Document NG4rrKj5JKyoGO8D8eLnjRbo8
HECYCLEO
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AR226-2665
en RESEARCH Precise Research. Proven Results.
AR226-2665
Analytical Report
Air Sampling Fluorochemical Report
DuPont Washington Works - Air Sampling Program Round 10 Exygen Research Report No. L0001667
Testing Laboratory Exygen Research
\ 3058 Research Drive State College, PA 16801
Requester Michael D Aucoin URS Corporation Barley Mill Plaza Building 27 Room 1260 Lancaster Pike and Rt 141 Wilmington, DE 19805
ALL DATA CONTAINED IN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH
Page 1 of 7
\ T: 800.281.3219 k. F: 814.272.1019
exygen.com
I f
Summary
Seven solid media samples were received by Centre Analytical Laboratories, Inc. (dba Exygen
Research) (Exygen) from DuPont Corporation. The media represent samples of air collected on
OVS tubes. Please see Table 1 for a completed listing of samples received and field air volumes
collected. Results are not reported for sample WWK-A-AMS2-E10 because of sampler
malfunction.
a The samples were analyzed for Perfluorooctanoic Acid (C8 Acid) using liquid chromatography
/ mass spectrometry (LCMS). The method employed is entitled "Method of Analysis for the
a Determination of Perfluorooctanoic Acid (PFOA) in OVS Airtubes by LCMS" (James Miller,
Exygen Research, February 17, 2003).
..'y . -L
The OVS tubes were separated into three fractions for specific fluorochemical analysis. Fraction A consisted of the filter, backing material and plastic ring. Fraction B contained the first bed of XAD resin and the PUF backing. Fraction C contained the second bed of XAD resin and PUF backing. Fractions A and B were extracted with 1 mL of methanol. Fraction C was not analyzed but saved for possible future analysis. Perfluorodecanoic Acid (CIO Acid) was added as a surrogate spike to each fraction prior to extraction.
Instrument operating conditions can be found at the beginning of each analytical run. Raw instrument data is given in Appendix A. Chain-of-custody information can be found in Appendix B.
ALL DATA CONTAINED IN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH Page 2 of 7
Results Summary
I ,,
Request#
Air Volume Sampled (L)
C8 Acid (mp/m3)
I
H I
WWK-A-AMS1-E10 A " WWK-A-AMS1-E-1Q 8 . . WWK-A-AMS1-E10C i
WWK-A-AMS1-E10 (Total)
.
: '
WWK-A-AMS3-E10 A WWK-A-AMS3-E1QB WWK-A-EMS3-E10 C
WWK-A-EMS3-E10 (Total)
'
.
1447 7
.
1447
:.'
1447 '
y
'
1413 1413 1413
<0.00007 <0.00007
NA <0.00014
0.0004 <0.00007
NA 0.0004
I : WWK-A-AMS4-E10 A . . WWK-A-AMS4-E10B ;
WWK-A-AMS4-E10 C
1 WWK-A-AMS4-E10 (Total)
. WWK-A-AMS5-E10 A
WWK-A-AMS5-E10 B
I WWK-A-AMS5-E10 C
7
WWK-AAMS5-E10 (Total)
1.410 1410 1410
, 1451 1451
1451
. v
<0.00007 <0.00007
NA
<0.00014
0.0003 . <0.00007
NA
0.0003
.
WWK-A-AMS6-E10 A WWK-A-AMS6-E10 B WWK-A-AMS6-E10 C
.
' 1456 1456 : : 1456
I WWK-AAMS6-E10 (Total)
<0.00007 < 0.00007
NA .
<0.00014
N A - N o t Analyzed. B fraction was below the quantitation limit, therefore th backup fraction does not require analysis.
I 1. "<" is defined as not detected at or above the reported level.
1 2. Sample results have not been corrected for blank results Or control spike recoveries.
3. Please note the following descriptions of the OVS sample tube fractions:
1 Fraction
Fraction Description
,.
