Document NEN7BOZ4zggGyz005bzymK5wb
CG 46 < DATE )
CODE YC-5--A ' PKG __
___k?H68_ (LOT NUMBEb I
EST. WT. 2131*`LBS,
:
ESSES
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TYPED BY: JNH
STANDARD HRS. __________
PREPARATION NOTES:.
wrfoev
-m. APPROVED'BY EWK 10/23/81
TINE
EQUIP MENT
BLEEDING
DALAHAR* YELLOW
03 PAGES
BTAIN FOR S6 (5-NITR0-2-AMIN0 ANISOLE) AIN FOR S23 (ACETOACET ORTHO ANISIDIDE)
CLEAN, DRESS, CLOSE 24* CLARIF PRESS - 15 FRAMES.
USE LBS
I N-CODE t ACCT I I IBS i---------------- |------ -
I 557-C | ! 46-C 1
I
* (55L"> G) WATER INTO V-,,.
IN FROM V-324 (HYDROCHLORIC ACID)
m .jab_______ RINSE IN DRUMS FROM S? <5"NITR0~2-
AMINQANISOLE)
- .v
* 1 0%_
___ JP.%.
::333L
.I
I
iMi ii/jz 1
I 28-D !
557-C I
441 938
zzmz
<?__
' MIN OR LONGER TO WET
.u
TO 37* <1295 G) AT 28-32* F (ICE) fa *330| 57-A
ON IN IN 12-15 MIN (SODIUM NITRITE)
STIR 30 MIN AT 28-32*F MAINTAINING^jKQfl+KI
FOR St 3. RECORD : TmE~ START J CR,,_jfc, KI______ NOTE:
t 725-A t .1 9/*
OCiT 2919821
(1) IF CR-, KI- ADD 20* "AS IS" INCREMENTS
(HYDROCHLORIC ACID)
, ASSUME 32%
RECORD: CR_________( + ) , KI_.^_______( + )
I _______ 1
i
! 28-D ` 1___
I
*2) IF CR+, KI- ADD 20* 'AS IS' INCREMENTS
1
(SODIUM NITRITE)
ASSUME 33%
_____ 1 725-A
i |______
RECORD: CR( + >, KI_( + >
yrr I SLURRYJN 50 GAL WATER IN DRUM & PRECOAT
I.
1 j CWAfRlF :'RESS WITH (DICALITE FILTER AID)
5 ! 777-A I 5
U^rTSLURRY IN 20 GAL WATER IN. DRUM FOR S 20
39-a j **
(TRiSULPHOIL SOAP D)
DV WHEN Si0 STIR COMPLETE, DUMP IN.: (DICALITE 4 TER AID) DUMP IN (ACTIVATED CARBON)
COMTYP JOB NAME * 46YC005AME PAGE 02
BATE PRINTED: 3/22/82
PAGE 02 OF 03 CG 46 CODE YC-5-A
t USE <E) | LBS
N-COBE' ACCT LBS
I STIR 30 MIN AT 28-32 DEG F MAINTAINING, +CR: 1
I
I +KI FOR S21. RECORD: TIME START^j^^i^ I
I
I CR-MjgS?V KI_^Wk __ NOTE:
X
I
57-A
I (1) IF CR-, KI- ADD 204= * AS IS* INCREMENTS !
I
I ' (HYDROCHLORIC ACID)
ASSUME 32% ]_______ | 28-D
t RECORD: CR
___ < + ) KI .,,( + )
f
I
I (2) IF CR+, KI- ADD 204= *AS IS* INCREMENTS !
