Document N23vY0pmgZvKwEqQOo3JoYXky

DIPHENYL AND CHLORINATED DIPHENYL DERIVATIVES JUNE 1935 HONS 0Si*3 COPY N 2 awoppwioK 1kl n>M nlitii to tti MiafHtan of Hfknil Bi CUluB< Dlftovl tutnltm, I* la aakalttat to tkaw at tka st. Laala flaat la amitlai with mtIii tkaaa aparatloaa rna tka Aaalatoa naat to tka Saat at. Laala naat. 1 taaartytloa la Slraa of tka atplpaaat aat ayaratloaa of tka Mykaayl aat DarlTaUraa ylaat at Aaalatoa, katk la toat at jrlata. Va kata lavaatlatot awr yraaaat ylaat ui ayaratlaaa tat kara lalital aat lapraraaaata that vault ka atvlaahla la a aa alaat. Tkaaa laimaaita ara aat nt la katk taxt aat yrlata. a attaapt kaa kaaa Mia to lay aat tka aao ylaat ar tatall tka atalpaaat, aa aaltkar tka alia af tka kwUtla*a to ka aaaaflat aw tka aayaaltjr of tka alta to ka laatallat la kaaaa. TO aaalat tkaaa aba taalga tkla ylaat aa art aaatlac a atBflata aat of yrlata, katk ably aat iatall, akaolaf tka aaliMaat aa it la laatallat at yraaaat. It la karat that soak af tka aqmlfBaat at Aaalatoa aaa ka aaat la tka aar ylaat. Bavaral aaMkara af tka Aaalatoa wtaalaatlaa kara arlttaa tka tarlaaa oaatloma af tkla raywt. Satoaaa tkaaa aaatlaaa tkara kaa kaaa aaaa rayatltlaa. It la fait, bavarar, that tkla la taalrakla far at St. Laala tlffaraat tfoaya My ka yrlaalyally lataraatot la latiwlSaal aaatlaaa. ata a part af tkla rayart ara tata akaata, kaat kalaaaaa, yrataat syaalflaatlaaa, ata., taalsaat te kaly tkaaa ka will aaaatraat aat ayarata tkaaa aalta. Tkla raywt la yraywat la qaatrayllaata, aaa cays kolas aaat to M. Dakota, two aayloa to Hr. LlTlasataa, aat aao aayy kolas hayt la tka Aaalatoa flloa. lira tiSTiSS I. I. Safari HONS 051964 T*BU Of oowpna S>fm THU 1* Pot** 00 Dlphawl aad Dlnhaarl ParlraUTaa B PMtlMatt - Pwmt and twwMt Dlphaajrl Plaat IljB*at Chlorinetla| Plaat BOX ibaorptlaa draalor Dlatlllatlaa Aroslor l||p laaeablp of Pleat* (Propoaad) HM l | it 31 34 40 44 Jte*M ttjlrtwrl *H PIpinay1 Dw1tut 01phenyl ttalt Ohloriaatlag Plaat BOX ibaorptlaa DlatlXlatloa of Crude iraolor TMw DlatlllaUaa Bbipplac Coateller* Diphenyl *ad Iraalar Operating Para* Behedile of Paeklai*, Oaakata and Suppllea Baat Balaata o Praaaat Diphenyl CoaTartar JU1 WfPatarlaa Paata ef Diphenyl aad Parl- Tatlraa * laboratory Bathed*. 3p*alfl*tloa aad laalaaaat AaalytWel Mathada Btaadard Spaalftaatlaaa Bqulpeent it T9 *a pb in 107 Xll 117 lit 114 lit 141 Ml 141 BaladU* af Prawlaa* Xlatlaa of Baaafaatarlaa Baalnaaat with Beta* Ml MB asi MONS 0519*5 HONS 051966 gisnon w>. x wtn <m Diraom. d Diraam. DBUTATITX8 HURTS KjOHMOlT, BOTH masrat md fboposid hi: ROOKS NaCULLOUQH (RRBUROH DCPUTKDrT) I. I. ROTOO (IROIRSKXRO BRPAHBRT) Th* trawlaga Rafarrad to la This Saotlon ara: xssm wit O-MSl - Dlphaayl Plaat - Dlagraaaatl* now Shaat or Fraasat Moat. 8a-*405 - Proposal Coavartar cult and Sayaratlag Iqulpoaat smmmo.WT 0-M8S - DlaornMtle Layout or Ohlorlaatlag Iquljmat 0-MM - Layout or Chlorlaatora a-a04 -- Buggsatad Layout of Chlariaatara for Propoaad Plaat B01 AR8CRHIO Ha Brawlasa jsmsjBxjm SaHMOT -- ProyoMd Layout of IMf Plaat WW 0-8M - Layout of Badar stiu SwgdOC -- Propoaad Dlatlllafloa Rqulpasat far Liquid Aroalara 8a-**0 - Prayoaad DlstUlatlau Kqulpaaat for Solid Aroolora ASSloaLT OP PURT3 (PB0P0SP1) SaHMOt -- Propoaad Oaaaral Layout of Plaat HONS 091907 Piranan. nun imamr X ul( for producing Alphanyl at St. Lonla having a oaposit? Of 1(000,000 lbo. par yaar ay raUow ana of too arrangananta. Tha float arrangement would ka the raaoral and lnatellatlon at Bt, lotto of tha praoant tbroo loot pot oalta without aubetantlal altaratloo. Buoh aa arrangawat flrad with aatural gaa at Sty par 1,000 ou. ft. would oaaa as laaraaao of aoat of (roduotloa duo to fowl aiaaa of O.lSty par lb. or $1,800.00 par poor orar that of Anniston aparatloaa. Haworor, bp tha allotaatloa of tha baamal atlll, whleh la latar dlaowaaod, tha raduatloa la ataaa aoata would off-oat tha adraaoa la oaa aaata aad tha total aoata of hoatlag would ba brought la llaa with tha haatlac aoata at Analatom. Tha aoooad peaalbllltp aad tha oaa whleh aaasa tha aoat doalrablo, aad oopoolallp aa If largo produotioa raqulrlag a aimbar of ualto aa ba foroaaa, la tha laatallatloa of a two load pot salt aoaiblaad with II haat exohangers aad aoatlauoua fraatloaotlag aolsaao. Siaaa thla arrange- ' > want would bare lowar hoatlag aoata thaa for tha 8 pot ualt with aatural gaa at Sty par 1,000 au. ft., tha aoata far fual would ba raduaad bp O.Sty par lb. of dlpbaapl or $>,800,00 par paar aa 1,000,000 lbs. Thaaa fual aoata aould bo bp tha owaa amount laaa thaa Aaalatoa aoata. Thora waald probably ba addlttoaal seringa la aalataaaaaa and labor whlah anaaot ba pradlatad at tha praaaat tlwa. Thla arraagoaaat la a ooaaldarablo Oapartara from tha praaaat Aaalataa praatlao aad lta daalga aad aonatruatloa ahould ba praaadoO bp Aerelopeeat work. Tha followlag aotaa .dlaauaa tha poaalbla aoaiblnatioaa that aap ba wood for tha production of dlphaapl ad tha aallaat faaturaa f tha praaaat salt aa anapared with tha auggaatad ualt. Tho outllaa far thlo dlaauaaloa lai HONS 051968 X. PlPhatfl OoaTartar X. Rant Paalan X. onirri Dlaaaaatoa 8. Raaator Taaaala B. hill and Firing Kqalpaant 4. Sattlaga B. Aatttaatla Control Iqaljaant 4, Piping aad Valaaa * StmVto 1. Toaparatura and Rata of Oparation 8. Patallad Ptaauaalon of Saggaatad Ta Pot Balt 8. Btaaratlon of Prodnata * DHla X. (qulpaast for Saparatlag Banaol--Alphan/l-- High BolXar Klxturaa I. Btoraga of Baaaol-Dlphaapl-Hlgh BolXar b. Ooaaaata aa Itaaa aa 11atad ahora ara aa foXXoaai HONS 05X969 + MPBtim. OOHTURTg -- fUW PK8I0B ITU 1.1.1. - OtHKHAl DI3CU88I0H Mpheapl 1* produced tr tbs besting of bsnsal Tepor to s temperature around gOO*C la albssd rsstsls frou which tbs sir Is oaslud-d, condensing these products and segsratlag dlphenpl from the benzene end other converted products. Tbs aoet desirable dlpheapl halt la oae la which tbs naxlmm atlllestlon of best la eoahlned with alapllcltp of operation sad low ooet of oonetruotloe. The aoat satisfactory type of roestor woaesl bee beoa fenad bp eetual Manufacturing experience la Anniston to bo a steel pot containing molten load through whleh the boaaoao Taper la passed. Although at first sight the lead bath appears to be aa inefficient beet exahciger, elope ptudjJuiaplwuo they it Is Oxeeedingl/ effltlciil. Tbs lead baihhae the purtleular advantage foren operation of this sort that sap aarbon foraed toads to float ei tho load surfaeo or be serried oat to a conveniently loeated trap retbor than to plag the apparatus. All subsequent dissuasion will be eonflned to load pot reaotora. The load remoter pot or pate asp be booted la various wepe sad map be ocabined with various heat ezeh- ago eppnratus. Tbs aore Inportent oeablnatlons are shown la Schedule 1. HONS 051970 !