I A Frit Extract B 1st set beads extract C 2nd set beads extract (not analyzed)
8
1
ALL DATA CONTAINED INTHIS REPORT WAS GENERATED BY EXYGEN RESEARCH
' ,i4
o ,3
<6. l 4
Page 3 of 7
OC Data
LCS Please note: One control sample was spiked with each perfluorooctanoic acid to give a final concentration of 500 ppb. Air was pulled through the tube at a rate o f 1-liter per minute for one hour (60 liters of air). The fractions were separated and analyzed. The acceptable range for control recovery is 75-125%.
Request # Control 1
C8 Acid (amount spiked - ppb)
500
C8 Acid . (amount recovered - ppb)
619
C8 Acid (percept recovery
124
Blanks
Request# WWK-A-AMSFBLK-E10 A W W K -A -A M S FB LK -E 10B
Voi. Of Air (L)
0 0
C8 Acid (uq/fraction)
0.74 <0.10
ALL DATA CONTAINED IN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH Page 4 of 7
}
Surrogates
.
: .. \
;
.
,
'.
I A surrogate spike (CIO Acid) was added to all OVS tubes to give a final concentration of 500 ppb in the extract.
Surrogate spike recoveries are given in the following table. There are no set criteria for surrogate spike
i recoveries. Advisory ranges are 75-125%.
,
S a m p le #
WWK-A-AMSFBLK-E10 A WWK-A-AMSFBLK-E10 B
WWK-A-AMS1-E10 A WWK-A-AMS1-E10B WWK-A-AMS3-E10 A WWK-A-AMS3-E10 B: WWK-A-AMS4-E10 A WWK-A-AMS4-E10 B WWK-A-AMS5-E10 A
' WWK-A-AMS5-E10 B
WWK-A-AMS6-E10 A WWK-A-AMS6-E10 B
Control Spike A Control Spike B
Amount Spiked
(PPb) 500 500 500 500 500 500 500 500 500 . 500 500 500 . 500 500
Amount Recovered
(PPb) 569 554
540 594 526 : 594 517
;
335 520
491 527 .
391 522
337
Percent Recovery
(%) 114 111
108 119 105 , 119 103 67* 104
.
98 105 78 104 67*
* Surrogate recovery outside o f advisory range.
,v ; v
l
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^
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7 77:/^
8:
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%
ALL DATA CONTAINED IN THIS
DRT WAS GENERATED BY EXYGEN RESEARCH
!A
I Page 5 of 7
Calculations
Request#
WWK-A-AMSFBLK-E10 A WWK-A-AMSFBLK-E10 B
WWK-A-AMS1-E10 A WWK-A-AMS1-E10 B WWK-A-AMS3-E10 A WWK-A-AMS3-E10B WWK-A-AMS4-E10 A WWK-A-AMS4-E10 B WWK-A-AMS5-E10 A WWK-A-AMS5-E10 B WWK-A-AMS6-E10 A WWK-A-AMS6-E10 B .
Control Spike A Control Spike B
Vol. Of Air (L)
0 0 1447 1447 1413 1413 1410 1410 1451 1451 1456 1456 0 0
C8 Acid : (raw-ppb)
738 12 <10 <10 615 <10 <10 < 10 396 <10 <10 <10 619 <10
C8 Acid (ug/fraction)
. ' 0.74 <0.10 <0.10 <0.10 0.62 <0.10 <0.10 <0.10 0.40 <0.10 <0.10 <0.10 0.62
v <0.10
C8 Acid (mg/m3)
0 .aCiO c I
<0.00007 < 0,00007
0.0004 < 0.00007 <0.00007 <0.00007
0.0003 < 0.00007 < 0.00007 < 0.00007
ALL DATA CONTAINED IN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH Page 6 of 7
Example Calculation
..
For sample WWK-A-AMS5-E10 A C8 Acid,
v
,'
= [396 ng/ml of C8 Acid x (1 mL) x (1 u g / 1000 ng) x (1 mg / 1000 ug) ] / [(1451 L) x (1 m3 /
1000 L)]
:
= 0.0003 mg / m3
Signatures
Pl Connolly, LCMS Team Leader
V
Date
John M. Flaherty, Vie President
Other Lab Members Contributing to Data James Miller
Date
ALL DATA CONTAINED IN THIS REPORT WAS GENERATED BY EXYGEN RESEARCH Page 7 of 7
Phone: 814-272-1039 Fax: 814-231-1580
Login Group: L0001667
Logins: Project:
mu
P0000419
. :
Project Storage:
.
