 0000..9000500007011718 0.9577 AAPppappgeeenn4ddiixx 1 I Page 4 MSMuaabddjeeecAAtvvtaaoiillPaarbbollteeecbbtyyiv33eMMOrffodorrerIInnIssnppeePccattliioomnneaavrnn.dd3CCM,ooppyNyoii.nnggC2aa:ss0CC4oo-nn6ffi3idd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00226600 33MMAA1100005500669933 SMoSouodurercclee ErCEMrooTrdoroerlw C Total LSaSoocuukrrcoceef Fit PTuPLoruatrceaeklEEEorrfrrrFoooirrt T0MMo8aat9xxa3lRR3ESraqror 0.8933 GTITEInnoeNteremDrmreEceeRpptt(F.M) YRSCHEM GENDER[F-M] YRSCHEM S`oSGuoEurrNccDeeER YYGRERSNSCDCHEHEREMM ChRReaamnneddaoolmmOSSpaaemmrapptlloeers Chemical Operators SIInun PPmFFmHHaSSroppyfppmFm.i RRRSSSqqquuuaaarrreee AG) Summary of Fit RRRMooSeoqoatutnaMMoreefeaRaAenndsSSjpqqouuraasrreee EErrroorr OOMbbessaeenrrvvoaafttiiRooennsssp(ooonrrsSSeuumm WWagttss)) OF AAnnSalauymisiosslooSffaVVuaarwriieaasnnccee D"2F2 Sum o11Lf33Sa.3q54gu45a5o0r07e7s88s 344 46 2236813 14.691735 28.236813 OF SLLuaacsmkkoaolrfSFFiiattues D22iF6s Sum o1Tf31S.0eq61u73ea79r80se33s2 "18 44 11342..606919113779330553 000..54467799066399666 000..51547175776788004444336 a -1.17704 47 MMeeaan6nSS7qamuuaswraee 033390 6.77254 0.33390 MMeeaa0nn4SSqq9uu1aarrsee 016M 0.449147 0.167439 2FF0R2aR8ti9o 2PP<0rr.oo2o0b80v>21oF9 <.0001 F2FRr6aatimioo PP2orr.oo6ob8v>r2eF5 0.0170 LEEsEstiiTmmaaTttee 0-01-04.08.639360477774889487 0.0466744 PPaarrSaaWmmEeemttoeorrrEEssttiimmaattReessal 000S.t11d014E20r59Sr2o79r -t013R33a3.4t4i7s5o OOBIII 0.103297 0.009111 S12 -3.37 5.12 Noam DF EEfcfetctSTuTeemsstot.fSauares Nparm1TLo oaDF1 Sum o337f.6S772q809u7a050r75e007s0 1 1 8.7629557 PPr<ro0bo0>bl0tlll 0<<0..0000000l0016l16 <.0001 1F 3FRA4aat0ii5oo 26260 11.3418 26.2440 LLo2ow0we7sr4r90o51S%4% 0--00250..5163570642600616224 0.0283126 PP0rr0obo0>bsF <oool 0.0016 <.0001 AAPpappgpeeenndd5iixx I I Page 5 UUppoppreeerro9sr5ss%ws 0-00-01.161.303693907666593989 0.0650363 MSMuaabddjeeecAAtvvtaaoiillPaarbbollteeecbbtyyiv33eMMOrffodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CMC,ooppyyNoii.nnggC2aa:ss0CC4oo-nn6ffii3dd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00226611 IMA10050694 3MA10050694 ChRReaamnncddaoolmmOSSpaaemrmapptlloeers Chemical Operators `IISnnuPPmOmOaArAAy ppofpmFmit RRRSqqquuuaarrreee Ad) Summary of Fit RRRMOMbSooeesoqoaaetutnnravMMoroaeefeftRaaiRAennoedsnsSjSsppqqoo(uunonaarssrreSeeeuEEmrrrrWoorrats) Observations(or Sum Wgts) 00.011194712m2337 000.0365.539195004088199924939 @ 0.635094 47 MSooSudourerclcee EECMrrorodooerul C Total OF AAnnaSalluyysmsiiosslooffSVVqaaarriwiaasnnccee MeanSquawe DaF33 Sum o1f335S.06q618u838a898r858e896s6 Mean011S3.q224u299a90r636e3 343 46 18702815 15.013959 18.702845 0.34916 LSaSoocuukrrcosefFit PuPLTuraorcueeklEEroErrfrroFooirrrt TN0Mo9aat9xxa5lRR0EsSraqror 0.9950 OF SLLuaaccmkkoooltfSFFiiqttaws MeanSquare D4aF12 Sum o1Lf40aS.0q9spu1aea92r7r2e3s18s Mean Square O0se0306 0.363896 i2 43 11055..000191343929525199 0.047111 I`nTITGtneoEtererNmmrcDceeEppRtt(F:M) GYYAERRGNSESDCCEHHREE[MMF-M] AGE PPaarr0 aammEEeesstttiee3 imrrmaaEEitssoettii|mmaattee0SssStW4dE2E4r7ro7r t(RR0aat8ii0oo 0-0.0033.0313098188839300309013 0000..011410205325640733673 -0303..08801010 00.000.000000338339990339 0011S 0.011206 0.011108 0030.80 0.03 SoSGuoEurrNcceDeER GYAYGERRENSSDCCEHHREEMM AGE Noam OFEfEfifcecttTSToeussmtt.ofSmeres Nparm DF TI o1 1 Sum o350f.02S172q700u033a655r866e755s 11[I 1 1 00003258 0.2206817 0.0003258 FF0R0aa7toi%o 0900..066003720920990 0.0009 FaFRrsaatitioo PP3orr.oon5bw2>ss1Fe7 0.0228 F1F7RPaR2ta6ii3oo PP7orr.on7ob2b>i4eF3 0.1211 Pr0Por4bo2>bsI6ltsyl 0000..0404030241463036 09738 0.4310 0.9758 PP0rr0oo0bb8>s3fF 0000..9440730351418030 0.9758 AAPppappgeeenndd6iixx IT Page 6 MSMuaabddjeeecAAtvvtaaoiillPaarbbollteeecbbtyyiv33eMMOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CMC,ooppyyNoii.nnggC2aa:ss0CC4oo-nn6ffii3dd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00226622 IMAI0050695 3MA10050695 MSoSooduurerclcee EnCEMrooordorewrl C Total SoLSuaourcrkccoeef Fit PTuPLouranrcaeeklEEEorrfrrrFoooirrrt 0MTMoa8atxx5al8RRESSrqqror 0.8758 GIITonneEterrNermrmcDceEeppRtt(F-M] YGERNSDCEHRE[MF-M) YRSCHEM SGoSEuoNrurcDceEe R GYERNSDCEHREM YRSCHEM ChRRoaamnneddaoolmmOSpSaeamrmapptlloeres Chemical Operators ISInnuPPOmOAAmAAapoprofpmFymit RRRSsSqqquuuaaarrreeeAdj Summary of Fit ROboRMRMsoSoeeeoqaartutnvnaaMMoroteefefisaRRoAnneendSsssSjqppquo(ouoannarrssSreeeeuEErmrrroWorerts) Observations(or Sum Wgts) OF AAnn'atSayusmsiosloofSfqVVuaarwnieaansnccoe Da2F2 Sum1o5f330S..1q6648u88a825r586e650s0 %44 46 1158.700124824855 18.702845 OF LaSLucamckkooiotfSFFqiitut aes D22iFs6 Sum o1ef22S3.3q62u911a29r365e15s9 "18 44 1520.13421298655 15.014285 00..111699077722211565 000o..6s513s865a400l179s524225 0.635094 47 MMeeamnnLSSq8auu2amr8ee 013.844143238 0.34123 MMeeaOmnamSsSqsauluaemrsee 00.142888919686 0.128998 FRSaaRabttiaeo PP05rr.0o4o0b0v8>4o0F7 0.0080 F3F7RAa8at4ti3oo PP03rr.0oo70nb82o>45FF3 0.0025 0E3Ess6tiim1msat6tse 00-.000303.5931210808926298813336 0.0090993 NNpaarnmTo 1[1I PPaarraaSmmUeeEttreeorrrEEssttiimmaatt(eeRssalo 000S.11t1d0244E02r026r65o33r t 3R22a0.t44i588o 00021 0.104425 0.00921 0% -3.05 0.99 OF EEfffeeccttSuTToemssottfSquares DF 1 Sum o3o3f.0xS17q700u00a0u88r33ee33s 1 0.3330469 P0rPobo>0bltli 0000..30008100736%19 0.3286 F9F2RR9aa0tii1oo 0970 9.2901 0.9760 L0oLwo0ew6rsr9595SS%% 00-0.0005.650852789757632379 -0.009463 P0Prr0oob0v>s%FF 03286 0.0039 0.3286 AApppappgeeenndd7iixx 1 I Page 7 U0Up4pp3ep6ra3r97o50s4%n 00-0.00.6.21310780763767812026949 0.0276616 SMMuaabddjeeecAAtvvataoiillPaarbbollteeebcbiyyv33eVMOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iid0dee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00226633 3MA10050696 3MA10050696 ChRReaamnneddaoolmmOSSpeaarmmapptlolrees: Chemical Operators IISnn uPPmFFmOOaSSrAAyAAofppFpoitmm RRRSSsqqquuuaaarrreee AG) Summary of Fit MRRRooSeooqatutnaMMroeefeaaRAnnedsSSjpqqouunaasrreee EErrrroorr OMbesaenrvoaftiRoensspo(onrseSum Wats) Observations(or Sum Wgts) 000.000399144788599399 011..-5"05473a7.01045s7585a535i87368 47 SoSMuoourdrecclee EEnCMroorodoerrwl C Total oF AAnnaaSlluyymssiiossiooSffaVVuaawrriieaasnnccee MemmSaume OaF33 Sum o1f101S161q0.1u162a206r090e955s7 Mean323S.07q706u006a606r985e8 443 110761.806760017 2.46665 46 117.18701 SoSLuaorcuckrceoef Fit PuTPLuoarruceelkEEorErfrrroFoorirrt [MTMoaatxxa4lRRESSraqror 0.9297 OF SLLuaaccmkkoooltfSFFiiqttams MemnSaare O4a1F2 Sum of97S78.q.828u202a33r377e334s Meana22S.n3q3i8u8a5s5r9e9e4 52 43 1100866..020646626003773 4.12116 GTITEInoneNteremDrmrcEceeRpptt(F-M] AYGYRGERSENSCDCHEHREE[MMF-M] AGE PPaarraammEeesttieenrraEEtssotti|immaatteesSsWE tRsio -OS5Es.7sa7t5il51ms6a67ts7e 01LS2.ti18dz20sE57sr5r6e6o3s5r t -R1s5ai5.t1ii71o o--000o0..400z44412e354s73353 0000..002028990777s86S53 --1111..1245927 0.0352765 0.029525 1.19 SGoSEuoruNcrDcseER AGYYGERRENSS.DCCEHHREEMM AGE Near OF EEffffeectSt TTuoemssottiSouwes Nparm DF [1I 1 1 1 Sum o6s6f.1S10eq011u5u5a00r8s4e33s 1[1I 1 1 se 5.0062176 3.5213341 F2F4RRaa7tli6oo 222L..004a927s39666 1.4276 F15RRa0at2io8o PP01rr.oo25bv0s>o2rF8 0.2274 F0F5RR7ast8ii9oo PP00rr.8oo50bw79>s85Fe9 0.8095 P<rPoroboo>b0Ialtlyl 0<00...l1026203l301S11 00.2136175 0.2387 P0Pr1ro2obb3>s1fF 00o0..11126n831s15 0.2387 PAAappgppeeenndd8iixx I1 Page 8 SMMuaabddjeeecAAtvvataoiillPaarbbollteeebcbiyyv33eMVOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00226644 3MA10050697 3MA10050697 SMooSuodruecrlece ErCEMrooordoraerll C Total SoLSuaocurkrcoceefFit TPPLouuatrrcaeeklEEoErrfmrrFoooirrrt 0MTMo6aat3xxa6lAR6ESSraqror 0.6366 `TTiiGonmeEtermeNrmrDcceEeppRtt(F-M) YRSCHEM GENDER[F-M) YRSCHEM SGoSEuoNurrcDceeER GYERNSDCHEERM YRSCHEM ChRReaamnneddaoolmmOSSpaaermmapptlloeers Chemical Operators iISnn uPPmFFmOOaSSrAAyRAofppFpoitmm RRRSSSqqquuuaarrreee Ady Summary of Fit RoMRReoSooqattunMaoMerfeeaRaneAndsSSJpqqouunaasrreec Eror Error OMbesaenrvoafcRoenssp(oonrsSeum Wars) Observations(or Sum Wgts) OF AAnnaSalluyymssiiossiooSffqVVuaaruriieaasnnccee D"F>2 Sum o1f0S729q..55u5809a799r646e110s p4s4 170.91.857870410 46 117.18701 OF LSaLuacmckokoiolfSqFFiiuttses D22i%Fs6 Sum 6of664S629q.59u997a90r730e36s68 "18 14029.359807004 44 109.58740 0000.020626134818535 0.0223.33 L"iasLe 1.578171 5 -4.4836 47 MeMaena3nS9Sq9uq9au8r1ee 23.4799096821 2.49062 MMeeamn2mS5Sq7uu6aa8rr2ee 22.3567661812 2.36611 44EEs8st6ii6mma3at7se --`0040..9044238s966565:43717 -0.022657 |PPaarSraaGmmEeetrteeorrrEEssttiimmaaRtteeasso 000S.23t38d382E831r80r10o454r t Ratio 11366 -11.69 004883 0.282119 0.024883 051 -1.56 -0.91 Npam OF EEfftfeecctStTTuoemssottiSquaes Nparm1[TEotnDF1 Sum 6o2Gf.0o0S0i4q8s5u6a3er43ie05ws9 1 1 2.0649335 PP<rro0bo>0blitll <000..310160627068514 0.3675 F2FRRaaattioo 02.8492714 0.8291 F1FR2Raa5tii6oo PP01rr2.oo52bb28o>58rF6 0.2288 F1F 0RR8aat9i1oo PP01rr4.o0o3b83v>9soF1 0.4335 LSoLwo2ewrr099515%% --051L0..027060G808S10141I613 -0.072806 PP0rr1oo2bb6s>4tF 00.31627654 0.3675 APAppappgeeennd9diixx 1 I Page 9 U3Uppp7pe3err91s5s3%w 000-..0312.2279791004333190036443 0.0274916 SMMuaabddjeeecAAtvvataoiillPaarbbollteeebcbiyyv33eVMOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iid0dee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00226655 3MA10050698 3MA10050698 GhaRRamanncddaoolmmOpSSeaarmmapptlloeers Chemical Operators `SIinnumMMm5Sa77r00yp5op0fmmFit RRReSqqquuuiaarrreee Ad) Summary of Fit MRRMORebSooeasoqoaetutnnravMoMoraeeffetRaaiRAennoedsnsSSjsppqqoo(uuonnaarssrrSeeeeuEEmrrrrWoorrets) Observations(or Sum Wgts) 000.011733666688204121 012L..I001070176716210202818 a -2.03122 47 SMoSouodurercclee ECMErrorrodooerrnl C Total OF AannaaSlluyymssiiosslooSffqVVuaarariieaasnnccee MemSaume DaF33 Sum o5f828S.73q305u515a555r5788e733s Mean2aTS.72q7mu58sa56ir19ee9 %43 46 65612l...0076s0004t15667117 1.22569 LaSSocouukrrocceefFit PLTPuuaorrcueeklEEoErrfmrrFoooirrrt 0TMMo9aat9xxa6lRR2ESSrqqror 0.9962 OF LLSaaucomkkooolffSFFqiittuaes MemmSaume D4a1F2 Sum o5Sf20aS.2q43mu72a2s1r398e52s Mean011S.12q217u706a981r8101e a2 43 2708577 0.232195 52.704577 0.11610 I`ITTnGneoEtereNmmrpDceEtpRt(F-M) AGYYGERRENSSDCCEHHREE[MMF-M) AGE PPaarraammEeesttieemrraEEissottii|mmaatteessSenor -701E0.s27t240i4m762at763e6 000S.t177d999E3r134r2s2o6r --`0000..002039384736853s82 0000..00012900078999912664 -0.001758 0.020812 t(RR2aat0io5o --1214..8149359 008 -1.83 -0.08 SGoSEuoNurrcDceeER AYGYGRERESNSCDCHEHEREMM AGE Nam OF EEfffiecctStTTueomssotiSqures Nparm1[TIo DF 1 S um of Squares aeooslss 2.7163591 11Lo I 1 ooosass 4.0909545 0.0087486 F2F2RRa1atii0oo 2303..023m013m67m72 0.0071 FR2Raaatomio PP20rr.0oo29bw73>s27eF4 0.0937 1F F0RRa2atii%oo 1PP10rr.0o0o8b2v6>3soF6 0.0865 PPr0roo0bv>3lots]l 0000..10104M43337T949 0933 0.0747 0.9331 PP0rr1obo4>bF 000o..901o7434r379 0.9331 AAPppappgeeenndd1ii0xx I1 Page 10 SMMuaabddjeeecAAtvvataoiillPaarbbollteeebcbiyyv33eMVOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00226666 3MA10050699 3MAII0050699 SMoSouodurerclcee CEEMrnoorodoreurl C Total LSaSoocuukrrcoceef Fit FPTLuuoasrcueeklEEorErfrrromFoeirrrt MT0Mao7atx1xa3lRA2EsSraqror 0.7132 TTIoneermrmeept Y`IGRGnEEtSeNNrCDDceEHEpRREt([MFF--MM]] YRSCHEM GSSEooNuurrDcceeER GYYERRNSSDCCHEHEREMM. GhRReamanendcdoaolmmOSpSaaamrmapptlloeers Chemical Operators SIInnuM8m577m00aopprfpommFyi RRSsqquuaarree Summary of Fit RSRRqoSoqutuaaMrreeeaAAnddSjjquare Error MORMeboeasoaentnrvoMoafeftRaiReonesnsSsppqofouonnarssreeSeuErmroWres) Observations(or Sum Wgts) OF AAnSanluymasoifslSooffyqVuVasaarrmiiiwaansnsccee D"F22 Sum o2f887S.31q34u346a6388r323e565s %44 46 61060161 52.713326 61.060161 OF LaLSaccukkmoooffiFFiiSttass D22iF6s Sum1o337f555S..1q11u499a990r2265e588s8 "18 44 2713326 17.514068 52.713326 000.011933766166599899 0112..0000939974404552546286 a -2.03123 47 MeMaenmWmSqSuuMarree 119803 4.17342 1.19803 MMeeamnnSSqsauuaemree 097300 1.35382 0.97300 Fa FRRaatiioo Pp30rr.0o4o3b8b9>3s4F6 0.0394 F1FR3Ras9tii1oo PP01rr.2oo33bv96>o15FF4 0.2365 AEEs7stii6mma7tae -1.767331 02973 -0.294733 0344 -0.039344 NNpaammnTo 11[I PaPraarmaSmeWetEtomeorrrEEssttiimmaaRtteeasso 000S.lt229d66sE66sr11r68o8s9r t -L6R6aS6.t6iI14o OIE 0.195665 0.017258 228 -1.51 -2.28 OFEfEfifcecttSTuTeomssottfSmuares DF 1 Sum o22sf.7S7nq11u8e8a3r22se99s0 1 6.2266074 PPr<oo0bb0s>0JltllI 0<00..00103902901511 0.0275 F2FR2Raa6tli0oo si 2.2690 5.1974 L2oLwo3ew0re3r999557%% --00020..6637801093207669587 -0.074125 P0rP.ro1ob3b9>s1FF oos 0.1391 0.0275 AAPppappgeeenndd1ii1xx I1 Page 11 UU1pp2ppee3rr0s98s56w4% 00-0.0100.99029934660500861163334 -0.004563 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00226677 3MA10050700 3MAII0050700 GhRfeaamnneddaoolmmOSSpaaemrmapptlloeers Chemical Operators I1SnunPmPFmFOaOrSSyAAoppfopFmmt RsRRSqSqquuuarrreee Ady Summary of Fit RoRRMoSoeqoatutnMaoMerefeaaRAnnedSsSjqpquouanarsreeeEErrorror OMbesaenrvoaftiRoensspo(onrsSeum Wes) Observations(or Sum Wgts) 0o0.o00i240062268872: 1-13.058.56607112188666667887 a -3.57167 47 MSoSooduuerrcclee ErECMrooordoraerll C Total DoFF3 AAnnSalsuymysoissiSooffquVVaaarrriaeansnccee MenSquae Sum of S6q2u5a6r5e7s 08s Mean Square 4ra3s3 11514456993..0201656816126569679 Sass 2.08552 3.46655 46 155.31826 SoSLuoarucrkcceoef Fi PLPTuuaorrcueeklEEoErrfrrorForoirrt 0TMMo9aat9xxa6lRR3ESrSqror 0.9763 OF SLLeaacsmkkoaoirfdFimtaes MemSqume DF a241 Sum o1af4sS35q.63u378a856r660e054s4 Mean Square SL50R0 3.54600 52 43 19906169 3.67565 149.06169 1.83782 TITneoermrmcept YGIGERnEtNSeNDrCDcEeEHpRREt([MFF-MM)] AGE YRSCHEM AGE PPaarraammEeestteearrtEEossttiimmaatteesSsWEmor (Rao -2o2E6.sw60t9in88m90as0t55e Std Error 1ox3m3s 1.334337 t Ratio 02080 -2.02 --o00o0..10z092w7731920801s15 0000..o033o33i052s381a14 --0o004e..659s89 -0.01721 0.035001 -0.49 SoSGuoEurNrccDeeER AYGYGRERSENSCDCHEHEREMM AGE Noam OF|EffefcecttSTTueemsstot.lSoares Nparm1TLoo DF 1 Sum o11Uf.2S2sq10u66ea60r2s4e45s 11[I 1 1 omsSI0: 1.5888669 0.8381204 Fao F Ratio 0310 0.3510 0s 0.4583 01s 0.2418 FFoeRaaotliieo PP00ro.6o6v1b0s7>15FF6 0.6175 FF1R9aa2t9oi5o Pp01r.4o90br20>96F5 0.4006 PPr0robo0>bI4tlI 0000..55054560967047 06284 0.5020 0.6254 PP0rr5oo5bb6>7eF 0000..36550520262s070 0.6254 AAPppappgeeenndd1ii2xx i1 Page 12 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbtyyiv33eMMOfrfoodrrerIInnIssnppeePccattiiioomnneaavrnn.dd3CCMoo,ppyyNoii.nngg2a-ass04CC-oonn6ff3ii0ddee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00226688 33MMAA1100005500770011 MoSSooduuerrclcee EnECMrooordoruerl! C Total LSoaSucoruckreocsefFit MTPPLTuouoaatrrucxaeelklREEoEESrrfrrrrqmroFoooirrrrt 05686 Max RSq 0.5686 TTIoenrmemcept Y`GIGRnEEtSeNNrCDDcEeHEpRREt([MFF--MM)] YRSCHEM SoGSuoEruNrccDeeER YGRESNCDHEERM YRSCHEM ChRReaamnneddaoolmmOSSpaaermmagptlloeers Chemical Operators SIInnuPPmFFmaOOrSSyAAoppfppFmmi. RRRSSsqqquuuaarrreee Adj Summary of Fit MORReMRbSooeasoqoaetnutrnavoMMroaefefetRaaiRAenonednssSSsjppqqofouuonnaarsrrsSeeceuEEmrrroWoreris) Observations (or Sum Wgts) OF AAnnaSalluyysmsiiosslooffSVVqaaurriwiaasnnccee D"F22 Sum o1f4S5S9q..au84i9a1s9r8a84e1s5s p4s4 114595.3819892861 46 155.31826 OF SLLuaomcckkoolotfSFFqiitut aes D22i%F6s Sum of682S278q.09u801a980r138e438s a18 44 11644799..808990998883113 00.00003308488898656 11-3.0885.540775017856596768 a -3.57167 47 MMeeamnn2SS3qauu0amr3ee 2S.a700698213 3.40681 MeMaenmSSSqaIuwarsree Imes 3.18813 3.72268 F0F RR7aatsioo PP00r.r.o75ob97>5t9F2 0.4579 FoFsRRsaateiidoo PPo0rr.oos8wb5s>s6eF4 0.6485 3EE3ss0ti6imm0aa7t8ee -CD-031O..913O891186N107S77334 -0.033553 NNpoaarmmTo 1vlo PPaarraaSmmUeeEttreeorrrEEssttiimmaaRtteaesso 0S0O3t.d94M9E4r85rE83o8r t 0-R77a6.t3i309o9 00.03299I9523 -0L.I6S0 0.029102 -1.15 OF EEtflfoeccttSTTuoemssottfSquares DF 1 Sum oa1Lf.sS22q2su88a9er40se7s0 1 4.5285163 P<rPoibb>0sIlt|l 0<00..250555055012212 0.2552 F0F3RR6aat0ii7oo La 0.3607 1.3293 L4oLwo2ewr0e9r7558%% --000408..938226213204170425588 -0.092205 P0Prsrosobbi>o2FF 0x 0.5512 0.2552 ArApappgpeeetnxd1li3ixx 1 I Page 13 U2Upppapelerir9as5lsd%x 000-.04242.6645s6108E190408117s89 0.0250987 SMMuaabddjeeecAAtvvataoiillPaarbbollteeebcbiyyv33eVMOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iid0dee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00226699 3MA10050702 3MA10050702 ChRReaamnneddaoolmmOSSpaaemmrapptlloeers Chemical Operators SIIunnmMwm85a55r66yppopof mmFit RRRSSSqqquuuaaarrreee Ad Summary of Fit RRMRSooeoqostutnaMoMreefeRaaAenndsSSjpqqouunaasrreee EErrrroorr OMbesaernvoaftiRoensspoonrseSum Wats) Observations(or Sum Wgts) 00o.016r26710o1294 011.3.10100602868281857173696 a -3.I2253 47 MSSoooudurerclcee ErECMrroroodoerrwl C Total DOFF5 AAnnSaSlsuuyymmsiososlf7ooSSff.aq6VVuu9aa3aarr3risa8eans5nsccoe MeMaenm2SSqa5uwaw6ree 4p%s33 5052723..86867679331300356681555 Lael 2.56446 1.22961 46 60.566451 SSLooauucrrkccoeef Fit PuPLTruaorceueklEEroErrfrromFoorirrt 0TMMo5aat9xxa7lRR3ESSraqr.or 0.9973 DOaFF SSLLuuaomcmkkoao5ofll2fSS7FFq1iiqutt0ua0ra2es7s MMeeamnm1SS2q5au5ua6mr1ee 241 2 550022...611776613330000063325887 008152 1.28561 0.08152 43 52.873065 GITEITnneoNteremDrmreEceeRpptt(F-M] AGYYGERRENSSDCCEHHREE[MMF-M] AGE PPaarraa2mmEE7eesatt6tmeei7rram8atEEt7ssoettii|mmaattee0sSsStmd9WE4rerEor t(R3Ra5ati1oo --D020..037a348107e98397182 00.0o.70192l941860s29343 --111347..579212 0004424 -0.03131 -0.004424 000846 0.02103 0.020846 021 -1.49 -0.21 GSSEoouNurrDcceeER AYGYRGERSENSCDCHEHEREMM AGE Npam DF EEfffeeccttSTuTeomssottfSquares Nparm1[Toa DF 1 Sum o32Jf.mS6asq36u8sa56r73ee60s4 11[I 1 1 o0ss96 2.7256630 0.0553796 FF29Ra5at9oi1o 2202..209215816960717 0.0450 FF20RAa8tsi5o PP20rr.1oo01bb86s>52FF6 0.1162 1F5FR7Ra7at0ii7oo 1PP05rr.0oo76bb71>o03FF7 0.0613 PP0rro0bo0>b1It1l] 0000..100040993126816 08329 0.1438 0.8329 PP0rr0oo9bv2>o6F 0000..8.103449232%986 0.8329 APApappgpeeenndd1ii4xx 1 I Page 14 SMMuaabddjeeecAAtvvataoiillPaarbbollteeebcbiyyv33eMVOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00227700 3MA10050703 3MA10050703 SMoSouodurercclee ErECMrroroodorerwl C Total LSaoSucourkrcoceefFit TPPLuouarruceeklEEoErrfnrrFoooirrrt T0MMo7aat3xxa2lSR9ESrqqror 0.7329 TITneoermrmcept IGYGnEERtNeNSrDDcCEeEHRpRt[E[1MF~-MM)} YRSCHEM GSSEoouuNrcDceeER GYERNSDCEHREM YRSCHEM `CRRhaaenmncddaoolmmOSSpaaemrmapptlloeers Chemical Operators SIIunnmMMm5sas5r86yppofopmmFit RRRSSsqqquuuaaurrreee Ad) Summary of Fit RRMRSooeqooatutnaMMoreefeaaRAnnedsSSjpqqouunaasrreee EErnroorr OOMbbessaeenrrvvoaafttiiRooennsssp(ooonrrsSeSuumm WWgatss)) OF AAnnaaSlluyyssmiiossSooffqVVuaarrreiaasnnccoe D"F22 Sum o72f.79S6.2q368u38a840r004e065s6 644 46 0566451 52.928445 60.566451 OF SLLuaaccmkkoooltfSFFiiattwss D22i%F6 Sum36o31f766S.5.q711u576a16r8622e205s0 w18 2169.21876484255 44 52.928445 0000.8.611522636181171 011..300019892666273757873)77 a -3.12253 47 MMeeaannSSSqa8uw9aarr0ee 12092 3.81900 1.20292 MeMaenaLmSqSauaausree 089871 1.41352 0.89871 F0FRr4aati8ioo Pp3orr.ooo1sbw7i>ss4FF.8 0.0515 FsFRRaastiioo Pp61rr.oo15bb7>o62rF8 0.1616 2EE9ss4ti6im5maa1ts7e --0020..3039443016725551937 -0.03379 NNpaarmmTo 11ro PPaarraaSmmWeeEttmeeorrrEEssttiimmaa(ttReessao 000S.2t206d66E667r7r33so11r t-111R117a0.t0i55o 00793 0.196063 0.017293 195 -1.74 -1.95 OF EEfffoeccttSTTueomssottiSquaes DF 1 Sum oa3Sf.esS6sqo4iu4m1as5ire6e0s5s 1 4.5927300 PP<rro0bo0>sl0t]ll <000..0000088S08818 0.0571 F3FR0Raa2tli9oo asi 3.0294 3.8180 LL3ooww4eer8r9d05s7%h --0030..07476838646036%79272 -0.068642 PPOrrooobmn>soF oon 0.0888 0.0571 APAppappgeeenndd1ii5xx