Document NERBVzR8o7Jv1aGaDaMRkbonV
From:
American Laboratories and Research Services, Inc.
?.0. BOX 15609
Hattiesburg, MS 39402-5609 601-264-9320
'
Date: October 9, 1990
To: Mr. William H. Cooper PPG Industries Chemicals Division P.o. Box 1000 Lake Charles, LA 70602
The following analytical results have been obtained for the indicated sample which was submitted to this laboratory:
Sample I.D. AA04887 Sample location: PPGHC
LL jl'l6 Cooling Tower Sludge (A)
Collected by: PREJEAN
Collection date: 09/07/90
Laboratory submittal date: 09/13/90 Time: 19:00
Received by: RLH
Validated by: RLH
Time: 13:30
Parameter: TCLP Extraction Method reference: SW846-1311 Result: done Date started: 09/20/90 Time started: 11:45
Parameter: TCLP Metals Method reference: SW846 3rd Ed Result: see appended report Date started: 09/27/90 Time starred: 09:00
Parameter: TCLP Volatile Organics Method reference: EPA 624 Result: see appended report Date started: 09/30/90 Time started: 19:54
Date finished: 09/21/90 Analyst: MJF
Date finished: 10/08/90 Analyst: JSC
Date finished: 09/30/90 Analyst: BB
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Mr. William H. Cooper Page: 2 October 9, 1990
sample I.D. AA04bo7 (continued)
Parameter: TCLP Semi-Volatiles Method reference: EPA 625 Result: see appended report
Date started: 09/28/90 Time started: 02:ll
Date finished: 09/28/90 Analyst: BB
Parameter: Selected Volatile Organics
Method reference: SW846-8240
Result: see appended report
Date started: 10/02/90
Date finished:
Time started: 21:18
Analyst: BB
10/02/90
Parameter: Semi-Volatile Organics Method reference: SW846-8270 Result: see appended report
Date started: 10/02/90 Time started: 22:31
Date finished: 10/02/90 Analyst: BB
Parameter: pH Method reference: EPA 150.1 Result: 7.69 SU Date started: 09/14/90 Time started: 15:00
MDL or sensitivity: 0.00 Date finished: 09/14/90 Analyst: KEL
Data for TCLP Volatile Organics ug/L
Component Name
Benzene Carbon Tetrachloride Chlorobenzene chloroform 1,2-Dichloroethane 1,l-Dichloroethene Methyl Ethyl Ketone Tetrachloroethene Trichloroethene Vinyl Chloride Pyridine
Concentration
Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det
Component MDL
10 10 10 10 10 10 10 10 10 10 500
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Mr. William H. cooper Sage: 3
October 9, 1990
Sample I.D. AA048a7 (continued)
Data for TCLP Semi--Volatiles ug/L
Component Name
1.4- Dichlorobenzene Hexachloroethane Nitrobenzene Hexachlorobutadiene 2.4- Dinitrotoluene Hexachlorobenzene Cresols, total 2,4,6-Trichlorophenol 2,4,5-Trichlorophenol Pentachlorophenol
Concentration
Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det
Component MDL
io io io io io io 20 io 50 50
Data for TCLP Metals mg/L
Component Name
Arsenic, TCLP Barium, TCLP Cadmium, TCLP Chromium, TCLP Lead, TCLP Mercury, TCLP Selenium, TCLP Silver, TCLP
Concentration
.016 1.3 Not Det
.05 . 04 .014 Not Det . 06
Component MDL
. 005 .1 .01 .03 . 04 .005 .005 . 03
Data for Selected Volatile Organics mg/Kg
Component Name
Concentration
Chloromethane Bromomethane Vinyl Chloride Chloroethane Methylene Chloride 1.1- Dichloroethene 1.1- Dichloroethane trans-l,2-Dichloroethene Chloroform
1.2- Dichloroethane
Not Det Not Det
39
100 47
Trace Not Det Not Det
25 150
Component MDL
io io 10 10 5 5 5 5 5 5
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Mr. William H. Cooper Page: 4 October 9, 1990
