Document NEE0DJoQdnxyd6d9ba8Bg94rD

Lancaster Laboratories A division of Thermo Analytical Inc Analysis LLI Sample No. TL 2795999 Collected: 10/ 3/97 at 13:45 by SN Submitted: 10/ 3/97 Reported: 10/24/97 Discard: 11/24/97 CWK-BD-49 Soil Sample TCLP ZERO HEADSPACE EXTRACTION Chambers Works Soil Reuse Job #6015-08-06 Account No: 07032 DERS/DuPont Env Remed Services Barley Mill Plaza, Bldg. 27 Routes 141 & 48 Wilmington DE 19805 CAT NO. ANALYSIS NAME AS RECEIVED METHOD RESULTS DETECTION LIMIT UNITS M F !1 11 il ii il ji it ii h ii 0948 3492 3500 3503 3504 0316 3506 3511 3515 3522 3525 TCLP Volatiles _ Vinyl Chloride N.D. 0.010 mg/1 1.1-Dichloroethene N.D. 0.0050 mg/1 Chloroform N.D. 0.0050 mg/1 1,2-Dichioroethane N.D. 0.010 mg/1 2-Butanone N.D. 0.015 mg/1 Carbon Tetrachloride N.D. 0.0050 mg/1 Trichloroethene N.D. 0.0050 mg/1 Benzene N.D. 0.0050 mg/1 Tetrachloroethene N.D. 0.0050 mg/1 Chlorobenzene N.D. 0.0050 mg/1 The volatile organic analyses were performed on a zero headspace toxicity characteristic leachate of the submitted waste. The leachate was prepared according to the procedure specified in the March 29 and the June 29, 1990 Federal Registers. A sample is considered to have failed the Toxicity Characteristic (TC) test and is therefore considered a hazardous waste if any of the volatile concentrations (mg/1) in the leachate exceed the following maxima: Benzene Carbon Tetrachloride Chlorobenzene Chloroform 1,2-Dichloroethane 0.5 0.5 100.0 6.0 0.5 1,1-Dichioroethene Methyl Ethyl Ketone (2-Butanone) Tetrachloroethene Trichloroethene Vinyl Chloride 0.7 200.0 0.7 0.5 0.2 The limits are published in March 29, 1990 Federal Register, pp. 11845-6. QUALITY CONTROL REPORT SAMPLE MDL SAMPLE UNITS BLANK DUP RPD MS MSD MS RPD 0948 TCLP Volatiles Batch: H972861BB 3492 Vinyl Chloride 0.010 mg/1 3500 1,1-Dichloroethene 0.0050 mg/1 N.D. N.D. 78 101 117 124 27 6 1 COPY TO DERS/DuPont Env Reined Services ATTN: Ms. Jill Meuser 1 COPY TO DERS/DuPont Env Remed Service ATTN: Mr. Tom Morgan P.O. LBIO-62248 Rel. L146 LCS LCS LCS LIMITS LCS DUP RPD LOW HIGH Questions? Contact your Client Services Representative Nancy Bornholm at (717) 656-2300 07:54:34 D 0002 3 130950 585617 320 0.00 00023700 ASR00D MEMBER AC :n Lancaster Laboratories 242b New Holland Pike PO Bnx12425 Lancaster, PA 17605-2425 717-656-2300 Fax:717-656-2681 Respectfully Submitted Ramona V. Layman Manager, Metals/Leachates See reverse side for explanation of symbols and abbreviations. 2216 Rev 8/41/9? DUP050464928 Explanation of Symbols and Abbreviations The following defines common symbols and abbreviations used in reporting technical data: N.D. TNTC iU umhos/cm C Cs! meq S ug mi m3 none detected Too Numerous To Count International Units micromhos/cm degrees Celsius (diet) calories milliequivaienis grarn(s) microgrambsj milliliter's'! cubic metertst BtVSQl MPN CP Units NTU F lb,.. kg rna 1 ui fib >5 um/rni- Below Minimum Quantitation Level Most Probable Number cobalt-chloroplatinate units nephelometric turbidity units degrees Fahrenheit pound(s) kilogram(s) milligrarn(s) iiter(s) microliter(s) fibers greater than 5 microns ir, length per rni < > Ppm ppb Dry weight basis less than - The number following the sign is the limit of quantitation, the smallest amount of analyte which can bo reliably determined using this specific, test. greater than parts per million - One ppm is equivalent to one milligram per kilogram (rng/kg;, or one gram per million grams. For aqueous liquids, ppm Is usually taken to be equivalent to milligrams per liter (nig/l), because one liter of water has a weight very close to a Idlograrn. For gases or vapors, one ppns is equivalent to one rnic roliter of gas per liter of gas. parts per billion Results printed under inis heading have been adjusted for moisture content Tb s increases use analyte weight concentration tc approximate the value present in a similar sample ws'hout moisture. U.S. F.PA data qualifiers: Organic Qualifiers Inorganic Qualifiers A TIC is a possible aldcrf-condensation product 6 Value is <CRDL, out >*DL B Analyte was also detected in the blank Estimated due to interference C Pesticide result confirmed by GC/MS M Duplicate injection o'easion not met t> Compound quantitated on a diluted sample N Spike sample no' vv-th.q control limits E Concentration exceeds Tim calibration range of S Method of standard auditions WiSA; usee the instrument 'or ca cuia: cn i Estimated value U Compound was not detected N Presumptive evidence of a compound {TICs only) W Post digestion spars out of conrot limits P Concentration difference between primary and * Duplicate analysis not withm. control limits confirmation columns >25% Correlation coefficient for MSA <0.995 U Compound was not detected X,Y,2 Defined in case narrative Tests results relate only to the sample tested. Clients should be aware that a critical step in a ct>em.cal or microbiological analysis is the collection of the sample. Unless the sample analyzed is truly representative of the bulk of materia! involved, the test results will be meaningless. If you have questions regarding the proper techniques of collecting samples, please contact us. We cannot be held responsible for sample integrity, however, unless sampling has been performed by a member of our staff. This report shall not be reproduced except in full, without the written approval of the laboratory. WARRANTY AND LIMITS OF LIABILITY - In accepting analytical work, we warrant the accuracy of test results for the sample as submitted. THE FOREGOING EXPRESS WARRANTY IS EXCLUSIVE AMD IS GIVEN IN LIEU OF ALL OTHER WARRANTIES, EXPRESSED OR IMPLIED. WE DISCLAIM ANY OTHER WARRANTIES, EXPRESSED OR IMPLIED, INCLUDING A WARRANTY OF FITNESS FOR PARTICULAR PURPOSE AND WARRANTY OF MERCHANTABILITY IN NO EVENT SHALL LANCASTER LABORATORIES BE LIABLE FOR INDIRECT, SPECIAL, CONSEQUENTIAL, OR INCIDENTAL DAMAGES INCLUDING, BUT NOT LIMITED TO, DAMAGES FOR LOSS OF PROFIT OR GOODWILL REGARDLESS OF (A) THE NEGLIGENCE (EITHER SOLE OR CONCURRENT! OF LANCASTER LABORATORIES AND (B) WHETHER LANCASTER LABORATORIES HAS BEEN INFORMED OF THE POSSIBILITY OF SUCH DAMAGES. We accept no legal responsibility for the purposes for which the client uses the test results. No purchase order or other order for work shall be accepted by Lancaster Laboratories which includes any conditions that vary from the Standard Terms and Conditions of Lancaster Laboratories and we hereby object to any conflicting terms contained in any acceptance or order submitted by client. DUP050464929