I1 Page 15 UUp2ppp4ee0rrs899550/79 000-.0200.055413003886s89155)727 0.0010617 SMMuaabddjeeecAAtvvataoiillPaarbbollteeebcbiyyv33eMVOrffdoorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00227711 3MA10050704 3MAII0050704 PArAapapgpgpeeeenn1dd1iixx J AAppppeennddiixx J Regression of flRRuaaornnoddcoohemmmisscaaammlpplloeenccguuerrnrrdeeennrtt,jjoyoebbaeernnsggwiinnoeereekrre//dllaaibbncgghrreoomuuppic((annl==:22n33d))::age: followed by Regrrereesggsrrieeossnssiiooofnnfeelqquuuoaarttoiicoohnnemooiffcffallluuooonrroogccehhneedmmeiircc,aallyeooannrsggeewnnoddreekrredaanniddn cyyeheaaerrmssicwwaoolrr:kb:eenddd iainngecc;hhefemomiliclcaoallw::ed by SMMuaabddjeeecAAtvvataoiillPaarbbollteeecbbtyyiv33eMMOfrfodorrerIInnIssnppeePccattiiioomnneaavrnn.dd3CCMoo,ppyNyoii.nngg2-aa0ss4CC-oonn6ff3ii0ddee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00227722 3MA10050705 3MA10050705 SMoSouodurerclcee EmECMroorodorerul C Total LSoaSuocurkrccoeefFit PuPLTuraorcueeklEEorErfrnroFooirrrt 0TMMo9aat8xxa1lRR0ESSrqqror 0.9810 TTIoneermrmcept IGGYnEERteNNSrDDcCEeEHpRRtE([MFF--MM]] AGE. YRSCHEM AGE S`oSGuouErrcNcaDe ER GYAYGERRESNS.CDCHEHEREMM AGE RRaaEnnndgdomomemeSSraaimmappnllee Engineer/Lab RSquare SIiunnmPPmFFaOOrSSy ppofpoFmmit Summary of Fit RRRRSoSqoqqutuuaaaMrrreeeesAAndd)Sjquare Error ORMMboeesoaaetnrnvMooaefftRaiReonenssSsppqooounnarssreeSeuEmrroWrats) Observations(or Sum Wgts) OF AAnnSalauymisiosslooSffqVVauarariimaasnnccee IOtF33 Sum o1f994S..3q110u839a773r338e111s00 219 22 23496691 14.309381 23.496691 OF SLLuaacmckkooiolfSFFiqittuwes O11sF81 Sum o101f3.3S.48q846u662a267r716e6833s 1 19 114043..04394069336881118 000.32300911800400784 0000..89826693747888892428878 23 -0.93898 23 MMeeaann3SS0qauu6as0rr8oe 033 3.06244 0.75313 MeMaeonmSSrqauuasmree 046618 0.770154 0.446618 F1F0RRa0at6ii3oo PP40r.r0o0ob16v>67oF3 0.0217 FF1RR7aa2ttii4oo PP01r.r5o74bo23>4b8F4 0.5438 0EE6sstIii6mma2at6ee 0--00005..65641611676686262666 DOI 0.0467532 -0.031175 NNpaarmmTo 11[LIo 1 PPaarrSaaWmmEeertteeorrrEEssttiimmaattReeassto 011S.2t44d134E057r0r588o47r t-R020a4.t64i)23o 00o0..002o31M84E47r25H74 0-1216..226S22 0.047633 -0.65 OF EEfffloeccttSTuTeomssottiSquares OF 1 Sum o5SLf.IiS1Sdq5Iu1s6a6s00rs00e7o7s 1 1 oanels 1.1148580 0.3226016 PP0rro6obT>bl2lq 0000..020611377726002 056 0.2386 0.5206 F6F8RR4ast0ii3oo 601..18a4a48sm000333 0.4284 LoL6wo2ewr0er9495750/6%6 -3.620476 0OO4NESS -1.011148 00S -0.033675 -0.130872 PP0rr0oo1bv7>o0F 0000..252033218876660 0.5206 PAArpapapgpgeeeerni2d2diixx JJ U2pU3ppep8re6r9s85s8%w 20-0.0113.281176128211218838958 00682 0.1271809 0.0685214 MSMuaabddjeeecAAtvvataoiillPaarbbollteeebcbiyyv33eMVOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00227733 33MMAA1100005500770066 SMooSuodurerclcee EnCEMrooordoreurl C Total LSaSoocuukrrcoceefFi TPPLuouarrcueekEEEomrrfrroFooirrtr Total Error MoaxssAS Max RSq 0.8418 `TITIGonneEtrcreNrnmreDceeEppRet(F-M] YGRESNDCEHRE(MF-M] YRSCHEM SGoYGSEuoRENurSNrDccCDeeEEHRREM YRSCHEM RRaaEnnrddgoromomSoSaraimmappollee Engineer/Lab Rsqure SInnuPPFmFOOmSSapopofrpmFymi Summary of Fit RSRRRqoSSuoqqtauuaraMrereeeAaAnGdSjquare Ertor MReOMboeasoanetnroMvofeafRiaReonenssSsppqoo(unonasrsreeSeuEmrroWrats) Observations(or Sum Wgts) OF AAnSarluyamsiosloioffSyVVqaasrurimiiaasnncscee D22F2 Sum o1f854S.66q830u61a479r708e0838s 220 22 23496691 14.631983 23.496691 DO2FF LSSaLuucammckkooo1loft0fSS9FFwqii1utat3ar7re1es7s 01852 113302..76791311818322796618557 20 14.631983 00o.331s75702m07: 000..0883951535583309303%E: z -0.9389E MMeeaann4SSaq2uuaasrree one 4.43235 0.73160 MeMae0nm5nS0qSu9qa7ur6ee 00.49069847s6 0.464783 Estimate Estimate ASE -1538619 o5Te -0.537774 OE 0.0233371 NNpoaarmmTo 11no PaPraarSmaGemEtenoterorrEEssttiimmaatteResasio 0o0S.taZ2d7sEM1rs3rE7Eo8r t -R2S5a56.t6i817o 0OBIS 0.208582 0.013818 16 -2.58 1.69 ODFF EEfffleoccSttSTTuuoemmssttoodfisSSqduuiuaerresss 1 42.086837156858 I 2.0866755 P<rPoorb0o>0blloq 0<00..1000001008610 0.1068 Fra F Ratio ee 6.6473 282 2.8522 Fr60aR5att8ioso Pp60r.0oo00b58r>88F4 0.0088 FF19rRa3it6io8o PP01rr.7oo9bv35o>6sFF8 0.1735 LL-02oo2w19.ew1r070e9498r6599ss%9 000s -0.972865 -0.005487 PoPrrooobb>noFF 00.l001860 0.1068 PAAappgppeeendn3idxi3xJ Page 3 UU-00pp0pp1.9ee9r07r792s255ss36k%9 ooszlsie -0.102683 0.0521614 SMMuaabddjeeecAAtvvataoiillPaarbbollteeecbbtyyiv33eMMOfrfodorrerIInnIssnppeePccattiiioomnneaavrnn.dd3CCMoo,ppyNyoii.nngg2-aass04CC-oonn6ff3ii0ddee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00227744 33MMAA1100005500770077 MSoSooduurerclcee ErCEMrooordoraerll C Total LSoaSuocurkrccoeef Fit PLTPuuaorrcueeklEEoErrfrrrmFoooirrrt T0MMo3aat8xxa4l9RR.ESSrqqror 0.9849 I`ITTnnGeoterEemrmNrccDeeEppRtt(F-M) AYYGRGERSENSCDCHEHREE[MMF-M] AGE GSSEoouNurrDccEeeR AYGYGRERESNSCDCHEHEREMM AGE RRaaEnnnddgoonemmeSSraaimmappnllee Engineer/Lab SIIunnmPPmFHaHrSSy ppofppFmmi RRRSSsqqquuuaaarrreee Adj Summary of Fit MRRRSoeooqoatutnaMMroeefeaaRAnnedsSSjpqqouunaasrreee Eror Error OOMbbessaeernrvvoaafttiiRooennsssp(o(oonrrsSSeuumm Wes) Wgts) OF AAnnSaalluyymssiiosslooSffqVVuaarariwaansnccoe DF33 Sum o211f606S.35q372u73a639r971e106s6 219 2318.390206348760 22 38.300386 OD1FFs SSLLuuaammccokko2lofo0ffSS3FFaqi8iuutt8aa4re1es4s '18 1 220110..955327746888400473510664 19 2I.926470 00.0a432s371511323 12L0.o5.07137a7342722s511552 = -2.54721 23 MMeeaannSSSqaauwarsree Lis 5.45797 1.15402 MMeoaannLSSqqiuuaagrree 01.517806062 0.57806 FaRRaa8tioo Pp4r.ro07ob12b2>9ssF5 0.0125 FF2r0Re5ati1i7eo PP20rr.3o50ob05n>61oF07 0.5060 2EE4s6ts2i7maa1t6e 0--00207..574446611280870013556 00036 0.0546509 -0.030306 PPaarrSaaGmmEeemtteeorrrEEssttiimmaa(ttReessal 011S2.t677d75E668r4r3M4o77r t -R21a17.t3i399o9 0000..0002814695755866633777 -012L5..I171S59 0.058963 -0.51 Noam OF EEfcfetctSTTuoemsstot:lSeuaes Nparm1Tro oaDF1 Sum o8BIf.oS9msq8su5ola9Tr7ise1ss6 11Lo 1 1 olousss 1.5233215 0.3048564 PP0rro1bo>8olt7fl 0000..201061814117877 062 0.2648 0.6132 F77RRa8ati6oo 0711..2703682060260 0.2642 LLooGwweIerrE9d55S%% --201609..12W889I0800823)0S53 OUST -0.044908 -0.153717 PP0rr0oob1b>1eF 0000..62201661412487 0.6132 AAPppappgeeenndd4iixx J J Page 4 U1pUappsepsre4r90o5nss%w 01-0..0125.8514858245400409207757 00931054 0.1542097 0.0931054 SMMuaabddjeeecAAtvvataoiillPaarbbollteeebcbiyyv33eMVOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00227755 3MA10050708 3MA10050708 SMooSuodurerclcee ErCEMrroroodorerwl C Total LSaSoocuukrrcoceefFit TPLPouuatrrcaeeklEEoErrfnrroFooirrrt 0TMMo8aat9xxa8lAR3ESSrqqror 0.8943 TInToteemrrmcept `YGIGnREEtSeNNrDCDceEEHpRRtE([MFF--MM)] YRSCHEM SSGoouEurrNcceDe ER GYERSNCDHEERM YRSCHEM RRaaEnnngddioonmmooSSraaimmappnllee Engineer/Lab `IISnnuPPmFmFaHHrSSyppofppmmFt RRRSqSququauarareree Ag Summary of Fit RMRRooSeooqatutnaMoMreefeasRAnnedsSSjpqqouuraisrreee EErrrroorr OOMbbessaeenrrvvoaafttiiRooennsssp((ooonrsSSeuumm WWagttss)) or AAnn"alSayusmsiosiooSffqVVuaaarrriieaasnnccee D2F22 Sum o211f626S.03q061u69a390r025e50s9 220 2328.320301338266 22 38.300386 OF SLLuaamcckkooloffSFFeiitut ame D12F52 Sum o11f488S0.1q148u882a239r957e706s6 08 242.30148332560 20 22.231326 000.43416191595550:55= 011.2.035056594147353200018ES 3 -2.54721 23 MMeeamnaBSSoqquusawrsee 8L.I03S45T3 1.11157 MMeaamnm1SS5qau1ua9mr5ee 015.501650285 0.50604 F7F2RRaa8tii1oo Pp70rr.0o2o0b2b4>83s1F 0.0043 FR20Ra9at0oi3o PP02r.0ro96bo93>4b8F3 0.0638 SEEss3tiimm0autee 0--00370..73115388875897S89 0.0318879 NNpoaarmmTo [11I PPaa0rrSataS3dmmG4eeEEttr0Meeror7rorrEEssttiimmaaRttt0Reeaa0sstoiKo 0000..223055370740150300337 -10.04 2178 -2.79 0.017033 1.87 ODFF EEfffoecctStSTTuuoemmsstot:oBifSeSqqouugawrleeoss 1 83.s6o8s29s8s1T9 1 3.8959557 PP<roubb>0st1 00<0..00007015021912 0.0759 FaFRRlaatisioo 7s.s81o15 3.5049 LLoo4wwe0er%r9Sd65S3%% --011420..2500558466885826843 -0.003642 PPorroobo>nF 00.001712 0.0759 APAppappgeeenndd5iixx 3 J Page 5 U2pU6ppep6re1r90s53s4%k 0--00021..88167286I21220T773S554 0.0674175 SMMuaabddjeeecAAtvvataoiillPaarbbollteeebcbiyyv33eMVOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00227766 33MMAA1100005500770099 MoSSooduuerrlccee ECEMronrodooernl C Total SoSLuoarcukrccoeefFit TPLPouuanrrcaeeklEEoErrfmrrFoooirrrt 0MTMo9aat4xxa5lRR3EsSrqqror 0.9453 InTTteoerrmmcept YGIGnEERtNeNSrDDCcEeEHpRRtE((MFF--MM)) AGE YRSCHEM AGE SoGSuoEurNrccDeeER AGYYGERRENSSDCCEHHREEMM AGE FRaaEnnngddmoonmemaSSraiaLmmappbllee Engineer/Lab `SIInun mPPmOOaAArAAypGopDfMmFt RSReSqqquuuiarareree Ag Summary of Fit RoRMRoSeooqattunMaMoreefesaRAnnedsSSjpqqouunaasrreeeEErrrroorr OMbesaernvoaftiRoenssp(oonrsSeum Ws) Observations(or Sum Wgts) OF AAnnaSalluyymssioisslooSffqVVuaaarniwaasnnccee OF33 Sum o1f857S.42q436u413a170r730e308s0 219 2157.720643703088 22 25.704738 OF SLLuaeccmkkooollfSFFiiwttaws O11F8s| Sum o11f515S..8q385u0557a572r751e598s9 1 117.246037020488 19 17.263008 000.23322m28i-34n7111 000..312955253623113199791:14 2 -1-56791 21 MeMaenm2SS8qa0uwa9sr1ee 02.5801835981 0.90858 MeMaenmoSSaqsuwaasrne LOT 0.88081 1.4072 F3F0RRa9at7ii0oo PPo3rr.ooo0swb9io>7arF0 0.0514 F0F6RRa2st6ii0oo PP00rr.7o6o7b2s7>6e6F0 0.7776 LEE0sstti0amat8tee -1.020183 00606M% -0.663796 00271 0.0323327 -0.03271 PPaarrSaagmmEeemttoeorrrEEssttiamat(teRessao 011S.tS5d127eE62r92r55o33r t -20R0a86.t61i55o 0000..000294323250281077579 -2.81 0O6T0.77 0.052319 -0.63 Nam OF EEfffleccttSuTToemssottfSquares NparmT[1Eoa OF 1 Sum o7o7f.1sS19q9uu55a3s7r8es70s0 11roa11 03ssie 0.5331884 0.3551409 PoPrsroobb>sJftlJ 0000..4005512315112 0593 0.4531 0.5393 FF79Raa1tci%o 070o..53s9810s619 0.3901 L4oLw3oew1re9r92959S6%% --0140..I136510S79042H99726 023 -0.056007 -0.142213 PPorrooolbblo>lfF 0000..5404159s13311 0.5393 APAppappgeeenndd6iixx J 3 Page 6 U2Up2pp7pe8er9r90g59s1%n 20-0..012.2717087609072001999919 00.01726016973189 0.0767938 SMMuaabddjeeecAAtvvataoiillPaarbbollteeebcbiyyv33eMVOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00227777 3MA10050710 3MA10050710 SMaoSoduuecr!cee ECEMnroroodoerll C Total LaSSocouukrrccoeefFi TPPLuouarrcueekEEEorrmfroeFoirrrt MT0Mao8axt9xa8lRA4ESSrqQror 0.8984 GTIETInoneNteremDrmrcEceeRppt(t F-M) YGRESNCDHERE[MF-M] YRSCHEM SoGSuoEruNrcDceeER YGRESNCDHEERM YRSCHEM RRaaEnnndgdonoemmaSrSaiamlmpapdllee Engineer/lab ISInnuPPmOOAAmAAaoppfrppmFymi RRSSRqSqquuuaarrreeeAd) Summary of Fit RMRRoSoeoqoatutnaMoMreefeaaRAnnedsSSjpqqouunaasrreee Error Error OMbesaenrvoaftiRoenssp(oonrsSe m Wee) Observations(or Sum Wgts) oF AAnSalunymsiosaoloffSVVwaiararimiaassnnccee D2F22 Sum of88iS..q00su886a6i5r5s9e90s0 220 21577.60168713489 22 25.704738 OF SLLuaacmskkoaolftSFFiqituas D1rFn25 Sum o1If2s5S6.0q000u205a259r391e15s5 08 126.168121233 20 17.618149 000.233111461505959::` 000.9L9235348686509565:6-:, 2% -1.5679/- 2: MMeeanPnSquurasre 40.8084039219 0.88091 MMeaenm1SSqu2um5awr0ee 01.322550439 0.32653 Fra F Ratio Pp40rr.0oo52bb82o>99FF9 0.0229 FR3aR8tati9ioo PP30rr.0o8o3b2n2>9k6F7 0.0326 LEEOssFtiiTmmaUattSee -1.987348 O000G764 -0.638727 0.007764 MNpaarmmTo 11[I P|aPraarSmaWemEtemteeorrrEssttmiamia(etRessao Std Error 002297S8 0.297785 t -R266a16.ti697o7 00.02I2S8I8E7S9 -O2.S7I9 0.015163 0.51 DOFF EEflfeecctStSTTuueemmssottoGlfSeSeqiuuaalresess 1 1 owes 6.8604184 0.2309580 PPrr<oobOb>0aI0ltIlI <000..60001014301213 0.6142 F1FR7Rata9ioo 0x2 7.7879 0.2622 L2oL6woe0wr8e95r51S3S% --L0120..I13610Ee68e15s51S63 -0.023865 PPorroooibbn>e3F 0o.s0l11z3 0.6142 APAppappgeen7endidxiJxJ Page 7 UUppp1p3ee6rr 69S158%4% -1.366184 001610298 -0.161298 0.0393931 SMMuaabddjeeecAAtvvataoiillPaarbbollteeecbbtyyiv33eMMOfrfodorrerIInnIssnppeePccattiiioomnneaavrnn.dd3CCMoo,ppyNyoii.nngg2-aass04CC-oonn6ff3ii0ddee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00227788 33MMAA1100005500771111 SoSMuoourdrecclee ErECMrroroodorerul C Total SoLSuoiurcrkccoeefFit PLTPuuaorrcelekEEoErrfrrrmFoooirrrt T0MMo3aat9xxa9lRR7ESSraqror 0.9997 T`ITIoGnneEttmreeNmrrDcceeEppRtt(F-M) YGYARERGSNESCDCEHHREE[MMF-M] AGE GSSEoouNurrDcceeER YGYAREGRSENSCDCHEHEREMM AGE RRaaEnnngddnooemmerSSiaaLmmappbllee Engineer/Lab IISnnuPPmFFmOOaSSrAAyAAofpppFpmim. RRRSSqqquuuraaerree Adj Summary of Fit MRRReooSaooqtutnaMoMreefeRaaAenndsSSjpqqouunaasrreee Error Error OOMbbessaeenrrvvoaafttiiRooennsssp(ooonrrsSeSuumm WWgatts)) oF AAnnSaalluyymssioissiooSffqVVuaaarriimaasnnccoe 1D"F33 Sum o211f121S.83q866u63a637r719e933s3 219 22 432424..112003006446001663 DO1FFs SSLLuuaammcckoko3oloft2fSS2FqFqii2uutta8ar8me7ss 181t 330202..02021312332677812283667 19 32.236613 00.220661900511388 1L.3"0305.02221s05563631816 23 -5.2038 23 MMeeamnnSSS9qasuuiaw6re0e esses 3.95460 1.69666 MeMaenm1SSqa7uu0awr6ee 010..007119330771336 F2F3RRa3at0ti8oo PP02rr..o13ob03n>60e7F8 0.1067 13F0F4RRa2at1ii1oo 13PP00rr.0oo46vb28o>18F1F 0.0688 2EEss1tiimm6astse o--D020o..e717s047s20s25ii74ss85 010788 0.0668187 -0.107688 NNpoaarmm[a 11[Lao 1 PPaarraaSmmGeeEttreeorrrEEsstitmaa(stRe.asbo 202S.t031d552E39r396r83o64r t -R200a39.t9i99o9 0000..00037752167246379737573 -I121S..131I696 0.071495 -1.51 OF EEfcfetctSTTueomssottfSquaes DF 1 Sum o99f.mS66q9iu5s67at6ri1es4s 1 1 Saenz 2.2771575 3.8493437 Pr0Poob3>bli2tll 0000..203m6231m72034 Olds 0.2610 0.1484 FSFR7Raa1tli6oo 5211..2736241248I6 2.2688 L6oLw6oew5re0r95S585%6% --016L..e04645a550s15M98i26 025737 -0.053899 -0.257327 P0Pr0ro2obb7>s3FF 000..202l6a261s710s30 0.1484 APApappgpeeennd&diixx JJ Page 8 U2pU3pp6ep6rer09S05e1%n 20-.1003.8600169590533s86099219 000..001448117995553006552 SMMuaabddjeeecAAtvvataoiillPaarbbollteeebcbiyyv33eMVOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00227799 3MA10050712 3MA10050712 SVoSiuourerclcee EETMrnoordoouerll C Total SLaaSuocukcraceere PPMTTLuouoaratruecxaelklREEoEEErfrrnrqrFooeoirrrt 0M5a2x3R0Sq 0.5230 TGTInonEetmrNremrDcEgepRt(F.M) VRSCHEM GENDER[F-M) YRS CHEM SYoGGSuRoEEruSNNcrCDecDeEHERERM YRSCHEM RRaaEnnndgdonomem oSSraaimmappnllee Engineer/Lab Rsqure InSPPFuFOmOSSmAAaRAoprfpoFypmtm Summary of Fit RMRSRRReoqoSSoaoquqttuunaaaMorMrrfeeeeeRaaAeAnndsdSpSjqqouunaasrreee Eror Error OMeeranvaoifoRnessp(oonrsSeum Wee) Observatoifons(orAAnS"aulSnymusimWsiagooitffVsSVa)ioaruriieaasnsnccee D2F22 Sum36of085S.08q015u149a44r454e479s9 220 22 "346..00805490576 44.100406 DO2FF LSSLaumacmcokkaolIoftfSSFsFmqeiutaiamrsess 218:2 362210151..800053437582752231716 20 36.085957 0000L..1001a8998919a15797003s3.3:-i 1.34324' 52023 -5.2033 2.; MMeeamnWSSoqwurearnse 41.800075202 1.80430 MenSaae Mean Square 150 1.25402 260m 2.62972 FR2aR0aitmiao PP02rr.1oo23bv23o>06FF9 0.1346 Fra F Ratio 0am 0.4769 par Prob>F 08805 0.8805 Esme Estimate SIEGE -5.326428 O0Is -0.688015 00U0GE -0.014068 NNpoaarmmTo 1 1 P|aPraOarSSmtauAdmeEetETntreeorSrrorrEEssttiimmaatRtt1eReasa2st5oi0o 0.426179 00Q5I06L 0.327563 -12.50 026050 -2.10 0.021701 -0.65 ODFFEfEoffcectSSt TTuueemmnstoto9fi0SSqw0uaa3rme0ss 1o1a 7o.n9s60a0l38e0 0.7582318 Poblf Prob>ltl <I <.0001 00s 0.0486 0s 0.5242 FFardRaiatilco oan 4.4117 0.4202 Lowrssw Lower95% esssls -6.215415 A; -1.371293 oss -0.059334 PP0rroo0bv>ssFF ose 0.0486 0.5242 raAApgpppeeennd9idxi3xJ Page 9 Upperssk Upper 95% aaa -4.437441 oem -0.004736 sos 0.0311988 SMMuaabddjeeecAAtvvataoiillPaarbbollteeecbbtyyiv33eMMOfrfodorreIrnIsnIspnpePecactitiimooennrvaa.nndd3CC,ooppyNyoii.nnggC2aa-ss0CC4oo-nn6ff3iid0de9ennttiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00228800 33MMAA1100005500771133 SoSMuoorduerclcee EnCEMrooordorwerll C Total LSSoaouucrrkccoeef Fi PPLTuuaorrcueeklEEoErrfnroFooirrrt 0TMMo9aat9xxa4lRA6ESsrqaror 0.9946 TGIETIonneNtemreDrmreEceeRpp(ttF-M) AYGYGRERSENSCDCHEHREE[MMF-M] AGE SYoGSGRuoEESurNNrcCDcDeHeEERERM AGEYRSCHEM AGE RRaaEnnngddnooommorSStaaimmappollee Engineer/Lab RSquare `IiSnunmMNm5Sa77r00yppo0fpmmFt Summary of Fit RRRRoSSSoqqqtuuuaaaMrrreeeeaAAndd)Sjquare Eror MORMeboeasoaentnrvMooafeftRaiReonesnspSspoqoonunrsasreSeeuEmrrWorg) Observations(or Sum Wgts) of AAnn"alsSyuysmisoslooSffqVVuaaarnriaeansnccee D13F3 Sum o1f006S.78q758u5474a090r242e505s 219 1167.684817996460 22 17.641966 OF SLLuaacmskokolfaSFriatams 1D1sF81 Sum o1Tf06eS.07q791u91a17r749e9377s 11 106.808976914403 19 16.887940 00o..0100i482747:14 00-0.909.464122017788248313 23 -3.01612 23 MMeeaannaSSaqsuusairree 00.3258183492 0.888839 MMeeao0nnSS9qauumaarrgee 00.099362184738 0.096143 2EE0ss0ti4imm1aa2tt4ee -2.114124 0o2n4o -0.170074 002% 0.0257524 -0.033236 NNpoaarmmTo 11Po l |PPaarrSaadmmEeetmteeorrrEEssttiimmaattReessao Std Error oL0m3e6 1.559036 t -0R11a73.t3i366o 0000..00024354134773407662 -00006..667823 0.051747 -0.64 DOFF EEfffeecctStSTuTueemmssOottoifuSSamquueawresess 1 1oa 00oO..e34me3782oc23l44l66:62a48 l 0.36666114 PP0rroo1bb9>oI1it0il 000..0441S79@4M1690 00.5534446 0.5284 FR F Ratio 0s0.5314 0380s 0.3805 ods 0.4125 FoFRrmaateiioo PP0orr.oo2vbn8o>2rF8 0.8372 F9FR7Fa0tai%oo PP90rr.2oo74bv08>o31FF0 0.2481 Lowerds Lower 95% Sam -5.3772 ese -0.658377 06l2 -0.061622 01S -0.141543 PP0roobba>FF 0000..5s452k748i444s96 0.5284 AAPppappgeeenndd1i0ixx J Page 10 UUhpppaeper e9sr5ss% 1.1489527 0OI3LsS 0.3182297 00.01715301721688 0.0750714 MSMuaabddjeeecAAtvvataoiillPaarbbollteeecbbtyyiv33eMMOfrfodorrerIInnIssnppeePccattiiioomnneaavrnn.dd3CCMoo,ppyyNoii.nngg2a-ass04CC-oonn6ff3ii0ddee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00228811 33MMAA1100005500771144 MoSSdoouuerrclcee ErECMrroroodoerrwl C Total SLoaSuocurkrcoceefFic PTLBuuoasruceeklEEorErfrnroFooirrrt 0TMMo2aat8xxa5lSR9ESqrqror 0.4859 GITETInneNotereDrmmrcEceeRpptt(F-M] YRSCHEM GENDER[F-M] YRSCHEM SoSGuoEurNrccDeeER YGYRERNSSDCCEHHREEMM RRaaEnnngddiooncmmerSSiaaLmmappb.llee Engineer/Lab `SIinnumMMms5a77r00yppoppfmmFi RRRSSSqqquuuaaarrreee Ad) Summary of Fit MRRReoSoaoqotuntMaMoreefeaRaAnendsSSjpqquouanarsreee EErrrroorr OOMbbessaeenrrvvoaafttiiRooennsssp(o(oonrrsSSeuumm WWegttss)) OOFF2 AnAanSlaSlyuuysmmsiiososlof0oSfSf3aq8VVuu7aaaarr3riiw6eaas4snnccee 22220 1110777..263254853174693606602642 22 17.641966 OF SLLuaamcckkoolotfSFFqitut aws D1rFz28 Sum of839S.01q178u804a405r572e23s3 8 20 1725602 9.070079 17.254602 00".00020217195958:5: 00-0.90192.2086878185338::-` 2 -3.0161: 2: MMeeaomnnSSiqauuaemree 0860 0.193682 0.862730 MeMaenaenSsqSuaoaur:ee LIE 0.68204 1.13376 F0FR2Raa2tii8oo PP00r.5rc20bo20>4b9F5 0.8009 FoRReaatsioo PP00r.r7o6bo90>1b%F6 0.7939 0EEss9tti6mi8amtSae 0-00-01.31.7440498666S80052 0.0007884 NNpoaarmmTo 1 1 PPaarrSaaummEeettreeorrrEEssttiimmaaRtteeasso 000S.22t2d9694E546r60r99o577r t-1-0R0la6.0t5Si8I1o ' 00IS006 0.226505 0.015006 00S -0.64 0.05 OOFF EEfrfiecctSSt TuuToemmsst0ot:ol3fSS6qqu1uaa7ree4ss 1oa 00.030521861I774s9 1 0.00238175 PP<ruobb>0slt]l 0<00..59503005005%15 0.9586 LLBoowweegrr99l5S%% -03-00.067.0161115075073882 -0.030513 F0F4RRa0st7li6oo 00.04002786 0.0028 PP0rr5o3bo0>b5F 00.95538065 0.9586 AAPppappgeeenndd1ii1xx J J Page 11 U2pUppep4rer9og5S%w 000-.03233.2242778088287179521518 0.0326895 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbciyyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00228822 3MA10050715 3MA10050715 SoSMuoourdrecclee EECMrroTrodooerull C Total LSaSocouukrrcoceef Fit TPLPouuatrrcaeeklEEoErrfnrrFooeirrrt 0TMMo9aat9xxa5lRR0iESsrqaror 0.9950 TInToteemrrmcept `IGYGnERtENeSNrDcCDEeEHpRtREt(MFF-MM]l AGEYRSCHEM AGE `SSoGouEurrNccDaeER YYAGRGRESENSCDCHEHEREMM AGE RRaaEnnngddioonmmeaSSraaLmmappbllee Engineer/Lab SI1nunPmPFmFaOOrSSyAAoppfpoFmm1. RsRRqSSuqquuaaarrreee Ad) Summary of Fit MRRReoSoaoqontutaMMoreefeaRaAenndsSSjpqqouuanarsreeeEErrrroorr OOMbbessaeenrrvvoaafttiiRooennsssp(o(oonrrsSSeuumm WWegrtes)) OF AAnaSnluyamsioisiosoSffoVVuaaarriieaasnnccee DF33 Sum onf00S.sa8qd4u6m6a11r2a2e11s 219 22 73358 72.471423 73.317544 OF SLLuaacdmkeoooitfSFFiiqttams D11Fs81 Sum o77f202S.31q160u074a430r057e730s0 31 19 nan 0.367353 72.471423 010.030141151s:5.