Sample I.D. AA04bo7 (continued)
Data for Selected Volatile Organics (continued)
Component Name
Concentration
1,1,l-Trichloroethane carbon Tetrachloride Bromodichloromethane 1.2-Dichloropropane t-1,3-Dichloropropene Trichloroethene Dibromochloromethane 1.1.2-Trichloroethane Benzene
c-1,3-Dichloropropene Bromoform Tetrachloroethene
1.1.2.2-Tetrachloroethane Toluene chlorobenzene Ethylbenzene Xylene, total
c-1,2-Dichloroethene
1.1.1.2-Tetrachloroethane
160 Trace Not Det Not Det Not Det
71 Not Det
74 Not Det Not Det Not Det
430 50
Trace Not Det
12 65 Not Det 19
Component MDL
5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5
Data for Semi-Volatile Organics ug/Kg
Component Name
Phenol bis(2-chloroethyl) Ether 2-Chlorophenol 1.3- Dichlorobenzene 1.4- Dichlorobenzene 1,2-Dichlorobenzene bis(2-Chloroisopropyl) Ether N-Nitroso-di-n-propylamine Hexachloroethane Nitrobenzene Isophorone 2-Nitrophenol 2.4- Dimethylphenol bis (2-Chloroethoxy) Methane 2.4- Dichlorophenol 1.2.4- Trichlorobenzene Naphthalene Hexachlorobutadiene 4-Chloro-3-methylphenol
Concentration
5200 Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det
2300 Not Det Not Det
Component MDL
300 300 300 300 300 300 300 300 300 300 300 300 300 300 300 300 300 300 300
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. Mr. william H. Cooper Page: 5 October 9, 1990
Sample I.D. AA04^d7 (continued)
Data for Semi-Volatile organics (continued)
Component Name
Hexachlorocyclopentadiene 2.4.6- Trichlorophenol 2-chloronaphthalene Dimethyl Phthalate Acenaphthylene Acenaphthene 2.4- Dinitrophenol 4-Nitrophenol 2.4- Dinitrotoluene 2.6- Dinitrotoluene Diethylphthalate
4-Chlorophenyl-phenylether Fluorene
4.6- Dinitro-2-methylphenol N-Nitrosodiphenylamine 4-Bromophenylphenyl ether Hexachlorobenzene Pentachlorophenol Phenanthrene Anthracene Di-n-Butylphthalate Fluoranthene Pyrene Butylbenzylphthalate 3,3'-Dichlorobenzidine Benzo(a)anthracene bis(2-Ethylhexyl) Phthalate Chrysene Di-n-octyl Phthalate 3enzo(b)fluoranthene Benzo(k)fluoranthene Benzo(a)pyrene Indeno(1,2,3-c,d)pyrene Dibenzo(a,h)anthracene Benzo(g,h,i)perylene Benzidine alpha-BHC beta-BHC delta-BHC gamma-BHC Heptachlor Aldrin Heprachlor Epoxide Endosulfan I Dieldrin 4,4'-DDE
Concentration
Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det
340 Not Det Not Det Trace Trace Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det
Component MDL
300 300 300 300 300 300 1500 1500 300 300 300 300 300 1500 300 300 300 1500 300 300 300 300 300 300 600 300 300 300 300 300 300 300 300 300 300 2400 300 300 300
300 300 300 300 300 300 300
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'/r. william H. Cooper Page: 6 October 9, 1990
Sample I.D. AAQ4fe7 (continued)
Data for Semi-Volatile Organics (continued)
component Name
Endrin Endosulfan II 4,4'-DDD Endosulfan Sulfate 4,4'-DDT Methoxychlor Endrin Aldehyde alpha-Chlordane gamma-Chlordane Toxaphene Aroclor-1016 Aroclor-1221 Aroclor-1232 Aroclor-1242 Aroclor-1248 Aroclor-1254 Aroclor-1260 l,2-Diphenylhydrazine N-Nitrosodimethylamine
Concentration
Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det Not Det
Component MDL
300 300 300 300 300 300 300 300 300 600 300 300 300 300 300 600 600 300 300
Comments: Reference Lab Report No. R1461.
If there are any questions regarding this data, please call.
SL 046165