*#- * *4 ****4**41- 4 * 4 ** 5**4 t- - -_ JL___________________________________________________________________________________ _ S Hctrl- * - 1* - ** ' city 4 Indie*t-- Kaqnlrad - IadlMtaa lot laqilnd sgaagjt 1 MOMS 051471 la ordar to dataralaa wblah *rraateaeat 1* Boot oooaoBlanl to laotoXl aot oporeto the Tartobi* ooot* for tb* varlou* *ob- blaatloaa aro ooaporad.i '. Labor aat aalntaasao* ooata will alao aatar Into tb* flaal obtalaabla ooat* but tbaa* aaaaot bo jMlotai at tbla Ub*. Tb* baaa* naad for tbaa* aonyutatloaa aro aa rollovai 1. Staaa -- SB/ par 1000 lba. at 100 lb*, traaaura and utlltalat oalf tb* lataat baat. Aqulv*laat to 40/ yar aillloa B. T. U. (Tbla la laaa the* tho aoat of ataaa (aaaratad for tb* Aaalatoa Dlphaajrl Oyaratloaa by a b*11 faa flrad bollar.). I. Natural (a* at 10.8/ yar allllau B. T. 0. (Aaalatoa ooat). S. fatar ooat 18/ yar 1,000 aa. ft. (Ararat* Aaalatoa vatar ooat, laoludlat *lty tad r*- olalaad vator.). Baat rotulraaaata aro takaa from tha h*at balaao* rotaatly Bata, aotaa and raaorda available at Aaalatoa. bar* aaab laforaatloa vaa aot avallabla, tf.laulaUon* bar* baaa aot*. Tb* laatollatloa ooata aro only oa a **ll**tl*a of laol*t*d ylaa** of oqulpaast aat *r* altbout *aa**oorl*a. So t*l(B* bov* b**a Bata aat tb* ooata or* oaljr yrollalaarf a* fallowai HOMS 091972 7 li Om I pot aonrartar - fired (OMd 1b drraacaMata 1*1) $14,000.00 8. Om 8 pat eoarerter - gtm rirad (Deed la drraacoeeBta > * ) 10,800.00 8. Om 1 pat Bearerter fee fired (Oaad la drranceaaat 4) T,000.00 4 Om 1 pet eoarerter - XlMtrte heated (raalataaaa) 8,000.00 (Dead la drraaceaeat 4) ,, a OaaMl Taperlaar la flu* oae Staak (Bead la drraaceaeata 1, 0, S, 4, *0) TB0.00 4. Baat esabeacer la Ooarerted Taper llaa (Om4 La IrraapaMBt 4, 8, * 8) Ta Halt aaaboatar la Cenrerted Taper llaa (Oaad la Irraataaaata 4*4) TB0.00 ,1 100.00 4a Btaaa Baatad 8anasi TaporlMr (Oaad la Irraapaaaat 4) 4, Oaatlaueua rraatloaatla* Oeltan (Oaad la drraacaaaat 1, 8, I, * 4) 400.00 ,1 000.00 10a Btaaa Heated Baaaol BtUl (Om4 la drraacaaaat* 1, 8, 8, 4, * 4) 3.000.00 11. rati Betted Mpheajrl Btlll (Oaad la drraaceatata 1, B, 8, 4 * 4) 8,400.00 18. Oeatlaaeae Baparatiaa Bqalpaaat (Om8 la drraacaaaat 4 aad prlea laaladaa aeat ef aeeeenrj derelojaaat aerk) 8.000.00 HONS 051973 e All oiMUtlou are baaad on Aaatetoa opmtlow, aaaelp Wit prodaolag 1,000 lba. of technical dlphmpl a dap, fhla earreipaeda to a total ooarereloa par paaa of 10X cooT.rted product#, TAX of eearorted product# kola# dlphaapl aad MX baiag high bollar. Tha prodaatloa of eoarertod prodaota require* thaoratloallp A8.9X at tha baaiaa* actually uaad, Tha daily raqulraaaata of baa,ana ara 4,100 lba. par dap. Thla la tha pretest arrangeeeot at Aaalatca aad aa ahoan aa aw Drawing #0-6081. Tha tMtallatlaa ooaatata of 8 gaa ftrad load pota, with baaeaae entering through a raporlaar loaatad la tha ataek for exit af oaabaatlaa gaaaa, and after eoararalca, that aatarlag a fraotloaatlag oalum ahlah partially oonoantratae tha ooarartad product#. Tha alxtura ahloh dlaohargaa froa tha bottoa of thla ooluaa raaa 60X-76X aoararted prodaeta, tha balanoa baiag baaaaoa. Tha partial operating aoata era aa followt- fuel far Coarartaw (datarad) Mphaapl dtlll (datarad} dtaaa far daaael dtlU (daflaat ratio aaeaaad as l/t to 1 aad TIX afflelaaap aad dl,ld0# baaaol dlatllled par dap) atar for ddghlagnator aad ooadaaaara aa ecatlanou* eolaaa, baaaol atill aad dlphaapl atUl Dapraolatlaa aa ttaaa 1,5,9,10m, totalllag | M,110.00 t m oa 1,000,000 lba. Total for Artoagaaaat da, 1 fir it. 0.81# 0.08 0.10 o.to ___ g.. 0.00# |g|aa Tha abora aparattaaa oould ba raduoad bp 0.18# bp naming tha oaatlaaaaa lilaa alth alnor alter*tleau at a hlghar taaparatara ao aa to deliver a dljhaiyl high hollar alztara aad tharabp allalaata tha baaaaa* atill. Thla arraagaaaat would ba Idantlaal to Arrangaaaat do, 1 raapttag that a boat onhanger would ha aaad to raeorar boat froa MOMS tha rapart laarlag tha ooavartar wait, Pwtaaa would flrat paaa thtaa* tha raparlaar haatad bp tha axlt flaw gaaaa aad thaa to.tha - boat oahaafar and thaa thread* tha load pet aalta, Tha ooarartad tepora aftar laarlag tha boat acohaaiar would paaa to tha ooluaa far aoaoaatmtlag tha ooarartad prodaeta prior to going to tha baasana atill. 091974 s Ob the aeauaptlon that tha haat exchanger oould racorar 60f of tha heat la tha converted report, which would papraeaat 191 af tha total haat reuulreneate, tha haat affleleasy of tha operation* would ba Increased from 46t to 691. tha partial oparatlnf eoata ara aa followi- fuel far Converter * Diphenyl Still (lateral) Itaaa (Baaa aa la Irraageaaat lo. 1) later (Baaa aa la Irraagaaeat lo. V taxoeptlag that laaa would) (be aaad aa oolwaa ) Depreciation aa Itaaa 1,5,8,9,10 k 11, totalling 128,900.00 Uff on 1,000,000 lba. ttt-U>jL^afewrl O.tt# 0.0S 0*10 0.17 .Bag? Total for Irraagaaeat lo. 2 0.75# lotai Tha abort operation* oould bo radaoad by 0.15# by naming tha goattmou eolane, aftar aafclag alaor altaratloaa, at a hlghar twaparotara ao ar to deliver a diphenyl and high boiler nixtare ead thereby ellalaate tha baaaeae atill. thle arraagaaaat would ba tha aaaa aa irraagaaeat lo. B eaeoptlag that one lead pot oould ba ollalnetad. Thl, would aaoaaeltata patting tha aaaa haat lato too pote that would be put Into tha three pote of irraagaaeat lo. g. tha partial operating aoeta are aa followi- ftr 1t`r fuel - tor Converter Diphenyl 8till Btaaa - Baaa aa U Irraagaaeat la. 1 (atar - Baaa aa la Irraagaaeat la. t BwMMUUoa aa Itaaa C,8,0,9.10 k 11, totalllag 0 19,400.00 0 101 aa 1,000,000# O.M# 0.08 0.10 0.17 ..ttttf MCNS Total for Irraagaaeat lo. 8 0.71 otai Tha above operattoae oould ba radaoad by 0.18# ty raining tha eoatlaaoaa oolwaa after aaklag alaor altaratloaa at a bl0ur teaparatara eo note deliver a dlpbeayl and high boiler alrtfre aid thereby ellalaate tha beaawa atlU. 051973 l. All iwii--t It tha mm m Arrang--t lo. > axoopt two of tho load pota would ba illrtiiM. Tba partial operating ooata art as follow!- Far lb. Utah--rl F--l > For C--Tartar * Diphanyl Still to-- - I-- -- Ait--g----t lo. 1 Watar Dapraelatl-- -- It--a 8,6,7,9,10 9 11, totalling t 16,t60.00 10JC an 1,000,000 lba. 0.14# 0*06 0*10 0,16 0.16 Total for Arr--gaaant lo. 4 0.674 ilTWI--ti iPi ,li Thla arrang--t eooaiata of a two 1--d pot e--Tartar --it. Tho ton--lag b----a la Taporltad --& auporhastad ia -- aoh--gar looatad ia tba ataak for wait o--boat!