-31013..9910553333420050::: 2 -5.3932` 2-- MeMaenaanSSmqauouamrsee 03.821829094 3.81429 MeMaenm4SS0qa0uu5aa7re8e 4.600753758 0.36735 SOEEs8stiSimImaaEttTse -5.985167 O 00E 02 0.1760337 00% -0.001162 0.0171392 PPaarraaSmmGeertteeorrrEEssttiimmaa(ttReessao Std Error 0396a1S 3.229618 t -R101a8.t38iS65o 000O..004O88663742M79S87 -00000..1302626 0.107197 0.16 Nam OF|EEfffloeccttSTuTeomusottfSquares Mparm DF I To1 1 Sum000o.0sf5OS00q6I00uS3a31rE2eN33s 1 1 11oa ooonsosss 0.00158323 0.09750555 PP0roobb0>sli4tll 0000..797011879990774 0877 0.9840 0.8747 F0FRR1aat3lieo 000..o001o030s020e47 0.0256 FoFRRoaattmioo PP0orr.ooo0bom7>s32FF9 0.9732 1F0F9RRa0at8ii4oo 1p0r.o9v0o4r4 02315 Prob>F 0.2345 L2oLwo7ew4re4r9s75s5%% -12.74479 OO8IsSEU -0.835511 0207225 -0.182762 -0.207225 P0Pr7roo1bv9>o7FF 0000..9987188794070 0.8747 AAPppappgeeenndd1ii2xx JJ Page 12 UU0ppp7epre49r5ss% 001L.1.717i789472s54375s883312 02415031 0.1792383 0.2415031 MSMuaabddjeeecAAtvvataoiillPaarbbollteeebcbyiyv33eMVOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00228833 33MMAA1100005500771166 SaSMoouduecrlcee ECnEMroorodorerll C Total SLoaSuocurkrcoceefFi PPTLuuoarruceelkBEoErfrorrForoirrt 0TMMo8aet3xax8lR1sESrqqror 0.8381 TTIneoerrmmecpr GEYGInENRtNeDSrDECceERHpR(tE[FMF--MM)] YRSCHEM GSSooEuuNrrcDeER YGYERRNSSDCCEHHREEMM RRaaEnnndgdnooemmaSSraaimmappnllee Engineer/Lab SIInunPmPFmFaOOrSSyAAoppfopFmmi RRRSsSqqquuuaarrreee Ad Summary of Fit RMRRooSeooqattunaMMroeefeRaaeAnnsdSpSjqqouunaasrreee EErrroorr Onsrvaions or Sum Mean ofResponse Observations(or Sum WWgattss) of AAnnSalsuyymsisosiooffSVVuaaarriieaasnnccee D2F202 Sum o7f002.S577q654u886a96r121e95s 220 22 730754 72.568929 73.317544 OF SLLuaacmtciokclaoSftqFFuittares DF 212 Sum o61f010S.8q6@7u971a76%r32e009s0 08 20 2568929 11.871629 72.568929 0o0.00t1808o271" 11-5.909..0030440888384327!:'! 2 -5.3932! 2-- MMeeamnSoSaqmuuawaree 36s 0.37431 3.62845 MeMaeneSnSoqSuaiaulree 51.4085891s1 1.48395 FoRRoaatnioo Pp0or.soa1ab02r>3sF2 0.9025 F3FRRaaatiioo Ppo3rr0.o4oib0sb>82eF5 0.0452 SEEsTstitEmaaNtse 0OO-.5IO1.664I27S88IB93G89662 0.0111116 PPaarrSaaGmmeeEttmeerrrEEsstiimmaa(tteRessao 00S.Otd66ds0Ei04rs3rl66oe4r t -R909a0.3t0i65o6 0030774 0.464516 0.030774 03%0.35 0.36 Noam OF EEftfeecctSTTuoemssottiSquwes Nparm DF Tpo o 1 1 Sum of Squares O0ueansmio 0.44622510 1 1 0.47306076 PP<rooub>mIbltl 0<00..777022209098515 0.7218 FR F Ratio oi 0.1230 0134 0.1304 LLooGwweTrrio9es05e%% --o0060m..s870I03e609000s565l73 -0.053081 PP0ra7obb9s>sFF 0728 0.7295 0.7218 AAPppappgeeenndd1ii3xx JJ Page 13 U4pUpp3peer1r9d5ms%n 01i-.40s1.732l311837e5704s2352 0.0753039 MSMuaabddjeeecAAtvvataoiillPaarbbollteeecbbtyyiv33eMMOfrfodorrerIInnIssnppeePccattiiioomnneaavrnn.dd3CCMoo,ppyNyoii.nngg2a-ass04CC-oonn6ff3ii0ddee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00228844 33MMAA1100005500771177 SoSNououecrclee EECMronordeoaerrlt C Total suc Source Luck arr Lack ofFit [oe Pure Error Toul Ero Total Error Nor ASy Max RSq 0591 0.9991 TTneoermrmep GGYInEERtNNeSrDDCcEEeHpRREtI[MEF--MM)] AGEYRSCHEM AGE sGaESouNucrDceEe R AYGVGERRENSSDCCEHHREEMM AGE RRaaEnnddroommnSSaamelplee Engineer/Lab Rquare SI0nu4Mm5555m56asporiopFmmyt Summary of Fit RSRRRqSoSoqqutuuraaMrereee nAAdgSjquare Ener ORMMboeeosaatennroMoveffiaRRoneensssSppqoo(uonnarssreSeeuEmrroWree) Observations(or Sum Wgts) DoFr3 AHnaClSyuasmisooioffSsvaVaaurrsiaseansnccee Sum re of Squares 2139 2823181.6.511279689749290014668 22 29.362824 iDOsFF SLLiaucmckokoiefStFitatres Sum2owfiSmq2uairsets 1w81i 2820810..a901s277521917s556s15 19 28.197906 00367. 0.03967. 011190 -0.1119(. 125 1.218237. 4esoy -4 6503` ES2-- MeanSquwe Mean Square om 0.38831 Lis 1.484I0 Rao F Ratio 026s 0.2616 prove Prob>F ost 0.8521 MemmSwwe FR Mean Square LSS e076 1.56512 [re0d100 0.02575 F Ratio 60.7697 Prob>F 0.1006 Esme Estimate SBEID -5.844133 ONT -0.126807 008 -0.018287 onus 0.0342181 NNpoarmmTo 11[I 1 parameEsimates Parameter Estimates SoS (Rai Probl Sid Error t Ratio 01ST 2% 00 2.014541 -2.90 0s 0 oem 0.301466 -0.42 00H 03 omE 0.053943 -0.34 O0cess 0S 067 0.066866 0.51 Prob>ltl 0.0092 0.6787 0.7383 0.6147 Etec Tost Effect Test OF SmoSumes FAme DF Sum of Squares oasis 01 1 0.26258648 I 1 0.17056194 oa odes 0219 1 0.38865284 F Ratio 0.1769 0.1149 0.2619 Lowers Lower 95% D0 -10.06059 ore -0.757779 Onis -0.13119 ole -0.105734 pubr Prob>F oe 0.6787 Te) 0.7383 06 0.6147 AAPpaepgpeeendn1i4dxixJ Page 14 Upperssw Upper 95% reen -1.627679 oSses 0.5041648 oosseiss 0.0946I56 0a 0.1741698 MSMuaabddjeeecAAtvvoaaillaParbbollteeecbbtyyiv33eMMOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CC,ooppyNyoii.nnggC2aa-ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00228855 33MMAA1T00005500771188 MSoSooduurerclcee ECEMrorrodooerul C Total LSaSoocuukrrcoceef Fit TPLPuuoarruceelkEEroErrfnroFooirrrt T[MMoaatrxxalhFREsSraqror 0.4851 ITGITnneEotereNmtmrcDceEeppRtt(F-M] YRSCHEM GENDER[F-M] YRSCHEM GSSEoouNurrDcceEe R YGYRERSNSCDCHEHEREMM RRaaEnnnddgoonmemeSSraatmmappnllee Engineer/Lab SIIunnmMMm5SaS5r86yppofpommFit RRRSSqqquuuaaarrreee AG Summary of Fit RRMRoSoeoqoatutnaMoMreefeaaRAnnedsSSjpqqouunaasrreee Error Error OMbesaenrvoaftiRoenssp(oonrsSeum Weis) Observations(or Sum Wgts) OF AAnnaSalluyymssiicssiooSffqVVuaararieaansnccee D22F2 Sum o2f080S.75q778u7666a252r656e595s 220 2280.356826852549 22 29.362824 DO2FF SSLLuuaamccmkkooa1ofrt3fSS.FFq4iqiut6ua6ra6e0ss6 218H2 21115385..511481166996599655509363 20 28.586559 00.000022706044933277 1-14.0116.9905557055033497552 El -4.65037 23 MeMaenn0SSq3quu1aar3ee Lay 0.38813 1.42933 F0FRRaaatimioo Pp00rr.7oo26bb75>s10Fr5 0.7650 MeMeaannL SSqquuawr2 ee 0FF5 RRaattioo 188999 1.12222 1.88999 PP00r.r7o5bo99>3b%F8 0.7996 AEEsEstii3mmaa6tee 0--00041..015875301323034361714 0.0074147 NNpearmm[a 11[I PPaarraaSmmdeeEttreeorrrEEssttiimmaaRtteesa.so 00OS.2t3d9I7E19r38Er1o48r t-21R027a5.t07i24o 0093S 0.291545 0.019315 038 -0.52 0.38 DOFF EEftfeeccSSt uuTTeommss0ottoi3fS3Sqq0uu3aur5ee8ss 1 1 02106617 0.39380354 0.21064617 PP<rroObo0>bl0tlll 0<00.0766000055051414 0.7051 F0F2RR1aat5tisoo 01s 0.2755 0.1474 LLoSoww2eorr693558%% -05-00.06.N772E663T16110ss83 -0.032874 PP0rr6oob0>fsF 07051 0.6054 0.7051 AAPppappgeeenndd1ii5xx JJ Page 15 U4pUp0pep4ro1r91d52s6%w 000-.40a4.45s0547s117i11720m26 0.0477039 SMMuaabddjeeecAAtvvataoiillPaarbbollteeebcbiyyv33eMVOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00228866 3MA10050719 3MA10050719 AAfpprppieenntddiixx K Page 1 Appendix K RReeggrre"esessgiiroeonsnsooifofnfllucuaqAAorlulrolaoetppchaoaherrnetmtmiiioicccfciiaappflalaunnooottnnrccuuoggrreeerrnnheeddnneeettmrrj,ja,oolyybbeeoaccarnhrhsseegmmwweiioonccrrdaaekkllreeooddappneeiinrrmdaaccytthheooeearrmmrsssii(nccnwaaol=l=rankA1ne)d)d:d:aaiggneec::hffeoomllillcooawwleedd by by regression equation of fluorochemical on gender and years worked in chemical MSMuaabddjeeecAAtvvtaaoillPaarbboltleebcbyiyv33eMOfrfodorIenrIsnIspnpeePcctatilioomnneaarvnn.dd3CC,ooppNyyoii.nnggC2aa.ss0CC4oo.nn6ff3idd0ee9nnttiaall formation Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00287 3MM0050720 3MA10050720 MSooSoduurerclcee EnECMroorodorerul C Total SoSLoiuucrrkccoeafFit PPLTuuaorrcueeklEEorErfrrmoFooirrrt TM0Mo9aat6xxa6lRR1ESSrqqror 0.9661 IGnITETeneNotrremDcmreEcepRptt(F-M] YAGYRGERSENSCDCEHHREE[MMF-M] AGE SY`oGSRGuoESuErNrcNCcDeDeHEEERRM AGE YRSCHEM AGE hoAAmlil cPPaaarlrtsiOccpipepraaannttssors Chemical Operators SIIunn mPPmFFaOOrSSy ppofpomFmit RsRRqSSuqquuaaarrreee Ad) Summary of Fit RRMOMRoboSeeosoqaaettunnravoMMorafeefetRaaiRAenonedsnSsSjspqpqouo(unoanarssrreSeeeEuErmrrroWorrets) Observations(or Sum Wgts) oF nAnaSailueymsiiossiooSffqVVuaaarriieaasnnccee DF33 Sum o2f440S.84q450u030a019r986e613s4 &60 63 29250145 24.853181 29.254145 OF SLLuaaccmkkooiotfSFFqiiutt aes ED5lF73 Sum o22f330S.89q869u611a156r534e357s5 3 60 22040..889559331116884117 000..11150570094363919 0000..63164004372359520698919 6 0.392284 64 MeMaennLSSqqauusairsee oat 1.46699 0.41422 MeMaeanmSiqSuaagree 033058 0.418623 0.330549 0EC0so6tii2mm6aa3ts3e 0-00O02..I502T6052L046446366134 0000079 0.0171146 -0.000079 NNpearamTo 1L1Looa 1 |PPaarrSaaGmmEeetmteeorrrEEssttiimmaaRitoeasso 00S.04t4d100E901r962r6o171r t R200a4.t11i066o 000.000.011100016409225872 -21L0..054sI50 0.010698 -0.01 DDFF|EEfffteeccttSSTuTueommssotto2if3SS9qq0uua0ar9ee9ss 1 1 020o..093099s03003025m2279709 1 0.0000227 PP0rro8bo7>bl6tl7l 0000..10082117696%747 0% 0.1267 0.9941 F7FRRaa0tiioo 5202..3037897180110 0.0001 F3FRR5aatt6ioo PP30rr.0o5w1b4s9>1E8F6 0.0198 FF1RR2aa6t6oi4o PP01r..ro42bo96>56bF34 0.4953 -o0ow7vee4rr1998550%%8 --000040..574094541904083032585 -00QI4TE -0.004992 -0.021478 P0rP0ro1obb9>s4FF 0000..19102921669s774 0.9941 AAPppappgeeenndd2iixx KK Page 2 U0pU8pp6ep6re6r97s54s3%w 00-0.0008.64026146152789494333 0021319 0.0392214 0.0213193 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbciyyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00228888 33MMAA1100005500772211 MSoSooduuerrclcee EnCEMroorTdoroerult C Total LSaSoocuukrrcoceefFit TPLPuoaurrcueeklEEoErrfnrrFoooirrrt TM0Mo6aat9xax1lR8RESrSqror 0.6918 `ITTIGnneotEeremrNmrcDceeEppRtt(F-M) YGRESNCDEHRE[MF-M] YRSCHEM SSGooEuuNrcsDeER YRSCHEM GENDER YRSCHEM CheaAmlnlicPpaaarrltiOicpcpieparanantttossrs Chemical Operators SIInnuPmPFmFOaOSrSdayfloppfpoFmmt RSRRqSSuqqauuuarrreee Adj Summary of Fit RRRMooSeooqattunaMMoreefeaaRAnnedsSSjpqqouuraairreee EErrrroorr OMbesaenrvoaftiRoensspoonrsSeum Was) Observations(or Sum Wgts) oF AAnnaSalluyymssiiossiooSffqvVuaaarriimaasnnccee D6F22 Sum o2f434.S.84q450u0300a299r044e114s 61 63 20250145 24.853204 29.254145 OF SLLuaamcckkoolotfSFFqiitut aws 3D330F1 Sum o11f05sS..1q885u330a881r128e840s0 630 20853200 9.015024 24.853204 61 000.111255200544833488 0000..636139328282323508082424 o 0.392284 64 MeMaena2nS2qSu0ua0sr0ee 20.420004437 0.40743 MeMaenomSSsqauluaaroee 0300501 0.510909 0.300501 00EEs9st8ii2mma4at8ee 0-0.0020.0552790508052566447383 0.017067 NNpaarmmTo 1l[I |PPaarSraaWmmEeetmteorrrEEssttiimmaa(ttReessao Std Error 0O.2I61E8 0.132618 t R002a.t444i4s5o 000912 0.10288 0.008912 192 -2.44 1.92 DOFF EEfffteocctStSTuuTeommssottoi2fS4Sq1quu6aar9ree3ss 1 1 Leases 2.4162931 1.4943613 PP0rro6ob8>vi3ot5]l 0000..00606150873285 0.0602 F5FR9Raa3tii6oo le" 5.9306 3.6678 F5F4RR0aat0ii9oo PP50rr.0o4o0b0b6>0e5F9 0.0069 F1F7RRa0at0ii2oo PP01rr.0oa77bb04>o08FF2 0.0748 LL0oo2wwe0er8r9395652%% --000040..5042605065272365665352 -0.000753 P0rP0roo1bb7>s8Ff 0062 0.0178 0.0602 AAPppappgeeenndd3iixx KK Page 3 UpU0pp3epre0r91d5s2%w 000-0.303.42008548048618822 0.0348868 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00228899 3MA10050722 3MA10050722 `APApappgpeeennd4diixx KK Page 4 SMoSouodurercclee ErCEMrroroodorerll C Total SoSLuoaurckrccoeef Fit LTPPuaourrcueeklEEoErrfrnrFoooirrrt Total Error MaexyRS Max RSq 0.9842 GTIETInenNoteremDrmrEcceeRppt(tF-M) AGYYGERRENSSDCCEHHREE(MMF-M) AGE S`oSGuoEurrNccDaeER YGYARERGSNSECDCHEHEREMM AGE `ChAAlenlmPcpaaarlrtiiOccppieparanantttssors Chemical Operators SIiunnmPPmFEaHHrSSy ppofopFmmi RsRRqSSqquuuaaarrreec Ad Summary of Fit RMoRRMOebSooeasqoateutnnravMMoroaeefeftaRaiRAenonedsnsSSsjppqqo(ouunonaarssrreSeeeEuErmrrrooWrreis) Observations(or Sum Wgts) OF AAnnaaSlluyymssiiossiooSffaVVuaaarriieaasnnccee OF33 Sum o211f747S.56q698u967a796r618e847s7 66ky03 2.594602 24.896914 42.594602 OO5FF SSLLuuacmmckokoo2lofl2fSSF2Fqqit3uuta5ar5ee7ss 5373 22040...686279723633393551557477 60 24.896914 0004s31185s64i2096116 00o"..6163a248d346i0126566s456 o -1.23054 64 MeMaenmSeSoSqauuamree 041095 5.89923 0.41495 MeMaeanmSSeqauuassree onus 0.424975 0.224452 AEEsTsttiEmmaaRtee 0--D010..437I8720018O8239682 000737 0.0480263 -0.005737 |PPaarrSaaammEeerttmaeorrrEEssttiimmaa(ttReessao 000S.t414d000E238r3l6r1oe24r t -R434a5.t22i5o8 000..00010110M014O7036066I712 -04435..335s445 0.010707 -0.54 Nparn OF EEfffteccttSTTueomssottlSquaes Nparrn1TLo oOlF1 Sum of Squares S78a2g%e 5.2393846 11Lo 1 1 onos 7.8221792 0.1191450 PP<rro0ob0>bI0etl]l 0<0..<0000000000007l17 090 <.0001 0.5940 eFFsRRaateiioo 11lo28a..s68sz25I61060 0.2871 1F 2FRR1aa6tii8oo 1PP<4rr.ooo2obv10o>6lFF8 <.0001 F1FR8Raa9tii%oo PP01rr3.oo83b9w5>3F3F4 0.3353 LLoo2wwe5er2r9695658%% 0-000-S.225.997550929560961334 002715 0.0259001 -0.027155 PP0rr0o0bo0>b7F <0<0..05000009000l017 0.5940 U0pUpp9epre1r97s5s1%w --0000.O..1T1960612I270S0182843S34 001S6s 0.0701525 0.01568 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbciyyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00229900 33MMAA1100005500772233 SMooSuodruerclcee ErCEMrooordowerrll C Total SoLSuaoucrrkccoeefFit TPPLuouarurceelkEEErorrfnroFoorirrt MT0Mao3axt0xa6lR8R.ESSrqqror 0.8068 ITTneoermrmcept YIGGRnEEtSNeNrCDDcEHeEpRREt([MFF--MM)] YRSCHEM S`oSGouEurrNcDseER `YGYRERSNSCDCHEHEREMM `ChAAellml PcPaaarnltciOcppiaepnraantttssors: Chemical Operators I`InnSPPuFFmHMmSSoappfprpFmmyi RSRRqSsququuaaarrreeeAdj Summary of Fit RRRMooSeooqatutnaMMroeefeaaRAnnedsSSjpqqouunaasrreee EErrrroorr ObOMsbeseaernrvvoaafitioRonensssp((ooornrsSSeuumm WWgetss)) OF AAn`alSnyusmiossofoffSVeVtaaurraiamaynsnccee DolF22 Sum25o11f077S1.5q576u780a85r550e429s2 @61 63 2594602 25.016059 42.594602 OF SLLuaacmckokolfoSFFliuittams 3D330F1 Sum o11f656S.27q738u805a509r969e909s9 6o3l10 225580..10216360000556990 000.31492136246939484 010.02.36369443000483334989 o -1.23054 64 MeMeamnsSSaqauuaamrree 04100 8.78927 0.41010 MeMaesnnaSSlqaauuamar:ee 0274335 0.541484 0.274335 2FR1R4aa0tii0o 2Pp<1rr.0o4o0b30b2>1s1F <.0001 FR1R9aa7t3oi8o PP01rr0.oo93b7o2>3f9F8 0.0329 SEE8ssttii1mmaa9ttee 0-10.-0u9032.S753T17669Ss53 0.0445754 NNppaarrrnnTo 1P1o PPaarrSaaGmmeEetrteeorrrEEssttiimmaaRtteeasso 0O0S.1tL1d032EN3r01r?5o72r t-113R44a64.t4i577o 0008 0.103217 0.008941 499 -3.65 4.99 OF EEtflfcecttSTTueemssottlSquaes DF 1 Sum o1f5S0S.a0q4s9u5e5a6s7r55te37es6 1 10.193737 PrP<oob0b>0sl0itIll 0<0.<.000000000005l15 <.0001 LoL2wo0ew9rer09d4557%% 000205..6518896219782954357 11.0266973 1F3F3RRa0st5ii4oo 248568 13.3054 24.8568 PP0rr0oo0bb0>SeF <0001 0.0005 <.0001 Appendix K Page 5 Appendix Page 5 K U1pUpp6eerr99o5s19%6 0--0010.6..7162075409151103035558 0.0624535 MSMuaabddjeeecAAtvvataoiillPaarbbollteeebcbyiyv33eMVOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppNyyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00229911 3MA10050724 3MA10050724 SMooSoudurerclcee ErECMroTordoorerull C Total LSaoScuourkrcoceefFit PPTLuuaorrcelekEEoErrfnrrFoooirrrt M0TMo9aat8xxa0lRR7ESSrqqror 0.9807 TIToneermrmcept `IYGGnEREteNNSrDDcCeEEHpRRtE([MFF--MM]] AGE YRSCHEM AGE SGoSEuouNrrcDceeER YAGYGRERESNS.CDCHEHEREMM AGE CheAAlmliPPcaaarrltiiOccpipeparanantttssors Chemical Operators SI1unnmPPmOOaAArARy ppofpoFmmt RRRSSSqqquuuiaarrreee Af) Summary of Fit RMRRooSeoqoatutnaMMroeeefaaRAnnedsSSjpqqouunaasrreee EErrrroorr Observations (or Sum Mean of Response Observations (or Sum Wats) Wgts) OF AAnnSaalluyymssiiosslooSffqVVuaaarriimaasnnccee [DF 53 Sum o1f559S.23q221u15a440r335e997s6 60 63 20530453 19.325057 24.539453 OF SLLuaaccmkkoooiftSFFiiqttues ED5lF73 Sum o11f088S.48q875u531a191r150e070s0 3 60 19325057 0.473957 19.325057 o00m.22i112t204s99 0000..365161767437551522215355 o 0.614523 64 MMeeaann1SSaquu8aarroe 0328 1.73813 0.32208 MMeeaa0nn3SS0qquu7aa2rr1ee 00.13530078261 0.157986 F5F3RR9aat6ii5oo Pr50r.o0o30wb92>6s4F5 0.0024 F2F0RAaa9ttii%oo PP20rr.3o0o0b9v0>3e9F4 0.3009 04EE3sts0i6mma3te7e 00-0.0034.1133573100326222321557 000028 0.0150521 -0.004228 PPaarSraUammEeortteoorrEEssttiimaRmtaea.so 000S.3t03d5954EI44r4%r44oS88r t 3R1a14.t22i13o3 0000..00000908914779443S55 -3.41 0S4e51.54 0.009433 -0.45 Noam OF|EEftfieccttSTuToemssott.fSquares Nparm1T[Io DF 1 Sum of Squares o3z7mseamy 3.7378707 11Loa11 006T0Is 0.7683549 0.0647015 PPr0ou2b2>bI2t]3J 0000...00210202121724 06556 0.1277 0.6556 nFFeRRasattisoo 12201..23360880055s963 0.2009 L0oLwo2ew1re9r999559%% --000040..9420797M710A194432339 002097 -0.004442 -0.023097 PoPrrooobb>osFf 000o..610p520571m672 0.6556 AAPpappgpeeennd6diixx K K Page 6 UpUIpp1epsra6ro9so56s%ln 1-0.00.1.0141M262s909363S0601S77 006A 0.0345458 0.0146413 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00229922 33MMAA1100005500772255 SMoSouodurercclee ErECMrroroodoerrul C Total SLSoaouucrrkccoeef Fit pPLTuuaorrcueeklEEorEffrmfoFooirrrt 0TMvo3aot1xxa5lRS0ESraqror 0.8150 TITIGnneEottrNeemmrrDccEeepRptt(F-M) YRSCHEM GENDER[F-Ml YRSCHEM SGoSEuoNurrcDceeER YYGRRESNSCDCHEHEREMM CheAAlmtliPcPaaarrltsiOccipipeparananittssors Chemical Operators SIIunnmPPmOOaArAAy ppoofpmFm.it RRRSsqqquuuaaarrreee Ad Summary of Fit RRRMSooeqooauttnaMMoreefeRsaAeondsSSjpqqouunaasrreee EErrrroorr OMObbessaeenrrvvoaafttiiRooennsssp(o(oonrrsSeSuumm WWegttss)) OF AAnnaaSlluyymssiiossiooSffeVVuaairriimaasnnccee D6F22 Sum o1f559S.3q1184u399a9766r599e855s 6&1 1290.533899475538 63 24.539453 DO3FF SSLLuuaammcckokoaLioftfeSSFFsqqiiuiutaoirenesss 333a10 114449..535848440909373365870809 61 19.389758 000.122800399988455734 000o..5516t6833i3779s994a557 6 0.614523 64 MeMaenm2SSq5auu8aar5ee 20.3517748865 0.31786 MMeeam0nnaSSqqmuu0aarrree 00.I4S79I0M162 0.151346 F8F1RR0aat0ii4oo PP80rr.0o1o0b0v0>0o8F4 0.0008 FR3R1aa6toi0o PP03rr.0oo10bw61>s51eF0 0.0011 02Ess8ti2i4mma7ut9e 00-0.0032.283157170274399791779 0.0125091 PPaarrSaaWmmEeemtteeorrrEEssttiimmaaRtteeasso 000S.t101d170E7r181r3o878r t 3R22a.t444i55o ome 0.090872 0.007871 159 -3.49 1.59 Nam DF EEfffteeccttSTuTeemssottlSquares Nparm1TLo oaDF1 Sum o3Sof.ES8Uq7sEu7a8Tsr7I1eS8s 1 1 0.8027714 PP0rro0bo1>bI7t1ll 000o..0u0001T00702019 0.1172 1F2F1RRa9at9ii7oo ass 12.1997 2.5255 -o0ow0veSerrH9IS5SS2%% 0-00.0400.954039920913110501626 -0.003231 PP0rr0o0bo0>b9F om 0.0009 0.1172 AAPppappgeeenndd7iixx KK Page 7 U0pU5pp2ep1ro4r98s50s%6w 00-0-0.05.12123135458686808s886 0.0282488 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggCa2a.ss0CC4oo-nn6ffi3idd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00229933 3MA10050726 3MAII0050726 SMoSouodruerclcee EECMrmoTrdoooerrull C Total SoSLoauucrrkccoefaFit PTPLuouarurceelkEEorErfrmroFooirrrt TM0Mo5aat0xxa2lRR5ESSrqqror 0.9025 I`nITTGnteoEtererNmmrcDceeEppRtt(F-M) GYYAEGRRNESSDCCEHHREE(MMF-M) AGE S`oSGuoEurrNccDeeER YAGYRGERSENSCDCHEHEREMM AGE GhAAelml ePPaaarlrtiiOccppieparanantttssors Chemical Operators IISnnPuPFmFOOmSSaAArAAoyfppFpoimm RsRRqSSqquuuuaarreee AY Summary of Fit RRRMSooeqooatutnaMMoreefesaRAnnedsSSjpqqouunaasrreee EErrrroorr OMbesaenrvoaftiRoensspoonrseSum Wats) Observations(or Sum Wgis) OF AAnnaSalyuysmsiiossiooSffqVVuaarariieaasnnccee DF33 Sum o11f154S406q.55u63a580r806e025s2 60 63 111656505...15183880666757 OF SLLuaamcckkooiotfSFFuiitat mws D55F73 Sum o11f313S464q.1u240a245r488e823s3 33 60 11515060..551330005668552 000.000868838717373525 011.4.50528488333691993734323 6 -4.28694 64 MeMaenmaSgSqsaueau0rlee 422..585080868808414 MMeeaann2SSq3quu8aarr3ee 53661 2.35833 5.36861 SEEssDtimmBaatee -5-000..25055222818752173 omen -0.04353 0.0265422 PPaarraSamdmeEetmteoorrEEssttiimmaaRtteeass l 000S.2t9d5986E96r22r14o48r t -RS25a30.t3i131o 0000..0o20252e677R611198949 --112L6..o060l30 0.026328 1.01 Np DF EEflfeeccttSTTueomusottlSquaes Nparm1[1I 1DF1 Sum o1lfs0oS.q33au5sa22r2e9e96s6 11[I 1 1 asi9ls 6.426227 2.549914 PP<rro0bo>0bltIll 0<O0..00014046046717 000..313111747484 FR4R1aa6toi3o 422l..so516l62le16as43 1.0164 F FRoRaaatrtisoo PPo1ra.os9ob4>e7FF5 0.1316 F0FR4Raa3tii3oo PP00r.3oa41b30F>96F3 0.9106 LL7oow2ewre39r560s/6 --L017O0..02M933S941I56970S354 O06 -0.097936 -0.026121 PP0rioo0bv>s7FF 00o0..10l3144lm687 0.3174 AAPppappgeeenndd8iixx K K Page 8 UUpp2pp2ee7rr94d50s93w6 0--00030.1.0020707874979065628443 00.00719028075535 0.0792053 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggCa2a.ss0CC4oo-nn6ffi3idd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00229944 3MA10050727 3MAII0050727 MSSoooduurercclee EnECMroTordoorerull C Total SoSLuoaurcrkccoeefFit PTPLuouarurceelkEEoErrfnrroFooirrrt 0TMMo5aat8xxa5lRR8ESSraqror 0.5858 InTTteoerrmmcept Y`IGRGnEtESeNNrCDDceEHEpRRtE([MFF--MM)] YRSCHEM SGoSEouNurrcDceeER GYYERRNSSDCCEHHREEMM GhAAoltml cPPaaarlnticOcppieapranantttssors Chemical Operators IISnn uPPmFFmOOaSSrAAyAAofpppFpimm.. RSRRqSqquuuaaarrreee Ad) Summary of Fit RRRMooSeoqoatutnaMMoreefeRaaAenndsSSjpqqouuanarsreee EErrrroorr OMObbessaeenrrvvoaafttiiRooennsssp(o(oonrrsSeSuumm WWegitss)) OF AAnnaSlauyimsiossfooSffqVVuaaarnisaansnccee O6F212 Sum o1f151S232q.01u180a008r881e160s0 61 63 111656535...101888808665776 OF SLLuaaccmkkoooftfSFFiiuttaws O333F1 Sum6o8f88S444q.16u669a60r078e860s0 63o1l0 11655833..040818090575666 00o.00a77t3229s999 011"..52058848424619104144656 6 -4.28694 64 MMeeaannbSSoqqsuuiaa0rrsee 250952 6.05405 2.50952 MeMaean2nSSq7qu3uaar9ee 228066 2.73099 2.28066 FR24Ra1at2oi4o PP20rr.0o4o5b1v8>21oF4 0.0981 F1FR1ra9at7ii5oo Pp01rr.3oo11bv91e>77rF5 0.3117 4EE3ss1ti2im3maa0to0e --000440..94355915206037706664 -0.027566 NNpaarmmTo 11[I PaPar0rSSatadmdm3EeeEtmt9rerooror1rEEss-ttiim3maat(tt1RReeassat0ioo 00.00.3022259S51233T34 -1-113129..915440 0.022117 -1.25 OOFFEEfffteoccSttSTuTueommsuotooffaSSvqqruuasaroeelss 1 1 mobi 9.4347501 3.8984466 PP<rroObo0>bl0tIll 0<00.02010035S007T411 0.2174 F3FR7Ra9tai6oo LSS 3.7596 1.5535 LLoowAwesr99rM5SSS% -04-.109.070M000554M664!49 -0.071792 PP0rro0obos>fF 0214 0.0571 0.2174 A`PApappgpeeennd9diixx KK Page 9 UUpp-p3eperse9arl5ss%s 000-.0300I.1l6S554644s861s85sl19 0.0166594 MMSuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggCa2a.ss0CC4oo-nn6ffi3idd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00229955 3MA10050728 3MA10050728 SMoSouodurerclcee EnCEMroorodorerwl C Total SLoaSuocutkrccooef Fic PuPTLouratrceaeklEEorErfrnrFoocirrrt TM0Mo9aat9xxa6lRR2ESSraqror 0.9962 TTInoeermrmeept GIGYnEERtNeNSrDDcCEeEHpRRtE((MFF--MM)) AGE YRSCHEM AGE SSGooEuuNrccDoeER GYYAERcRNESSDCCEHHEREMM AGE CheAAlmlliPcPaaarlrtiiGccpipepaarnnattossrs Chemical Operators SIIunnmMMm55a77r00yppopof mmFit RSRRqSSuqquuaaarrreee Adj Summary of Fit RRRMooSeoqoatutnaMMoreefeRaaAenndsSjSpqqouunaasrreee EErrrroorr OOMbbessaeenrrvvoaafttiiRooennsssp(o(oonrrsSeSuumm WWagttss)) DOFF3 AnnSaa'luSsyumsimioso1floo4SffS8qeVV2uaau3arra0rii1weaa5snnsccee 6@30 77915540...244853323003766019915055 63 90.253710 OF SLLuaamcckkooloffSFFqiittuams D557F73 Sum o77f505S.30q048u864a433r335e596s6 3 60 7530695 0.346339 75.430695 000.111662242233177 0L.1L1o.221s220e41422s94 tg -1.9.1564 64 MMeeaannGSSoqqsuuaairr0ee 411..292545717101880 MeMaena3SnqS1ua2aur7ee OLS 1.31727 0.11545 (EE2sst0timm4aat6ee --0`10o..3023823020T44I947669 0012026 -0.038776 -0.012926 |PPaarrSaaammEeettmeeorrrEEssttiimmaaRtteeassl 000S.lt77da00lE00er27rs7o2s2r t-R111a78.t7i525o 000..o001o18l191S8226s556a43 --02120..608112 0.018637 -0.69 NNpeaarrmTo DOFF EEfffleocctStSTuTueommssottoaifiSSeqqluuaoarneesss 11I [I 11 540S..01609691000017707039 1 1 0.6047597 PPr0ro0bo>8blt0ll 0000..0000477836s990 0406 0.0485 0.4906 F3FR3Rata8ioo 4300..40368501906080 0.4810 F3F 9RRa3at0ii2oo Pp30rr.0oo91bv32>s06rF2 0.0126 aF FRRaistiioo 1PP01rr.0o4o3b1v3>0osF2 0.0335 -o2owv6ee2rr39S150%/96 --00020..6667923328H139899 0050205 -0.077289 -0.050205 P0Prr0oob1b>s9FF 0000..40005447083s659 0.4906 A`PApappgpeeennd2di0ixx xK Page 10 U0pU1pp7ep8re3r90g56s%5w 0000..01007308203382086s61352 002033 -0.000263 0.0243533 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggCa2a.ss0CC4oo-nn6ffi3idd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00229966 3MA10050729 3MA10050729 SMoSouodurercclee ErECMroorodoreral C Total SoSLoauucrrkccoefaFit PTPLuouarurceelkEEoErrfrmroFooirrrt 0TMMo5aat8xxa6lRR0ESSrqqror 0.5860 I`nITTGtneoEtererNmmrcDceeEppRtt(F-M) YRSCHEM GENDER[F-M] YRSCHEM GSSEoouNurrcDceeER GYYERRNSSDCCEHHREEMM CheAAmllil cPPaaarlrtiOipcceippraaanntttossrs Chemical Operators ISInnuMMm5577m00agpofrppmmFyit RRRSSqqquuuaaarrreee Af) Summary of Fit MRRReooSaoqotnutaMMoreefeRaaAenndsSSjpqqouunaasrreee EErrrroorr MObesaenrvoaftiRoensspo(onrseSum Wats) Observations(or Sum Wgts) OF AAnaSnluymasiosliooSffyqVVuaasraniawiansncscoe Ool2F2 Sum o71Lf46aS.02q231u158a812r2555e555s &61 63 90253710 76.035455 90.253710 OF SLLuaacmckokoffoSFFtiiuttams O33nF1 Sum3o338f876S.3q666u678a731r305e005s0 63o1t0 76035455 37.368155 76.035455 000..111525797595313757 01.1L91.i2419t1596e614s156 o -1.94564 64 MeMaeanTnSSqiauuaewree 71.210096183 1.24648 MMeeamnn1SSq2quu4aa7rr3ee 126561 1.24733 1.24561 F5FR7Raa0tii3oo Pp50rr.0oo70bb05>o34FF3 0.0054 F1FR0Raa0tiiioo PP01rr4.oo09bv09>o13Fr4 0.4993 LEEsEsttiSmmaaTtoe --3010..2036486330524s37554 -0.04655 NNppaorrmnTo 11Lo PaPraaramSmoWetEtmoeorrrEEssttiimma(atoRessai 000S.2t21d330E199r9r6s6o84r t -R717a92.t2i18o4 O0ISSST 0.179949 0.015587 299 -1.91 -2.99' DFEMElfofeccttSTTueomssottlSquaes OF 1 Su m of Squares wasuasd 4.534934 1 11.117067 PPr<roObo0>bl0t1ll 0<00..0000060641011212 0.0041 FR3Ra6atmtio 89m 3.6382 8.9187 LL2ooww0eer3r9135SS%% --0O02..O771T040T343I030I616S656 -0.077719 PP0rr0oo6bb1>e2F 000 0.0612 0.0041 `APApappgpeeennd1di1ixx KK Page 11 U-pUpplep2rolr96956sR%t 00-0.0101.012661155693965532332 -0.015382 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggCa2a.ss0CC4oo-nn6ffi3idd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00229977 3MA10050730 3MA10050730 SMoSouodurerccloe ErECMrroTrodoorerlu C Total LSaSoocuukrrcoceefFit TPLPouuaurrceelkEEoErrfmrrFoooirrrt 0TMMo9aat8xxa2lRR3ESSrqqror 0.9823 T`ITIoGneEntrmeNemrDcpeEptRt(F-M] GYYAERRGNSESDCCEHHREE[MMF-M] AGE SGoSEuoNurrcDceeER YGYARERGSNSECDCHEHEREMM AGE ChoAAlmllePPaaarlntiOicpcpieparanantttossrs Chemical Operators I1SnunPmPFmFaOOrSSyAAoppfpoFimmt RSRRqSqquuuauarrreee Ad) Summary of Fit RRRMoSoeoqoatutnaMMroeeefaaRAnnedsSSjpqqouunaasrreee EErrrroorr OMObbessaeenrrvvoaafttiiRooennsssp((ooonrrsSeSuumm WWagttss)) OF AAnnaaSlluyymssiiossiooSffaVVuaaarrieaansnccoe DF33 Sum21ofLS770q.98u98a185r553e336s6 &60 63 219.0668 211.08153 219.06689 DO5FF7 SSLLuuaammcc2kko0oioof7lfSS2FFqqii0utut2awr3ee1ss 5373 212017330..3828701792952323133 60 211.08153 000.00033166144755322 -011"..83087817561561764734 6 -3.8617 64 MMeeamnn2SS6qau6ua1ar5ee 23.5616810739 3.51803 MeMaenmSSSqequusairsee 129308 3.63513 1.29308 FF0R7Raa5ti6io6o PP00r.5oa72b52r>69F6 0.5229 FaFRRsaatitioo PP20rr.2oo81bw14s>18eF2 0.2148 BEEOsstiiEmmaaRtse -3.083552 DDo9e6l2 -0.119692 00S -0.028921 -0.01353 PPaarraaSmmGeeEttreerorrEEssttiimmaa(tteRessao 01SL.t31d0I7E31r47Tr3o44r t -R202a6.t36i303o 0000..000333022130287078684 --0000..45933090 0.031176 -0.43 Noam OF EEffffeeccttSTTueomssttoiSwaws Nparm1[Lao DF 1 Sum o0O2f.8s5S34qa65u8a1s0r69eE07s 11Loa11 Oge2ses 2.8366160 0.6625603 PPr0ou0b>b0Itl8l 00O0..6S0391I58018 066s 0.3728 0.6659 FFouRRastctio 0000..8118085068563313 0.1883 LLSooww4eer r6995S0%% --0005..70742279763357361719 007SER -0.093347 -0.075892 PP0rr6oobsb>tFF 0000..636369778528918 0.6659 `APApappgpeeennd1di2ixx KK Page 12 U0pUp7pep4ra0r95s53s5%n 000-.0404.83878584110044346636059 00882 0.0355046 0.0488322 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggCa2a.ss0CC4oo-nn6ffi3idd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00229988 3MA10050731 3MA10050731 AAPppappgeeenndd1ii3xx KK Page 13 SMoSouodurercclee EECMrrorodooerul C Total SLoaSuocurkrcoceefFit TPPLuouarurceelkEEoErrfrnroFoorirrt Tw0Mo9aat8xxa2lRR3EsSrqqror 0.9823 TITeneermrmcept `IYGGnEREteNNSrDDcCeEEHpRRtE([MFF--MM)] AGE YRSCHEM AGE SSaGouEucNrecDeER YAGYRGERSENSCDCHEHEREMM AGE CheAAmlliPcPaaarrltiOiccppieparanantitossrs Chemical Operators SI1nunPmPFmFOaOrSSyAAgopfppFmmi RRRSSSqqquuuaaarrreee Ag Summary of Fit MRReRSooaqoontutaMMoreefeaaRAnnedsSSjpqqouunaasrreee EErrroorr OOMbbessaeenrrvvoaafttiiRooennsssp(o(oonrrsSSeuumm VWleWtgtss)) OF AAnnaaSlluyymssiiossiooSffqVVuaaarrieaansnccoe DF33 Sum21of1S720q.98u961a85r553e336s6 &60 63 21906689 211.08153 219.06689 OF SLLuaaccmkkooollfSFFiiuttams D55F73 Sum2o20f077S32.q520u70a292r323e131s "630 2211131..008887119552333 000.0003316614575232 -101.3.8808771655116677843 o -3.8617 64 MeMaenm2mS6qSu6aa1wr0ee 351805 2.66179 3.51803 MeMaenam3SSqq6uuae3ree 129308 3.63513 1.29308 F0F3RR3aat6io6o PP00rr.5oo7bv25>o60Fr6 0.5229 FaRRsaatkiieo Pp20rr.2oo8bb11>o18rF2 0.2148 GEEOssttiEmiamStae --000301..018981392656152922 00S) -0.028921 -0.01353 PPaarrSaaGmmEeetrteeorrrEEssttiimmaa(tteAess.so 01LS.t31dI07E1r74Er38o4r t Ratio 02633 -2.63 000O..00323022O328007884 --000049..933009 0.031176 -0.43 Nam OF EEflfeeccttSuTToemssottiSquares Nparm1TLo oaDF1 Sum o052f.855S34q665u068a150r69e707s 11[a 1 1 oeesen 2.8366160 0.6625603 PP0rou0b>b0Ilt8l 0000..63605921501818 0669 0.3728 0.6659 FF01Ra5at5oi1o 0000..811805806568313 0.1883 LLSooww4eerr69d5S7%% --000570..77492253763547361719 00S -0.093347 -0.075892 PP0rr9oobb5s>1FF 0000..363676792529818 0.6659 UpU0pp7ep4re0r99d53s5%w 000-.0404.3s875s845l100434e636s59 00am 0.0355046 0.0488322 MSMuaabddjeeecAAtvvataoiillPaarbbollteeebcbyiyv33eMVOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00229999 33MMAA1100005500773322 MSoSooduurerclcee EMECrroTrodoorerull C Total SLaoSocuukrrocsefFit TPLPuuaorrcueeklEEoErrfnrrFoooirrrt T0MMo5aat2xxa4lAR0ESSrqqror 0.5240 TTInoeermrmcept Y`GIRnGEtSENeNrCDcDEeHEpRREt[IMFF:-MM)) YRSCHEM SGoSEuoNurrcDceEe R YGYRERNSSDCCEHHREEMM CheAAlmllePcPaaarrltiiOccppieparanantttssors Chemical Operators IiSnnuPPmFmFOaOrSSyAAoppfppFmmi RRRSSSqqquuuaaarrreee Ad Summary of Fit RRRMSooeqooatutnaMMoreefeaaRAnnedSsSjqpquouanarsreeeEErrrroorr OOMbbessaeenrrvvoaafttiiRooennsssp(ooonrrsSeSuumm WWagttss)) OF AAnnaSalluyymssiiosslooSffqVVuaaarriieaasnnccee Dol2F2 Sum o2f0S771q.37u320a224r280e809s0 &61 63 21506689 211.74409 219.06689 OF SLLuaamcckkolooftSFFeiittuaws D303F1 Sum1o101f070S7.4q.42u467a6494r646e181s 630 61 20174409 104.27948 211.74409 000.000303313474232767 0.1130.8808616637311317226 6 -3.8617 64 MeMoaann3SS6qau6uaa1rr0eo 31 3.66140 3.47121 MeMeaanmSSSqaquusawrkee 347598 3.46660 3.47598 F1FR0Ras5tii8oo PP01r.o3o08bo58>4f5F8 0.3545 F0RR9a9ati7oo PP00r.r3o9o0b9m3>7r7F3 0.5037 3EE5sst6ii2mma9at8ee --0030..1153363732000946i948 -0.037059 NNpaarmmTo 11ro |PPaarSraWammEetmtoeorrrEEssttiimmaaRtteeasso 000S.t33d008E27r099r9o46r t -R099a4.t22i40o0 002012 0.300294 0.026012 42 -0.44 -1.42 OF EEfffteeccttSTTueomsuottfSqures DF 1 Sum o007f.06S66sq85Iu173a636r080e858s 1 7.0457385 PP<rrooobb>0olftlll 0<00..610650599093313 0.1593 LoLw4oew3re09rl55s%% -04-0.003.0737737303153252 -0.089073 F0F1RRa9at6li3oo 2098 0.1963 2.0298 P0Pr6roo5bb9>s3FF 00.16559933 0.1593 AAPppappgeeenndd1ii4xx K K Page 14 U2pUpp7peor8r98d5s9%w 00o-.204.d67178e48439r22922 0.0149549 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggCa2a.ss0CC4oo-nn6ffi3idd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00330000 3MA10050733 3MA10050733 SMoSouodurercclee ErECMrroroodorerul C Total LSoaSuocurkrccoaefFit PLPTuuaorrcueeklEEoErrfrnrFoooirrrt TM0Moaa9txxa7lRR4ESSrqqror 0.9974 IT`nTIGtnoeEterermNmrcDceeEppRtt(F-M) GAYYEGRRNESSD.CCEHHREE[MMF-M] AGE SSGoouEurNrccDeeER YGYARERGSENSCDCHEHEREMM AGE ChAAeltml ePPaaarlrtiiOccpipeparanantttssors Chemical Operators `IISnnuMMmms5as5r66yppopfommFt RRRSSqqquuuaaarrreee Adj Summary of Fit RRRMSooeoqoatutnaMMoreefeaaRAnnedsSSjpqqouunaasrreee EErrrroorr OMObbessaeenrrvvoaafttiiRooennsssp((ooonrrsSeSuumm Wes) Wgts) OF AAnnaSalluyymssiiossiooSffqVVuaaarriieaasnnccee DF33 Sum o610f052S.58q29u280a024r427e206s0 &60 63 75 872896 65.590476 75.872896 DD5FF SSLLuuaammcckok6ooio5flfS3SFqq9Fiiuu6tta8ur8ee1ss 5373 65500...153199993063548597896166 60 65.590476 0o0.0193s5252's_9"8_ 0.3110.00901242525595d558 pH -3.10248 64 MMeeamnnS SSqouuamra ee wFFs RRaatiioo 10937 3.42747 1.09317 PP30rr.0o1o3b3s1>5e5F3 0.0319 MeMaenmLSSqaauaulree 006is3 1.14731 0.06453 1F 0RRa7ati%oo 1Po7Pr.roo7ob7b>m9sFr0 0.0177 27EEs6st5ii8mma7at3se -2-00.07.03636560682927883 0-00.60I3S0339 -0.006153 NNppaarmmTo 11[[EIa 1 PPaarraaSmmGeeEttmeeorrrEEssttiimmaaRtteeasso S0td1006E.69r6r535o393r t 4R42a.20t2i464o 000.000.0111176999753S49 --10213..616569 0.017379 -0.35 OFE|fEifofeccttSTTueomssottiSquares DF 1 Sum of Squares SJiimes 5.1113761 1 1 ois: 3.1321284 0.1370284 PP<rouOb0>b0lltIl <000..0000903M5046716 0725 0.0957 0.7245 F4FRR1aati7ioo 422o..868s7665s5272 0.1253 LLooww0e7er29r0s56n%8 -4000.0.0067706525301061418 -O0.00W6I63l064 -0.040916 P0Prr0oob3o>s6FF 000o..0m008a93554s776 0.7245 AArppapgpeeenndd1ii5xx xK Page 15 Up-Up1pe4p5re9r96s57s%9w --0001..0004205779846s47s89 00.000.220880665005992993 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOrffodorrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggCa2a.ss0CC4oo-nn6ffi3idd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00330011 3MA10050734 3MAII0050734 SMooSuodurerclcee CEEMrmoorodoarerll C Total SoLSuoaurcrkccoeef Fit PPTLuuaorrcueeklEEoErrfrrrmFoooirrrt 0TMMo6aat1xxa9lRR9ESSrqqror 0.6199 TITnoeermrmeept IGGYnEERteNNSrDDcCeEEHpRRtE((MFF-MM)) YRSCHEM SSGoouEurNrccDeeER GYYERRNSSDCCHEHEREMM CheAAlmilePPcaaarrltiiOccppieparanantttssors Chemical Operators S1Iu0nmMMm55a55r56yppofppmmFit RRRsSSqqquuuaaarrreee Ad) Summary of Fit RRMRooSeooqatutnaMMoreefeaaRAnnedsSSjpqqouunaaserr.ee EErrroorr OOMbbessaeernrvvoaafttiiRooennsssp((ooonrrsSSeuumm WWagttss)) OF AAnnSaluaymssioslooSffqVVuaairriiwaasnnccee DoF22 Sum1o610f501S.74q125u47a5353r909e151s 61 63 75 872896 65.727505 75.872896 OF SLLuaamcckokoiolfSFFqikut aes D3331F Sum o32Sf68eS.8q8s08u4a2s5r92ae81s 630 61 65727505 28.842984 65.727505 0o0.110i35337e1136 01L3...10o10305s82304s12873 6 -3.10248 64 MeMaenasnSqSouaauoree 51.007725700 1.07750 MeMaenmLiSgSqauuawree 01.9168194832 0.96143 FR4R7aa0toi7o PP40rr.o07ob0b>27eF8 0.0126 F1FR2Raa3tii%oo PP01rr.2o23ab30>7F7F6 0.2807 2EEss9tiimma0attee -2.983898 000339M1 -0.372352 -0.034091 |PPaarScaUammEeertteoorrEEssttiimmaa(ttAoessmo 000S.t221d51E656r66r16o88r -t112R33a28.t8i314o 001492 0.167307 0.014492 235 -2.23 -2.35 Npam DF EEfffieocctSTTueomssttofSquas NparmTr1o oaDF1 Sum o5S5f.3oS3q36gu69a9u6r6e3y3s3 l 1 5.9624437 PP<roo0bb0>s0lltIll 0<00..00000291098918 0.0219 FFaRasatseio 45.5953361 5.5336 LLowoAewarsIr9S95i5e%% --00307..0074660163599100057844 -0.06307 PP0rr0oob9v>8oF 0o.0o2m98 0.0219 AAPppappgeeenndd1ii6xx K K Page 16 U2pUpp5epr2or96s5s0%k -020-."00505.5002133617742882 -0.005112 MSMuaabddjeeecAAtvvataoiillPaarbbollteeebcbyiyv33eMVOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppNyyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00330022 3MA10050735 3MA10050735 AAPppappgeeenndd1iixx LL Page 1 AAppppeennddiixx LL Regression equaAAtllillopnpaaorrtftiifccliiuppaaonnrttoccchuuerrrmreienncttaljjooobbneegnneggniidnneeeree.rr//ylleaaabbrsggrrwooouurppk((ennd==i:n,c77))h::emical and age: Reffgoorllellsooswwieeoddnbbeyyqurraeetggirroeenssssoiifoonnfleeuqqouuraaottciihooennmooiffcaffllluuooonrroogccehhneedmmeiircc.aaylleoaornnsggweeonnrddkeeerrdaaninndd cyyheeeaamrrisscwwaoolrrakkneedddaiignne. cchheemmiiccaall SMMuaabddjeeecAAtvvaatoiillPaarbbollteeebbciyyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00330033 3MA10050736 3MA10050736 MSooSudourerclcee CEMErorordooaerrll C Total SLSooauucrrkeconefFit PPLTuuaorrcueeklEEorErfrmroFooirrrt T0MMo3aat8xxa7lRR8ESSraqror 0.9878 I`nTTIGneeoEtrremNcmrDeceEppRtt[F:M) YGAYREGRSNESCD.CHEHREE[MMF-M) AGE SSGooEuuNrecDneER GYAYGERRENSSCDCHEHEREMM AGE AAElulnpgPaairnrteiiaccripipaLaannbtss Engineer/Lab SIIunnmPPmFFaOOrSSy ppofopmFmit RRRSSSqqquuuaaarrreee Ad) Summary of Fit ORRMMRboSoeesqooaaetutnnravMMrooaeefeftaaiRRAonneednssSSjsppqqooouurnraasserrSe.eeuEEmrrrrooWrrs) Observations(or Sum Wgts) OF AAnnaSalluyyssmiisos oofffSVVaaanruainasnccoe. D5F33 Sum o21Tf4s4S..7q111u66a373r6685e508s8 333 36 6635438 22.471780 36.635438 OF SLLuaacmskkooollfSFFiiqttuas D3EFY2i Sum o2nf20oS.4q04su26a5i6r11ee68s2 3331 2.1780 0.446618 22.471780 000.333838606686141181 0000..59832234550022830043558 -0.94033 37 MMeeaanwnSSqwunaarree 040..667882001992662 MMeeaaonneSSsqquumaasrrsee 000..446448668662118886 FeFRFoaatinioo PP60r.0ro90bo31>3b0F2 0.0010 FFLRasaitolilo PPo1rr.os5ob4v>s1oF1 0.5735 2EE0ss7tii1mm3aut2se 0--o002a..I40k837z4412s3384%e62 0046474 0.0189436 0.0146474 PPaarraaSmmGeeEttmeeorrrEEssttiimmaaRtteeasso S0O0t.Bdl8SEe5Or0srI1o2S8r t -R222a4.t64i4o4 0000..00102262615149664092322 -0002..58865772 0.026443 0.55 Noam OF EEfflfoeccttSTTueomssottlSauwes Nparm DF I To1 1 Sum o4odf.sS6ieq6ou6lea2sr6Tme7es9 11Loa11 0089349 0.5193576 0.2089349 PP0ruo0bb0>El8a 0000..300018L2305334 058M 0.3888 0.5834 F6FRR3aat8lioo 0600..377806656221857 0.3068 L3oLwo8ewr0e9r0533%% --O03O0..T78SM7011BI80I13SS55 OO0MIS2 -0.025188 -0.039152 P0rP0roob1b>s3FF 0000..38308818x83883 0.5834 APApappgpeeenndd2iixx LL Page 2 U0pUpp3eora4r91s5e6%x 0--00000..6039394076175765547379 000..000666383440447665553 SMMuaabddjeeecAAtvvataoiillPaarbbollteeebcbiyyv33eMVOrffdoorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00330044 3MA10050737 3MA10050737 SMooSuodurerclcee EEnCMroTrodooerrull C Total SoSLuoaurcrkccoeefFit TPLBouuatrrcaeeklEEroErrfmroFooirrrt T0MMo7aat2xxa6lRR1ESSrqqror 0.7264 GITEITnneNotereDrmmrcEceeRpptt(F.M] YGRESNCDHERE[MF-M] YRSCHEM SGSooEuurNrccDeeER GYERNSDCEHERM YRSCHEM AAEltlngPPiaarnrtesieccripipaLananitoss Engineer/Lab SIIunnmPPmFFaOOrSSy ppofppFmmi RRRSSsqqquuuaarrreee Ad) Summary of Fit RMRRoSoeoqoatutnaoMMrfeeeRaaAenndsSSjpqqouunaarsreeeEErrrroorr OMbesaenrvoaftiRoensspo(onrseSum Wats) Observations (or Sum Wgts) OF AAnnSalauymisiosslooSffeVVuaarwriieaansnccee. D3F22 Sum o211f.33S.69q985u50a477r7212e353s 3634 36 36635438 22.680715 36.635438 OF SLLuaoccmkkooollfSFFiiuttaws D1i1Fs]9 Sum o111f2.0S.60q652u58a816r610e022s2 3415 34 2.680715 10.022112 22.680715 000.333488400499900188 000.09.38834141063637973515 3 -0.94033 37 MeMaenmGnSoqSmuuamrreee 60.6967170386 0.66708 MMeeaaOnnsSSeqqcuu2eairrzee 6e8lal 0.666242 0.668141 1F F0RRa4atii%oo 1PP00rr.0oo40bv50>s93FF6 0.0003 F0F9RR9aat7ii2oo PP00rr.5o9o1b9v0>7o0F2 0.51(X) Esa Estimate L612 -1.615211 D409 -0.439047 00233 0.0293537 NNppaarmmTo 11[I PPaarSradammEeemtteorrrEEssttiimmaa(ttReessao 0S00tl.d2260E0rN99r2Eo88r t -R277a67.ti782o2 00071 0.163982 0.01072I 274 -2.68 2.74 OF EEflfeeccttSTTueomssotiSquaes DF 1 Sum o4Saf.OmS70q80iu189anI7rS1ee08s 1 5.0008180 PP<ro0bb0>01S1]1 0<00..000009L1018313 0.0098 F7FRaRaaetlisoo 7.496 7.1685 7.4966 pL2oow0wee0rr59315S6%% 0--000270..707774522062956916366 0.0075663 PPorroobo>nbF 00.00101%3 0.0098 APAppappgeeenndd3iixx LL Page 3 U1pUp1pep8ro9r99950s6%w --00011..0110S085I59797a909l767 0.051141 SMMuaabddjeeecAAtvvataoiillPaarbbollteeebcbiyyv33eMVOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00330055 3MA10050738 3MA10050738 SMoSouodurercclee ErCEMrooordoruerl C Total SoSLuoaurcrkccoeefFit PLPTuuaorrcueeklEEoErrfmrrFoooirrrt TM0Mo9aat8xxa9lAR5ESSraqror 0.9895 InITTGtneEoterNerrmrecDceEeppRtt(F-M) GYYAEGRRNESSDCCEHHREE[MMF-M] AGE SGoSEuoNurrcDceeER GYYAERGRNSESDCCEHHREEMM AGE EAAnltlgPPiaaorrtaisrccLipapaabnntss Engineer/Lab SIIunnmPPmFFaHHrSSy ppofpomFmit RsRRqSSuqquuaaarrreee Adj Summary of Fit MRRReooSaooqtutnaMMoreefeRaaAenndsSSjpqqouunaasrreee EErrrroorr MObesaenrvoaftiRoensspo(onrseSum Wets) Observations(or Sum Wgts) DOFF3 AAnnSaSaluuyysmmsiiosos2lf4ooSSff5qq5VVuuaa9arra8riiw8eaa3snnsccee 33*33 3205045...56a155219Im687587634 36 55.181656 OF SLLuaaccmkkoooflfSFFiiqttuas D3xF2| Sum3o30f000S.5q807u438a3707r131e868s 31 33 06274 0.578056 30.621774 000.34495440560727353 000..93926965343026279295353 3 ?.5975 37 MeMaenmsSSiqauswasrryee 09293 8.18663 0.92793 MMeoaOannSSsqquuaearoe 00.59738880666 0.578056 4EE0ss7tt8im5maa9tt0oe o-400.3m.065s766860e50895s552 00189228 0.0256075 0.0189228 NNpaarmmTo 11J[EI 1 PPaarraaSmmWeeEttmeeorrrEEssttiimamttaeRssaio 000S.t919d999E232r446r4o747r It 4RA2a.l9t1il21o 00..0o010m29N5s3O3B6z266l1S4 -1021..60091112 0.030868 0.61 PPr0ro0bo0>bl0tl2l 0000..30001000062622 0541 0.3192 0.5441 DDFF EEffftoeccSttSTuTueommssottoTifSSqqouuaarmeessmasFFRAaitsio 1 1 07o0..s99342a970004r19%73e74 8.5432 0L3os 1.0227 1 0.3487090 0.3758 FsF RReaateioo PP80rr.0oo80bb20>o22rF4 0.0002 FLFReraaatiiroo PP01rr.3o6o6b2b1>4e6F2 0.5616 Lloo6ww0esr99r75S2%S --0006..9090026907600762S957 0067 -0.025909 -0.043879 PP0rr0oob0n>2oF 0000s..330110996222 0.5441 AAPppapgpeeenndd4iixx L L Page 4 UU2ppp0ep5r9e94r55s7% --0002...0710772572901044245557 000.80177712254 0.0817245 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggCa2a.ss0CC4oo-nn6ffi3idd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00330066 3MA10050739 3MAII0050739 SMoSouodurercclee ErECMrooordoraerll C Total LSaSoocuukrcoceef Fit PuPTLouratrceaeklEEroErrfmroFooirrrt 0TMMo8aat5xxa3AlR7iESSrqqror 0.8537 `ITTIGnneotEeremrNmrcDceeEppRtt(F-M) YRSCHEM GENDER[F-M] YRSCHEM S`SoGouEurrNccDeeER GYYERRNSSDCCEHHEREMM AAEltlngPPiaarnnteicecoriiapLnaantbtss Engineer/Lab SIInun PPmFFmHHaSSroppyfppmmF.it RRRSSSqqquuuaaarrreee Adj Summary of Fit RoRRMoSoeoqattunaMMoreefeaaRAnnedSsSjqpquouanarsreee EErrrroorr OOMbbessaeernrvvoaafttiiRooennsssp(ooonrrsSeSuumm WWagttss)) OF AAnnaSalluyymssiiossfoofSfqVvuaaarrriieaasnnccee D3F22 Sum2o200f427S.1q201u14a11r817e734s4 334 36 5.181656 30.970483 55.181656 OF SLLuaamcckokalotfSFFqitut aws D11iF9s9 Sum o22f28S.09q87u981a886r6s0e0s00 331445 33800..990777001448688332 00.03423808775'414 00.0829.554544049450;0s049 7 -2.59-.5 .7 MMeeaannSSaquulmaorrseee 09100 12.1056 0.9109 MeMaenm1SSq2euu0aar5ee 053813 1.20519 0.53813 4EEsst9tiima%mtae 0-o0-0s.305.m745280629013662 0.0390561 NNpaarmmTo 11[I PPaa0rSrSata2Emdm4eemE5ttroee5rrror3rEEssttiimmaat(1ttR4Reeass2ati7oo 00.002.0141M249S551l2652823 -1-24239..1299279 0.012528 3.12 OF EEffffeccttSTTuoemsscttiSuares DF 1 Sum o8sBf.iES12q2su2ss5a00sri4e0s5s 1 8.8530880 PP<roub0>b1)1l1 <00O..000000M05212 0.0037 F8FRR9aatt0ioo 97191 8.9170 9.7191 1F3F2RRa8at9ii7oo 1Pp<3rr0.oo20bv80s>91FF7 <.0001 F2F2RRa3at9ii6oo PP20r.r0o2o5b3v9>91oF6 0.0591 LL3oow9we8re68r3550%%8 0--003.9.099668916l63620e38 0.0135966 P0rPr0oob0b>s2FF 000% 0.0052 0.0037 AArppappgeeenndd5iixx LL Page 5 U2pU9ppep9re2r83s53s2kk 0--0002...611948895222177358386929 0.0645156 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggCa2a.ss0CC4oo-nn6ffi3idd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00330077 3MA10050740 3MAII0050740 SMoSouodurercclee ECEMromrodooerul C Total SSLooauucrrkccoeef Fit PLPTuuaorrcueeklEEoErrfrrrFoooirrrt TMM0oaa9txxa6lAR2ESSrqaror 0.9642 TTIneotrmemrcept `IGYGnEREteNNSrDDcCeEEHpRRtE([MFF:-MM]] AGE YRSCHEM AGE SGoSEuoNurrcDceeER AGYYGERRENSSDCCEHHREEMM AGE AEAlunlpgPanarrctieicrcpiiapaannbttss Engineer/Lab `IISnnuPPmOOmAAaAAroppyfpomFmit RRReSSqqquuuiaarrreee Ad) Summary of Fit RRRMoSoeoqostutnaMMoreefeRaaAenndsSSjpqqouunaarsreeeEErrrroorr OOMbbessaeenrvroavftaiRtoenissop((onoonsrrsSSeuumm WWagttss)) OF AAnnaaSlluyymssiiosslooSffqVVuaaarriieaasnnccoe D3F33 Sum o211f272S.30q030u036a655r536e6677s 333%36 233799..333434003115003336 OF SLLuaomdkeoaoilfSFFqiiutt ies D3F2| Sum o22f551S..9q942u206a67222r838e877s E3Y31 23ns3% 1.407248 27.333536 000.23430200551115,9j99 000..319216140022110100:2545 E] -1.621 2 . 7 MMeeannGSSoqqmuuaiarsee 08259 4.00219 0.82829 MMeeaanonSSqqusuauree L725 0.81020 1.40725 FaF sRRa3at1ii9oo PP40rr.0oo80vb36o>1F8F9 0.0068 F0F5RRa1taisoo PP00rr.8oo50bb73a>51rF7 0.8031 2EE9ss3ttii0mm8aatt)ee --00200..s950329007849%93639 omasesl -0.002986 0.0256936 NNppaarmmTo 1l[[Ia 1 PPaarrSaaimmgeeEttmeeorrrEEssttiimmaattReeassll Std Error 0019m6 0.937648 t -2R33a0.t81i33o 000..0o102o82293m992l723e13 --00021..8182829 0.029164 0.88 OF EEfffloeccttSTTueomssottfSqores DF 1 Sum o660f.088S19q052u38a918r03e381s 1 1 osaser 0.0129048 0.6428967 PPr0ro0bo>0blt9ll 0000..%0000000l638487 0387 0.9014 0.3847 FF8R3aastoiio 0o08..00m3112e55%64 0.7762 LLAoowweSer r9I55%% --04009..O089S300I801E119S49S414 0036: -0.051658 -0.03364 PP0rr0oo0bb6>s8FF 0000..3990800041167448 0.3847 AArpappgpeeenn6ddiixx LL Page 6 UUpp0ppee2rr8998556%% 0--0001I..4s1055s2652e868s584d946 000..000884555006228775779 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00330088 3MA10050741 3MA10050741 A`PApappgpeeennd7diixx LL Page 7 MSSoooduuerrcclee EEnTMroorodouerrll C Total SSLooauucrrkccosefFit PLPTuuaorrcueeklEEoErrfrrrFoooirrrt 0TMMo7aat2xxa6lRR9ESSrqqror 0.7269 TTIneotnemrncept YIGGRnEEtSeNNrCDDcEeEHpRREt(IMFF--MM)] YRSCHEM SSGooEuuNrrcDceaER YGRESNCDHEERM YRSCHEM AAElnlngPpaiarnrtecieicrpiipaLanantbtss Engineer/Lab SIIunnmPPmOOaAArAAy ppofpoFmmit RRSSqqquuuiaarrreee Adj Summary of Fit MRRReoSooaqotutnaMMoreefeRaaAenndsSSjpqqouunaasrreeeEErrrroorr OMObbessaeenrrvvoaafttiiRooennsssp(o(oonrrsSSeuumm WWgattss)) OF AAnnaaSlluyyssmiissooolffSVVaaurrwiiaasnnccee D32F2 Sum o11f11S.3oq36u6r3a36e6r77em11s 334 36 39340103 27.976432 39.340103 OF SLLuaamcckkoololfSFFqiitut aws D11iF99s Sum o111f770S.27q238u314a195r9020e848s 315 34 2976432 10.744524 27.976432 000.222848878880::577 000"..321904067772011:00:3235 7 -1.621:2 .3 MMeeamnnSSSeqabuuiaasrraee 088s 5.68184 0.82284 MeMae0na9mS0Sq6au9ua4ar3ee 060 0.906943 0.716302 F6F9RPa0at5ii2oo PP60rr.0o9o0b0b3>5e0F2 0.0030 F1FR2Ra6at6ii1oo PP01rr.3oo22bb68s>6r9F1 0.3249 2EEs1stii0mmas9tee 0-2-00.0511.33520367362726049 0.0152746 |PPaarrSaaWmmEeetwteeorrrEEssttiimmaa(ttReessal 000S.t221d23E241r43r33o11r t Ratio 92097 -9.17 001907 0.182123 0.011907 128 -2.94 1.28 Nem OF EEftfieccttSuTTeomssottfSquares NparmITLo oaDF1 Sum of Squares AL8A5E9 7.1348529 1 1 1.3541118 PPr<roo0bb0>sl0ltIll 0<O0..200000W05E18 0.2082 F8FRR&aatt0ioo LeE7 8.6710 1.64`7 L2oLwo6ewr0er9795s9%% --000290,.96000096622047023669 -0.008923 PP0rr0obo0>sbF 0208 0.0058 0.2082 UpULppepere9sr5ds%s 0-00-0l.1361.666765I218T701S52 0.0394721 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOrffodorrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggCa2a.ss0CC4oo-nn6ffi3idd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00330099 3MA10050742 3MAII0050742 SMoSouoduterclcoe ECEMrroroodoerrul C Total SoSLuoaurcrckcoeef Fit PPTLuuoarruceelkEBoErfonrFoorirrt 0TMMoa9atxxa9lAR9ESSrqqror 0.9998 TITnoetremrmcept `GIYGnEERteNNSrDDcCeEEHpRRtE([MFF:-MM]] AGEYRSCHEM AGE GSSEoouNurrDcceeER AYGYRGERSENSCDCHEHEREMM AGE AAEllngPPanarerteiicrcpiipaLananidtss Engmeer/Lab IISnn uPPmFFmOOaSSrAAyAAofppFpoimm RRRsSSqqquuuaaarrreee A) Summary of Fit MRRReooSaooqtutnaMMoreefeiaRAnnedsSSjpqqouunaarsreee EErrrroorr OOMbbessaeernrvvoaafttiiRooennsssp(ooonrrsSSeuumm WWgtt)s) OF AAnnSaluaymssioslooSffqVVuaawrriieaasnnccee D3F33 Sum o511f311S.48q853u366a690r065e526s6 3363 36 5293017 53.456962 65.293017 OF SLLuaaccmkkoaotflFFSiitaws D32F2\ Sum o5Sf302S.0aq413u43a327r232e3565s 31 33 5330...440551663997662226 00..11s0861i824e776 011.S.212750726267875458676 3 5.65628 37 MMeeaanSnSoSqaausuaimrsee Lil 3.94535 1.61991 MeMaenmLSSq0qu1aur0ae 00173 1.67010 0.01371 SEEssTtiimmaNattse o--oo30s..r756o77il17s89e439s93 0063657 0.0270165 -0.063657 |PPaarrSaaGmmEeetmtoeorrrEEssttiimmaa(ttReessao 11S.t033d21E$11rS2r867oS6r t -R222a8.t28i03o0 0O.0o00.023Ws53aT54s85Se86 -002L..8S821e13 0.040785 -1.56 Noam OFEtEfefcecStTTuoemsstotlSquaes Nparm1T[oa DF 1 Sum o8BLf.oS0soq90u0ssa59r9sse5Ds0 11roa11 Issesss 1.0563257 3.9462586 PP0rro0bo>0blt8ll 00O0...002N30528134 O11 0.4251 0.1281 F FaRRsaaettiioso 04o2..4e69539s24115 2.43E 1 FR24Raa3t8oi5o PP20r.a0o48bb32>5F2F5 0.0822 12F1F6RRa0at4ii2oo 12PPo1rr.ooo6bbn7s>4?EF2 0.0717 LL6oowwee3rr9ds5S%% --11600..003949422514470323577 0les -0.04105 -0.146634 PPorrooob>mbF 000o..a40sm2352l13 0.1281 Appendix Aapgpeend8ix LL Page 8 U-pUpp0eplreor9su5es%x --000100..5009151512002168631318 0019319 0.095083 0.0193199 MSMuaabddjeeecAAtvvataoiillPaarbbollteeebcbyiyv33eMVOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00331100 33MMAA1100005500774433 Appendix L Page 9 Appendix Page 9 L SMoSouodurerclcee ErECMrroroodorerul C Total LSaSocouukrrcoceef Fit PTuPLoruaurecelkEEroErrfnroFoorirrt 0TMMo6aat0xxa9lAR7SESarq.ror 0.6097 ITTneoerrmmcept YGEIGRnNEtSDeNrCEDcRHeEp(REtF(M-FM-)M]) YRSCHEM SGSooEuuNrccDaeER YGYRERSNSCDCHEHEREMM AAE1n1nPpgaairnotieiccrpiipaLanantbtss Engineer/Lab IISnn uPPmFFmOOaSrSAyAAofppFopimm RSRRqSququuaarrreee Ady Summary of Fit RMRRoSoeoqoatutnaMoMrefeesRaaeAnsdSSpjqqouunaasrreeeEErrrroorr OOMbbessaeenrrvvoaafttiiRooennsssp((ooonrrsSSeuumm WWegitss)) OF AAnnaSalluyymssiiosslooSffaVVuaaarriieaasnnccoe D3F22 Sum o5f777S..4q8808u8399a277r299e077s 3364 36 6s293017 57.403220 65.293017 OF SLLuaaccmkkoooltfSFFiuitwws Dl1IF9s9 SumSo23fi15S.4q9o8u2a211rn02e94s 334l45 57403220 25.481096 57.403220 000.011622900818.177 011.S.202e9699s9931360:`s818 7 -5.656:8 : 7 MMeeaanm3SS9qa0uua9mr0ee Les 3.94490 1.68833 MMeaenLSseqsuaaorla LEE 1.68011 1.69871 SEE2sstii6mmaa6tee --S0050..S156568I10212S56586 -0.018225 PPaarraSamWmeEotreeorrrEEssttiimmaaRtteeasso 000S.2t36d330E28r9/rT4oT1r17-t012R7a.0t00io0 00U0S 0.260877 0.017056 07 -2.11 -1.07 Nam DF EEfffieccttSTTuoessmttofSas NparmTL1 oonaDF1 Sum o77Lf.5S5oq33u59ma94r4oe46s6 1 1 1.9278040 PP<ro0bb>0l0tl 0<00..200090442020810 0.2928 FFaRAdatesio 4L.4I6S35 1.1413 F2F3RRa3at6ii6oo Pr02r.o1o31nb32>6s0F6 0.1120 F0F9Rraa8tii%oo PP00rr.3oo91wb86s>9e6F0 0.5166 LL6ooww3eer6r998550%% --0L16O..00B383I816R38%27A19 -0.052886 PP0ru0o8bb2>F0F 00.20942280 0.2928 UU4ppoppe8err3o96s5s6/%t6 -00040..0029128060309649953554 0.016436 MSMuaabddjeeecAAtvvataoiillPaarbbollteeebcbyiyv33eMVOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppNyyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00331111 3MA10050744 3MA10050744 AAPppappgeeenndd1ii0xx LL Page 10 SMoSouodurercclee EECMrromTrdoooerrul C Total SoSLuoiurcrkccoaef Fit PuPLTuaorrcueeklEEoErrfmrrFooairrxt TMM0o5aat9xxa7AlR1iESSrqqror 0.9971 TTIenoermrmcept YIGGRnEEtSeNNrCDDcEeEHpRREt((MFF--MM]] AGE YRSCHEM AGE SoSGuoEurNrccDoeER GYYAGERRENSSDCCHEHEREMM AGE aEAlnnlpgPanarretieiccroitapaannbttss Engineer/Lab SIInnuMMm5Sm77a00rp9apoylmmFit RRRSqqquuuaaarrreee Ady Summary of Fit MRRReoSoaoqotutnaMMoreefeRaaAenndsSSjpqqouunaasrreee EErrrroorr OMObbessaeenrrvvoaafttiiRooennsssp(o(oonrrsSSeuumm WWagttss)) OF AAnnaSluaymssiosiooSffqVVuaaranieaansnccoe D3F33 Sum o3f002.S737q646u977a566r033e388s 333 36 fae 32.349503 33.117141 OF SLLuaamcckkolootfSFFqiitut aes D3F2i Sum o33f202S.02q29u556a331r334e630s0 31 33 3239503 0.096143 32.349503 000.000263151'09'29 003.0919.90990605050:t00)8552 7 -3.19558 :.7 MMeea0an2mS5Sq5au8sa1ar9ee 000..592885005228887889 MMeeaannLSSqoauouamr>ee 001..000990667119142 F0F2RRa6at1ti0oo PP00rr.8o2ob26v>19oF0 0.8529 1FF0R4Raa8tt3ii5oo 1PP00rr.2oa44bb80e>36FF5 0.2406 3EE4ss8tii2mm5aat7ee --0030.1.0412082513522230057887 0007I6S 0.001537 0.0047368 |PPaarSraaWmmEeetmteorrrEEssttiimmaaRtteeasso 0S11tL.9d009E20r00r506o36r t Ratio 3046 -3.41 0000..00103292196670022526736 -0000..10065663 0.031727 0.15 Npam OF EEfffecetSTTueomssottlSaares Nparm1[Lo aDF1 Sum000o.3f30S8sq70u8e6ai4ri0er7s 11[I 1 1 cass" 0.00341911 0.02185078 P0rPo0ibo0>bl1st7|l 0000..59053503137377 0882 0.9533 0.8822 FF0r3Re0ati5ie7o 00o0..003n0923i5357 0.0223 LSoLwoSewreS9r55I%% --0050..8G55S35008M15I887312 008812 -0.051413 -0.059812 P0rP5oab3b>7FF 000o..905933s5333273 0.8822 U-pULppaep0errr9sd5ssl%w 000-.2012.157494907477636956453)13 000..000665994224888556999 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00331122 3MA10050745 3MA10050745 SMSoaoduuecrlcee ECEnMroorodoaerrlt C Total SLoaSuocurkrcocsefFit PuPLTuraorcueeklEEroErfrrnoFooirrrt TM0Mo3aat2xxa3lRR3ESSrqqror 0.3233 ITTIGnenEotereNmrmrDccEeeppRtt(F-M) YRSCHEM GENDER[F-M] YRSCHEM GSSEoouuNrrDcceeER YGYRERSNSCDCHEHEREMM AAElllnPPgaairrnticicecpirpaiarantbtss Engineer/Lab SIuInnmMMm55a77r00y9ppopfmm.Fit RRRSSqqquuuaaarrreee Ag Summary of Fit RMoRReoSoaqotutnaMMoreefeaaRAnnedSsSjqpquouararsreeeEErrrroorr OMbesaernvoaftiRoensspoonrsSeum Wets) Observations(or Sum Wgts) OF AnAanlSayluysmsiiosslooSffqVVuaarariwaasnnccee D3F22 Sum of Squares 074s57e87 0.745787 334 36 B18 32.371354 33.117141 OF SLLuaacmskkoaolrfSFFqiittuaws D111Fs9 Sum o2f994S..19q9155u99a409r144e311s 315 34 2371384 22.411413 32.371354 0000.00324229:282 00-3.90719.579075335754:59858 7 -3.195:8 ..7 MMeeaOsnnSSqwusaarree 00.535722089994 0.952099 MeMaenmomSqSsuwawmree L960) 0.52421 1.49409 FoFRRsaatnoioo PP00rr.o36ob9b>m1eF7 0.6789 FR03Raa5tiimo PP00rr.9oo38bb53>o03Fr9 0.9833 3EEsst3iimmaSatse 0--D030..1013239665077744378 0.0049036 NNpoaarmm[a 11ro PPaarraSamGmeEetrteorrrEEssttiimmaaRtteeasso 000S.2i12d5950E800r00r22o633r -tB1R033a6.t43i3o4 002808 0.195906 0.012808 038 -0.65 0.38 OF EEfffoeccttSTTueomssottiSquwes DF 1 Sum of Squares 0o83l1s17 0.39853117 1 0.13955278 PPr<oub>b0ItsI 0<00..75050202022010 0.7042 F0FaRRaltasioso oles 0.4186 0.1466 LoELwoewOrsr99E55%% --00035..0582242843788175842 -0.021125 P0Pr5roo2bb2>s0fF 0702 0.5220 0.7042 AAPppappgeeenndd1ii1xx L L Page 11 UU2pppp8ee2rrs79654%4 000-.2022.737810123937737692947574 0.0309325 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggCa2a.ss0CC4oo-nn6ffi3idd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00331133 3MA10050746 3MA10050746 SaSMoouducerlcee EnCEMroorodorerll C Total LSaSaocuukrcoceefFi TPLPuuoarruceelkEEoErmfrmoForirrt M0TMao9atx0xa5lSR8ESrqqror 0.9958 T`ITIoGnnetEermerNmrccDeeEppttRF-M] YAYGGERRNESSDCCEHHREE[MMF-M] AGE SYoGGSRuoEESruNNrcCcDDeHeEEERRM AGEYRSCHEM AGE AAlElnPPgaarrrteiiecciorpoiananttnss Engineer/Lab IPSnFuPFOmOSmSAAaopfrpo7pymm4 RRRSSSqqquuuaaarrreeeAd Summary of Fit RoMRRoeSooqatutnMaMoreefeaaRAnendsSSjpqqouunaasrreee EErrroorr OMbesaernvaotfiRoensspoonrsSeum Wt) Observations(or Sum Wgts) of AAnnSaaluyymssoisisSooffquVVaaarrriieaasnnccee D5F33 Sum8o6f112S.95q956u532a395r94e477s 333 36 88862.12506220556 88.210203 OF LSaLmcacokkalolSfqFFiiuttaes DF 2132 Sum 0o85f35S.68q878u883a85r950e0333s 31 8602.5366275353 33 86256256 00p.002222r115511 1L4.es061616m667713n3343 0 -5.73 r2 37 MMeeamnonSSqeouuasaree 2608 0.65132 2.61383 MeMaenm2SS6qa4uam0re3e 02.366841053 0.36735 FfF0ARsa2tiioo PP00rr.8oo2bb64o>91rF2 0.8613 FF73Ra0at6ii0o PP70rr.2oo3wb60o>61FF4 0.2861 SEEs4stti5mmaa6itoe -5.523456 O00B1I0SS 0.2341119 00056 0.0199578 -0.00946 pPaarraaSmmGeeEttmeeorrrEEssttiimmaattReeassio 01LS.te06ds6sE35sr6re86ot4r t -R303a3.t73i22o2 000O..O03S42I285S40O93S84 0000.1.4478772 0.051808 -0.18 Noam OFEfEfofcecttSTTuoemssott.iSouwes Nparrn DF oTo t 1 1 Sum o011f.53S36qS54u60a50lr12e665s4 1 1 11oa ome 0.5764525 0.0871452 PP0rroo0bb>0olft2il 0000..44601706762442 082 0.6417 0.8562 FOFRSRatsIioo 0.5188 0o20os 0.2205 0.0333 Lower Lower95% 89S -8.912253 0477 -0.427171 0066S -0.066504 Olle -0.114862 P0rPaoubeb>sFF 00Oo..s6s4a47ls16T74 0.8562 AAPppappgeeenndd1ii2xx L Page 12 U2Uppp1peer3r96s5s9%w -002.0B.891193s540i36e965s59 009594 0.10642 0.0959429 MSMuaabddjeeecAAtvvataoiillPaarbbollteeecbbtyyiv33eMMOfrfodorrerIInnIssnppeePccattiiioomnneaavrnn.dd3CCMoo,ppyyNoii.nngg2a-ass04CC-oonn6ff3ii0ddee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00331144 33MMAA1100005500774477 MSooSudourerclcee ErECMrroroodoerrnl C Total SSLooauucrrkccoeef Fit PTuPLoruaeurcelkEEoErrfrmForairtx TMM0oa7at3xxa6lAR9ESSrqqror 0.7369 T`ITIGnnoetEeremrNmrcDceeEppRtt(F-M] YRSCHEM GENDER[F-M] YRSCHEM SGoSEuourNrcDceeER YGYRERSNSCDCHEHEREMM AAElnlnpPgaanrrctiiecciripipaaannbttss Engineer/Lab IISnnPuPFFmOOmSSAAaofrppppFymim. RRRSqqquuuaarrreee Aj Summary of Fit RRRMooSeoqoatutnaMMoreefeaaRAnnedsSSjpqqouunaasrreee EErrrroorr OMObbessaeenrrvvoaafttiiRooennsssp((ooonrrsSeSuumm WWagttss)) OF AAnSalunymsiosioaoSffqVVaiuarraiiaeanssnccee. EDn2F2 Sum o8f161S.38q864u663a651r800e022s2 333%64 888868..223114003224000332 OF SLLuaacmckokolfoSFFliiuttaws D11iF9s Sum o662f332S.101q303u992a11r199e111s 315 34 8826633..42304343424010212 0o.0c00232u61i1e12s30 1-1.0s55.9903a335568n84552 3 -5.7372 37 MeMaenmoSSqaxuuaworee 25951 0.93340 2.53951 MeMaenaSnSqSualaurae 15485 3.32312 1.54695 F0F3RRa6st7ti6oo PP00rr.6oo3bv56>o71FF6 0.6951 FR2a Raatoio PP20rr.0oo16bb48o>85rF2 0.0689 SEEsEstiiImmaaSitee 000-.5022.31387136184860637567 0.0132347 NNppaarmmTo 11[I |PPaarrSaadmmeEetmteeorrrEEssttiimmaa(tteRessa.o 00S.0t443d001E889r33r93o252r -t41R420a.t752i45o 0ONBIE 0.31995 0.020918 0630.74 0.63 DOFFEfEfofcectStSTuTueommssotot1if3SS9qqu%ua1ar4ee5ss 1 1 Losses 1.3956145 1.0165846 PP<rro0obv0>sI0ltlil <000..40406s603316 0.5312 LoLwoGeweredr97985S6%hl --0006..404614023708752673 -0.029275 F0F5RRa9tai%yo 0a 0.5496 0.4003 PP0rr4oob6v>%oF 032 0.4636 0.5312 AAPppappgeeenndd1ii3xx LL Page 13 UU4ppp9ep8re89r152s% 000-.4088.S8895778T389a929d917s72 0.0557446 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggCa2a.ss0CC4oo-nn6ffi3idd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00331155 3MA10050748 3MA10050748 SMoSouodurercclee EECMrrorodooerul C Total LsaSoocuukrcocefoFit PLPTuuaorrcueeklEEoErrfmrrFoooirrrt 0TMMo9aat9xxa9lRR5ESSrqqror 0.9995 TTInoeermrmcept YIG`RnEGtSENerCNDcDEeHpEREtR(M(FF-MM)l AGE YRSCHEM AGE SoSGuoEurNrccDeeER GYYAERGRNSESDCCEHHREEMM AGE AAE1t1nPPgaanrrotiiaccripipaaanntptss Engineer/lab SIIunnmMMm55a55r56yppopof mmFit RRRSsSqqquuuuaarrreee A) Summary of Fit RRRMSooeoqoatutnaMMoreefeaaRAnnedsSSjpqqouunaasrreee EErrroorr OOMbbessaeernrvvoaafttiiRooennsssp(o(oonrrsSeSuumm WWagttss)) OF AAnSnaluaymssioslooSffqVVuaarariiwaasnnccee DEF3y3 Sum o3f545S.35q801u170a077r706e6366s 333 36 S0618465 44.807703 50.618468 OF SLLuaemcckkoololfSFFeiitut ams D3xF21 Sum o44f407.S07q828u151a979r454e858s 1 33 44044..808020757777050353 0o0.11 1o14477n9955 01v4..6i01316s459a23652s512 3 -4.61966 37 MeMaenaonSqSiuqaueree LTE 1.93692 1.35781 MeMaena1Snq9Suaa0rre om: 1.39944 0.0257`+ F1F4Rra2at6ii8oo PP01rr.2o4o5b2v2>6e6F5 0.2526 5F4F3RRa3at6ii6oo 5PP40rr.1oo3bb03a>6mrF6 0.1071 TEE0sst0iimm3aut9se --o00701..4100s000393293s272s29 007996 -0.045945 0.0719096 PPaarraaSmmUeeEttreeorrrEEssttiimmaa(ttReessao 011S.t222d0400E20r856r11o777r t Ratio S0E4 -5.83 