I
I (SODIUM NITRITE)
ASSUME 33% |_______ | 72S-A
I RECORD: CR ___ (+> KI____ ___.__( + ) |
|
|
I j {
CV RJjfcM'O" (970 G) WATER INTO V- J&C
5 NSTALL TEMP CHART
POUR IN (SODIUM HYDROXIDE) M__Z3L_,
7-D 447
,ADJ TO 37 * (3611 G) AT 66-70WF (ICE)
13X330
57-A
CLOSE STACK DAMPER
POUR IN N-39-A SLURRY FROM SI 2 & STIR FOR
DV 4&T\ WHEN 1-5 STIR COMPLETE,' TEST DV 6 RECORD:
6 I I-CCR___ffeei( + >i; KKII___^^TT(( + )i TTEEMMPPJ?J.?.^L_(28-32*F)
NOTE: (1) IF CR-, KI- ADD 204= AS IS"
INCREMENTS (HYDROCHLORIC ACID) ASSUME 32%
RECORD: CR;___ ..,_( + >; KI_,,____ _ ( + )
(2) IF CR+, KI- ADD 204= "AS IS INCREMENTS
(SODIUM NITRITE)
ASSUME 33%
3RD : CR___ C^^( + >; KI__________ ( + )
^STAI TURN OHJiStgrAGITATOR, CHOP & ADD ICE
i OFF AGITATOR
J^KtfTPUMPVBV THRU CLARIF PRESS INTO DV
MAINTAINING TEMP AT 28-32 DEG F
RECORD: TIME START J2&&6Z0O1AI. MIN
CV f,
DUMP INTO CV FROM S2 (ACETOACET ORTHO
ANISIDIDE) NOTE: BREAK UP LUMPS
LOJ-^
4= X
%
w%* WL*JL 1
i__.
ft 10 MIN TO DISSOLVE 'EN STACK DAMPER
I
IN UNDERSURFACE IN 20-25 MI
TIC ACID) M_
__,
'6 & .%
STIR 5 MIN & RECORD: PH_#iV__(5.8-6*3)
If NECESSARY, ADJ TO PH
& RECORD
PH_$Jl(5T8--6,3> SODIUM HYDROXIDE ASSUME 50%
ACETIC ACID
ASSUME 70%
WHEN S22 CLARIF COMPLETE, WASH DV <S4)
LINES, PUMP (, PRESS FOR 20 MIN OR- TO A -CR
TEST ON A SAMPLE OF TOTAL PRESS EFFLUENT
WHICHEVER COMES FIRST. COLLECT
IN
,,V CS22) . RECORD: TIME START_3jeSix^
0R+) '= J* . S
TIR 5 MIN & RECORD: TEMP.^*f_-C28-32*F)v& .
IF NECESSARY ADT/TO 28-32KF7 RECORD 3ML.*F
* RECORD: V0L^^gr!5L.X
57-A
46-C
1240
30-D 685
7-D 30-D
57-A
DUP050061378
^T-YP-' JDB NAME = 46YC005AME PAGE 03
DATE PRINTED: 3/22/82
EQUIP KENT I
I PAGE 03 OF 03 CG 46 CODE YC-5-A
I USE < E > LBS
n -^c o d e ACCT . LBS
WHEN S 31 COMPLETE/ ADJ CV TO 44- <4268 G) |
AT 80 - 84 DEG F
CHECjL, ACCURACY: HT ._J3_h_DEG F 6 RECORDER I
DEG F.
IMMEDIATELY RUN IN DV THRU UNDERSURFACE
DISTRIBUTOR IN 60-65 MIN. MAINTAIN CV AT
I I 80-84 yDfEcGu Fi-
ir .
>
i LJ^CORD: TIME -STARTTOTAL MIN.
X&3r\ STIR 1 MIN. DISCONNECT TRANSFER LINE AT
[ ' | CV IMMEDIATELY
\3*r \ RECORD: DIAZO ,,jgffZ <-) BASE
<+) 1
1 PH 4.3-4.?)
NOTE: <1) IF DIAZO.+ / BASE - & PH BELOW
4.3, ADJ TO PH 4.3-4.? RECORD: pH_________
(SODIUM HYDROXIDE)
" ASSUME 50%
(2) IF DIAZO +`, BASE - 6 PH ABOVE 4.3 ADD
St 100% N-7-D TO 55 GAL DRUM ' ASSUME 50%
ADJ WITH WATER TO + OR - 25 GAL. ADD 2*
100% N-46-C (ACETOACET ORTHO ANISIDINE) 6
STIR TO DISSOLVE. POUR IN CV 6 STIR 1 MIN
(3) REPEAT ABOVE AS NECESSARY TO - DIAZO,
SASE.
TO 190-194 DEG F IN 58-62 MIN.
R 30 MIN AT 190-1.94 DEG F RECORD:
TIME START
___ .
FLOOD TO 94<9174G) & STOP AGITATOR .
7-D 7-D 46-C
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