-- gaaoa. Thla mpaab--tad b--a--a wapor attalaa additional raparfcoat ia -- --Obaagar -- tba wait ooBwartod Tapora fr-- tho owTartar --It. Thaaa partially aoolad eoarartad Tapora thaa --tar a ayataa of ool--m --ioh a--tl--oualy dlabhargo tho ad|artad b--x--a, diph--yl --d high hollar, . Thla ayat-- ia aa aho-- -- Drawing fSe-fe--B. Tho partial opartting ooata ara oa folio-- Hr tti F--1 - For 0--Tartar Sta-- (atar Dapr--lati-- -- It--a C,(,6 A 1C, totalling 11,000.00 0 101 -- 1,000,0004 O.lAp - 0.16 0.11 Total far Arraagan--t lo. 9 O.SCp HONS 051916 This arrangeaent oanaiats of (Laflo pot electrically boatod. loot exohaagers oro provldod to have the exit converted vapors condense and lapert tbotr hoot to the taonalng bensane vopor. Coloane mold bo provldod for aoperating tho baneeoe-dlphenyl- high boiler. The above spele la Idantioal to the Dam operations excepting that lnatead of tho lead pot. Poo woe oarbaa taboo noting aa reals tore aad bested bp elestrloltp. la tho Poo progosa, beasaae vapors are delivered dlreetlp froa the top of the beaeaae ooluaaa to the heat sxohsager. Poo to tho hoed of the load la oar process, it oould probably bo laadvleable to operate this colossi under 16 lba. preaeore to save the Merer of vaporising the boaeol. The partial operatlag ooete are aa follooi- Iv M> PimwX Usetrialtp *0 K.V. 1/We Thai for PlphsRpl Still Btean later IpfMcUtioa on Itens 4,7,6.10 * U, totalling 16,600.00 1 on 1,000,000# Total for Arrangenent 6 0.86* 0.08 0.01 0.16 AM 0.68# lotei If the heatlac-OM doao bp ladeotloa. the Installation ooat oould be Increased bp I 10.000.00- U6.000.00 aad the operatlaf cost np to O.ltd par poind dlpbenpl. froa the above. It la evident that Arrangesant lo. S la the cheaper to operate. ' This, hooover. la followed very closely bp both Arrangerante Bos. I I I olth the eontlaasns eoloan operating *o ea to ellalaate the bensol still. If 1.1.1. - RucTon vssssu Tbs pot* oeod la thia proceaa have long Ufa aad loo aalataaiaaoe osot. Preeuaably these pots oould be Bade larger aad for greater oapaoltles. bat the life of mob pots and the aalatansaoe ooeta aa ooaparad olth the present pots oaaaot bo prodloted. HONS 051977 Our axparleoot with pota 1* linltad to waldod pota f low carbon ataal and alao Cruolbla Btool Coapany'a Raalatal Bo. 7, ahrowdwn 15-SW and alokal 0-t. Thaaa pota hare bats aada tgr tao fabricator*, tat thoa* aada by tha Blaw Inox Canpaay ban baaa aoat aatlafaotory. Tha pot uaod on prabaatar Bo. 1 (tho lowaat tnaparatura pat) ta haanor waldad low oarbon ataal. thaaa pota hava laatad all aad tba laat lot purohaaod waa la lStt, henea tha haaaar aaldlng. Pota alaetrloally aaldad would ba equally aa food. Tha dapth of tha laad la tha pot la about SO*. Tha Inlet plpa for bnim vapor with diatributor la aada of 1B)( ohroniun, alokal ataal. Tha dlatrltator plpa la aoearad to tha ataal oowor talch la thaa waldad to tha pot. Tha pot aaad on prabaatar Bo. (tha lntanaadlata taaparatara pot) la electrically waldad Cruolbla Btaal Coupaay'a Raalatal lo. 7. Tha dapth of the laad In tha pot la about 4". Tha laiat plpa for beaaana vapor along with dlatrltator la aada of ISgC ehroaa - tf alekal ataal. Thla dlatrltator plpa la (toured to tha oaat ataal oovar taiob la thaa boltad to a eaat ataal flanga(Vaa Itana Type) on tha pot. Tha gaskot aaad la a VI8* dlanetar aaaaalad ooppar hoop. Tha eonvartor pot (tho hlghaat tanporatora pot) la electrically woldod Cruolbla Staal Coapany'a Raalatal Bo. 7. Tho dapth of tho load la tha pot la about 42*. Tha Inlat plpa, aana at abova, la taourad to tha oaat ataal oovar whloh la boltad to tha flaago on tho pot. Tho gaakot uaod la braldad aabaatoa. Oua to tha axtraua tauparaturaa, tha boltad covara on tha eoovartar pat hava bam trerublaaona whan Inaulatad. Tha bolta would atrotoh and tha Joint would laak. Bara aovara aro now balng oparatad aad tho bolta tlghtanad aa laaka dtvalep. Alloy bolta havw boon triad M when tha pot waa coolad, thay oontraotod aad thaa had to bo aaltad off. It la but aaldon aaoaaaary to antar tha prahaatar pota) It la roo--ilad that whathar ona or two art aaad, that tha haada ba waldad to tha ahall and thaa lnaulatad. Thla praaunad that atldtra art avallabla who oaa aaka high freaaure walda la oarbon ataal. Tha oonvnrtor pot abould hava althar a boltad oovar or o waldad oovar provided woldara aro avallablo tao oaa aaka praaauro Walda la high ohronlun - high alokal ataala. Balding la aot My aftar prolongad axpoaura to thaaa high tanporatora vaport. It la btUsvad that tha prafarrad aonatruetlon would bo alloy bolta with thick waahwra nadw of a aatarial taoaw ooafflolwnt of aoepanaion la Mgbar thaa tha bolta and taloh would oauew tba bolta to looatn ta cooling, Such would than bo lnaulatad, which would ba ao appllad . MONS 051978 that it could readily b# raaored for aooeaa to the bolt* or loo rMortal the eorer at the pot. It bao boM nuppeetad that tba afttatort or ooataotera bo Mad la tha load of thaaa pett to todaoe tba Mbbla alia aad thereby laoraaaa tba ocotnot bataaao tba bcatena vapor aad tba aoltao load. Tha ariaalaatloa at Aanlatoa haTa had ao orperltace with tneb darloaa, bat It la thalr baliaf that aalnttoaao* ooata alpbt bo aaffiolMt to offaat tha (tin la capacity or recovery attaiaad through lta ate* It la aMpootad that tba abaft of aoeh a ooataetor would althar dlatort or alaa eat ltaalf la tba aubaar(ad boartac la tba aoltao laad If aueh bearing* aero ate. Wo wadaratnad that tha St. bouie Raaaarob Department baa Mparlaaatad alth auoh a ooataetor la a baatad laad raaotor veatel. Tbair experience ahould abundantly bare praoadanoa over oar baltafa. If 3- l. i. - mis t riBiHQ tmrf -KT Bagardlaf fael la tba laat St. Loola Plant, aa bar* data aa follow*i- Prlea par IllllcB . 8*T.*Ji Saitlat. tlaetrlolty attuned at 1/1# / l.WJI. City Oaa TSO STW/oa.ft. k a alrt-- prlaa of 88#/ll Paal OU - MMMd at tOftta aad 7.M# par (al. 1 priced I S#/(al. Coal - at(Mad at 10,800 WB par lb. aad prlead at ll.it par nat toa I 1.46S 0.TS4 P,ttl 0.060 Tha above data aad prlaet, ataaptlti thoaa lndloated aa a*need, aara aappllad ty lr. 0. Duftola la hit lattar to I.B.ftiford aad dated lap 7, UU. (Tba averape prlea for 1,000 BIO natural pat et Aaaiatoa la 10.(08/1 oa. ft. or t0.6 par aUUoa B.T.0.) In tbla aattar of boat, the (uldinp principle ahould be tba ohaupaat fuel that oaa bo olaaalp handled aad ahoaa hurniap aquipant eaa be ao ocatrollad at to --Intala falrlp eleto teaperaturea la tao prabaetar or prabsatara aad very oloaa taaparaturaa altbla tba oaarerter pot. Xt It believed that fuel oil would aoat aoarlp aeot tba at ora epeclfteatloa. it innlston n have fired with both fool oil and natural pi. it preeaat, oar firing ia with natural pi, ftrad tangentially around tho pot and through high pressure burners sa both ssecud prahoatar and ooorertar, Thora art t high prataara haraari on tha first prahaatar. Tha aattlaga oppoalta tha laad bath ara radlaat and hiiTa aeooapllahod a aery nearly parfact haat application. Rhatsrer ^rpo of fuel need, it would ba dselrabla to attnla a alallar radiant setting. Proa oar pat experience alth all firing wa hare foaad thin to ba difficult, and with a production laas than wa hare attainad with natural gaa. Firing with oil will aooawhat lncraaaa tha maintenance on tha pots. Xt la belltrad that next to gar(nhleh la allalnatad only oa aeeonat of its high ooat), faal oil would naka for tho ehaapaat soft. Groat eara ooat ba axartad In tha dsalgn and application of anh fuel oil firing equipment In order to attain tha daalrad production with a mlnlnun of aalntananon eoata on tha pota. Pat iiiu.i - Bwaagfi Tha aattlaga for