0.0002.03030430206366373 --L011S..945O340 0.03734 1.93 Norn DF EEfffeeccttSTuTeomssottiSquares Nparr1nT[I oDnF1 Sum o02sf.o7S2sq61su7oa15r9le77as4 11ro 1 1 Sosa 3.055014I 5.0357474 P<rPoo0bb>0sllt0ll 0<00..6610066300212 0068 0.1431 0.0628 F0F1RRa9at6ii3yo 0223..2721505908061)13) 3.7087 LoLwo9ew4srdr9sS5ES%M% --0009IS..540O84S05N56833E284 000059 -0.108262 -0,004059 PP0rr6oo6bv0>o2F 00o0..01a6466d30s12 0.0628 AAPppappgeeenndd1ii4xx LL Page 14 UpU-pp4ep5ra6r90o95s2%%s 0-004.0.335766620969392444 0147779 0.0163723 0,1478779 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00331166 3MA10050749 3MA10050749 MSooSudourerclcoe ErCEMrroroodorerul C Total LSaSocouukrrcoceefFit TPLPuuoarruceelkEEoErrfnrrFoooirrrt [TMMxoaatxxalARESSrqqror 0.3732 TI`nIToGtneEtemrerNmrcDceeEppRtt(F:M) YRSCHEM GENDER[F-M] YRSCHEM GSSEoouNurrDcceeER YGYRERSNSCDCHEHEREMM AAEltlnpPgaanrntociacpriaLpnaanspt.s Engineer/Lab SIunmMMm55a55r66yppoppf mmFit RRRSSqqquuuaairrreee AQ) Summary of Fit RRMRoSoeoqoatutnaMMroeefesaRAnnedsSSjpqqouunaasrreee EErrrroorr OMbesaenrvoaftiRoensspo(onrsSeum WWegttss)) Observations(or Sum OF AAnnaaSlluyymssiiossiooSffqVVuaairriieaasnnccee DF22 Sum o9f0.0S.87q7477u355a400r511e088s 334 36 S0618468 49.843450 50.618468 OF SLLuaamcckkolooffSFFqiitut aws D111F]s9 Sum31o11f788S.21q191u135a38r895e5822s 315 34 9843450 31.729598 49.843450 0o".o000i145s23s51l11 1-1".0262.1110009477207676881 3 -4.61966 ;7 MMeeamn0mSS3qausuawriee 0L.36897581 1.46598 MeMeaanonSSoqasuuahmreee 0F.A9T5E3T3R6 2.11531 F0FRR2aat6tioo Pr00ro.7o2wb66e>49rF3 0.7693 FRoRaaastooiro Pv00r.3or44b58>}06F.7 0.9486 4EE7sst6iimm0au6tee O--1w040O..17s126i479e02l695s15 0.0051619 PPaarraaSmmUeeEttreeorrrEEssttiimmaaRtteeass.o 000S.32t31d410E302r29r44o344r -t11R055a5.3t3i266o 001s 0.243093 0.015893 032 -0.52 0.32 NNpoaarmmTo ODFF EEftffoecctStSTuuToemmssc0ttoiafS0Sq1q9uu6aa2rr2ee5ss 11Loa11 ols? 0.40198223 0.15464711 Pr<Poob>b0Ist|J 0<00..606007003819 0.7473 F0F2RRas:tt2oo 00.12075452 0.1055 LSoLwaoew%reir9s95sSs%% --0O050..Q63I729314135l146668 -0.027136 PP0rro0obv>%oF 00.76407339 0.7473 AAPppappgeeenndd1ii5xx L L Page 15 U4pUpp1epr3er95o5s7%w 000-.34036.631663747326255572994 0.0374602 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbciyyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00331177 3MA10050750 3MA10050750 APAppappgeeenndd1iixx M Page 1 Appendix M Appendix M SSccaatttteeripplloottss`(m(aaalnneddcrrheeeggmrrieecssassliiooonnpsse))rooafftoffrlusuo(ornrooc=chhe5e2mm)iiccaaanlld lleeenvvgeeillssn eooeffraafllallbccfl(1eemm=iicc2aa8ll) participant participant with years worked in chemical male chemical operators(n =52)and engineer/lab(i=28) with years worked in chemical SMMuaabddjeeecAAtvvataoiillPaarbbollteeecbbtyyiv33eMMOfrfodorreIrnIsnIspnpePecactitiimooennrvaa.nndd3CC,ooppyNyoii.nnggC2aa-ss0CC4oo-nn6ff3ii0dde9ennttiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00331188 3MA10050751 3MA10050751 1vMiFallOeeSCpAClrhafeapPrommmaisrectcniaBycptliapOYpapnnRoetsrrEsatOteHorrEssM = In PFOS ppm By YRSCHEM 1 " LT we Foie . EH) : wd" TT 5 ass APApaopgpeeenrdd2iixx 1 M Page 2 souco Source Noel Model ErError Coat C Total TomTerm mere Intercept YRSCREM YRSCHEM -- Lwfi -- POWW R IInn PPFOSFdfpOpm=S=S00..ul7L2L5i8mi2n2ne9pm9a4e4r+aa+Fo0iprrf0t0F.y10i19m96611 RoRRRRSSoqqqqtuuuuMaarrrrieeeeAnAldySjquar Summary eErr of Fit OvRMMioeeroaatvnnaMooieffoRaRennesssSppqo(ouonnarssrSeeeuEmrroWrg) Observations(or Sum Wgts) or AVormoiofaSvaawriesasnce Analysis of Variance DF |1 5050 Sum of Squares \Tn 1.789373 H21o1m6e7s09 21.187429 51 22.976802 ozCEsmutiammlsateee SPPtaaOSdrrqMaaEEmmsrreeroltotrererrEEssittiimmFRa2aaaett0lsei7eos OOOH 0.2829416 Ooms 0.136981 22.0057 0.0196069 0.009541 2.05 YRSCHEM YRSCH0QoE,ogM0s7rm7ae8r7:e-, 0o.0Dn0.es56se5904ot93ns( 5 0,49465F 5< MenSame Mean Square hn 1.78937 oans 0.42375 Fro F Ratio am 4.2227 pot Prob>F oss 0.0451 Pool Prob>fq 004I 0.0441 0051 0.0451 owrsh -ower 95% 0070s 0.0078068 00004 0.0004424 U000Up.s0pp5sNpe5wrTa8or0I9no7I5es6As%w3 0.0387713 SMMuaabddjeeecAAtvvataoiillPaarbbollteeecbbtyyiv33eMMOfrfodorreIrnIsnIspnpeePcctatilioomnneaavrnn.dd3CC,ooppyNyoii.nnggC2aa-ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00331199 3MAT0050752 3MA10050752 IInn PROSdippm PFOSdfppm = = 00..007788S5S5PP+o+lo00y.n`0l0o5S8m7yi7u1a1n3lm3FFYYmoiiRtRaoddmSSefregCFCigyrriHHeaeEeEe=Ml=M22--000.000225555 YRSCHEM"2 YRSCHEM^2 RRSRsqSqquuiuarreeeAg Summary of Fit 0o[.ia1s5rz21i1a4dn1 ObRRMRMuSooeecqooaartutnnMvaMooareeffeiaaRRoAnneendssSSsjppqqoouuonnaarssrrSeeeeuEEmrrroWrret) 00o0..s661s331u007s355s3:4i:' 5 0.494651 Source Observaotirons(orAAnSa"ulSnymismiWsigaoiotffssvaV)aiaurrmiieaasnsnccee 5: MemSauwe Erste EMoSMnoodudecrelcle D2F2 Sum o1f35.S.54q485u90a589r8636e848s Mean Square 019799597 1.74793 pF44.r3R3a9o9t66iw55o Col Error C Total 549 51 29680 19.480934 22.976802 0.39757 oor Prob>F 0.0175 TInToeerrmemey. 0ESs0stimmSaatae PPaarSraamGmeettTeerr EEssitmiamMatateeslso ole Std Error t 0dRatio PPoroobe>blstHl LLoo0wewzres9wr5is% YYIYRnRRtSSeSrCCcCHeHHpEtEEMMM?2 0.0785522 0001SM 0.0871341 000.000.031036E285M37949 2022..05457187 00o0..060o3186l3682 -0.25371 0000000s6 0.0190526 YRSCIEM^2 -0.002546 0.001229 -2.07 0.0436 -0.005016 PAAappgppeeendn3idxi1xM Page 3 UUppopdeelrros9di5sa%ln 000..0411015005s820110)45717 -0.000076 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbtyyiv33eMMOfrfoodrreIrnInsIspnpePeccattiiimooennrava.nndd3CC,ooppyyNoii.nnggC2aa-ss0CC4oo-nn6ff3iid0de9ennttiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00332200 3MA10050753 3MA10050753 c-- icen All Participants Male Chemical Operators In PFHS ppm By YFISCHEM mw so amt : 2Pg ETP : : = or AAppppeendnidxiMxM Page 4 -jTou o Term Intercept YRSCHEM =[rorH or. P*romd fi a*te=2 I Linear Fit oes s5nss esr InPFHSdfppm=-1.5385+0.04363YRSCHEM Summary of Fit se oan RSquare 0.29335 i EEA RSquare Adj 0.27922 ete ss Root Mean Square Error 0.653321 iEaT men ireh MeanofResponse -1.06736 mEoo or A TENE Source pea aSmeem Model Observations(or Sum Wgts) Analysis of Variance DF Sum of Squares 1 8.859630 5:'. sn Mean Square wTeinm8.85963 eeF Ratio fpiae20.7569 Error C Total 50 51 feaom Estimate -1.538462 21.341385 30.201015 pEcEaEn Parameter Estimates SEER Std Error t Ratio oem Te 0.137478 -11.19 0.42683 Prob>F oy ow Prob>ltl TGRmI oemns <.0001 <.0001 Lower 95% -1.814595 0.043628 0.009576 4.56 <.0001 0.0243941 nUmea Upper 95% Oem -1.262329 0.0628619 WFateaAaka byb Sr e spinr ansCopying a Corral maton Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00332211 arose 3MA10050754 In PFHSdipp=m -17114.PP-oolt0y.nn1oo0mm0ia7al8l FFYiitt ddReeggSrreeeeC==22-H0.E002M15 YRSCHEM"2 In PFH Sd fppm = -1 RSquare .7 114 + 0 .S`1uS0mu0m7m8amrYayRrooySff FiCHEM Fit -0. 002 15 YRSCHEM 033381 "2 RRRRoSSqoqqutuuaaarMrreeeeaAAnddjSjquare Eror 000.0363.0003676366373833)11 MORMboeesoaaetnrnvMooaefftaiRRoneenssSsppqo(ouronsarserS.eeuEmrrWoreis) 0.64077 i "106753 -1.0673, Observations(or Sum Wgts) 5'. Source OF AAnnSalauymiscissiSooffaVuVaaarrriieaasnnccee MemnSauwro FRalo EMoSrMoodoudererlcle DF22 Sum o211f0.0S.01q089u82a020r010e0233s Mean05SS.4oq01du4a10ir09oe0 11PF22r.2Ro2a77bt77iF44o TErroorw s4t9 2300.210119001152 0.41059 P<r0o0b0>1F C Total 51 30.201015 <.0001 TTIneoermrmcept IYYYnRRRteSSSrcCCCeHHpHtEEEMMM~ YRSCHEM^2 1EEss7tt1ii1mmaa4tt7ee 00-0.1110.0070201771174794S976 -0.002155 PPaaSrrGaaEmmemototerrr EEssttiimmaatttReeasslo 000S.lt106d6SE280r0r202o66r -t11R20a0.t911i39o9 00049 0.034429 0.001249 732.93 -1.73 P<Prro0ob0b>0SIltl|I <000..00000900058212 0.0908 L2Loow0we8sr9r91S50S6%% 00-.0200.0300134569961220516 -0.004665 APApappgpeeenndd5iixx M M Page 5 UU-pp1p3ep7re597r58s%7 000-..1016.69309799360677783117 0.0003549 MSMuaabddjeeecAAtvvataoiillPaarbbollteeebbciyyv33eMVOfrfodorrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00332222 3MA10050755 3MA10050755 IManalePeOGCAhhiAAealmlpmipPcpcaaamrltlcBiOyOcpppirpenYaarnRatsttSosorCrsHs EM TM In POAA ppm By YRSCHEM 7 wd .. SEaRS fA fu Eafe ss C0wo ads PAAappgppeeenn6didxiMxM Page 6 SMoSouodrucerecle ECEMnroorodoaerlt C Total YTTInRoneetSrrmeemrCeceHppttEM YRSCHEM -- tarts -- .rea' r i P4to-id :t del e i IIn POAnAppP m ==00S5.O u55nL57im7n1e1em33aA a+ra+oFr00rif0t.Fy10A t1669911 Yg YRRSSCCpHHEEMM RRSRRSRqSoSqqqouuuutrMaarrreeeeeaAAdndjSjquarcSEurmmrary of Fit 00o.003g0.1070n59297n70559796869 OMbReMsoeaeoarntnvoaMoftefiaRRoneensssSppq(oouonnarssrSeeeoEmrrWoret) 0.515758 07397129 0.739719 Observations(or Sum Wgts) 52 DoFF1 aAnS"asluSyumssimosoofo1iSf3SvqV5uaua0arar8riie4eaas7snnccee MeMaens1nS3aq0uua8wr5ee FSF0RR0aat3ii!oo 5s0i01 f1r13313e..03303i00023842272 0260 1.33085 0.26601 PP50rr.o00ob0v>%3e1F 51 14.631169 0.0298 0EEstsS imaate PaoSSPrtaloadroEamEmsermertsotrererr EssitmtIismRRtSaaaottlIeisoso P<rPoobb>aslltll LwoLwowewr9sw5s%% o0lBI 0.5571329 0.010008573S1 52.2103 006 <.0001 noors 0.3391425 0.0169091 0.00756 2.24 0.0298 0.0017251 Upperss Upper 95% ors 0.7751233 oom 0.0320932 SMMuaabddjeeecAAtvvataoiillPaarbbollteeecbbtyyiv33eMMOfrofdorreIrnIsnIpsnpePecactitiimooennrvaa.nndd3CC,ooppyNyoii.nnggC2aa-ss0CC4oo-nn6ff3ii0dde9ennttiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00332233 3MA10050756 3MA10050756 In POAAppM = 0.3+0PPol05oy.n15io0m09iy0a2lnFYFrttodRdaemggrSrieeeeCa==-22H0.E003M13 YRSCHEM?2 In POAAppm = 0.30559+ 0.10002 YRSCHEM -0.00313 YRS01EM^2 RSquare `SummaofrFyil 02676: Summary of Fit MRRRReRooSSSaooqqqtuutnuaaaMMorrreefeeeRaaAAennddsSjSjpqqouuaanrrseeeEErrrroorr 000.062.27237676772632:18''1. 00.74360776130+ OOMbbessaeernrvvoaafttiiRooennsssp(o(oonrrsSSeuumm WWegitss)) 5: 0.73971! 5:: Sourco OF AAnaSlunysmisoaooiffVSVaiaqrriaiaassnnccee MeanSque Rao EMSoMroodurderelcle Dwo2F2 Sum1o0f337S.91q915u15a555r579e990s0 Mean01LS.2q991u55a78r799e9 PF83r.R9o9ab55ts2i2t6o CErTroorul 4st9 1101.673115156799 0.21869 P0r0o0b0>5F C Total 51 14.631169 0.0005 TInToteermrmcept Esimas PPaarrSaaAmmEeerttoeerrrEEssttiimm(aaRtteeasso 03E0st5i5ma8t8e 0S1td2E6r2ro5r t R2at4i9o PPrr0ob0o>lbIetlll LLoo0wwe0errI9s65sN%% IYYYnRRRteSSSrCcCCeHHHpEtEEMMM'2 0000..11300000050053118583776 0000..0102225025161222656 3323..9494889 0000..000001001600212 0.0591644 0000206 0.0495226 YRSCHEM^2 -0.003133 0.000911 -3.44 0.0012 -0.004965 AAPppappgeeenndd7iixx 1 M Page 7 U0pU5pp5ep2re09r15g2%s9 0000...01510555021050350100822889 -0.001302 MSMuaabddjeeecAAtvvataoiillPaarbbollteeebcbiyyv33eMVOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00332244 3MA10050757 3MA10050757 re All Participants aT Male Chemical Operators TS In PFOSAA - B YRSCHEM -- ens Appendix M Page 8 Taw s Lm * JDD 'I r ' t' I' r' r 0 5 10 15 ?0 ?S 30 1?5:0 wrSource SouModel oeError = C Total TomTerm fo Intercept EW YRSCHEM Lim '1 Linear Fit wrrssSsELwnsrtemscyma In PFOSAAdfppm=-3.8496 --0.02457 YRSCHEM ALR Summary of Fit sigue a RSquare 0.021349 cond oe RSquare Adj 0.001776 Sia so Root Mean Square Error 1.604937 JUonTSSe ve on% MeanofResponse -4.11489 Observations(or Sum Wgm) I Analysis of Variance or RR ry roe OF Sum of Squares r sem ese (oe 1 2.80958 a amas em 50 128.79120 3 = pes 51 131.60078 TE rum. tam: SE Estimate op o T -3.849596 Parameter Estimates Std Error t Ratio 0.337727 -11.40 52 Mean Square 2.80958 2.57582 F Ratio 1.0908 Prob>F 0.3013 Prob>ltl <.0001 Lower 95% 4.527939 Upper 950/6 -3.171253 -0.024568 0.023524 -1.04 0.3013 -0.071818 0.0226812 FRE A CORI PH SIAL MMaaddee AAvvaaiillaabbllee bbyy 33MVffororInIsnsppeeccttiioonn aanndd CCooppyyiinngg aass CCoonnffiiddeennttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00325 33MMAA1100005500775588 wiz All Participants Male Chemical Operators In M570ppm By YRSCHEM 1" . ow fi m=en Appendix M Page 9 su a i -.DC I I I ] I'1 ' YRSKP erTerm mBoIntercept YRSCHEM =.f=4 pr sfBTEowrrAeoe,yrenenESoRoe ErE swcreagtHnhemEi% ne Source Model BOL Thm imoom Error BofEmdmETBa tTEOeBIEEI EeIm wE2mTE CTotal Linear Fit In 570ppm = -1.3268 -- 0.04752 YRSCHEM Summary of Fit RSquare 0.12927: RSquare Adj 0.11185S Root Mean Square Error 1.189837 Mean of Response -1.83989 Observations(or Sum Wgts) 52 Analysis of Variance DF Sum of Squares Mean Square 1 10.509261 10.5093 50 70.785564 1.4157 51 81.294825 F Ratio 7.4233 Prob>F 0.0088 Estimate -I.326808 Parameter Estimates Std Error t Ratio 0.250377 -5.30 Prob>ltl <.0001 Lower 95% -1.829705 Upper 95% -0.823911 -0.047516 0.01744 -2.72 0.0088 -0.082545 -0.012487 te ty topstories on Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00326 -- 3MA10050759 MPaallEoeGCGhhASselenmlpimpPcpaearam)ntliBcOcpyopiopeuarArnnaotsStosorHrssEN In PFOSA ppm By YRSCHEM Tr mw FR Sw le -- Bodh and. -ot Rt wa | -T7.00Y6 S 100{ I I- I 6 . 1Sda20 285 30 385 MINN Page 10 AAppppeendnidxiMxM Page 10 ESSMoNroiouuodrrsrecclee ECroroar t C Total TomTerm Inept Intercept RCH YRSCHEM InPFO=S-3U3n0Ao4a7r-Fd0048i6S pm LinearFit YRSCHEM In PFOSAdfppm =-3.3047 -- 0.04865 YRSCHEM Soma aiFi Summary of Fit Rsque ooss) RSquare 0.0581 Raure AG oo: RSquare Adj 0.03926: Root ein Square Err fre Root Mean SquareError 1.89008-- MenofResponse yee Mean ofResponse -3.8300, Ofnerations (orSam Wes) v Observations(orSum Wgts) 5: Ao of Vasanca Analysis of Variance or "EmoSuam Memsawe Frm DF Sum of Squares Mean Square | 1101808 Wh Sow 1 11.01808 11.0181 50 mee iS poe 50 I78.62062 3.5724 5 19.6870 frees 51 189.63870 F Ratio 3.0842 Prob>F 0.0852 Gan PSaormfaEstiimRaatees Poni ows Uppmosw Estimate rr ri rr -3.304729 Domes oom 1% oo Old Ooms -0.048653 Parameter Estimates Std Error t Ratio 0.39773 -8.31 0.027704 -1.76 Prob>11I <.0001 0.0852 -ower 95% -4.103591 -0.104298 Upper 95/6 -2.505866 0.0069914 MSMuaabddjeeecAAtvvaoaillaParbbollteeebbcyiyv33eMMOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo.ppyyNoii.nnggCa2a-ss0CC4oo-nn6fi3fd0ie9dnteinatl Information Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00332277 MAT0050760 3MA10050760 E-- S All Participants Male Chemical Operators In M556 m B YRSCHEM iy -1 DO awe Ln . AAppppeendnidxiMxM PPaaggee1111 E10 HY -6.00 TR .. f . r . T. r t5 20 25 Y$SCF1[V I I. 30 2Term Eexm Intercept YRSCHEM wrSource Model E5EError C Total =tisv ~1 som Safnpases LinearFit In M556dfppm = -2.6395 -- 0.0315 YRSCHEM Summary of Fit = a. RSquare 0.075514. =. so RSquare Adj 0.057024 EE ute a Root Mean Square Error 1.06350` a i Mean ofResponse -2.97966 LL Observations(or Sum Wgts) 5: tTLeE wen Analysis of Variance mr DF Sum of Squares Mean Square "ZZ 1 4.619303 4.61930 50 56.552145 1.13104 1 &= fi 51 61.171448 F Ratio 4.0841 Prob>F 0.0487 bgoww BE--EE--E--E oy em Estimate SEER EEwm mOEmE -2.639497 Parameter Estimates Std Error t Ratio 0.223793 -11.79 Prob>JtJ <.0001 -ower 95% -3.088999 -0.031503 0.015588 -2.02 0.0487 -0.062812 omum Upper 95% OER -2.189996 -0.000193 a -- Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00332288 iio 3MA10050761 m-- e, All Participants Male Engineer/Lab In PFOS pprn By YRSCHEM nw ;End TN . c >t AAppppeendnidxiMxM PPaaggee 1122 we aTerm Intercept Em YRSCHEM corSource Model Error C Total S 10 1S 20 2S JD J5 ~0 7RSCNE4 ---- lreor fi i -- Poymri ft ~7:e=? vor Linear Fit 53h In PFOSdfppm =-1.2515+0.03365 YRSCHEM Summary of Fit ro J. RSquare 0.20812. RSquare Adj 0.177604- EE ert sre Root MeanSquareError 0.886126 et bo Mean ofResponse -0.6614: Em 3 Observations(or Sum Wgts) 2f or eCmEaEi ee AnalysisofVariance DF Sum of Squares Mean Square 1 5.365639 5.36564 reF Ratio 6.8333 26 27 corn a DEE rr ore Estimate SEER IEEE -1.251482 20.415689 25.781328 Parameter Estimates Std Error t Ratio 0.28106 -4.45 0.78522 Prob>F 0.0147 Prob>>tl 0.0001 -ower 95% -1.829204 Upper 950/6 -0.673759 0.0336488 0.012872 2.61 0.0147 0.0071897 0.0601078 Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00332299 3MA10050762 In PROSdifppm = 1.6361PPo+oll0yy.nn1oo3mm2ii2aa2llFFYiittdcReaggSrroeeeCs=22-H0.E002M82 YRSCHEM2 In P FOS dfppm = -1.6361 Rsquare + 0.`1S3u2m2m2aYryRoSfCFiH. EM Summary of Fit 030774 -0.00282 YRSCHEM^2 RRRRSSoSqqoqtuuuaaaMrrreeeeaAAnddjSjquare Ener 0000..28235450252700047767::0' MRMeOboeasoanetnrMvooaefftaiRRnoeenssSsppqoo(uonnarssreSee.oErmroWret) 0.84508() 066142. -0.6614: Observations(or Sum Wgts) 2t: SMoSoouduecrclee ErEMCrrolrodoorerult C Total OF AAnnSalauyimsiossiooSffaVVsaarrriieaasnnccee MeanSqure D22F2 Sum o1f777S.5.q982u251a740r027e758s08 Mean Square 0S9a61 3.96354 2Fd5 2175.788514322580 0.71417 27 25.781328 FF5R5Ra9ati9to PP5or.ooa5tb40>r91F9 0.0101 TTInoeermrmcept IYYYnRRRtSeSSrCcCCHeHHpEtEEMMM2 YRSCHEM^2 LEEssItiimmSaatse 00-0.1101.33602328262411418983 -0.002819 PPaarrSaaGmmEeemttoeerrr EEsstiimmaatttReeasslo 000S.t3O3d36SE6r9H2r97oO7r t Ratio 42487 -4.87 00045 0.053479 0.001489 1892.47 -1.89 P<rPor0bo>b0lsltllf 0<00..000020290009616 0.0699 L2oLwo3ewreRr9s5DS%% 0-0.2OO0.0023Z2S208OK87SE32SR33 -0.005885 AArppappgeeenndd1ii3xx MM Page 13 U0pUpp9epro39r5s0%s 000-.2002.404920243233646566604643 0.0002466 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggCa2a.ss0CC4oo-nn6ffi3idd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00333300 3MA10050763 3MAII0050763 InPMFaMHalSpAllpoelaoEPEarnmnrggtBtiiicynonieepnYearnNRsLtlSsaaCbbHEM In PFHS ppm By YRSCHEM -0m5wD : SD - =< AAPpappgpeeendn1i4dxiMxM Page 14 -3155D 4-1 : i 19 + a -15D I I , I , I , I' I' I' 1 PS TR EREwe 0 5 10 IS 2D 25 JD JS 40 wo 11SCIIEW SMoSouodurerclcee ErEMCroTordoorerull C Total ITnToteermrmcept YRSCHEM Intercept YRSCHEM -- ties li -- Fa we ri ivee=? IInnPPFHSFdfppHm==2`S -L9S2il.5nui92ne5md e2a2am2r+r+FaoFiif0f 0trt..Fy00it44.11p0066YYp RRSSCCHm HEEMM RSRRqSqquuuaarrreeeAdj Summary of Fit 000.222143431011015t MRRReoSoaoqotutnMaMoreefeaRaAenndsSSjpqqouuanarsreeeEErrroorr 0002..7298172480005005::h; OMbseearnvaotfiRoenssp(oonrseSumWes) x -2.2322.1 Observations(or Sum Wgts) 2t; OF AAnaSnluymasoislioSoffyaVuVasaarrriiieaansnsccee MeanSquo D2F1| Sum o2f77S.989q88u818a77r969e11s Mean7T0S.3q9o5u86a86mr70e9 726 27 52860307 24.871516 32.860307 0.95660 FF8R3Raa5tt1io3o PP80rr.o30ob5o>m1fF3 0.0077 2EEss0tii5mma2astt1ee 00.0-0424.I19005S52882I12 PPaaSrrUaaEmmeMltorerrEEssitmi(amRtaeatesls 000S.t03d312E0r02Sr18o9r t Ratio 928 -9.52 0.014208 2.89 PPr<ro0bo>WbItlll 00077 <.0001 0.0077 iL-SoowwEeerrE9S5SS%% 0OUSSH -3.589879 0.0118541 U-pU2ppe3pruo9sr5ed1/ls6 0002621 -2.314561 0.0702621 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbciyyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00333311 3MA10050764 3MA10050764 In PFHSdfppm= 3.571PP5+oo0ll.yy1nnoo9mm9ii7aaY ll FFiitddR eeggrreeeS e=-s2 0C 0045H4YRSECHEMM?2 In RSquare: PFHSdfppm = -3.5713 + Summary of Ft 0.19973 YRSCHEM Summary of Fit -- 0415082 0.00454 YRSCHEM^2 RRRRoSSSoqqqtuuuaaaMrrreeeeaAAnddjSjqure Eor 0000..8.4445400350000664888153 RMOMeboeasonaeotnrfvMoRaefteaiRsonenpsSsopq(onuonasrsreSeeuEmnWorats) 0.85404.1 223224 2.2322.1 Observations(or Sum Wgts) 2 i SMaSouodurerc!cee OF AAnnSalsuymysiossiooSffqVVuaaarnimaansnccee MemSawmo 2DF Sum legs of Squares 30% Mean Square 1F0F0RRa2ta5i8oo EnCEMrooordoraerlt 22725 31118248..822663324045737570720798 079% 7.31276 0.72939 1PP00r.a0o00bb20>5r6F8 C Total 27 32.860307 0.0006 TTIenerermrmcept SEEssttiiSmmaattee PPaaSrrWaaEmmeawttoeerrr EEssttiimmaa(ttReessslo 0St3d9Er8r6or t1R0a5ti1o PP<ruoob0b>0llla LLoowwNenr r9n55%% IYYYnRRRteSSSrCcCCeHHHpEtEEMMM"2 00-0.3110.9950977714233243447 0000..0003035SI94SM80O646:16 -133030..7572010 <0O0..0000000010811 00o.0o0-8408.8e422l7M31s43 YRSCHEM^2 -0.004538 0.001504 -3.02 0.0058 -0.007636 AAPpappgpeeenndd1ii5xx M M Page 15 U2pUppepresr9o5s%i 00-.3203.N18I107001E430I19S55 -0.00144 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbtyyiv33eMMOfrfoodrrerIInnIssnppeePccattiiioomnneaavrnn.dd3CCMoo,ppyyNoii.nngg2-aas0s4CC-oonn6ff3ii0ddee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00333322 33MMAA1100005500776655 MaAlAieh PPEaanrrgtiiicncpoiapaanrnittLssab InniPOMa le,,Enmg:ineeYYrRR/SSLaCCbHHEEMM TM S wo : Appendix APpapgeend1i6x MM Page 16 2 bg : :iw HEE 70 w15 e20 YR5,H[V 2E 5 .oE35E4 MSSoooudurercclee ErCEMTrotrodooeurrll C Total TTIneatremmrcept YIYRnRtSeSrCcCHeHpEtEMM ---- mirimtri ---- hPC4wte Fiakg7eee-)2 InPOAApp=M-16Ln4i2en9eaarr+FFi0itt.01806YRSCHEM RSqIunaPrOeAAppm =SS1uu.m6mm4a2mr9y+aoo0frf.FF0yii1tt806 YRSCHE0.M063626 RoRRRSSSoqqqtuuuaaaMrrreeeeaAAnddSjjquareEcror 00.002673661238 00.903257260I23 M`RMeOoeaboasntenroMvofeaftRaRienoesnsSsppqoo(uonnarsrsSeeeuEmrrWorats) 0-.119.3332526262302323 Observations(or Sum Wgts) 28 OF AAnaSnluymasoisfloSoffyqVuVaasarririiaeansncscee MeanSqusre 2D%F1I Sum o2f121S..7q553u44955a611r799e151s Mean011S8.5q57u544a516r190e9 22n76 2224422..82783449386667555 0.87460 FFR1a7Rat6t6ii7oo PP01rr..o1o7b96b>56F3F7 0.1953 LEE6ssttii8mmaa0ttee 0-.0100.I16884002S58T77229 PPSaaErraarmmoeettreerrEEsstti(imRmaaattteiesos 00S.Ot220d99IE66Sr62rE2o6S6r t -SR51a5.t35i43o4 0.013585 1.33 P<Prro0ob0b>a0IltIlI <00..101909505313 l2olwo2ew5re2r95S59S7%% --0020..0200599288569777 UpUppLpoe0rro93s56% 00.0-0144.550993883111666 MMaaddee AAvvaaiillaabbllee bbyy 33MVfofrorInIsnsppeeccttiioonn aanndd CCooppyyiinngg aass CCoonnffiiddeennttiiaall IInnffoorrmmaattiioonn:: SSuubbjjeecctt ttoo PPrrootteeccttiivvee OOrrddeerr IInn PPaallmmeervrv.. 