Company Name: DuPont de Nemours & Co, Inc.
Submitted By:
Michael D. Aucoin
: ' . '
Login Type:
Immediate Receipt o f Samples
,
Started:
T
-.
Date Start:
01/19/2004
.
.
Due Date:
02/02/2004
;
7
Received Date: 01/17/2004
.'
Received By: AMMERMAN, MARK
Spread Sample:
:^
Label:
;v
Project Title/Type: Analysis o f PFOA in OVS Tubes / ROUTINE
Exygen SD/PI: MILLER, JAMES
7
Login Notes:
-.
Conform Notes:
.; .
Conform COG Sample: Conform COC:
Conform Sample: ; Conform Request: 1
true True
True True .
-
. .
77
7 . ^
.
Package PKD002255
Carton .
Packages / Containers
Mail Date / Condition
Shipper/ ID
1/17/2004 12:00:20PM Package & Contents Uncompronra'sed
FEDEX . 8363912984560200
Temp. Control/Temp
None 23.3
.ta in e r#
C0026135 C0026136 C0026137 C0026138 C0026139 C0026140 C0026141 C0026142 C0026143 C0026144 C0026145 C0026146 C0026147 C0026148 C0026149 C0026150 C0026151 C0026152 C0026153 C0026154 C0026155 C0026156 C0026157 C0026158
Gross W eight 6.3 g 6.3 g 6.3 g 6.1 g 6.1 g 6.1 g 6.2 g 6.2 g 6.2 g 6.2 g 6.2 g 6.2 g 6.3 g 6.3 g 6.3 g 6.2 g 6.2 g 6.2 g 6.2 g 6.2 g 6.2 g 6.3 g
. 6.3 g 6.3 g
e
Container Type
Other
:
Other
Other
Other
Other
. Other
Other
: Other
Other Other
.
Other
Other
Other
; Other
Other
Other
Other
Other
Other
Other
;
Other
Other
Other
Other
P re s e rv a tiv e NONE NONE NONE
. NONE NONE NONE NONE NONE
7 NONE NONE NONE NONE NONE ` NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE NONE
Direction / Handled By RECEIVED
AMMERMAN, MARK
Mfg. ID
. Miscellaneous Item Key None
1/19/2004
Login.rpt
IC O C
Description
^
U0 54
Report Version: Dec 22 2003 10:44AM Page 1 of 4
Instance:
R0080901
R0080901
I*
I . Sample ID ' 91667-0001 J 1667-0002 L0001667-0003 L0001667-0004 L0001667-0005 L0001667-0006 L0001667-0007 L0001667-0008 L0001667-0009 L0001667-0010 L0001667-0011 L0001667-0012 L0001667-0013 L0001667-0014 L0001667-0015 L0001667-0016 L0001667-0017 L0001667-0018 L0001667-0019 L0001667-0020 L0001667-0021 L0001667-0022 LQ01667-0023 L0001667-0024
.
Matrix GAS GAS GAS . GAS GAS GAS GAS: . GAS GAS GAS GAS GAS GAS GAS GAS GAS GAS GAS GAS GAS GAS GAS GAS GAS .
Fraction OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes OVS Tubes ; OVS Tubes OVS Tubes OVS Tubes OVS Tubes
Samples
Sample
WWK--AMSFBLK-E10 A
-
WWK-A-AMSFBLK-E10 B .
WWK-A-AMSFBLK-E10 C
WWK-A-AMS1-E10 A ;
WWK-A-AMS1-10 B
WWK-A-AMS 1-E10C
:
WWK-A-AMS2-E10 A
' WWK-A-AMS2-E10 B . 1 _
' WWK-A-AMS2-E10C : ", ; `
WWK-A-AMS3-E10 A
WWK-A-AMS3-E10 B :
WWK-A-AMS3-E10 C
WWK-A-AMS4-E10 A
WWK-A-AMS4-E10 B
WWK-A-AMS4-E10 C . . .
'
WWK-A-AMS5-E10 A
WWK-A-AMS5-E10 B ;
,
WWK-A-AMS5-E10 C
WWK-A-AMS6-E10 A V
WWK-A-AMS6-E10B
.