thaan pota ahould ba of atool plat# and Aapta and aupportad on oultable foundatlcna. Tho atool oottlng Should bo lined with a eenblnstlon of rofraetorloa and Insulating brisk or liaad with insulating refractories, In tha past wa hare Mad a first quality flrsbrlok whlob nan beckad by natural sll-o-e*l. Iba teopernture* of thosa shall# arorago WC, ahicb represent but Mall boat loaaae. Such lining! ahould ha satisfactory unlaas such tauparaturaa would oaks for paraanal disconfort. Tha insulation orsr tha top of tha pota ahould ba (tsal platawork lined with all-o-oal and designed for quick moral and raplecauant. ITT 1.1.5. - Sg^9VJffiLeK''T Automatic tanporaturs raoordtng and control aqulpnant la rary nacaaaary. Wa hara found tUson-Vaoulm equipment wary satisfactory. Unlink aqulpnant by other aanttfaotmrars would bo equally as aatlsfactory, - The tenpersture of the load In aaeb pot and also tha npera fron aaeb pot arc recordad by naans of pyods and a six point WUeon-Hatulan Tapalog, Tha control Is through tbs pyods Is the lsad bath *loh ara also eonaaetad to Wllsaa-faaulea patastloaatar oontrols ahleh aetnsta inorlean Radiator Coapaay'a *>tor operated mires on tho high pressure natural gaa linns to tha soeond prahaatar and eonrerter. Thera Is no tenperatore oontrol . /r device an the first preheater for rack 1* largely heated by the coabustloa gaa** leaving the lotting* of tho ooeond preheater and converter. On tba flrit preheater are too high pressor* burners which *ra annually operated aad era need aa oondltloaa nay warrant to booat the tBiparatura of eoabuatloB gaaaa froa tho aettlnga of tba other two pota. Tho firing on the aecood prohootar aad ooBwartor la by gaa directly piped aad for alalaoa requiresante aad withcot regaintlob< Additional gaa to aniataia eonataat taaparatorea la tba load 1* pasaad to the aaaa bornera by the Ueoa-Maeulaa oantrol operating the Aaerlcaa Radiator too point valves, that la opm or eloeed. Controla to bold oonatant taaparatarea la the too hottaat potf would be required whatower saa tba type of fuel need. Tba flow of baaaaaa to tho unit la saintainad at a fairly oonatant rata by aeana of a Eohutta i Koortlng Rotanatar and aaaudl operation of a throttle mlwe on the liquid baaaaaa feed llna. The euooeoa of auoh aa arrangaaeet depanda on a punp with unvarying dellwery. Aa we hare found auoh aa arrangeseat eo oetiafaotory, It la racoonaided that auoh an installation aad practice be aontlnuad la the new plant. PI l.l.d.- PPIKO A TAtTK? All piping for carrylag the heated wapora between the Ulet to the first preheater and the dlaobarge froa the lead trap, whether auhwarged la lead or alaewhere la 18J( ehraalaa and ME alekal. Ooaaeetloaa are either welded or alae by weldad flanges with tongue and groowa Joints with goakote of etool and aaboatoa end node by the Qoetae Qssket h Paoklag Ccopany. Tho lnlat vapor piping to tho ooawortor and tho plplat botwoeo the ooawertar and the lead trap ahould pernlt of raadlly dlaacsmtlng for aooaaa to tho interior of tho pot or alec cleaning the hard and daaaa osrbea adharlng to the piping between converter aad trap. Vp until not we have never ueed valvet ca the pipe llaee far handUug the heated baaaeae or beasane-dlpbanyl aixtures. Usewbere gate valve* are ueed la pipe lines ooaveylng the odd olutloae. HONS 051911 PIPHsm OOmHTSB - OPERATION ITKV l.t.l. - TMPnATQRX AND RATI OP OPERATION hrra oparatad our unit owar a oonaldarabla ttagt f tanparaturaa. la janaral, tha loaar tba tanparatura, or down to about 7*0*0, tbara la but littla oonraraloa. At tanparaturaa of 800*0, tha aonwaralon la about ftOi, of able* 70/ la dlpbaapl and so/ la Rich bailor. Tbaaa taata aauaad ua to oparato altb tha wapora arouid 040*0 altb a ooaaaraloa of 10/ of ahlah 78/ la dlpbaapl and 08/ la hlfh bollar, and ahlob aa aalaulatad aould aatca our dlpbaapl raqulrananta at tha ahaapaat aoat. Aa tba high bollar la with onlp a llaltad aarkat, Ita alaUaaa produatloa aould ba daalrablo. Thla aaa ba attalaad bp lowar tanparaturaa and a loaar aooTaralou par paaa. Tba baaaftta of auoh a raduotloa la hi(b bollara preduoad mat ba offaat bp tba aztra proaaaalag aoata. Aa to tba rata of oparattoa of our praaaat aqulpnaat, aa ksoa It baa dallp aapaaltp of 3,000 lba. par dap with a aaararalaa of 18/ par paa. Tba abopa produatloa aould ba Mlatalaad altb a faatar faad of baaaol, loaar taaiparnturaa aad a loaar rata or aoBraraloa par paaa, but at what aaoaeap la not known. HONS 051982 /7 iHBrcm oomam mtaiup Diaousaion or bpoo*8TO two pot mtttb 1SHL Mj. Fusl ftrli|, oil, or soil, 1* lilltaM b; Its lsssr Mil, at shown In ths ooapsrlsoa gltss tn this rsyort. For ths anion ntlllnstlon or host, s host sxshsngsr is dsandod to rsoovsr ths host In ths flus gss. Is this ssss onporlosa hss shora thst otporlnatlon snd slight supsr hosting f bonnsns In s sstltfsOiory nsthod of rsoororlns tbs hst In ths fins cosos. On ths prosont dlphsnjrl soassrtor alt ths nos gssss srs dlsohsrgsd ot 000*0. In ths jrsyossd nnlt ths flus (nosi srs to bo dloohsrosd st 000*0. Oontlnuono frostlonstlon of ths rssstlon products Offsrs posslbllltlss of loosr sost squlpnsnt, loos off-orsds yrodnots, host ssosany, loosr loosos of Mtorlsl, snd loosr lobor oosts. OtIllation of ths host is ths rssstlon jrolosts ror ths opsrstlon of ths sontlnuous frsstioMtins solans Is tu athod of obtslnlng ns; Ian host ssomnqr. Ths ouccootod dlpbsnrl alt Is shown so s dlsgroaotlo flow shat In Drswing Ho. Oo-OdOO. loot onpolF All hoot lo suppllsd to two lood pot* flrod lndoysndontlF osd sontrollsd sotomstlallr by ths lssd tonporotwros. Fra ths Inforation suppllsd on St. LonIs fool sosts, (Ml oil lo rssosnsndsd so tho ohospoot, sxsspt sosl whlsh Offsrs oonpllsstlons of handling snd sontrol. Ths fins gssss loorlnc ssoh at srs ooohlnsd snd a*s*A through sn lnoulstsd Otssk ooststhing Ttpsrlslng snd sopsrhsstlng all for bsnaa. Ths fins gssss srs dlsohsrgsd to msts st 000*0 HCNS 0519*3 *6 lho boat bal--oo, show also ob Drawiai *o, Eo-MOB, li baiod -- thi flow at Ml Ui, of bm par hour ahlch plsaa calculated production ot 8,MO lbi. of dlpboayl par dap. It la alaa taaad upon aaturol faa aa mUttta at lialata. Oil flrl>| MU nabs aa apprsclabla dlffar--ee. Tho total boat mppllad la fUM Mt. (ponad 0--tlprado thlto) par hour aa ooaparad ritt l.Ul,Nt f.0.0. par boar far tba praa--t Bait ar Off. It should bo aotad that la tha praaaat ualt additional baat la omppllad for Iha fraotlsnatl-- of produata la tba fora of ataaa la tha b--a-- atill aad pas la tba ljh<--l MUX. liquid bauau at storapo tanparatura (a poapad thranph Iha saportaar aad raparfaaatar ooil laoatad la tha ataofc Uhara It la aaarartad lata vapor aad aaparhaatad to t*C. Tha baaaaaa vapor paaaaa thrsupi tha baat --ehanpar ahara lta tanparatura la ralaod to 4*0*0. Fron tha baat --ohanpar it paaaaa to tha flrat laad pat Santalala| land at 7*0*0 ahara tha tanparatura la ralaad ta IMrC, Tba baaaana sapor at 0M*0 than antara tba