Document N2M8ox6MmJ44QmVBKwQnpdz98
Er
ANALYTICAL REPORT
PFOAPFOS Anaysis ot: DoEo20218 Wika Gromnite Town a Newton Novo 0. ree 39 Trinity Street Tomer Wirchoell .aareotgon Nay 15,2008
A
/91500)
DEP2.soWe.a000ss
Case Narrative
:
D8E020218
axcoptions ae noted below: The results included in this report have been reviewed for compliance with the Laboratory
Quality Manual. Al results have been found to meet all requirements of NELAC and any
Tohhreisspiorenepspoorrret.tsahDaoillnsnoooftnhbfaeecrtreoeprrssoudasundcefdoeoxicoetpetsihnafuvlel,bwaietnhopurtotvhiedwerdiottneneaapcphrocvaatlaoanfatahtel1a0b2o5r6a6t1ory
`TShaempolneeArwiataelrasnadmRpelceeipprtesented in this report was received at the TestAmerica Denver
labo atarteampt erao turr eoy f1.2ConMay2, 2008.
S`Atnaanlydtaircadsstandardswere prepared using the aid form ofthe compound periorooctanaciccd
(PFOA). PFOS is a commercial prepared and certified solution.
Perfluoro-n-{1,2,3,4-"C,joctancic acid was introduced at the extraction step and was used as.
ainntionatuecmeadl satta1ndaaredxftoarcqiuoanntietaptionanodf PvFsOA.sePderfaluoarno-1i-[m1a,2l,34s-"anCd.JeodctaonrateQsuulfaonnatteawaosf
`STD Eahmexpe lsaetmpSv lrOesPapDerEocNs-eraGntt.no0ddi0As1inn2ao.lthyisnsirseport wera analyzed fo the target anaes by TestAmerica acFanordrtrwiidagiteessr.exstarEmaapclctohesdsuaasm2ip5nl0ge msioLs lsadplipikuheodatswoeifehxetartcahhectsiiaonmnteptmlaeelchissntiaaqcnudiaedrwfde,idhpvrmiiteohrth1toamneLxotlroafccot6inNodni.HiCAoInfesdoelutCtih1o8en sample is passed trough the cartidge, the analytes are eluted with 4 mL. of methanol. The
final volume is brougthot mL using methanolandthe extract is analyzed by LC/MS/MS.
MetOCh Samopld es
baTthcehMoeft2ho0dsaBmlapnlkesisopfrtohceesssaemdarmeaagtern.t wTatheermseptikheoddbwiathnksuwrarosgantoen-adnedtepcrepatariehderweipthoretaicnhg
limitforthetarget analytes.
EleavcelhsbwaetrcohwiisthpirnepsatraebdlswihtehdLcaobonroaltoHriysC.ontrol Samples (LCS). The LCS recoveries for both
AnalyticalComments
ihTnheseufafcimcceoitepnihtaobsdlaemrpLelqCueSirvaeondlauyMmsSes/sMdueSbtmDai.tceodu.ld MneotthobdeprpoecrifioornmeadndfoarccQuCracbyathcahve81b2e3e6n20v,eridfiueed btyo No other anomalies were note.
Testanerica
1 DEPZ.SDWB-000094
EXECUTIVE SUMMARY - Detection Highlights `Demo20n1e
PhEnETERW DETECTABLE PARNGTRRSmest REoPaORrTING mass
AveTmoIoON ee
TestAnerica
2 DEP2-SDWB-000035
METHODS SUMMARY `emoz2oats
PATER
MReLmToIOL
o/us/us, pEoR
RN -1c-0012
References:
EY SopeevreartninTgrenPtrocLeadbuorrea.tores, Denver, Facility Standard
MPERTEHEOADRNTION
Testanerica
3 DEP2-SDWB-000036.
METHOD/ ANALYST SUMMARY Demozo218
fmorwryrIc
over
om -1-0012
Jaqueline Bonnett
References:
om OSpeevreartninTgreaPtrocLeadbuorrea.tores, Denver, Facility Standard
nowrsT n__ 003601
Testamerica
4 DEP2-SDWB-000087
SAMPLESUMMARY `Deso20210
Hos swpLEs cure: sues 1
bSuaetne
sue rom
TG 001 MORRIS LAKE RAW
05/01/08 07:00
wToore)ic:ena ei ere ed 52 oe eee 0 neers etnin rdodof ee cd i.