33M,, NNoo..CC22--0044--66330099 22881122..00333333 3MA10050766 3MA10050766 rove 100r StEmI sc PolynomialFitdegree--2 RE In POAAppm = -2.1643 +0.15169 YRSCHEM-0.00382 YRSCHEI\1^2 J fl Summary of Fit fo sz RSquare 0.257455 I Ses RSquare Adj 0.198052 ie ow Root Mean Square Error 0.849296 oi 3 Mean ofResponse -1.32623 Observations(or Sum Wgts) 28 gee oror p EAAEEE eweets r(aam Source Model Error C Total Analysis of Variance DF Sum of Squares Mean Square 2 6.252264 3.12613 25 18.032601 0.72130 27 24.284865 F Ratio 4.3340 Prob>F 0.0242 en ne FEEEn pr i Term Intercept VEC YRSCHEM YRSCHEM^2 Estimate -2.164287 0.1516874 -0.003821 Parameter Estimates Std Error t Ratio 0.337972 -6.40 0.053746 2.82 0.001496 -2.55 Prob>ltl <.0001 0.0092 0.0171 Lower 95% 2.860348 0.0409971 0.006902 --p Appendix M Page 17 Up Upper 95% -1.468226 0.2623777 -0.000741 te late 901 op cion CopCott. le Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00333344 -- 3MA10050767 MalAAlel PEPanarrgttiicncpieapsaninitLssab IInn PPFFOOMSSaAAleAApEongmmiBnBeyefYYllRRaSSbCCHHEEMM wn AAPpappgpeeendn1i8dxi4xM Page 18 T = .r W . T r s , r .n+o,sT r 5 , r 8 . r e, wi YASCRIP, MSSoooduuerrlccee CEEMromordoowerll C Totai TTIneotrremnrcept IYYnRRteSSrcCCeHHptEEMM SwLrio fi InPFO=SLLi5in.nAee1aa4rr1FA1Fiit-t d0.01i64YpRSpCHmEM RInqPuFiOrSeAAdfppmS"=uSm-um5.am1rm4y1oa1offr--FFyi0it..0164 YRSCH0E02M6437 `RRRRSSoqqqouuutMaarrreeeeaAnAddSjjquareEror 0-01.0300.9210943124304308978 ObMRMsoeeeoaartnnvoMaotfefiaRRoenenssSsppqoo(unonarssreSeeuEmrroWreis) 1.399249 sam28 -5.4287 Observations(or Sum Wgts) 28 oF AAnSanluymasicsliooSffyVqVausarariiimaansnsccee MenSque 2D6F1I Sum510of291S7.0q255u713a5r127e222s2 Mean111S.9q225u777a59r1s0e2 226 27 55220...119880005834979424 1.95790 F0FRP6aRtasitoo PP00rr.4oo62bw51o>1F0F3 0.4270 5EE1ss4tt1iim0maa5tt5ee 00l603 -5.141055 -0.016403 PaPSraWarEammmeeottreerr EEssttii(mmRaaattbeeoss 000S.0tA4d24B0E33rI8r212o62r t-L1R01Sa8.tE5i18o 0.020326 -0.81 PPr<ro0bo>0blt1el 0420 <.0001 0.4270 lLooGwwOee0rrS9SB5Sl%%6 COSSISs -6.053316 -0.058184 UpU4ppp2ee2rr899755%9% 00ST -4.228794 0.0253771 SMMuaabddjeeecAAtvvataoiillPaarbbollteeecbbtyyiv33eMVOfrfodorreIrnIsnIspnpeePcctatilioomnneaavrnn.dd3CCMoo,ppNyyoii.nnggC2aa-ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00333355 33MMAA1100005500776688 In MVSMsaaA7alllleppEPEmaannrgntgBiicyncrieioVpeaarAsnn/tSasLsaCnbHEM -in M571 -m B YRSCHEM we B | 2f | Boge f w fF e AAPpappgpeeen1dn9idxi4xM Page 19 T waaa Ase SouSource Soir Model Emr Error Coat C Total TomTerm Inert Intercept RSCHEM YRSCHEM =?read Loon Fu Linear Fit In SToppm = 3.1804 + 000328YRSCHEM In 570ppm =-3.1804+0.00328 YRSCHEM SummaeirFyi Summary of Fit Rsqure ocoss RSquare 0.00186 RawrAd oes RSquare Adj -0.03653 RootMeanSqrEr 10295 RootMean Square Error 1.024495 Nianof Response Simon MeanofResponse -3.12301 Observations (or Sum Wes) EH] Observations(orSum Wgts) 28 Aas of Varanco Analysisof Variance or "GmoSuam Memnsuwe Rao DF Sum of Squares Mean Square | 0030840 ose ooi 1 0.050840 0.05084 % mame lows por 26 27.289336 1.04959 n Tas oss 27 27.340175 F Ratio 0.0484 Prob>F 0.8275 amis SParHameEtercanimaRtaeiso Pov Lowerss Estimate Sli oe 57 coo aww -3.180449 ows ous 0m osms 00s 0.0032754 Parameter Estimates Std Error t Ratio 0.324948 -9.79 0.014882 0.22 Prob>JtJ c0001 0.8275 Lower 95% -3.848383 -0027315 Uppers Upper 95% assis -2.512515 0036 0.033866 MSMuaabddjeeecAAtvvaoaillaParbbollteeebbciyyv33eMMOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo.ppyNyoii.nnggC2aa-ss0CC4oo-n6nf3ifd0ie9dnteinatl Information Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00336 MAT0050769 3MA10050769 Japoncouns All Participants yn Eros Male Engineer/Lab rn By vRBDEM In PFOSA ppm By YRSCHEM a . -)hnDC - - . Ct gel ILa -- -- | "3 D . I . ,' I f ' 1 ' T . TTT RE 5 IC 15 ?D ?5 3C 35 ou`ISchiv -- es Appendix M Page 20 Sauce Source StModel HrError EoC Total omTerm Tran Intercept frYRSCHEM -w-1'i fr Linear Fit InPFOS5A198.d00p16o4YRmSCH=EM In PFOSAdfppm =-6.0798+0.01464 YRSCHEM Say tF8 Summary of Fit Rs oor RSquare 0.014659 Re Ad Goria RSquare Adj -0.02324 Ro anSureEr ool Root Mean Square Error 1.620061 NoHo Sion Mean ofResponse -5.82314 Ohsaton or Sum Wg) F Observations(orSum Wgts) 28 Aoi vaca Analysis of Variance or Miia demswme ao DF Sum of Squares Mean Square : Ts ion ow 1 1.015219 1.01522 % atem dou pat 26 68.239528 2.62460 FR] f= 27 69.254747 F Ratio 0.3868 Prob>F 0.5394 J J--t--+ RR Estimate Some ovsem nk om Then -6.079806 dowises baw Ge ome comm 0.0146365 Parameter Estimates Std Error t Ratio 0.513848 -11.83 0.023534 0.62 Prob>ItJ <.0001 0.5394 Lower 95% -7.136028 -0.033737 oeewm Upper 95% -5.023584 0.0630103 MSMuaabddjeeecAAtvvtaaoillPaarbboltleebcbyiyv33eMOfrfoIdornersInpIsenpcePtcatilioomnneaarvnn.dd3CC,ooppyNyoii.nnggC 2aa.ss0CC4oo.nn6ff3idd0ee9nnttiaall formation Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00337 MAMO0ETTO 3MA10050770 AAPppappgeeenndd2ii1xx MH Page 21 AaAllllPPEaanrrtgiiiccnpieapaarnritLssab wT IInnMM55M55a66lpep-EmnmgBiBnyeeYYrRR/SSLaCCbHHEEMM an . -2.A - m LEin +7 E Bu] T ws, . -61 - wor | Dp.sSi. n10I.1sI 5 o.m2I 0 o.s25Io.a3DI.3s5 oe10 YRSCHEM SSMooouudrrecclee ErECMrooordoraerll C Total TTIenorrmmeept YRSCHEM Intercept YRSCHEM SwLiim R InMSSfppm L= 4o.L5ia5n2era8rF+Fit0t00037 YRSCHEM RSqInuMi5r5e6dfppm =S-`4uS.m5um5am2r8my+aoof0frF.Fy0itt0037 YRSCH0E0M00015 RRRRSoSSqoqqtuuuMaarrreeeeaAAndfSjquareError 0-"1.0020.09003703820840145855 ObRMMsoeeeoaartnnvMooseffiRaRoenensssSppq(oouonnarssrSeeeuEmrrWorets) 1.297208 5362E5 -4.54625 Observations(or Sum Wgts) 28 oF AAnaSrluyasmicsliooffySVVqaasruriimiaasnnsccee MemSquare D2F1| Sum o3f007S.050q00u100a466r686e101s Mean0o1S.o6q0o8u0o2a0s7r6s5e6 zn26 27 pie43.751480 43.752141 1.68275 FF00rRa0et0ie4o PP00r.r9o08bo03>0f3F4 0.9843 Esta Estimate 4595 -4.552795 000M 0.0003734 PaPSrauarEmaremetotererr EEsstii1mmRaaattleeoss 0O0S.At04dN81IE18Mr44rM4o4G6r t Ratio L0T02 -11.07 0.018844 0.02 PP<rooOb>o0llltl 0983 <.0001 0.9843 LLooSwweerEr9s5SS%k 00% -5.398529 .3.03836 UU3ppp7pe0r0e90r65s]% 00310) -3.707061 0.039107 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbtyyiv33eMMOfrfoodrrerIInnIssnppeePccattiiioomnneaavrnn.dd3CCMoo,ppyNyoii.nngg2-aa0ss4CC-oonn6ff3ii0ddee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00333388 3MA10050771 3MA10050771 AAPppappgeeenndd1iixx NN Page 1 AAppppeennddiixx NN SSccaatttteerrpplloottssfe((maaannldderrceehggerrmeesisssciiaoolnnsos)p)eoorffafltlouurosorro(ocnchh=eemm1ii2c)caaallnlldeevveeenllgssinooeffeaarllflllccahhbee(mmnii=ccaa9ll)ppaarrttiicciippaanntt female chemicawwliiottphheyyreeaaatrrossrsww(oonrr=kkee1dd2ii)nnaccnhhdeemmeniigcciaanlleer/lab(n =9) MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbtyyiv33eMMOfrfoodrrerIInnIssnppeePccattiiimooennraavnn.dd3CCMoo,ppyNyoii.nngg2-aa0ss4CC-oonn6ff3ii0ddee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00333399 3SMMAA1t1000000s55000777;7722 FasoaAluCl pPhaarortsimccaigpaaGnnptssoaors InpoPm FYAOSCHSEM Female ChemcialOperators In PFOS ppm By YRSCHEM < IJ AAPpoappegen2ednidx iNxN Page 2 = wn-100 : wIe 5 0 10 20 15CHEN TomTerm nerIntercept YRSCHEM YRSCHEM SNoSMEiuooourdrsrecclee ECrlroor w C Total Liw 11 LinearFit Linear Fit In PFOSATopm = 001326 000779 YRSCHEM In PFOSdfppm=0.01226--0.00779YRSCHEM SummaorfFyt Summary of Fit Rquue o00sss? RSquare 0.008557 Rare AG "000059 RSquare Adj -0.09059 RootMean Squr Ero Priced Root Mean Square Error 0.578093 MeanofResponse "0st MeanofResponse -0.05134 Overvtons (orSumWi iH Observations(orSum Wgts) 12 Ansofvyarasrca Analysis of Variance or "Sots Memsawe Fra DF Sum of Squares Mean Square | Quik Ooms ows 1 0.0288427 0.028843 0 SR oma pr 10 3.3419208 0.334192 n Ses 3 11 3.3707635 F Ratio 0.0863 Prob>F 0.7749 ome PaSrdaEmmeotrer str(aPtaetso Pobl Lowes Estimate 00s amas 00 0% owes 0.0122559 D07w omens 0 ome Oo -0.007787 Parameter Estimates Std Error t Ratio 0.273326 0.04 0.026506 -0.29 Prob>ltl 0.9651 0.7749 Lower 95% -0.596757 -0.066847 Usparsst Upper 95% Gear 0.6212687 oss 0.0512728 MSMuaabddjeeecAAtvvaoaillaParbbollteeebbcyiyv33eMMOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo.ppyyNoii.nnggCa2a-ss0CC4oo-nn6fi3fd0ie9dnteinatl IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00334400 MAT0050773 3MA10050773 stig All Participants rl rn Female Chemcial Operators ris mop vscren In PFHS ppm ByYRSCHEM Bet AAppppeendnidxiNxN Page 3 i, : a" oo 8 a54 sitTerm ua Intercept 5. YRSCHEM =Lim Ft sons rear LinearFit AE oss vascre In PFHSdfppm =-2.3774+0.05385 YRSCHEM a Summary of Fit sigs J RSquare 0.275351 ey on RSquare Adj 0.202886 EE te EL Root Mean Square Error 0.602463 Ss tm ome" Mean ofResponse -1.93766 woo sOarEe Source So rsh Model pos 3 Tim Error BF. Cogpoosof JV[SeEs--TEm--Ean CTotal Observations(or Sum Wgts) Analysis of Variance OF Sum of Squares 1 1.3791706 to 3.6296113 11 5.0087819 Estimate -2.377407 Parameter Estimates Std Error t Ratio 0.284848 -8.35 12 wesw Mean Square wes 1.37917 Tie 0.36296 om F Ratio Co3.7998 =i Prob>F 0.0798 cy Prob>Iti ml<.0001 wa Lower 95% Gu -3012092 0.0538465 0.027623 1.95 0.0798 -0007703 ttn Upper 95% -1.742721 baw 0.1153959 de Avaiaio by 3 for nspectan and Copying a Gnfdental formation Made Available by 3M for Inspection and Copying as Confidential Information: Fryer by Sb const Sob Subject to Protective Order In Palmer v. 3M, No.C2-04-6309 281122..00334411 swatoosarre 3MA10050774 Jo. c All Participants Female Chemcial Operators ronan In POAA ppm By YRSCHEM . = :Eo EH AAppppeendnidxiNxN Page 4 m + 'G yi-Kll enTerm joIntercept Bom. YRSCHEM w gm o EaLoieln,Etou e--nJ EQ= --pUEEoRE -- eweaJ geonoaussi Source Linear Fit In POAAppm = 0.32148 -- 0.03055 YRSCHEM Summary of Fit RSquare 0.079815 RSquare Adj -0.0122 Root Mean Square Error 0.715366 Mean of Response 0.072008 Observations(or Sum Wgts) 12 Analysis of Variance DF Sum of Squares Mean Square rtaeeF Ratio Model 1 0.4438781 0.443878 0.8674 Error C Total 10 11 Shoamre Estimate 0.3214819 5.1174828 5.5613609 c SEa ESO, Parameter Estimates R Std Error t Ratio oR Wene mamEen Tmenn 0.33823 0.95 0.511748 Prob>F 0.3736 Prob>JtJ 0.3643 Lower 95% -0.432145 Upper 95% 1.075109 -0.030548 0.0328 -0.93 0.3736 -0.103632 0.0425361 O Hate aettrSD lrnecnndCA oma CoreRore Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00334422 -- 3MA10050775 Anpancomns All Participants Fame CrametOpaaors Female ChemcialOperators Pros oom By veSCEM In PFOSAA ppm 8y YRSCHEM | AAPpaopggeeen'dnsidxixN Page 5 go ~~ 324 T-- | "an + : . I ? I 7. ID 2C woYRSCH;u Sours source Sie Model EreError Cow C Total TomTerm nent Intercept VRSCHEM YRSCHEM =W3 r1 Leura Linear Fit In PROSA456A7 M-00f569oYRSpCHmEM In PFOSAAdfppm =-4.5678 --0.0569 YRSCHEM SaraFyt Summary of Fit Rsque asass RSquare 0.06068 RqueAl o0mas RSquare Adj -0.03325 Root ean Sauce Ero stanes Root Mean Square Error 1.543965 MeanofRespone Sams Mean ofResponse -5.0325 Observations or Sum Wet) fi Observations(orSum Wgts) 12 Anaotvyariaance Analysis of Variance or Mamoitm emSuae Frio DF Sum of Squares Mean Square | rr Sms oa 1 1.539949 1.53995 0 sawn D606 eet 10 23.838281 2.38383 i 25m a 11 25.378230 F Ratio 0.6460 Prob>F 0.4402 Gunso SPatamnon EsiimRaaekso Publ lowrssn Estimate SSO omy aa om oman -4.56783 aos Ooms os osm dies -0.056899 Parameter Estimates Std Error t Ratio 0.729997 -6.26 0.070792 -0.80 Prob>Itl <.0001 0.4402 Lower 95% -6.194374 -0.214635 Upperosw tipper 95% Dai -2.941286 oles 0.1008375 MSMuaabddjeeecAAtvvlaaoillaParbbollteeecbbtyyiv33eMWOfrfodorrIenrIsnIspnpeePcctatilioomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo.nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00343 MA10050776 3MA10050776 FomaloAAlCl hPPeaarmrtcsicaciplpaaOnnptsesrators Female Chemcial Operators IInn MM557700 ppppmm By By YRSCHEM YRSCHEM ARrpoappgeeenn6ddiixx NN Page 6 SMooSuodruerclcee ErCEMrToordoorerult C Total TTIneoerrmmeept YIYRnRtSeSrCcCeHHpEtEMM FE 1-31 .-a3B ] 0 . . " a 10 20 wo IRS LHE4 Ee In 570ppm = 2.1LL0ii0nn9eeaa-rr0FF.iitt0371 YRSCHEM In 570ppm Requare = -S`2Su.um1m0mm0aa9rr--yy0oo.ff0FF3iit7t.1 YRSCHEM 0111759 RRRRSoSqoqqutuuuaarMrreeeesAAnddS)jquareError 0o00..001221m92197335449 MRMOboeesoaaetnnrvMooaefftRaiRenoesnsSsppqoo(unonarssreSeeuEmrrWoreis) 0.721322 220927 -2.40387 Observations(or Sum Wgts) 12 OF AAnnaSlauyimsiossiooSffqVVuaaarrieaansnccoe MeanSquwe 1D0F11 Sum o005f.26S60sq53iu406a6144r077e59s Mea0e0n.5S6s2q5ui04a60sr45e8 n10 It Ss769m4 5.2030495 5.8576974 0.520305 F1FR2Aa5at8ti2oo PP01rr.2o2o8b5v8>8o2F2 0.2882 2EE1ss0tii0mms0att3ee 00709 -2.100903 -0.037098 PaPraSarOamEmemeottreerr EEssttitimmRaaattleesos 000S.03t3d344E011r070r4o346r t-RL66ai.t11iz6o6 0.033073 -1.12 Pr0Poo0bb>0slit1ll 0282 0.0001 0.2882 LLo2ow8we6er0r98d50S%8% COWL -2.860804 -C.110791 UpU1pp.ep3re4r9190505%1% 00s -1.341001 0.0365942 MSMuaabddjeeecAAtvvataoiillPaarbbollteeebcbyiyv33eMMOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppNyyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00334444 3MA10050777 3MA10050777 iy All Participants aader Female Chemcial Operators emt In PFOSA ppm By YRSCHEM Co ---- - I | " | -?1~ Ll | i ; bi | stopsre Appendix N Page 7 -6.00 da10 `llljc-w -ITerm Intercept YRSCHEM EoSource Model Error C Total =Ift! 7 or Linear Fit IInn PPFFOOSSAAdffppppmm == -44..66222266 ++ 00..00776644 YYRRSSCCHHEEMM ts Summary of Fit rer oon RSquare 0.095234 Be, fe] RSquare Adj 0.004758 rn tt Root Mean Square Error 1.624037 Ei A Mean ofResponse -3.99866 Et een " Observations(or Sum Wgts) 12 J Analysis of Variance iv DF Sum of Squares Mean Square LL ToEE Tym 1 2.776184 2.77618 =mF Ratio 1.0526 10 fcoem11 Estimate 26.374947 29.151132 EprEcEarEe Parameter Estimates BEER Std Error t Ratio 2.63749 Prob>F mnProb>ltl i mm0.3291 Lower 950% -4.622563 0.767855 -6.02 0.0001 -0.333461 0.0763964 0.074464 1.03 0.3291 0.08952 ome Upper 95% -2.911665 0.2423128 a unto yt pcm cro sn Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00345 SI 3MA10050778 FomalesuCpraormecoanpsears All Participants Female Chemcial Operators mwsspmovesorew in M556 ppm By YRSCHEM -25 : i . Bn AAopopngeenydnidxixN Page 8 -S0 "3 sbi w a 0 10 20 1ISCHIN sEVoSMorooutuodrreecslre CErrroorat C Total TomTerm Inert Intercept Vestn YRSCHEM =trafi Loot Linear Fit InMS=3S.14694 -d005i942pYRpSCHmEM In M556dfppm=-3.1494--0.05942YRSCHEM SamaalyFa Summary of Fit Rqure oispers RSquare 0.159673 RareAG aorseit RSquare Adj 0.07564I RootMenSqrErr asioiss RootMean SquareError 0.940158 Mean of Response Fri Mean ofResponse -3.63466 Ovsrvton orSumWet) i Observations(orSum Wgts) 12 Aas ofVararco Analysisof Variance or "Thoisqmm ManSwwe Frio DF Sum of Squares Mean Square | fr ows owt 1 1.679525 1.67953 sss Gime Pues 10 8.838975 0.88390 i 10518500 fir 11 10.518500 F Ratio 1.9001 Prob>F 0.1981 Gao [ Sater -- Rm Publ Lowers Estimate Slew omen 70 col aime -3.149387 Sowa oki 13% owl cissel -0.059421 Parameter Estimates Std Error t Ratio 0.444513 -7.09 0.043107 -1.38 Prob>ItI <.0001 0.1981 Lower 95% 4.13983 -0.155471 Upporosw Upper 95% oie -2.158945 oot 0.0366281 MSMuaabddjeeecAAtvvaoaiilaParbbollteeecbbtyyiv33eMMOfrfoodrrerIInnIssnppeePccattiiioomnneaavrnn.dd3CC.ooppyNyoii.nnggC2aa-ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122.00334466 MA10050778 3MA10050779 FanJauapaErncgpraanms All Participants Female Engineer/Lab _In PnFOSPppmrgByyvoYARSSSCCHHEEoMM__p__m 0 | -060 - AAPpoopepe'ensdnidxixN Page 9 Zfog i ~ 1 1 . [ . I ~ . 1 . a-26D TT a48I 84Ws 0 1D 15 2D 25 30 35 ISCHN SoSNouausrecoe EmECMrorerdooreralt C Total Tsreourmmc VInRtSerCceHptEM YRSCHEM irm f1 Lows Linear Fit In PFOSUfopm = 1.3939 + 001024 YRSCHEM InPFOSdfppm=-1.8939+0.01024 YRSCHEM Summaryof. Summary of Fit Rsqure ous RSquare 0.058759 RsaureAd ours RSquare Adj -0.0757 Ro: Mean Square mor 00s Root Mean Square Error 0.505477 Nico Response aosol MeanofResponse -1.80801 Ovscoaion or SumWes) 5 Observations(orSum Wgts) 9 AnsofVyarsco Analysis of Variance or Bisa MemSawe Frio DF Sum of Squares Mean Square | Oiesss "Ones own 1 0.1116544 0.111654 7 Uiissor ows pew 7 1.7885504 0.255507 : 15002046 os 8 1.9002048 F Ratio 0.4370 Prob>F 0.5297 Gran PSaurfmmootre EsimRatees Poni Lows Estimate dol oa 8% <a amis -1.893913 om 0016 06 0597 omews 0.0102397 Parameter Estimates Std Error t Ratio 0.212779 -8.90 0.01549 0.66 Prob>ltl <.0001 0.5297 Lower 950k -2.397059 -0.026388 Upporssw Upper 95% woes -1.390766 Obes 0.0468678 MSMuaabddjeeecAAtvvaoaiilaParbbollteeecbbtyyiv33eMMOfrfoodrrerIInnIssnppeePccattiiioomnneaavrnn.dd3CC.ooppyNyoii.nnggC2aa-ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00347 MA10050780 3MAII0050780 | w]e | FeAAmlnlipPaaErntnicgcoirpoaanantsrsia n Femaploe mEnBge yinveAerS/CLaHbEM In PFHS ppm By YRSCHEM APAapogppeeennd1i0dxixN Page 10 HS a -- ( - 1 - I - 1 - I - I - TA ws C 5 Ic IS 20 25 30 JS wow1iD[w TomTerm incr Intercept VRSCHEM YRSCHEM Sauce Source Nie Model EroError Cow C Total =Leo ti [roe Linear Fit InPEH=39S06 +H003p0LS YpRSCmHEM In PFHSdfppm = -3.9868+0.03015 YRSCHEM Summaorl Fyt Summary of Fit Rque oisions RSquare 0.138988 Rqure Ad anisos RSquare Adj 0.015987 RootMeanSquare Er as25i69 Root Mean Square Error 0.925469 Mean ofResponse 573389 MeanofResponse -3.73389 Obseraions or Sum Wet) 5 Observations(orSum Wgts) 9 Ansys variance Analysisof Variance or "mois Mnswwe Frais OF Sum of Squares Mean Square | Gos "osdmn io 1 0.9679134 0.967813 7 soos owews pone 7 5.9954503 0.856493 s ase osm 8 6.9632637 F Ratio 1.1300 Prob>F 0.3231 Esimwa [ Safer r -- iFaks Pod wero Estimate SO OME om <n sows -3.986788 oor omss 106 omy mers 0.030147 Parameter Estimates Std Error t Ratio 0.389573 -10.23 0.02836 1.06 Prob>111 <.0001 0.3231 Lower 95% -4.90799 -3.036915 Uppeeosw Upper 95% does -3.065586 oom 0.0972088 MSMuaabddjeeecAAtvv{aa0illaPabobltleeecbbiyyv33eMWOfrfodorrerIInnIssnppaePccaitilioomnneaavrnn.dd3CCMoo,ppNyyoii.nnggC2aa.ss0CC4oo:nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00334488 amA10050781 3MA10050781 au parcpuns All Participants FormaEngranrian Female Engineer/Lab 0PM pm8 vaSCHEM In POAA ppm By YRSCHEM IE |. ad i" _' 0 CTT G 5 to . Rd. IS ?o ?, 30 3" aY.