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November 1, 1990
Nike Thompson BF Goodrich P.O. Box 57B Plaquemlne, LA 70766-0678
Deer Nik*.
Hero la the answer to your Inquiry about the MlniMonltar. You `specifics!ly asked about availability of refurbished HlnlMonltoro and about the oompasltion of the plastlo begs.
Present deliveries are from 4-6 weeks but should Improve to 1-2 weeks by January 1990. The plaacio bag is made from polyethylene and should be used for only short term storage of the MlnlHonttor. To minimise contamination of the bags and therefore the monitor* the bag may be stored In a desleeator <not the one used for the via! kits) with "protection charcoal,-
Copies of the current price list and the operating procedure are enclosed for you to distribute at the upcoming meeting. The price llet includes the cost of analysis of samples submitted to REAL.
Yours truly.
Ph.fi., President
ec. Other BF Ooodrleh plants via KT.
BFG50859
POST OFFICE BOX 3341 BATON ROUGE, LOUISIANA 70821 * TELEPHONE 504 - 387-0676
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RHttKW etfVIRQNMtm * AWM.VTICAL Ult, INC.
November i ie9ki
Dear Customer,
This letter Is to Inform you of severe! change* that have occurred at REAL, Inc. A1 thouoh the Baton Rouge address and phone No. will be active for some time the use of them may slow order processing.
We have had massive da I ays in processing orders for mew or refurbished monitors and must apologize for them. Deliveries should bs improving shortly*
The density of the charcoal has changed again and the new recommended charge will be printed on all bottles shipped
after September 5, 1990. If you use the premeasured vial, you needn't make any changes in your procedure. The adsorptlon-deeorption -properties are Identical to previous batches. The new charcoal has a narrower mesh range of 20-36
mesh, fewer snail particles, and will appear to have a somewhat larger size than the 80*40 mesh,
To keep you up to date ve have Included with this letteri
1. Price list 2, Procedure 9. Material Safety Data Sheet
You may Place orders and return MlniMonitcra via U*S Mall to; 1
REAL, Inc,
P.0, DOR 1067 Lecomptv, LA 71346
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You may return MiniMonitors via UPS, Federal Express, etc. using the physical address*
REAL, Ino, 43 WlUy Rd. Lsaonpfce, LA 71346
You may Place orders or make UiquIpIm at the telephone No.i C3LQ) 776-6410
Yours truly, Kenneth D, Relszner, Ph.D,, President
26424002
BFG50860
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POST OFFICE BOX 3341 - BATON ROUGE, LOUISIANA 70821 TELEPHONE 604 - 387*0679
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0-20 MlnlMonltor for measuring vinyl chloride
136.00
0-20-U MlnlMonltor uncallbrated
96.00
0-20-1 RecalIteration and replacement of MlnlMonltor
696.00
(Each monitor ! recalibrated* inspected and
clement led. Each MlnlMonltor is replaced with
a rebuilt MlnlMonltor manufactured from dismantled
parts and a certificate of calibration Is supplied.
Rebuilding Includes replacement of the membrane
and front plate.)
4
0-21 Activated charcoal for MlnlMonltor (lOOg)
622.00/1000
0-22
Pre-measurtd charcoal sample vials, 10 vials/pk. complete with open top capo and eepta for desorption and analyeio and a label-tMlnlmonltor Is filled with charcoal and the eharcoal le returned to the vial for desorption)
623.00/pk.
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Analysis of MlnlMonltor charcoal sampis for vinyl ohlorldsi Prices are based on a minimum of 4 samples per week. The setup charge Includes the price for analysis of a blank which Is to be submitted by client with tne samples. Quantity
discount schedule below does not apply. Ask for quotation or quantities above 10 samp I es/week,
Samples recleved by Friday of one week will normally be analyeed and reported on by Wednesday of the following week.
19.00/sample 26.00/
setup charge
QUANTITY DISCOUNT
6-9 ia-19 20-60 so
la* 16% 20* ASK POP QUOTE
PRICES.2.90
26424003
BFG50861
POST OFFICE BOX 3341 BATON ROUGE, LOUISIANA 70H21 * TELEPHONE 504 387-0679
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MINIMONITOR
RECOMMENDED OPERATING PROCEDURE FOR MEASURING VINYL CHLORIDE IN AIR
Also Freon 12#*
1. Pour 1.05 g of activated charcoal (Cat, No* 0-21 or 0-22) into the MlnlMonltor and attach th* monitor to an Individual as close to the breath 1no zone aa Is practical.
2. After exposure. normally X to 8 hr, pour the charcoal into a 7 mL glass vtat, seal the vial with a teflon faced silicone aepturn(Cat. No, 0-26) and refrigerate the sample at -20 oc If it is to bi stared far more than 6 hra.
ANALYSIS
1. Cool the sample to -20 oc On e freezer) and add 5 irtL af cold (dry ice) carbon disulfide slowly so that no charcoal or solvent spatter from the vial. Standards are prepared (n the same way except the carbon dlaulfida is added to an empty vial (use no charcoal to prepare standards).
Natei The desorption apparatus (Cat. No* 0-24) in figure 1 lo particularly convenient for desorption because it allows the carbon disulfide to be measured at room temperature.
2. Recap the vial immediately after adding the carbon disulfide and allow to stand 80 minutes*
3. Shake the vial at 10 and 20 minutes after solvent addition.
4. Inject S uL into a gas chromatograph equipped with a flame lonizati.cn detector* The column used should be ehosen to separate possible Interfering species that ocour In the environment being sampivdi however* a 6 ft 1/S In, Chromosorb 102 (Johns Mansvllle) or a 20 ft. 1/8 in* FFAP column are oomnonly used. An Internal standard that la not removed from solution by the charcoal Is recommended.
5- Calculate the concentration from the equations
where
"* BFG50862
k constant c concentretion of vinyl chloride* ppm t * time of exposure* hr w volume of vinyl chloride, uL 9 25 oc
26424004
POST OFFICE BOX 3341 . BATON ROUGE, LOUISIANA 70S21
TELEPHONE 504 307-Q679
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STANDARDS
The standards <or calibration, of the oae chromatograph are prepared in the same way that the samples are except that the carbon disulfide la added to an empty vial (use no charcoal to prepare standards)* Pure vinyl chloride vapor (40 uL) Is Injected into the headspace above the S ml of carbon disulfide. Shake well after the addition of vinyl chloride. A teflon lined ellleone septum (Cat. No. 0-26) is recommended for sealing the vials.
REAGENTS
Only activated oharcoal Cat. No. 0*21 (or 0-22 In vials) or equivalent should be used. Carbon disulfide (reagent or speotrosoopic grade) should be as pure as possible to speed analysis time.
calibration of the monitor
The monitor should be calibrated before use If not purchased calibrated. Expose the device to a known concentration (10 ppm) of vinyl chloride for a given period of time (2 hr). This can be done conveniently by placing the monitor In an aluminum or glass chamber (Cat. No. 0-25> with the calibration gas moving through the chamber at about l L per minute per monitor being exposed Permeation tubee Are probably the most accurate source of vinyl chloride standards, while compressed gas standards are more convenient. The calibration constant can be calculated from the equation!
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# To facilitate rapid addition and removal of charcoal a vibrator (engraver) should be touched to the badge clip.
** The same sampling and desorption procedures can be used for Freon12.
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BFG50863
POST OFFICE BOX 3341 - BATON ROUGE, LOUISIANA 70BE1 * TELEPHONE S04
387-0679
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