Bertnxmbtosrgbe ppcr,scpevsp3,wrnnaoveemiptiench chitoyr,,ne,nti, l,prl yre., ct, elkpl,nye, pn,Vo,
Testhnerica
s DEP2-SDWB-000098
Cash in advance / Prepaid sales
Client Sample TD: MORRIS LAKE RAN
mic
DLaotte-SSamapmlpel8e..d.:.: 0DA5E/00210/20168-0070:100 DWaotrek ROredceeriv3.e.d...:: 0K5W/G0H2N/L0R8A
PPrreepp BDaattche#......:: 8051/20325/2008 Dilution Factor: 1
AAnnaallyyssiissDTaitmee....:: 0065:/2059./08
Method.........: DEN -LC-0012
Matrix.........: WATER
oeraomsngTER Pron.
msvur
RiEPrORTING ours
w
00..0000030 uuag//uL
`ascumsmopuraoTns 13c4 ROS
`pREeRcCoEvNETRy 8&s
RoeacorvsaRY ((5500 -- 220000)0
Testamerica
6 DEP2-SDWB-000039
QC DATA ASSOCIATION SUMMARY oamozoats
snout 001
sample Preparation and Analysis Control Numbers
wx nmvLeYToICAL WTR DEN -Lc-0012
LBANCrCKHW
rmza.rcms 123520
Ms ow
Testanerica
DEP2-SDWB-000100
THD LARK RREORT
mc
ClLoti-Lsoeatmpnl.e.t.:: RDGEE2O02200201080-520 WorkOrder f...: ELVIRA
Aoalysis Date..: 05/05/08
PPrreepp
BDaattec.h..#......::
05/02/08 8123520
Dilution Pactor: 1
Matrix.........: WATER Analysis Time..: 05:46
P=amETER ros
rwestr w
wREaPOrRTING mars 00..0010095 uuag//LL
DeBmo-1c-0012 DEN -Lc-0012
s1u3R4moPaRTOE. 1304 PROS
BBEcRoEvENRTY 1B0y0
`mRaBrcosvRY ((5500 -- 220000))
norE(sT ) TT
ppp
Testamerica
8 DEP2.SDWB-000101
`TABORATORY CONTROL SAMPLE EVALUATION REPORT
swe
C105lLoitL-oeStamnp#l.e.td.:: RD8OEE02200201080-520 WorkOrderf...: RELVIAC PPrreepp DBaattec.h..#......:: 0951/20325/2008 A`hnoaallyyssiiss DTaitmee....:: 005/:0599/08 Dilution Factor: 1
Matrix.........: WATER
n=mTER ros.
EPECROCVEENRTY cnw
RLEDCaOIVTESRY ((03 -- 115200)0
MDEETHO-DLc-001z Dm -ic-omz
`sommoaTs 2T33c4e RpOrSo
ecRoRcvaeNTy a52
LREpCaOrVsERY ((5500 -- 220000)0
Cwloirn)v:epera Seiook reehd
Testamerica
. DEP2.SDWB-000102
LABORATORY CONTROL, SAMPLE DATA REPORT
me
C103lLoitL-oestam#np.l.et.d:: RDU8BB002200201000-520WorkOrder 4...: RELVIAC PPrreepp BDaattec.h..#.......:: 1052/30522/003 AMnnaallyyssiissTDiamtee....:: 0055/:0539/08 Dilution Factor: 1
Matrix.......WA.T.E:R
rPoAmavErsn ros.
semroiwes 0o..220000
eaAvsoTRnED murs 00..21636 waaun
meemcrocvmsTr mon
n
oDwanm --11.c5--00001122
1s3u0m4mooParTosn 134 pros
RpeecRocavNeTRy @52
RLeocaorvsRY (50 - 200) 150 - 200)
Bloroe(rs)r:epo hee dog ekof id
Testanerica
10 DEP2.SDWB-000103
LABORATORY CONTROL SANPL EVALUATION REFORT
me
1C08lLoitL-oeStam4np.l.et.d:: RDI9EE002200201080-520WorkOrder ...:RAAVIAD PPrreepp DBaattec.h..#......:: 08152/30522/008 `AAnoaallyyssiiss DTaitmee....:: 0065:/1029/08 Dilution Factor: 1
Matrix.........: WATER
eam
pREmcRocvEeNmTy RLEmCwOmVzEsRY semion
rerooas
oss
03--133200)) Dpmm --1cc--oo0mzz
`is3m0R4oa2ArToEa 1304 PROS.
sPeEcRoCEvNeTRy a2
RLEoCaOrVrEsRY ((5500 -- 220000))
Cmoolrbaise)v:errat osoi 70 8 7 es de
TestAmerica
nu DEP2.SDWB-000104
LABORATORY CONTROL SAWPLE DATA REPORT
spe
CICSlLoitL-oeStam4np.l.et.d:: RDS8EB002200201080-520 WorkOrder 4...: RGLVIAD PPrreepp DBaattec.h..8......: 0851/20325/2003 Aonaallyyssiiss DTaitmee....:: 0065:/1025/08 Dilution Factor: 1
Matrix... WATER
ParaoanaTER eros
soevreer vaerosTaRED outs smmerccoavrmTy emo
ooleaae 0v..010500 vaafltu "8s
DDmExN 1106--00001123
`ascumemoparnTosn 134 Pros
meeacRocveaRTy 2a
RLecoovaERY ((5500 -- 2200000
CBooim(es)ertlr og etof re hd ---
Testhnerica
12 DEP2.SDWB-000105.
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