WWK-A-AMS6-E10 C
. Control 1 A
-
Control 1 B
Control 1 C
... . -.
. . '. ' .
. :,
. ..
.
..
Date Sampled Date Received 01/15/2004 01/17/2004
01/15/2004 01/17/2004 01/15/2004 01/17/2004 01/15/2004 . 01/17/2004 01/15/2004 01/17/2004 01/15/2004 . 01/17/2004 01/15/2004 01/17/2Q04 01/15/2004 01/17/2004 01/15/2004 01/17/2004 01/15/2004 01/17/2004 01/15/2004 01/17/2004 01/15/2004 01/17/2004 01/15/2004 01/17/2004 01/15/2004 01/17/2004 01/15/2004 01/17/2004 01/15/2004 01/17/2004 01/15/2004 : 01/17/2004 . 01/15/2004 . 01/17/2004 01/15/2004 01/17/2004 01/15/2004 01/17/2004 . 01/15/2004 01/17/2004
01/17/2004 01/17/2004 01/17/2004.
Date Due 02/02/2004 02/02/2004 02/02/2004 02/02/2004 02/02/2004 02/02/2004 02/02/2004 02/02/2004 02/02/2004 02/02/2004 02/02/2004 02/02/2004 02/02/2004 02/02/2004 02/02/2004 02/02/2004 02/02/2004 02/02/2004 02/02/2004 02/02/2004 02/02/2004 02/02/2004 02/02/2004 02/02/2004
I I I ! I I I
i
1/19/2004 I Login.rpt
0 55
Report Version: Dec 22 2003 10:44AM Page 2 of 4
Instance:
R0080901 R0080901
''.001667-0001
Container
0 ^26 13 5 /Other /NONE
L0001667-0002
Container
C0026136 / O ther/N O N E
L0001667-0003
Container
C0026137 / Other / NONE
L0001667-0004
Container
C0026138 / Other / NONE
:
L00Q1667-0005
Container
C 0 0 2 6 1 3 9 /O th e r/N O N E
L0001667-0006
( Container
*. C 0026140/O ther/N O N E
wm ' , - - ' . I u - 01667-0007
Container
g C0026141 /O th e r/N O N E
1 L0001667-0008
9 Container
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1 00026142/Other/NONE
-L 0 0 0 1 667-0009
1 Container
C 0 0 2 6 1 4 3 /O th e r/N O N E
| L0001667-0010
Container.
H| C 0026144/O ther/N O N E 9 .
L0001667-0011
9 Container SI C0026145/O ther/N O N E
.
g L0001667-0012
Container
' J0026146 / Other / NONE
1
m 1/119/220004 Login.rpt
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Method
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Report Version: Dec 22 2003 10:44AM Page 3 of 4
R0080901
! L0001667-0013
Container
C0026147/ Other /NONE
n
Method
. J01667-0014
Container
;
00026148/Other/NONE
Method . ------------
| L0001667-0015
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1 Container
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| L0001667-0018
Container
00026152/O ther/N O N E
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1 Container
| J026153/ Other / NONE
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1 Container
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C:
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-------------
L0001667-0021
Container
0 0 0 2 6 1 5 5 /O th e r/N O N E
;/
Method
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L0001667-0022
Container
C002615 6 /O ther/N O N E
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1 Container
C 0 0 2 6 1 5 7 /O th e r/N O N E
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I , 1/19/2004 I | Login.rpt
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.