oonsurtor pot sontalalap laad at 041*0, la tba oansartar pat tba raaotlan to dtphanpl aad Up hollar aooara aad tba raaotlan pat-- aro dlacharpad at TM*0. Tba (aaaa ara aonsldarad to raaoh aa actual tanparatura of 081*0 at tba aarfaoa af tba laad but daa to unasoldaUa baat laaaaa ara dallvarad OnM tha laad trap and eyol--o enrbou trap to tha haat utshaajnr at T00C. In r--oil-- pasoo laaslni tha baat --obaapar at 04*0 pass ta tha rabollar of tha diphaapl ml--a, supply baat far tba fractionation aad dlSttUsti-- af dlph--pi. laasa it Mr, --tor tha rabollar of tha otrlpplap rt--, laasa at **0 aad --tar tho baat uub--nr of tha rabollar of tha b--a--a --la--. Tba pa*** laasa at M#*C aad po to tho esad--aor Uhara tho b--a--a --I bobsartad produt alrtura is ooadaatad aad fr-- ahlab tba Ipdrop-- la aaparatad. Tba liquid at 04*0 flan lata tha baaa--a oolu-- la --loh th* b--aana 1* dlatUlad off aad raturaad to tho b--a--o food took, ft-- tha bott-- af tba oaln-- a alrtura af dtgtoupl. Up hollar, aad tha lapuriUoa praaaat la --all mam't aad a--talalnp a traoa of b----a lo tttobarpsd aa llqold at tho belllap point of iM*C aad Q-- lata tho otrlppiof ml--i la tho otrlpplap oaln-- tho traoa of bonmans topothor with tho --purity uhlch bolls t--a*ora hot-- b--a--o --d dlphnpi 1* dlatUlad off topathar *lth a --all ans--t of diphoupl. Tha llqold ft-- tha rabollar at MD*6 flora Into Iha dlphaagrl sal--. MONS 051984 k (3 Tho diphenyl ooluau separates the diphenyl fron tho hIM bollar| tho dlphsayl distilling fron the tap a purified notarial ready for aala ar production of ether products and tha hlM hollar discharging froa tha rebollar at Its boiling point MOC. It ahenld ha notad that tha flow af tha hot raaatloa (asas la itrlctlf ooontar-currant to tha llqald products being fractionated. ' AaiJUaitt (hafar ta Drawing lo. So-MOS) As has already baaa polatad out tha pu oonsunption la U$ af tha prosalt requirMeets. Tha ataok loaaas af tha proposad U ara raduoad to 11.71 aa eoaparod to IT.71 far tha prasast unit. Vila perosntaga radactlou la obtainad by lovarlag tha ozlt tMperaturu trm MS ta MO*C. Via actual saving la haat la groatar than this duo ta tha saallar Mount af flua (asasi tha ataok loss for tha proposad Wit balas M,770 F.C.V./hr. aa ooaparad with 01,660 P.C.V./hr. for tha prssaat unit. tha vupuriaer and suparfaaatar ooll la tha ataok la plaaaad ta absorb lTt,Ofl P.C.V. par hour, laataad af 1*7,M0 P.C.V./hr., aa at yraasat and raising tha banama vapor ta This la aoooaplishsd tp tha Installstlau af additional hast transfer surfaoe and tha higher tonparature af tha fins gaaaa leasing the lead pots. The loaa by mlHitlan and eeareotlou fran the ataok and flues la raduoad fron 140,AM P.0.0<Ar. ta 40,000 P.O.O^br. by Ineulatic*. Tha haat auohangar operating an the hat rsaetlen gaaaa and beating tha bansans taper fron BQC ta 4MC raoatara 18S,7 P.O.O./br., tklah la Bars thus tha haat uaafully absorbed la tha prahaatar lo. 1 load pat af tha praesut unit, absorbing 107,AM D.C.Va/br. Tha high toaporaturo Mffaraasa sedating In this hast auohangar requires only a far squars | feat of hast traasfar aurfaos. Thu snail alto naksa possible tha reduction af hunt looaoa ta a tary lea figure. The beat Input ta tha first lead pot af tha preposed salt la considerably leas than that of the aaoond pot of tho present unit. The aeeead pat af tha preposed unit resales* approodnatoly the asas bnabt aa tha preetat third ar ocatarter pot. Tho total useful haat raealrad by tha bsasms vapors In tho tao laad pots la slightly lass la tha aa* unit thaa In tha prosant ana. This result la obtained by Insulating tha laad pats against haat lass to a Utah grastar srtaat thaa la dons at prasat tad reading vapors at hlghsr sapaahaat. davaral Mall ohangas la oooatraetlon ara naaasaary to aako thin posalbls. HONS 051985 I :r The atalwfc taaparatura la tho rebollera of tha fraotioaatlng oolaaaa la USC la tha bauu oaloan, Tha calculated amount of raboll host Including laaaaa far tha thraa fractionating alaaaa > 177.000 f.C.V,/hr, Sa ardor to keep tha taaperetore dlffaraaooa high la the raboll are tha alnl-- taaparatura of tha reeotian gaeea la*ring tha beaiaaa oolaan rabollar ni eelected M J80*C, Thle alee aarraa tha porpoaa of giving a reeerre heat (apply of 40.000 7.C.0, par hoar la tha raactloa gatoa above M0C, dloh la atill a high aaoogh taaparatura for hoat transfer. Tha heat atoheager aaa daalgaad to absorb tha heat la tha raactloa gasec froa 7N*C to 0.6*C leaving tha proper amount for frastloaatlaa porpoaaa. Tha heat la tha raactloa produoto froa 8S00 to tha owolMtUg taaparatura sad tha lataat hoat of tho ooadaaolag products oro aaatod alaco It la believed that tha eeparatloa of tha hydrogen 111 Bake tha fractionation easier. If tha prasaaoa of hydrogen doaa act affaot frootlcaatloa too adversely, there la an additional (apply of hart available. Ip ao aaaa baa tha equipment for tha propaaad salt baaa detailed* Tha following construction notat are recorded to aopplaaaat tPadag #M0. Tha flrat or preheater pat U1 be Bede of Crucible (tael Oaapaay'a kealetal la. 7, or equivalents lth the oovor aaldad on. replacing tha proaat boltad oonatructloa. Thla ansblae tha head of tho pat to ha lagged. Tha aoeoad ar poaberter pot vlll be made of Crucible Pteal 0napeay*a Beeletal Pa. 7, ar equal, oaat ataol eovar bolted on and all inaalated aad Pleh has bean pravloualy dascrlbad. The heat exchanger would be oonetructed of ataol or paadbly nlokal (hraa( ataol aad will ha arranged aa that tha hot gaaao paea ttnapl tha tPOlda Of the tnbea and tha eoldar baaiane vapora pass over tha oatalda of than. The boat aaohangara ea tha battoa of tha fractionating alap dll be of tha aaaa typo, hot gaaoa lnaldo of tho tuboo aad tho balling llqulda oataido. All oolaana will ho of tha packad type, tho baaiana ooluaa dag X/V Xaaohlg kings (ad tha othars^da. HONS 05198b 2t (ho vaporiser and supsrhsatsr will be iad of oollsd pips la *a lamlstod it*ok, g solid pore ia th* stack will b* used to Mala kick flu* (a* velocity. The easing should bo of the split type * previously described. The setting end flrioc equipsent far the pot* woald bo de*i|a*d to aeet the feel selected, |i, oil, or eoil. aaeeikle Oueretlne It la eatloir*ted that there will be mb* difficulty la the laltial starting of a diphenyl wait snob as i* proposed, partlowlarly la regard to the balaaoa of the heating swrface of the moUoaatiac oeluan* and the position of the feed to the eolaans, After the equlpaent is la adjustaant it should giro no aore trouble tkaa the present equlpnaut. Thera nay be a tendency for onrbon to 0*11act inside the tubes of the beet exchanger la spite of the (folsae traps. This carbon will probably b* hard and should not dsarsasa the boat transfer nach. Arrangesante would be nada to wake It easy to oleaa out those tubes. The beat balance is baaed upon the esanptlon that tha specific heat af tbs bnsssns sapors sad rsection gssos art