Document NE979y57e6rbLeL1y78bkLZ9E
BOILING POINT
TEST SUBSTANCE
Identity:N -Ethyplerfulorooetanesulfonamide;may alsobe referredto as U 1464, ETFOSA, ETPOSA, F-6309, or FX-12. (1Octanesulfonamide,1,1,2,2,3,3,4,4,5,5,6,6,7,7,8,8,8heptadecafluoro-N-ethylC-A,S # 4151-50-2)
Remarks: Materialisa white solidofuncharacterizedpurity.
METHOD
Method: The boilingpointwas determined as a partofthe OECD Guideline104, 'Vapor PressureCurve, Dynamic Method" study.
GLP (Y/N): No Year completed:1998
Remarks: Extrapolatimoenthodused.
RESULTS
Remarks:
Laboratorytestingwas notcompleted. Values were extrapolatedusingthe temperatureand pressurecurves obtainedforthe testsubstance duringthe vapor pressure study. The extrapolationasre below:
Pressure (mm Hg) BoilinTgemp., 'C
42
171.6
58
178.8
68 1 86
181.8 186.4
94
190.2
760
423
r'=, 0.9961
Pressure (mm Hg) BoilinTgemp.,OC
47
174.4
75
183.8
86
188
95
191
106
193
760
407
0.9960
CONCLUSIONS
Remarks: The boilingpointofthetestsubstance was estimatedusing temperatureand pressure curves.
DATA QUALITY
Reliability:Klimischranking= 3. Resultsare from extrapolationT.hese studieslackanalyticadlatafordeterminationofthe sample purity.
REFERENCES Study conducted atthe requestof3M Company by AScl Corporation, Duluth,MN OTHER Submifter: 3M Company, EnvironmentalLaboratory,P.O. Box 33331, St.Paul,Minnesota,55133 Last changed: 5/18100
P4ROM AScl Corp.
PHONE NO. : 2 18 722 2592
Nov. 30 1998 04:31PM P2
AA
AM
m
4m"
Novembe3r0,1998
ASclCorporation
4444,AirpBaoruklevCa)rudlu,Mrhi,nnes5o5c81a1
(2187)22-4040
Fax(21782)2-2592
Ms.SusaBneach 3M F-nviroamentalTechnology & SafetyServices 935 Bush Avenue St.Paul, Miniiesota55133
Dear Ms. Beach:
I am writingin responseto your requestof boilingpointinfotmationfortestitems U1463 and U1464. Unfortunatelywe did not obtainempiricalvaluesfortheboilingpointof eitheritem. Although experimenw valueswere not obtained,we didextrapolatvealuesusing thetempemture and pressurecurves obtainedforboth items. The tablesbelow summarize the extrapolations.
Tc3tItem-Ul461-
Rol ng Tomp, OC)
Pres=e (twnHg)
BoilingTemp-
42
174.6
37
172.2
55
179.0
48
176.4
67
197.2
68
188.2
81
.190.2
83
191.6
%
197.0
93
195.8
760
474
760
482
r2.0.ggog
TestItem U1464
42
58
68 83 94 760
Lr2.LO.9961L
171-6
178.8 181.8 186.4 190.2
423
47
174.4
75
183.8
86
188.0
95
191.0
106
193.0
760
407
r2_0.9960 -
FROM
ASct Corp.
PHONE NO. : 218 722 2592
No,. 30 1998 04:31PM P3 -
November 30, 1998 Ms. Beach - 3M Co. Page - 2 -
Iapologi2ethattheextrapolvedvalueswere allwe can provide.The boilingpointforboth compounds shouldhave been determinedbeforevaporpressurdeeterminationP.leasecallifyou need furtherinformation.
Sincerely,
Joe Amato Deputy DirectorA,Scl-ETD