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DATE PRINTED: 1 2/03/81
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CODE RT-618-D *.Pi$6, *
PROCESSES .
APPRO
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fi 2 9 mi '**'G2H3l"
< JRT-618-D <S)
<"d at e")"" Tl o t ~n u mber T
TYPED BY: JMH
ST. WT. 2760* LBS. '" STD/ HRS' 1 ___ TIME___ ,__M
JJG 3-18-81 EWK 11/12/81
! \I
COMTYP JOB NAME: 32RT61BDMS
PREPARATION NOTES:_______________
EQUIP MENT
NAME: WATCHUNG RED Y
PREP 1
'1 I RECORD:__l_____BATCHES SINCE SPARKLER LAST i CLEANED. AFTER 4 BATCHES, CLEAN, DRESS i SPARKLER & PRE-COAT WITH 15$= DXCALITE 1 FILTER AID
2 I OBTAIN FOR S11 2-CHLGR0-4-AMIN0T0LUENE-51 SULFONIC ACID
3 | OBTAIN FOR S24 3-HYDR0XY-2-NAPHTH0LIC ACID 4 1 INSTALL DV & CV RECORDER & CONTROLLER CHART
I NOTE:' NOTIFY PRESS ROOM AND ROPE OFF AREA UNDER V-922
921 / 931
RUN 10-(10G> WATER,-INTO
& ADJ TO
1x80-100 DEG F
sT'Tx ABD IN 1-2 MIN. DRESINATEX-'
X^^LSTIR 2 MIN & RECORD: PH_Z?~i__<9.5-r10.5)
^xf STIR 20 MIN OR LONGER FOR S27
922 .3
RUN 34" (70OG) WATER INTO V-922 WEIGH IN V--926 SODIUM HYDROXIDE & RUN IN,_
m _aP-___ TURN ON AGITATOR & STEAM & DUMP IN FROM S2
! 2-CHLORO-
LOT tG0X %
4-AMINOTQLUENE
-SxSULFONIC
_*L15____ _
J^CIjPx-'
_2LJLl_____ _
w^L-atfPsp in ACTIVATED CARBON
DICALITE FILTER AID
HEAT TO 212-214 DEG F, RECORD HT_^LiJi_* F
LA___ DEG F WATCH FOAM
RECORD BY__<fk_< + ), IF NECESSARY ADJ TO +BY
ODIUM HYDROXIDE
ASSUME 50%
STIR 30 MIN AT 212-214 DEG F, THEN SHUT
OFF STEAM
WATCH FOAM
NOTE: RECORD: SPARKLER PRESSURE___ __PSI
J^fF NOT ZERO, NOTIFY SUPERVISOR
yT CIRCULATE 15 MIN OR LONGER THRU SPARKLER
UNTIL SOL'N IS CLEAR. MAINTAIN AT 190-195
FOR S19 & RECORD: HT.__________DEG F ANDnREpCpnORR,nDF:R* START L^S^dJnMppTOp *TAL MIN__SU2___]
CLARITYjLh]jL.. NOTE: SAMPLE FROM HOSE SHOW TO SUPERVISOR FOR O.K.
NON-BLEEDING
N32911
DUP050464687
MAKING INSTRUCTIONS:BATCH UNIT
EQUIP MENT
OF 3 CG 32 CODE RT-618-D <S>
l USE t N-CODE I ACCT
I LBS |
I LBS
904 !*ri-f?DN 1 1 (50G> WATER INTO V-904 4 ^[Vr \ WHEN SI7 COMPLETE, PUMP IN V-922 THRU
I
I SPARKLER, MAINTAIN V-922 AT 190-195 DEG E*. I I RECORD: START,, TOTAL MIN___ __ . I
MM MM
MV MM
........... I-- MMMMMMM ~<M
--mm >< VMMM MMMM -- MMMMMMMM MM MM -- MM-- MM -........
MISC l^T WEIGH IN PT, FOR S35 SODIUM NITRITE^ _/
5i
___ iJzfi..
!
I |
l-ST--| MEASURE jLlSJ/UNITS IN V-928 FOR S33 . j > |
i I HYDROCHLORIC ACID
M_____!______,--3S1Lx Oitfr=]
725-A 28-D
332 .
CV 6
er
RUN-16" WEJ8H IN
(1530G) V-926
WATER SODIUM
INTO V-_^gE|L HYDROXyj: 4 RU,
'*%
I 7-D I 507
DUMP IN FROM S3
3-HYDR0XY-2NAPHTHOIC ACID
LOT IsSL--
I 253-C !
r.7L*ri
>
vi.?
I T---------- I
!