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Report Version: Dec 22 2003 10:44AM Page 4 of 4
' Instance:
R0080901 R0080901
Sam pler(s):
AC, SO, RK
DuPont Washington Works Air Sampling Program
FedEx A irb ill #: 836391298456
Event Number
E v e n t10
Pump# 669842 669908 669901 669890 669796 669865 Hours
.0 1 2 3 4
Field Blank:
Station # AMS-1 AMS-2 AMS-3 AMS-4 AMS-5 AMS-6 Minutes 0 60' 120 180 240
^ iiii^ W W K -A-AM S1-10 W WK-A-AMS2-E10 WWK-A-AMS3-E10 W W K-A-AM S4-E10 W W K-A-AM S5-E10 W W K -A -A M S 6-E 10 Hours 5' 6 . 7 8 9
Calibration (pre) l i l i
1.022
14-Jan
0.997
14-Jan
1.001
14-Jan
1.014
14-Jan
1.006
14-Jan
1.009
14-Jan
Minutes
Hours
; 300
10
360 11
420 12
480 13
540 14
Start Time I m i i 0620 15-Jan 0630 15-Jan 0629 15-Jan 0635 15-Jan
; 0645 '15-Jan 0652 15-Jan
Minutes Hours 600 15 .660 \ 16 720 17 780 : 18 840 19
Stop Time Calibration (post) Total Minutes Total Vofume
0615
0.995
1462
1447 liters
0622
1.003
blank display
0623
0.9703
1473
1413 liters
0630
0.951
1479
1410 liters
0635
1.023
1481
1451 liters
0645
1.023
1483
1456 liters
Minutes
Hours .
Minutes
V 900
20
1200
960 / 21
1260
1020
22
1320
1080 1140
23 24
1380 1440
OQ
yes WWK-K-AMSFBLK-E10 yes or no
ID D
Weather:
14- Jan Cold, 36 F, snow flurries, breezy
15- Jan Cold, about 27 F, snow flurries, windy
SAFER operational:
yes yes or no
C om m ents: Total minutes column is the reading from the monitor counter.
Pump 2 had a blank display and was not running at sample collection time, due to the GFCI freezing. Replaced the GFCI before next test.
2/9/2004
Page 1 of 2
airdataevenflO
Another Calculation 1474.427 VALUC
1451 86245 1453 1175 1502.4?45 1506.728
059
* 2/9/2004 !*SS I
Page 2 of 2
y
airdataeventIO
PROJECT IN P O R M A flQ N C lient (nam e & address):
CHAIN OF CUSTODY/ANALYSIS REQUEST FORM
Exygen Research Sample Receiving * 3117 Research Drive * State College, PA 16801, USA T: 814.231.8032 * F: 814.231.1580 exygenresearch.com
Page 1 o f _ [___
ANALYSS REQUESTED
Project M a n a g e r (N am e & E-m ail Address):
C S o A tA A jiiS V in & W vGoCKS
Phone: Fax: Sam pler:
j R .'fD rv fa lX
,
Project N am e:
( A le 53ooiNvi)V(riA
P.O. # :
v/ 3
Q u o ta tio n # :
Please fill o ut this form co m p le te ly to ensure correct analysis and proper handling o f your samples.
Composite Number of Containers
SAMPLE ANALYSIS' - M - c . '
ExyLIAAS# Client Sample Identification
Collection Collection "
Date
Time u
vJvV .-A-A A '& Pbl^-E lD w M O A -ftrasi w vU\A- f) - ftra?v5 - PsIO
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0 6 to t)(o i S
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WwD L - ft -fH A A ic r A M
LAB USE ONLY
Me-- - / " I 1
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0433
yr i
CHAIN ;OF CUSTC
Specify Matrix Comments
\ A ir
\ t ...
\ A
L1 _ ._ _
\ \ \ y 7
Relinquished by
DM ------- Y y i \
Date
Time
1 1u
1 3 D
r/M jcft A ' 4 0
& J
Received by
:
D ate
Tim e
S . Gpn '
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OTHER INFORMATION T H A N )Q
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PROJECT R EQ U IR EM ENTS Results Deadline:
Laboratory Report Options: Q Sample results only Q Add case narrative Q Add quality control summary F I Add calibration summary d l Add raw data Other;_________________ .