+.St1u PAAapcgpgeeennd11isxixN Page 11 sous Source Voie Model EoError Show C Total TomTerm nec Intercept VRScHEm YRSCHEM -M it Unat Linear Fit 1a POAApP =-2368+ 000283 YRSCHEM In POAAppm =-2.5628+0.00289 YRSCHEM Sommer alPe Summary of Fit Rsqure aires RSquare 0.001765 RqureAt Dates RSquare Adj -0.14084 RootbeanSureEre ais) Root Mean Square Error 0.848257 NeamofRespone rif MeanofResponse -2.53853 Observation or Sum Wet) 3 Observations(orSum Wgts) 9 Ans of vararca Analysis of Variance or MSmoitaum Mensa Frio DF Sum of Squares Mean Square | omer "Oxbs oom 1 0.0089035 0.008904 3 Smee ones poor 7 5.0367756 0.719539 : Sauseror ons 8 5.0456791 F Ratio 0.0124 Prob>F 0.9145 Ewe [ SoEmr-- (Rms Pub Lowrssx Estimate Shims owl aa od sons -2.562785 Goons Omsws Ol Gos oom 0.0028915 Parameter Estimates Std Error t Ratio 0.357071 -7.18 0.025994 0.11 Prob>ltl 0.0002 0.9145 Lower 95% -3.40713 40.058575 Userosw Upper 959/6 ines -1.718439 ook 0.0643584 MSMuaabddjeeecAAtvvlaaoillaParbbollteee cbbtyyiv33eMWOfrfodorreIrnIsnIspnpeePcctatiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo.nn6ff3iidd0ee9nnttiiaall Information Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122.00334499 amAt0050782 3MA10050782 =-! ~. wrialmoen. All Participants Female Engineer/lab sro In PFOSAA ppm By YRSCHEM oe AAppppeendnidxiNxN Page 12 E S.SO f s -5 00 -6 SC -Gwmr. Term Intercept YRSCHEM -1.00 S 10 1S 70 7S C 3S YRSCHN --= _ Lr or(i wTo rwiBiogrneiEneWssgteCvSnJTee rpEreweo= epawis) re Source Zz TEE Model = Error EE fESmEe SmRSEoEEmEEyEEoa swWmma5 CTotal Linear Fit In PFOSAAdfppm = -6.1434 --0.02633 YRSCHEM Summary of Fit RSquare 0.103266 RSquare Adj -0.02484 Root Mean Square Error 0.957088 Mean of Response -6.36431 Observations(or Sum Wgts) 9 Analysis of Variance DF Sum of Squares Mean Square 1 0.7384073 0.738407 7 6.4121225 0.916018 8 7.1505298 F Ratio 0.8061 Prob>F 0.3991 Estimate -6.143411 Parameter Estimates Std Error t Rata 0.402883 -15.25 Prob>ltl <.0001 Lower 95% -7.096087 -0.026333 0.029329 -0.90 0.3991 -C.095686 pu Upper 95% TaEmR -5.190736 0.0430203 Erol hryaie-- Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00335500 ---- 3MA10050783 FamAAallll oPPaaErrtniigcciipnpaoannwttrssLab Female Engineer/Lab iInn MM557700 ppopmm BByy YYRASSCCHHEEMM . z 1 . ARPpappgpeeenndd1ii3xx NN Page 13 Zand T as T Er F r -f I' 1 t - S3 5As8 8s S 10 15 20 wo YRSCH-V MSSoooduurerclcee ErCEMroorodoerrwl C Total TTIoneermrmcept YRSCHEM Intercept YRSCHEM Smit :rW ft In $70pp=m 3L.iLnine5e+aar2r0F0Fii13tt2135 YRSCHEM In 57 RSqure 0ppm = Summaroyf Fi -3.5233+0.0121 Summary of Fit 5 YRSCHEM 0030399 RRSRRoqSSouqqtuuaMaarrreeecaAAnddSjjquareError 00-".8000.4.3116000238891918292 MObRMesoeaeoarntnvMoaotfefi'aRRoneensssSppq(oouonnarssrSeeeuEmrroWrars) 0.846298 42136s -3.42136 Observations(or Sum Wgts) 9 DOFF1 7751 8 SEEss2timme9atee 00121493 -3.523279 0.0121493 AAnSanluymasoisloiofSfyVqVauasrwriieiaasnnsccee Sumsoo0af.r1Ss35qss7u1aai8re4se5ys sa707315 5.0135469 5.1707315 PSPaadrrEaammmeeottroerr EEssttRiimmaaattoeess 000S.t033d255E96r423r47o47r t -R909a8.t48i979o 0.025934 0.47 MeMaeonmISSsqaTuuiawsrese 0o.n15e7R18l5 0.716221 F0F2RR1aat9li5oo P00Pr.6ro2o5b1v3>9s7FE5 0.6537 P<rPoOobb>NIitIlI 06Sy <.0001 0.6537 L4oLw3oew6re5r96s57s6%% 40.306156676 -0.049176 U2pU6ppep8re0r98s58s3%w 0-20.7684078833 0.0734743 MSMuaabddjeeecAAtvvataoiillPaarbbollteeebcbyiyv33eMVOfrfodorrerIInnIssnppeePccattilioomnneaavrnn.dd3CCMoo,ppNyyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00335511 3MA10050784 3MA10050784 FomAaalll oPPaaErtntigccnpioapeannrttissLab In PFemE alpepEmO ngBiyneVS eAr/SLCaA bHEM in PFOSA ppm By YRSCHEM wl | - AN Llbe Lind . io a HERE RE AEE 'D o'wS C 25 1SCHEN || | AEA) ;D 1S APAppappgeeenndd1ii4xx N N Page 14 SMooSuodruerclcee ErCEMrroorodoarerll C Total TIYnIToRneetrmSremrcCceeHpttEM YRSCHEM L"I Fi IInn PPFORSAOdfpSpmAS==Ludi-L5inm5n.eie25maa28rr8a5pFo5Fiifr++.tpF0y0i0.t0m0077 YYRRSSCCHHEEMM RRRSSqqquuuaarrreee Ady Summary of Fit 000.0.0010232898757979 OMRRMRboSoeesoqoaaetutnrnavoMMroafeefteRaaiReAonnesdnsSSspjpqqoouuonnraassSrreeeeuEEmrnrooWrrs) 11-5.0664.0016553999983353227 9 -5.46983 Observations(or Sum Wgts) 9 oDFF| AAn"alSnyusmiososiofSfVqVauyaraririaeasnsnccee Sum of0S0q5u2a1r2e3s MMeeamnonSSqgquuaiwree FForRaiotioo 7871 1110888..100050553523121113127973 25902 0.05212 2.57902 PP00r.8ou05b21r>00F2 8 18.105239 0.8910 SEEsstiiTomamtse PPaarSraaGmmEeetmteerrEEsstti(immaRatateeoss 0St6d0Er1r2or B18 t Ratio PP<ruobb>0l11i1 LL7ooww0err0d9s5k%% 0096 -5.528517 0.0069962 00212 0.676012 0.049212 014 -8.18 0.14 0MI0 <.0001 0.8 Cie -7.127044 - 910 0.109374 U3Uppp0oewrmr90o5s8%n 0123366 -3.929989 0.123366 SMMuaabddjeeecAAtvvataoiillPaarbbollteeecbbtyyiv33eMMOfrfodorerrIInnIssnppeePccattiiioomnneaavrnn.dd3CCMoo,ppyNyoii.nngg2-aas0s4CC-oonn6ff3ii0ddee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00335522 33MMAA1100005500778855 o_li All Participants Female Engineer/Lab pe In M556 ppm By YRSCHEM -- =AAppppeendnidxiNxN Page 15 weTerm Intercept YRSCHEM I $i Ewwnaetor"imnpeesi%: Source 2 1m Model Error mn aTZps mr wm CTotal =Lrca it Linear Fit In M556dfppm = -5.0701 + 0.02647 YRSCHEM Summary of Fit RSquare 0.119476 RSquare Adj -0.00631 Root Mean Square Error 0.886382 Mean of Response -4.84805 Observations(or Sum Wgts) 9 Analysis of Variarxe DF Sum of Squares Mean Square 1 0.7462412 0.746241 7 5.4997153 0.785674 8 6.2459565 Parameter Estimates F Ratio 0.9498 Prob>F 0.3622 Estimate Std Error t Ratio Prob>ltl Lower 95% -5.070124 0.37312 -13.59 <0001 -:.952419 0.026472 0.027162 0.97 0.3622 -0.037757 omUpper 95% -4.I87828 0.0907015 Made Available by 3M for Inspection and Copying as Confidential Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00335533 3MA10050786 ret Appppeennddiixx OO Page 1 Appendix 0 Appendix O WSShccasottttweoorrrppllkooettdss(awaennrdde rroeeggyrreess1ssiiohonness))foofmf ffllluuaoorrtoocc(hhnee=mmiic3c6aa)ll wllietveehlsevoosffrerraawlnnvddrosokmmedssaaimmnppilleem who worked were only in the film plant(n = 36)with years w )rked in film Made Avalabl by 3fo Inspection and Copying as Confdental formation SSMuuabbdjjeeeccAttvtatooilPParrbooltteeeccbttyiivv3eeMOOrrfoddreerIrnIIsnnpPePcaatlilmomenreavrvn..d33CMMo,,pNyNoio.n.gCC22a--s00C44o--n66f3i3d00e99ntial Information: 2881122..00335544 i 33MMAA1t00005s00778877 [[og--i Random Sample arWaro es hom Only Film Employees mbre (Maintenance Workers Numbered) J------ InPFOS ppm By YrsFilm 19 mt vo Jia werLo .?3 .39 400 -J2S I .?1 eS so tToatdI, .so : z.] -t.00 TT EE 5 10 1S 2C i~ JG veYf5! fit Page 2 AAppppeendnidxiOOx Page 2 TomTerm men Intercept Ym YrsFilm -- Im ri souen Source brModel BrError EEC Total POVF6 ri dme:=? J Linear Fit FOstfom= 5300 1000813 YF 1nPFOSdfppm=-2.3024+0.00313 YrsFilm SumaFna Summary of Fit Rae sous RSquare 0.002948 RenAg ie RSquare Adj -0.02638 Roo en SqueErer ou RootMeanSquareError 0.585965 NeufRests ris MeanofResponse -2.25946 Chivaton onSum We) % Observations(orSum Wgts) 36 RootoVarasrco Analysis of Variance or hui Mensawo aio DF Sum of Squares Mean Square " Ooms ootats oi 1 0.034516 0.034516 u Nein oss per 34 11.674079 0.343355 3 ied wn 35 11.708595 F Ratio 0.1005 Prob>F 0.7531 Cunae S[ at -- i Pon eres Estimate SS Chee hh em Sune -2.30237 Ga cums om omn oon 0.0031336 Parameter Estimates Std Error t Ratio 0.166902 -13.79 0.009883 0.32 Prob>ltl <.0001 0.7531 Lower 95% -2.641553 -0.316952 Ura Upper 9510/0 ew -1.963187 oom 0.0232187 MSMuaabddjeeecAAtvvataoillPaarbboltleebbcyiyv33eMOfrfoIodrnerIsnpIsenpcePtcatiiloomnneaarvnn.dd3CC,ooppyyNoii.nnggCa2a.ss0CC4oo.nn6ffi3dd0ee9nnttiaall formation Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00335555 aMA00S07E8 31VIA10050788 AAPppappgeeenndd3iixx 00 Page 3 TTIeonrmcmest YIYYrnratfseFisriclilempmnt YrsFilm^2 10PFO=S2.d5PP1oo1lfl7yy+nnpoomm0ii.paa0ll62Fimi0t8ddeYaggrrreeees==22-F0.i00m21 YrsFim: InPFOSdfppm = Rsquare Summary of Fit -2.5117+0.06209 YrsFilm Summary of Fit -- 0.0021 YrsFilm^:'. oss RoRRRSSSoqqqtuuuMaaierrreeeanAAddSjjquare Eror 000o..s00072280173299453381552 ROMMboeesoaaetnnrMvooaefftaiRRnoeenssSsppqo(ouonnarssrSeeeuErmroWress) 0-2.225.7520592935346166 Observations(or Sum Wgts) 36 MSSoooduurerclcee ErEMCrroroodoerrul C Total oF AAnnaSalulymsyicssiiooSsffqVVuaarariiraasnnccee MemSame D3F22 Sum1o0f007S.9q937u771a718r45e523s3 Mea0oOn.maS4sq8sul8ia7Er2sse6 333 35 11708595 10.731142 11.708595 0.325186 F1FR5Ra0tai9oo PP01rr.2o5o3b0v7>2o3F9 0.2373 2EE5sst1iimm0ast0ee -00C20..0005621G210079080792 -0.002097 PPSaaUrrEaammmoeertterr EEsstt(iiRmmaaattleess 000S.t202d003E37r970r03o11r -t11R22a1.t733i33o 0001231 0.035933 0.001231 1701.73 -1.70 PP<roub>b0lltl <000..00009099803%014 0.0980 LLoo2wweer0r99%5S%% --00020.90l02160110I631T27 -0004602 U2pUpp0epromr9o5ms%n 000-.1021.303050591M17909248475:52 0.0004084 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyNyoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00335566 3MA10050789 3MA10050789 LaOOPnRnRleayyanFinFciidSlseommomEEmSnSmaapprlmicoppvlyleeeeaesissn Ln PFHS ipm B YrsFilm rage 4 AAppppeendnidxiO0x Page 4 Cl 21 [ER TS . EON wo Te 4s 10 1; 20 Yulin nda souSource Sie Model EoError Show C Total TomTerm ncIntercept Vem YrsFilm =i -- LrW It -- hamstan2 -- pow.d 11 saee=? Unearre Linear Fit PFS ppm = 47313 + 0003S Vem laPFHSdfppm=-4.7215+0.00958 YTSFilM Summary oP Summary of Fit Rsque ooitsos RSquare 0.011809 frome Diels RSquare Adj -0.01814 Rook eanSauce Err asi RootMean Square Error 0.882741 MeamotResponse "skess MeanofResponse -4.58683 Obivaion or Sum Wes) s Observations(or Sum Wgts) 35 Anofavansce Analysis of Variance or "Uhuteae Memswwe Frio DF Sum of Squares Mean Square | ame 00M 030 1 0.307286 0.307286 sels omelet 33 25.714619 0.779231 u 250m505 sn 34 26.021905 F Ratio 0.3943 Prob>F 0.5343 Goinae SPabaraerEshiaaots Publ owrssn Estimate Sm Gam mm cowl Swmm -4.721471 Gms 00s; 06 ome ames 0.0095783 Parameter Estimates Std Error t Ratio 0.26122 -18.07 0.015253 0.63 Prob>ltl <.0001 0.5343 Lower 95% -5.252924 -0.121454 Upson Upper 95% soon -4.190018 ows 0.0406102 MSMuaabddjeeecAAtvvalaoillaParbbollteeecbbtyyi v33eMWOfrfoodrreIrnInsIspnpeePcctatiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo.nn6ff3iidd0ee9nnttiiaall Information Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00335577 MA1005070 3MA10050790 AArpappgpeeenndd5iixx O Page 5 TTIoneemrrmcept YIYYrnrntsseFFriicinlempmet2 YrsFilm^2 IInWPPFFHSHdSfippppm=m= -55.330PP01oo1l9y9yn+n+Sooum00mim..ia1m1al66la55rFF22iiy3tt3ddoYYfeerrggFssirFrF.ieeileelm==m22-- 00.0000554488YYrrssFFiillmmy'22 RSRRqSSuqquuaaurrreee A) Summary of Fit 000.222505262107999666 MRRReSooaqootutnaMMoreefeaaRAnnedSsSjqqpuuoaanrrseeeErrororr 000..47277507986940469998666 OMObbessaeenrrvvoaafttiiRooennsssp((ooonrrsSeSuumm WWgeitss)) 3s -4.58683 35 Source OF AAnanSluaymssiosiooSffaVVoaarrriieaasnnccee MeanSauwe MSMEoonodmudoreerclle D2F22 Sum o1f669S.54q574u7838a262r373e505s Mean30SS.8qa20u8wa96r1n1e2 ECroroar l 32 34 2.021505 19.443670 26.021905 0.60761 C Total FsFRaRaaittinoo PP50r.r0o4o0b1v9>3F4F2 0.0094 SEEs3stii0mmaw6tee 00-.05110.6630550S23143838361334 -0.005481 PPSaGarEmaremoelrtoerr EEsst(iiRmmmaatiteoess 000S.t202d995E22r299r98o96r -I1t 1R883a.t121i00o0 00006 0.050289 0.001706 3213.29 -3.21 PPr<ro0bo0>bI0tllI <000..000000003025015 0.0030 LLooSwweerSr9s5Ms%% 0O-.05u00.6e80298o789R96587:744 -0.008957 UU4ppp7ep0r5e90r55s3% 00-.0432.066707706265606080852623 -0.002006 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOrffodorrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00335588 3MA10050791 3MA10050791 random sarc Random Sample en Only Film Employees " tnsaroWm=oBry ahrainnes 1| (Maintenance Workers Numbered) 3 Le Te Ee AAppppeendnidxiOOx Page 6 Te Ss wos ow on TomTerm Toma Intercept erm YrsFilm sauce Source ShaModel omError Ea C Total -- -lkwll ~ mite: ?0 ,vw Ft a=7? Weo=nSo3s5a5s001p79Yen Linear Fit im 1nPOAAppm =-3.5336+0.01719 YrsFilm mao Summary of Fit Rau vous RSquare 0.040923 Ra Al vont RSquare Adj 0.01186 Ro eanSueEr ogists Root Mean SquareError 0.838584 NenofReam on Mean ofResponse -3.29191 Oban or Sum Wi) H] Observations(orSum Wgts) 35 Anotavasca Analysis of Variance or Viet Mensano Fru DF Sum of Squares Mean Square i om oem en 1 0.990187 0.990187 Bo Auge ows reer 33 23.206369 0.703223 Fir an 34 24.196556 F Ratio 1.4081 Prob>F 0.2438 Emo S[ E -- hale Pov lowes Estimate Sm omen Tm Th Then -3.533607 Goes oo ils om ome 0.017194 Parameter Estimates Std Error t Ratio 0.248153 -14.24 0.01449 1.19 Prob>ltl <.0001 0.2438 Lower 95% -4.038476 -0.012286 pees Upper 95% Teen -3.028739 oouere 0.0466736 MSMuaabddjeeecAAtvvataoillPaarbboltleebbcyiyv33eMOfrfoodreIrnInsIspnpeePcctatiiloomnneaarvnn.dd3CC,ooppyyNoii.nnggC2aa.ss0CC4oo.nn6ff3idd0ee9nnttiaall formation Information: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 28122..00335599 amat00s0762 3MA10050792 16POAAR=p -3 9PP5ooll8yy+nn5oommii0a.a1ll31FF1ii3ttddYoeggrrroesses_?F.2-0i00l40m1 Yrs 1nPOAAppm = Rquare - 3 .9 58 5 +`0S.u1m31m1a5roYyfrsFFitilm Summary of Fit -- 0.00401 YrsFilm,".' 0179823 RRRRSSoqqqouuutaaarMrreeeeaAAnJd)Sjquare Error 00o0..7118s27789558s062923 ROMMboeesoaaetnnrovMoafeftaRiRenoesnsSsppqoo(unonarssreeSeuEmrroWres) 0.787509 3290931 -3.29191 Observations(or Sum Wgts) 35 SMoSouodurrecclae ErECMrrolrodooerrult C Total OF AnnaaSluyymsosisiSooffawVVaaarrrieaansnccee MesnSoae DF22 Sum o1f449S.38q354u5151a040r699e155s Mean220S.60q127u70a551r551e5 332 34 24196556 19.845461 24.196556 0.62017 FR3a5Rta0ti8io0o PP3orr.o5oob0s>t8eF0 0.0419 TTIenoermrmcept YYIYrnrtriseFirisclelmpm?t YrsFilm^2 PPaaErrsaaimmmetatoterer EE|ssttiimmaaSttGeeEssror 0-33E1.9s95t35i88m155a070t:e4 000S.2t02d9596E600r08r00o688r 000013 0.1311467 -0.004013 000d 0.050806 0.001724 t(1RR3aa3til7o lP'<rr0oob0>v0It1ol -12223..5353587 0<0o..o000zl01e404d616 -2.33 0.0264 AAPppappgeeenndd7iixx O Page 7 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeebbcyiyv33eMVOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo,ppyyNoii.nnggC2aa.ss0CC4oo-nn6ff3iidd0ee9nnttiiaall IInnffoorrmmaattiioonn:: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00336600 3MA10050793 3MA10050793 oFraRynanFddioommmESSmepamlmpopylleeees ((MMaoiinttaeOnnnalanynccFoeilWWmoorrEkkmeeprrlssoyNNeouemmosbeerreedd)) = InPFOSAApomBy Vesim In PFOSAA at m 8 YrsFilm wtIb a Ego-5r5C 3SandTe . .. Lo . : = "1 Fan etek ee py: .29.t ..12.3& TUTTT,Er wens . , I , , 5i AAPpappgpeeennd&diixx 0O Page 8 ITnTeoerrmimept Yoskilm Intercept YrsFilm SoSMuoourdrecclee ErECMmroreodorertl C Total =irmQ 1aPFOSAAdIppmUn=Lei-naear6rFF.iitt+1010040831 YrsFilm ]nPFOSAAdfppm = -6.1143 + 0.00041 Rsquure SummaofrFyt Summary of Fit YrsFilm 000031 RRRRSoSSoqqqtuuuaaMrreeeeaAAnddSjquare Eor 00-".0700.0900308300072324717 MOebRMsoeaeoarntnvoMoaeffiRaoRennesssSppq(oouonnarssreSeeuEmrrWorats) 0.739574 "6.1083% -6.10856 Observations(or Sum Wgts) 35 oF AAnaSnluymasiosliooSffyVaVauasrrwiiimaasnnsccee MemSquare D3F1| Sum o1f008S.00q005u000a005r5155e133s Mean Square 0o5s49s70 0.000553 333 34 15050564 18.050011 18.050564 0.546970 FRooRaoatloioo PP00r.9or07b04e>18F0 09748 6EEsst1iiema6ltee 0000063 -6.114269 0.0004063 SPPUaarEraammmoeerttaerrEEsst(tiiRmmaaattoeess Std Error 000212S7 0.218854 t Ratio 701093 -27.94 0.012779 0.03 Probl Prob>ltl <0 <.0001 09% 0.9748 LL6oowwee3rr9S05S%% 0589) -6.559529 -0.025593 UpU5ppe6pro6r99d50s0%t 0026053 -5.66901 0.0264053 MSMuaabddjeeecAAtvvaatoiillPaarbbollteeecbbtyyiv33eMMOfrfoodrrerIInnIssnppeePccattiiioomnneaavrnn.dd3CCMoo,ppyNyoii.nngg2-aa0ss4CC-oonn6ff3ii0ddee9nnttiiaall IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 22881122..00336611 3MA10050784 31VIA10050794 HarteOnonaFnRlrayyaensnFPdiduloWommmomEESnmSmaapaprvlmisoppiylNeoeeoeemssbored ny vse (Maintenance Workers Numbered) Ww In M570 By YrsFilm a sn FE Eom 3T, o E = d . = | win" . a Tow 8a as| =1rra fi LoaFni Linear Fit M0 = 45040-00e8s4i4 1nM570=-4.8046 --0.00844YrsFilm Summary alFi Summary of Fit Rsque ameter RSquare Rqure Ad anzsos RSquare Adj Root Mean Square Err Lowen Root Mean Square Error MeanofResponse Sonal Mean ofResponse Observations or Som Wee) % Observations(or Sum Wgts) 0.006167 -0.02306 1.089533 -4.92021 36 source or AoMimuoSfwVwarmssnca Menswae Fra Source Nos | o250ish of 020 Model Ener u D3ataze TE par Error Cow 3 weirs res C Total Analysis of Variance DF Sum of Squares Mean Square 1 0.250458 0.25046 34 40.360826 1.18708 35 40.611285 F Ratio 0.2110 Prob>F 0.6489 TTaemen [ P Emanr --Sao far v Rae e ob Term Intercept Yom Domai oom 0s os YrsFilm Parameter Estimates Estimate Std Error -4.804612 0.310334 -0.008441 0.018377 t Ratio -15.48 -0.46 F'rob>ltl <.0001 0.6489 Paes AAppppeendnidxiO0x Page 9 MSMuaabddjeeecAAtvvaoaillaParbbollteeebbcyiyv33eMMOfrfoodrrerIInnIssnppeePccattiiloomnneaavrnn.dd3CCMoo.ppyyNoii.nnggC2aa-ss0CC4oo-n6nf3ifd0ie9dnteinatl IInnffoorrmmaattiioonn: Subject to Protective Order In Palmer v. 3M, No. C2-04-6309 2881122..00336622 3MAT050795 3MA10050795 OnlRRyaaFnniddloommmEmSSpaalmmoppylleeees. ((MMaaiinnttOeennnlaaynnccFeeiWlWomorrEkkmeeprrlssoyNNeuuemmsbbeerreedd)) IInnMM555566ppopmm By By YVrrssFFiilmm. -100 am-2 00 n-300 "-100 " gin E,-5 DO . 3F-o6o0n0 fe $m-1 Do an-8 Do anAM ~ no-1)DD TS D .21 I ` 5 .39 12 r 1 I r on 8 ID 15 viTafim 888 I1 tD 1 ' 25 3) -S-eIriw H | 1aMSS6dfppm =L-i6Li.nn0ee3aa8r1FFii+tt000926 Yrskilm Squ1anrMe556dfppmS`=uS-m6um.a0m3rm8y1aoo+ffr0FFyii.t00926 YrsFil0m 0982 RqRRRouSSouqqtuuraaMrreeeeaAAnddSjjquare Bor 0-1".0200.10003252319320825952 MObRMesoeaeoartnnvMoaoetffiaRRoneenssSsppqo(ouornarssrSeeeuEmrrWorets) 1-".552.91913111133036669 Observations(or Sum Wgts) 36 SMoSouodurerclcee EnECMrooordoraerll C Total OF AAnaSlunymsiosisooSffVqVayuarraiieaasnsnccee MeanSque D3F1' SumS0of000S.33q308u01a151r1222e488s Mean00LS.3aq3u00na11er13se3 333s54 So336652 50.035524 50.336652 1.47163 TTInoeermrmeept YrsFilm Intercept YrsFilm PPaaErrsaaimmeemltaoesrrEEssttiimmaatSteeGssEror {Rao 0-G6E0.s0Ot23i8m51Ia0ts9e 000S.t033d045E45r556r3o212r t-01R704a.t447i57o 0.0092556 0.020461 0.45 FF0R2Raa0toi4o Pp0err.so2vb0is>4sFF6 0.6539 Pr<Por0bo>0b10o1l1llI 06s <.0001 0.6539 AAPppappgeeenndd1ii0xx O0 Page 10 MMaaddee AAvvaaiillaabbllee bbyy 33MVffoorr IInnssppeeccttiioonn aanndd CCooppyyiinngg aass CCoonnffiiddeennttiiaall IInnffoorrmmaattiioonn:: SSuubbjjeecctt ttoo PPrrootteecctiivvee OOrrddeerr IInn PPaallmmeervrv.. 33MM,, NNoo..CC22.-0044--66330099 22881122..00336633 3MA10050796 3MAII0050796