aaanatially the tea* and ia given by tha equation! a, = O.CM e 0000*7t t(*0) The prellalaary mlpnl daalga is hassd upon tbs foregoing pacific best and upea tbs asnal beat transfer ooeffldants applying to slallsr probltn*. . (ho validity of thoso relationship* has beta pertlslly verlflsd by data furnish*d by the Dos Chenical Cenpaay on their diphenyl Wkit ia ooaasction with tha patent suit. (b* fraotionation oalonlatione base bom aada using PaoulVs law la th* oaas of tbs beaeant ooluaa, sad wxperlaent&l data for the diphenyl oolam, Those data are not as ooaplet* as oould be daslred. It 1* rsooannsdsd that developnant woik be don* to verify the speolflo heat, boat transfer, end fractionation relationship* before th* nasi dselga sad iaatallstioa of the equipsant should*the suggerted type of oontlaMous separation bo adopted Instead of th* batch per*liana la wso at present. This developnant sorb aead not be expensive or lwgthy. MOHS 0519*3 22 julm The mMuU* of two lead pots. i bwt BohuiWi end ooetlauou* freotiooatlng wqulpatat using thw heat In tba (iim, ti kali been deeeribed, fires tha lowest oaloalated operating ooat. iv*"* V* ' Thi* represents a sarlng af 0.84 cents par lb. orer our promt praetioB. Tba ooabloatlen af two lead pots. a baat exchanger and raplaoeaent of tha present benaaae still bp an improved eontlnuoui ooloan gives a calculated operating aaat 0.08 cants par lb, aara tha tba tealfi aalng oontlnuous fraotionatism equipment. la tbaaa oaloalatloaa ao reduction la labor ooata bare boat aaaanad baaauaa of tba difficulty and uncertainty of arriving at a reliable figure. Thera eeeae to be little hope af reducing labor eoata with the promt type af equipment whereae tba oatiaaaaa tgrpa of equipment definitely offers each a possibility. OB a produotioa of 1.000.000 lbe. of diphenyl a year tba aaigaetod sqaipunt, shown on Drawing 8e-t408. would aaww I 1.400.00 par year. MOMS 051988 23 rowam WAiiABum or batubai oab at bt. loots Thle 1* vlttn after the receipt of Hr, Uvlngetoa'e Xottor of June 14, relative to natural goo oat directed to Mr, leva, ea< alee after writing our reoaanenAetleaa, et ebleb time we 414 aet know that aetural gaa night be available. It la latereatlag to learn that yon now bare eneelleat preepeete of taping etratght aatural gee (1,000 >10) at teat St. Male for Ky per 1,000 ea. ft. for the flrlnr of the diphenyl eearerter malt, aatural gee affor4a a nearly perfect application of beat. Betural gaa eoetlag SOp per 1,000,000 >10 with ita high efficiency aad eaee of ban411ag aad kurblng woul4 probably be well la Hoc with fuel ell et tb.ty per 1,000,000 HU with Ite lower efficiency, greater expeaee of handling, atorlng aad bwralag ea4 tbs aeooupaaylng greater coat of Maintenance on the lead pete. la to tba Monthly gaa regalrcaeata, we refer to oar May, 1080, produatlon of 80,000 lba. of diphenyl. Uelag the average gee coat per pound of diphenyl produced for 108B up to fuae let end aa average prlee of gaa at ao.Sf per 1,000 eu. ft., the Monthly gee requlrcHenta are ldt,000 aa. ft. About tOl Of tkle gaa la need on the eoanector wait aad the talanoe for dletlllatloa purpoeeo. If the euggeated two pot unit with beat asehnagere, aad eeatlaueua aeparatloa devleee, are laatalled, a Monthly prodaotloa of >0,000 lba. at dlpkeayl would require 08,000 eu. ft. of gaa. The Matter of natural gee preeeure la at Mueh lapertanee. All of our buralag equlpnent on the dlpbeayl eoaverter unit, etllla, eta., are ef the high preeeure type which require aatural gee under a eervlee preeeure ef as lbe. per aq. laoh. HONS 051981 24 igABAitt_ar_jPR0tJWT3 - ami psaimt inn 1.1.1. - iqomnvT rat separatum imzowJii'HnrnrHIOH BOIL'D WIXTOHK3 Dw Tipori laotlng tin Mmrtor wait mtw fraotlaaatlag xltn, ahlah rovni noma of tha dlpbaayl oat dallaara atxturt of OO-TBjC itirnM produota and banaaat to atoraga taaka prior to distilling for tha fnrthor raaoval of tha banasna. Thoro la a atlll for distillation or dlphsajrl aad also n atlll for raflalag tha high hollar. Ixaaptlng tha ona fTastlonatlng aolaaa, all oyoratlona ara hatah. Thara aoaiaa to ho ao good raaaoa whjr auah dlatlllatlon aoald aot ha nada oontlaaoua. with larga yrodvatloa. tha daalrability of oootlBooua oparntlon raid ho aora spparua' than on opcratlona aa llaltad aa at pamti im t.i.a. - storaok or bh'ooihsxpidkyihqqh boil Wo hara ao apaolal adrltaa rolatlra to tha atorago Of haaMl, dlphoayl and high hollar. At jriia&t w# tior th# hoaaol aad high hollar la amorhoad ayllndrlaal taaka and with oatira aatlofaction. Tha 11fold dlphaarl from our atlll la aaaght la raataagnlar paaa, abort It aolldlfloa and la than dunpad out, hrokaa aad paakod late ooatalaara, althar for ahlpaaat or far farthar proaoaalag. A hottar arraagsaaat for haadllag tha tlphaapl would ho to flaka on a ah111 Whbol or la a atoraga taak, laaulatad aad with ataaa aolla. HONS 051990 2S- BKSCMMCTWriOlW itmi b T baat aoaprebend tba n.0* of hoot la tba oonvartar alt, fcaat balanaa aoa raaantly ui> and a oopy of wblab 1 da a port of thla raport, Thla boat balanaa will aot bo *1rtuaoad bara, axaapt to point out Banna of obtaining (rantar bant aaonooy la tbo no* plant. It would aae.u tbnt fual oil aould Mat naarly Boat tbo aoadltloaa aa not out In ItoB 1.1.9. Tbs oOBbuatlon pna laavlng tbs pot aattlnga should bs sore fully utlllisd In Vnporlnlng th* benzene end superheating tbs vnpor. Thla enn bs attains! by laaulrtlng tba sotting of tbu boat exchanger and also building tbs exchanger of aucb an aras tbnt tho utaoat In upsrbast aan ba tapartad to tho lnsoalag bonasns TSpora. Tbs laaalatst tana on tbla rooslver should ba of tha split typo, auob id so uas oa the dipbsnyl still, In ordor that It oan ba opaasd ap qalakly at tlnas of abut down, bsnaol failure or othsrslas, and tbsrsby provost drnago to 'ba hsat saobangor. 9uob a split ass Baton tha soils of tha anohangsr rsedlly aooaaslbla for lnapaotlon or rtpairs. Tha tops of the pota sltb all ooansctlng piping should bs thoroughly tnsulstsd. Thors Is s lnrgs caount of boat la tbs vapor lsavlng tha sosvartsr unit. 1 oultabls axahnngar .111 aavs pnrt of this boat by further lnsranslng tho auporbsst la the lnsoalag bsnnol vapor and thereby rsduos tho fnal roqulrnaantn. Bush an oaebaagor Is rossasaaded. Prsa tha partial ossta as shon la Ttsa 1.1.1., tbs aslaetlon of tbs oqutpnant aarroaa down to sitbsr Arranganents Ho. I and Ns, 9 with tbs bsnaol still sllalnetsd or also drreagsasat No. 9. Of drraagaasnt No. (, It sea bs oald that It la tbs old throe pot aosvsrtOT unit, sddsndod by tho host sxobnnger and sltb tbs ssltaaa abroad so aa to allalnsts tbs bsnaol still. Tbo systoa sould ba aontlanoua axoopt for tba asparatlon of the dlphenyl and high hollar sblab sould bs dona In batah aqulpaent. Ia tbla daalga there Is little of thr expsrlnsatel and sould mka for e good oparatlng plant. MGNS 091991 Arrangement Bo, 9 la tha aaoa oa Bo, t but with oaa of tha laa pole ellMlaeted, Tha eoonomlae