DuPont Washington Works Air Sampling Program
Sam pler(s):
AC, SO, RK
FedEx A irb ill #: 836391298456
Event Number
Event 10
P u ilip fliil 669842 669908 669901 669890 669796 669865
Hours 0 1 2 3 4
Station # MS-1 AMS-2 AMS-3 AMS-4 AMS-5 AMS-6 Minutes 0 60 . 120 180 240
Exygert ID WWK-A-AMS1-E10 WWK-A-AMS2-E10 WWK-A-AMS3-E10 WWK-A-AMS4-E10 WWK-A-AMS5-E10 WWK-A-AMS6-10
Hours 5 6 7 8 9
C alibration (pre) o a i l i i i l i i l i Date
1.022
14-Jan 0620 15-Jan
,0.997
14-Jan 0630 15-Jan
1.001
14-Jan 0629 15-Jan
1.014
14-Jan 0635 15-Jan
1.006
14-Jan 0645 15-Jan
1.009
14-Jan 0652 15-Jan
Minutes
Hours Minutes Hours
300
10. 600
15
.360
11 660 16
420 12 720 17
480 13 780 18
540 14 840 19
Stop Time 0615 0622 0623 0630 0635 0645
Minutes 900 960
, 1020 1080 1140
Calibration {post) Total M inutes
0.995
1462
1.003
blank display
0.9703
1473
0.951
1479
1,023
1481
1.023
1483
Hours
Minutes
20 1200
21 1260
22 1320
23 1380
24 1440
Total volum e;
Field Blank:
yes WWK-K-AMSFBLK-E10 yes or no
W eather:
14- Jan Cold, 36 F, snow flurries, breezy 15- Jan Cold, about 27 F, snow flurries, windy
ZD ZD
SAFER operational
yes yes or no
C om m ents: Total minutes column is the reading from the monitor counter.
Pump 2 had a blank display and was not running at sample collection time.
1/15/2004
Page 1 of 2
airdataevent10.xls
1 li'" '
Proven Results.
Sample "Condition Upon Receipt" Form
. Protocol it c Exygen Study #"
, Date & Time Received Condition o f Samples
OocoY ( 7 rtod /(.L I i f / n h n tic
Temporary Storage Location Initials & Date
Ocaa 2fiCf o,[f ifcy
. Waybill #
.
in
;
Comments:
j ' T "f-'t't
QrAVORD praeess-lounr.SampleCondiuonoiiReoeipt.doc
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M ay 24. 2002/3
J05 Research (Drive VSI.W College, PA ffjiiO (. USA
: 800.281.3210 F: 014.232.1 UP?
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. P ackages o ver 150 tbs. Delivery commitment maybeiater in some areas.
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. F- ] FedEx 1Day Freight*
Next business day
* .CaHfor Confirmation: _
5 Packaging
r i FedEx Day Freight
'-- > Second business dey
p i FedEx 3Day Freight
t-- I Third businessday .
* Declaredvalue limit S500
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ZIP
JJredEx Envelope*
FedExPak*
Includes FedExSmall Pak,FedEx large Pak, and FedEx Sturdy Pak
Other
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/ 6 Special handling
Include PidEx eddtass m Section 3.
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Availableoniytr FedExpriority trpiighl and FedEx JDay to selctZIP codes-
|-- > nuuu vveeKaay |___| at FedEx Location
Not available for
FedExFirst Overnight
*T5oes this shipment contain dangerous goods? -- - -- Oorhrjx niusthe checked. ------------
.-- ULU aturcay 1 I at FedEx Location
A..v..a..i.la..b..l.e..o..n...ly..lor . FedExPriority Overnight
and FedEx20aylo select locadons
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I___I As per attached
\__ 1 Shipper's Declaration
Shipper's Declaration , net required .
. Dangerous Goods (including Dry Ice) cannot be shipped in FedExpackaging.
|-- 1 Dralce
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| | Cargo Aircraft Only
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7 Payment Billto_
1 1 0b ta in Recip.
We cannotdefiver to P.Ovboxes or P.O. ZIP codes5.. . ___/
(------------------- - Enter FficlEs.A c c i No, o r Credit Card No. below. -- i-- :-- | H~ ; .hAccccli wMoo..
{^ S e n d e r. , | | Recipient
P {Third Party j~ ] Credit Card . j }Cash/Check
; DepURoor/Suite/Room
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Total Packages
Total Weight
' Total Declared Value*;
Total Charges
.3 H .
SMS
V: $ .' .
.00
Credit CardAudi.
' *0 u r liability is limited to SIOO unless you declare a higher value..See back lor details.
8 Release Signature Sign to authorize deliverywithout obtainingsignature.
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By signing you authorize us to deliver this shipment Without obtaining a signature
. and agree to indemnify and hold us harmless from any resulting claims.
Questions? Visit our Web site at fedex.com
or call VBOO.Go.FedEx- 800.463.3339.
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