ADJ TO 70-90 DEG F & STIR TO DISSOLVE
STEAM EJECT V-921/931 INTO CV
1
I
922 WHENJ5U-9 COMPLETE, SHUT OFF PUMP & INSERT i
7 T%2 FOOT PLUG. -
... i
RUN IN 10* (207G) WATER"i HEAT TO 190-195 FI
CIRCULATE 15 MIN THRU SPARKLER*
!
PUMP V-922 THRU SPARKLER INTO V-904
i
RUN IN 5" <103G) WATER INTO V-922 & HEAT TO I 190-195 F, CIRCULATE 15 MIN THRU SPARKLER |
PIMP' V-922 THRU SPARKLER INTO V-904
I
fEN MTY BLOW OUT SPARKLER INTO V-904
I
HE^f TO 165-r70 F (SMPL TO SUPVR FOR 0*l<*> I
IN N-2S-D FROM S21 IN 12-15 MIN & STIR [
MIN AT 165-17 DEG F
|
-TO 129"(3409G) AT 23-30 DEG F AND
|
:CORD: TEMP 45=2-_-*F,
___ " ICE 140X330] 57-A
\9*r \ RUM JN-N--725-A FROM S20 AFAF (5-10 MIN)
|
|
Irf^fi^RINSE IN PT
3^T STIR 3 MIN AT 28--:35 DEG F MAINTAINING
|
I +CR, +KI FOR S4L, AND RECORD:
I
| TIME START__4^S_,, CR_,?_( + ),Kl_rtl--< + 5 I
'.f 1 . . .1 '
I
1
.1
,1
NOTE (1) IF CR-, KI-, ADD 20* AS IS IN-
1 CREMENTS
HYDROCHLORIC ACID ASSUME 32%
] RECORD: CR (+). KI
(+>
i. (2) IF CR+, KI-, ADD 20* AS IS INCREMENTS
i SODIUM NITRITE*
ASSUME 33%
l RECORD: CR
< + >, KI._____
J
I | 1 28-A
1 i * 11 jT" 1 725-A
1
11
I______:
1 1 |___ -
li1 >
",5|'
. -< *
DUP050464688
' ^
--
EQUIP v M&4T
3 OF 3
MAKING INSTRUCTIONS:BATCH UNIT
,, . . I USE 1 N-COtlE 1 ACCT
CG 32 CODE RT-618-B <S-)r~; ,f,J.BS [
" | LBS
UMP INTO CV BARIUM SULFATE
, 180
ADJ TO 37* (3496G) AT 28-32*F
ICE '
34X3301
TEMP__fStOL-DEG F 6 VOLUME
IN FROM DRUM AMMONIUM CHLORIDE
273 MIN
` *.
ATELY COUPLE DV THRU UNDERSURFAl|
BUTOR INTO-CV IN 45-60 MIN. MAINTAIN
AT 28-32 DEG-'T. RECORD: STfiRT_/OJjteflP
TOTALS IN
__
'
3 MIN & RECORD.. EttSE _JrT___C + ),
_ZX__. <->, PH__X.'lL__ (9.0-9.8)
i
FlNAk TEMP 2D__DEG F
<--
SARY, ADJ TO PH 9.0-9.8 AND RECORD l *4* .
SODIUM HYDROXIDE ........ ASSUME-50% 1 SO . J
^HYDROCHLORIC ACID
ASSUME 32% 1___ ILj .
HEAT TO /^-VSftDEG F IN 65-70 MIN AND
I ' l
RECORD: HT_!rT5_DEG F & RECORDER JSl S_DEG F I
NOTE: AT 174-17,6 F, OPEN WATER SPRAY
lI
1 1/4 TURNS
.
JI
--
s<~' /
i.
\ 1
1 1
_* C600G) WATER INTO DV
I
AGITATOR & STEAM & DUMP IN BARIUM
1620 I
#1 16-B r 1620
& STIR TO DISSOLVE
WHEN S44 COMPLETE, IMMEDIATELY STRIKE pv
DERSURPAGE DISTRIBUTOR .INTO CV IN MIN. MAINTADL CV AT i$V~'/g$6T>EG F.*l
STARTr,mBMT0TALTMIN_J3______
CV TO 198-202 DEG F IN 10--12 MIN ,
5 MIN AT 1
F
T0 180-190' (V"18,00OG)
RECORD: PHjLS__<9.0-9.4> 6 STOP AGITATOR SHUT OFF WATER SPRAYS
l
START
FIN
WHEN INSTRUCTED BY PROCESSING AREA HALF WAYi
THRU PRESSING, DUMP IN, STIR 5 MIN & STOP !
i
1
AGITATOR. RESUME PRESSING. I-OCTANOL
- 1-10 i 588-A | 10
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