batwaaa the two arraaganoata ara alight. It would aaan that a deolalaa batwaaa tho two would bawa to ba deferred uatll tba fuol aad firing aqalyaeat hra booa workad out. If the yreaent throw yot oottlag oaa be ooorartad to tha bow fuel with but little obaaga, Arrangement C ohould bo Boot, On the other band, If naw ee* Urge are required for proper firing, thwa Arrangement 9 ohould be followed. Arrangement Bo, 6 la deal gawd for tha ultimate la heat aaoaanp aad for the ooatlawoua oapwratlaa of tba banaaaedlphoapl--high hollar. The heat offleleaer of the wait would he gO,i Ft oonpared with *8,1 attained at Aaalaton at yreaoat. A further uaa of tha heat la the wayora would ba to attain the loelrod ooatinueua aoparatloa In aoluama, Ba hawa newer atteapted auob adyarntloa but o^nnot ate a alngle reaaon ahp It would not work. Before auob an lnetelletlon la aade, It la reoammeadad that aultabla deweleyeant work be done prior to tha final doalgne. Should a yroduetlon grantor than that of the preeeat Balt be doalred, ad la oomblaatloa with eoatlanoua aoparatlon, auob night bo attained br two or more oata, oaeh of two land bath pete, end eonnaatad to a alngle aat of eolmaaa. High boiler, Ita dlapoaltloa or permeation bee not booa yrawloualy dlaauaaed. It la bellowed that whalower of tba refined troduat la daalrod, that it aen boat ba made oa tha bateb at111 that wo are ualng at yreeeat. MOMS OS1992 27 0T18 OKA ir narorAOnnu flOl Tho MlnUi ralatoo to tho froooat float Ml It* oporotloa. Oopaoitgr for Ohlorlaator Utt ua US4 UM Ut UM UM UM MSI SOM tM(000 lbo. (04,000 in,ooo m.soo m,ieo 181,000 186,000 140,100 140,500 181,180 Thor, oro throo ahlorlnotori o Om m Drorla* #0-0081, Bioh of thooo 1, roaorrod for oortoto eoapOMdo, aaaolgr lo, 1 for UM oad UM| lo. 0 for SOM, SOM oad 08M aod Oo. 8 for U40, UM, U84, UM aad UM, Tbo lo, 1 ohlorlaator oaa bo oporatod eoattaooaaljr, Ohlorlootoro b, lull owoaot both bo oporatod ot tbo mo Um m ohlorlaatoro. Iho proooat prootloo lo to ohlorlaato U mo ohllo tho othor oorro, oo o ootch talk, Tbo aaathljr oapooit/ of tbo flat oould bo tbo capacity of ohlorlaator lo, i aoktiic Arooloro #UM ood UM olthor otaAr or to oosblootlao plao tho eopoeltp of Ohlorlaatoro lo, > or lo, S oporotlBf oliflf to prodaoo thooo Arooloro, oUotod to tbo UUddul oblorlottor, olthor olatfy or ti ooabtoatloa. lbo folloatag donerlptleo oaa bo ooot coolly folleood V roforrlhf to Dro*lo( #C-MM, Magra-tlo kyoat of Chlorlaatlaf biolfoot, Tho ohlorlaatlac oqolpaoat Sh oo at tbo proaoat Uaa oaaaiat, aooaotlally of throo S ft, la dlaaotor a Id ft, otool ohoUo oot nrUuU/i Boob aboil OMtalaa o ootalpat 00,0 of Ino turolaf, oloood la a ST* dlaaotor kgr ft, loaf otool aloooo, 4 00U of 1* H#t Otool plpo lo orooldod S tho oaaalor 00000 botoooa tho ; oatalpot oIooto and Ohlorlaator OboU, Thlo ooil la ooaaaotad to 00 olthor otoaa or oatar 00 rowlrod. HONS 031993 Chlorln* 1* fad latalk* bottaa of tht ohlortaator dlraotlgr tontt tba o*taly$t mm. Tba ri.lng pi o&ojm elrealatloa of th* okargo. k Otatrlfttgsl pMp la prorldad for aach ohlorlnator far ikkUaui alroitlatlaai Alok ritbdrawa Mtarlal from tha bottoa mt dailrar* It to tba top. laoh ohlorlnator la raaarrad for a oartala cl*** of prodncta, oaa for 1101 ul 11at. aoothar for MU, E060. and IMi, aad tba third for Utt, U,UM,1190 and Utt. thla la a tar? aooaooarr prnoantloo alaea tba eatalyat uii la alaoat laposelblo to aloM aad Plata! n*a Iroolor altb aaotbar la dotrloantal to gaalltgr. thla la particularIf trpa of aI ajar rrm alight aaounta of tbo orpataillaa iroolor* AIM and 11(9 altb tba otbara. Tbo (hlorlmator for 11(9 aad list la prorldad with an aaarfontp latorpal oblorlao aupply pip* alnoo continuity of oparatlon a thla Mtarlal la nlaoat oaaantlal. Tbo ohlorlnator for 1169 aad 1169 la aaad dapandantly Of tbo otbor tao aad la prorldad With it* nan trap and salting tank. Only ana of tbo otbor too ohlorlnatora It la oporatloa at a tlaa, tbo otbor balag aaod aa a trap. Oaa salting pot aorroa tbo Otbar to oblorinatora. 1 blowing task aqulppad altb a ataaa ooil and air llftrlbutor la prorldad for all cfalorlaatad product* azcapt 11(9 Md 1169. tbo air blowing rmoraa tbo HOI. tbo Halting point of Iroolor* #11Cg aad 1169 Is too high to ponait air bloalag la a atoM baatad tank. Chlarlsa la raealrad la liquid fox*, at tha prasaat tlaa, aad la oaarartad to rapor aa aaadad la a otoal task baatad by hot watar. Tbo aoeoaaary piping la prorldad for HC1 (a* froa tbo ohlarlnatlan Milch la paaaad through a trap aad than to tba HCl ahaarptlaa gyatM. HONS 051994 IsjfC.V \y HONS 052093 iKTlfif *>4 Dost JSWtUiEtiT.I npo>stws m wim imo i$raan& 5?itTEKJ*SS rantovi *>ra*P .... ti4 HONS 052094 fjfifPi sggfli.M- Sf&JRL .. .'.''SIPS... sYim E</S-W* t 1300 e3oi 13 - n!.F?rk Dipituvi TetsMif.A. HlH OClLE.l OlailLLEO #1400 e iw 6 I4B> 14 AK5LWS cuoat. A'.OCLC'rt - TO i A- 1401 4nt-ta.c* ;5 111? 1403 Mocl OR 114? I4V5 AXOCIOR ;? 1146 1406* AWCuOl jf I ISO 1407 AROClOR j) I 154 1406 AA.C.-OR i! 1160 140!) AnocLOS if 115? 1..4.1.1 AROtlOR#n05 (4:? Aaoct-M j 1160 1413 AXOCtOn if 1169 1414 AfOClOK J 2565 14 If AnXi OP f SI65 1430 AKOOlW ' 4065 1433 AWOl.CO f 508f) picTiun> Mrocir* 7o:a. 1431 AnOCLOS if |6I0 143? ABOClOD t 1040 1433 1435 143` 6 1437 1430 1!>1-3>9* 1440 144? 1443 1450 1453 ARCELOR if 1343 AH'a.t* 1240 AOOO.OA | 1373 Aiwiei oa 1; izv ARPCl-OR ? 1360 A01.41 OR / (362 AAPCiMt ,? l?64 ARC* .61) f I36P AR0CI.6R f 1369 Anocicm if 4405 AR')C` en if 5450 145' AROCUMI if 6443 ATOCiCY) rzjr CNS 0530(5 *U> l*t HONS 052096 tQUlK. $ W total *5 ' ' U|,,- ** R-'K'"' , 10/: Hmi.m* lu.| toss ' J* hi OOlLf" (WO I ) P) htt'fe* KilrrltU fcjOWl* *,*( lw*f * IIJTA Pi Ml tilin' Iwpl'H I*''** HHtftWI II EltdMMW Fvildll n iikU| |Mf(t Cl*flftSlM t kxNf*>fM f kivftMt < 1ltl k ______ Coil Bvik ( WPKPWC AND IHIPNNO GM1 I Btftti bi** pp> in* um * p h(f jk tkkw : .... M telbr. . M LaMr * Mri - , .*://.. h. L W*9mh Pt.n\\ JAVtVVC ,P iiMI tU'i|f Cquf|>. A BWf. Jt. Lfn*|ji*fMii|.., y lAiPirlilr*| C**t f tj *f t *w' y..'' J! Uktt Unkfitn ____________________ fi lto* Cm LnH # <* Itt Jt llltklh| | Wtlfkhi| , cmi , BteW* tortfttori ,, lffWlW| UftMoff -- .. .. taniltftri In .... , hteltellMMint Nr t*lm ln*eM*rjf . iHfwiri | .. *"* '/ - > fli - `J .1*1, ..... .. , . IM I . I'Htrf.el- /!<> I i* rt.oi'i lot . ^MODUCT 6 itf'Wt SYMBOL. SCH 6*1300 MONTH OF f^A ioj5 ^ ll/OOM ** |jtl 4 Amrunl H rtf Ik. 1 Pr Ik. -IVU-t! NOs * i-rt'S-v -no'j ' L /V !-vt IVu I (i n/<t/+:*;r) t/, *>n f 7 ill. Eo0S * Kj tOlAL EQUIP.* PRODUCT VWUit mu<U' BYMPOL $CH6.|403 THIS MONIH Amount I) Pei l*< YEAR 10 MIC Amount fl Per l*. | MONTH OR '//. BUDOtT Amount 103 3 io 4 Pei U. 01 |tf flWSN/i. urt*"*11* ?; \ v i ve-c -?-P_ox> , (r '/V I Nt' 36,-00 ,5*5 -R75 ,W5 675 yo D 'PtiENVt PI frtt ORINE ,, tfoliriilt Vi** i'p y rt.lttm* 1,4.10*0' RilMt*' v***#***"'1 f/p CM* * |*f* (i,.- ^KKfxlC1! >9 infAlOf ,4CeO*'tn* ,;(J JS-OlllECT EflPME ..... .* 1|* ............... .. . ..... . _ww4tfft*rrolon .__ /.3rf7 f Cjf- t r//j < v < P S' 7 P M - ole i // V/ v'd-./Vo 6 !d:^: 3 7TH "J nr n* >6 .-- .vm 'Jl * -. <> i IV 5# 172 6 406 ||2,m 7.5/6 17 901 o002 i1 .*004 600 li <6?l *150 I' 142 ,too ; .050 ,035 |: .037 l! ,100 |L 117 c0?0 I1 ,020 ,001 ,001 ,005 .C05 ,010 .OOP ,6l`3 605 .000 : 102 ; 0? I IW . ite .013 009 259 .371 *eo2 .976 flp'460 |;P 97~ PACKING AND IHIRNNO C0*1 IfHlt UH* h|i (m . lift Cwlofl* 14 Co'Aoj* i lift* Witui ttr thf UN'7* WU!, < j iNttbortet _ ,'*! ttortf' If*#. A >4 ,,>11 to NrprKIn# trtiP*rfcin| Colt *Mp tf / P*I*P tot* link Cert UU* Cm limit ICI bfcMo, A Wolfhby HUItMBp*n| Clt tMMNk J*fnlw> Ap*l| lo.cntmpi V*tllN#P (A , biitoAcoMFoi L. Ctwlo) bwntor) . , btROMA 01 ...... I *MM 4 fa 3-5 1 ; vd . *M* . INIS. MONIN found* | Amount S. s o: :ef' ~"JT6o" u,Uvjj* Tff / 7 S. f> C- (e l#i .77 oT TJ.o'L, 36# ___ ^(,-.->1 V j?7,! HONS 052101 , .if/? /aR It c'il C' ^.^telMifi ABj. IBM UtAUnl*i_ . J............... 30P1 filmy' MCNS 052103 it <t.IOTAl * `.'"'0I'1, (r^.rW,.\/ ,V* CMvCMYl jt piwrNYL #VCHtWfWC ' PMMMl < lt* it* livp<lri ln**(M* tr ft |>frU*4r*fFutlOll O VeMK <***> ft**! *M*pwM >i ftthfCT HUI'Afc.i' N'IMHMIIWI lywWM _..................................... iftritemiriltn IftltMlf'lb* _ `flttNM 4IM> MIWIN0 ton., trtn < Ctfkfljfl Id UMI ' Wb* f`H PMfiJ Of#*!. W-/fi/`'V<r W****** A_0W_f_. __ ., / e*i 'iMvi,, bit* Um.0i M IwIMi " m bVU^ | *tt,l.l, .'<f in.T <e.Y<r CmI Mnm d*tnWt| .............. ' dvr'rU'fr Vilr*< In __ ***<_.. . ______ .'.... ............ Hie*** 1 ft's* 1 *4-Wi ?.; /Y'J < tJi'( oi,fYny t r r,. c.tr vt Phoduci WUOE AROCLOR # 1)54 SYMBOL frOM 6-140/ month or //, < ,,,S1 * TOTAL I : ' *' ,.y. . rV* P* . .... a,, .j-t., _ i-, ; i^fy Uf*"''"* . `l#r . ttll'l`11 n-Miw Viioiil k ('<*> k' *Y* fO flHffCiolh IS I4i>clro4<-Irfurl0i| 17 ll(><kifl| ............... , TRODUCT SYMBOL . MONTH Cl" BVbClt IftT " .1 J .;< <: _ _ . . . j;.................. r .................. ................... j, ............... .. t*MHH>cr *>wl?*r............................. . . . j- .. . _____ j "` !t _ j ' .... .. : ;> "~ii*w!nltirHtC>HiiiU ........._.. ( SICKINS ANO IMfflMNO COST.. . . ... . ,, ____ ...i*i (nor ..... m. *|f-e*** , _ __ ____ _ ift trtw . . ___ __ n ____ S Cirl*yi_ ' lb UMi< ... ......Mi UMi I linkCi'l-Fci. IJ|__ . ____ **t _ f .., ^ ... ; Sliln| ....... ... . . ______IlMift tin's- S fldpt- . . . K ,, Ja . ' l*w* -1*js Cm ' _ |.................. 1< c... ... -- : .. IMIS MONTH !- TT i i-............. :. . fe* ___ 4*55...l,\: . YUfMObtlf ... .1. 0 W ICl ............. .. *| lUtkins 4 WflfWi*| ' ' "........ . Vitihifplng Cut I niftiufn fnnlorf Sytnlnt tnvtntofy Trmfcwtf in tptoi la Hmwai Put _. Chum 0i|>rl ( . iMpptt ...... i! ' II i. - jT ... i: 1- 1 Y'zrf^i i -: J....... , 1) .. _!! . Bulrk,- ..... i. , r.. i ; - ' ii s" ` " ' . '! ! ' ~ir 1 ... f_`..j. ; f .............. 'i :: s piiidt * i. ' ' .......... *1 1 ' i ! i i i .. '| _ ............. ii------------------- | .......... HONS 052105 t*iti>fkatri *iJ) ill (*i MHf> A .. $i (if m.TrMfilsLMrl M.Merlh St* tiiMWIn Ml Mil i>li Hurt* ,tfT, ,, total EQUIP. 9 rnilRltHVl .1! it'lf'MNf ** SimiCnH v^li. wtrHH U*W i W*tK *i** 1* Cito1olritFwtl 11 ttoeklnj feMIttPi**! t.itywri , I.W'IMf *"< !! 1 1ICHi*mMi T Coil Awi* 1 PMKHKtMOtHirnnoCQii j b"lh . [#IP* ....................... p bl' 0M .. 1* tirtoni ^ IP* Im.IIii i,f .tP*>RlK( E, fcM VMRt t|l> .Ipf * w>Mt .Mil PtM*| 0*1 Jl If . f tow lk C* 4 UW C*t Lul* I tltw ICt j? WUtklUf I I... ................... . IW R>lplnf Ciil I 11*km*' lintutotji j lp*l*f IwMltfy ^ liMtltriif In . ^w< ___ . __J. ,lililtAwim1f_ / a..._. ( .,, . wjJi PRODUCT C'VJut ARcOaOf^ 1 168 SCH6-MI? ,. Ut\ tl lilt i A||. If, 11 Uit Perth Lw.* <>* rtEtT. tOTAt...*. . Ej'MiNf ..... eou,r* ..... fen? Bfci#f Aiwei/'R-mos.mi i-uo7 STOJ? gutiiito /.fine, on /f |?M. "V'l 1119 (BipiiCKuiifc VT*. oc\.o 140X14II. 107 { Rip Oi>hfnC............... I!- jsi tnto' L 1437 AKOCIOK /l. . . jci.teyi25.Jj-u^-(Ki * ntll Im WpIfrtiU aj^r.I.W 4.UW ^ IWfiUl 0 S|Nrt,** . j|J *** 'n vh *< turp" 'll itHtftCtoiti l,llllw* H.fwo In,..*!"' [I*.**... IH.tH . - f|T PVM . . ... <>n<U2*6e*D`RtCT iC'^'PE jDffttW?!!___ r M>fiH CWWMlM W W* rnwuvt J0-14 13 PWK9 A*t|*irriMtcofit ttf U. l M|. cm .... . ......... IfcUM ......... . _ . .. M. Cl'UM. ,,. Ml* U*W ..................... R . P**. W .,, . *(* jit JTlL^G^ ; ifui en [> y r h|(|l y 4 . 41 lt>*f JJ UMi In Ltttfi t UK* id" ' Lit i Wl|hM3| UK oti ~7J oil V>vM*ni . fpMHffttfto...... -f1l*t1C*1WH Afm_v_v_M_f__t. D*. ^lltfN`51rl J __ &>l __ J/. __ i.ijy I -1.?r) cry.-Oj'. I .y/?i' ... . 'P'XJA* T/iTi-S i -/.//y .-/ .//a* ; r. *:&.:fv'h YEAR 10 MH 11 y / pi\ iii "n\/4_ MOWS 052109 Uv.***t. * C^fOTAL f ( r5**w ... . wfgSrSjSk<->.p: tllWlNt jffi LROOLOR 1406 uO tftUOC AftOCCOR W jwoewt.......... |)| ClORIHt mIS MakoIKcioJrM*CJU4III5.. iJiin . PRODUCT CMOC AflD CLOR # S5 SYMBOL SCH 6-1414 MONTHOF, yij ol i i,ii <+. /.vTi>/j ___ v\7/>? i'?, J> t $ j: | ' V v ` I.yf< 1xu.. J.z't P-.i -. .y -WlOLj. V . i.xei ?*>C> HONS 052110 '*&--..-Tvrvlr f . :)5r|j7i'V. - fWftM ."w ,, ... 5s5*... EQUIP. PRODUCT CRIOC AfiOCLOR * 3105 , /#* SYMBOL Spll 6-M16 . MONTH or.-Vy ; v tt !i / |iutor U4 H Hotie4e*FiMW i to li Irwril fUl W fcwl^w*l ____It WllM rp'rtikntVfrtwii CM..t._w_i_r MCKINO MO AMirtlAA COt. I' tomll .................. . |t toft ton . .. .. HiUtof 0 toll tortoM .. . .... M C*r*yi ft tow . < Utof M Mto'i . m uw ft Ut*t totrliii ft.ftM. !( I'Hp i >K|i Ln.W mtp&'n___ ______ )tJ tofcl*| toll , Vm~|. . vV. IJ tapir <J l II Utot \**kw* _ totor to* lull ' toW I Cl ' O toUrMni I . totl toll'll* toll 0Wwn tavtnler) . . .. . Iiflll* Inviftlory __tw_il_l'f_lt_0j _._________ toutto amivm tor_ . Ci**f*( ti***irt*ij___ ______ _______ I. kttiut ( 1 toiim IV' U - * I l*lk u... I I. j v A TP' <<> HONS 052111 ! gvCST. ItPf'B- i* i**!> equip. f _.. [&* I ^ l . ' ;3'*TlLtCft fl,0H i'r'U'* [ I*0f i< 6'SI l FD Mtc*. X If l*p**>*lM V't**' ' III IM. fl<t I'll " HUIrrlcl { ft Utlt aarf vffUn ' 0 it'ifoCIMh b fl. If *' M Mi >| I* U, irHtiiM) 10 ftNtrCM* If E'crltetrt n RoeMKf ttrtrl ftNimPH , || N*< . _ I*if !f> |WtM III __ ____ ____ ... [ CaartMfM I TU1 CaNwclaa __ fcnmc ADO tHIPPlAO com Ictiflf . iflwif , Kt* Cam UMi ....................... . .. _ ... ift|l tklllM* 14 C*fl>0* UfwM>l*6ir< fee. w*r Mf UMf lKf ItVAt tlC'lNf Mirt.*Hagf A (. .It*l.A*prMaf__________ ttlil Prtlf Ctil 9*>m* yQGr . ... Lata* U*k Can UM fi IhIi (lM tCl lolkhln) A Wtt|Mi*| 1*ii t*Win|~Coi~l UlMltiH* iMVitUiy litnifema In _________ ____ _ ... labile kMituKl fi. Clf>bf liwairtai) ................... OKpr.tr<1 f iMppttf PRODUCT SYMBOL CRyX A:C0^'.{;R if 4rt>Z> SCrt 6*!4?0 MONTH OF /y /4/ , / r; i tVDGV /1>*' Igieunf Pel lh j| Pci I .?w .iS | ??63 3.(Vi' II I*,*41 ] .?00 .W' ( .0*0 |1 ow> i F .f*0 l .nsi i 010 I, i .,o0:(,0r> 1 .-an I l .**9 i I 7.71? 1 TUB 10 DAIf I /H // .-> c/1. ( HONS 032112 L**T LO0. * fl*.***>- C*rl* , . . , .. - : jsgrv -. - urtn/mi S'^pira........... fcisTtiiW 4oh ,8r>ur* . . J*6tnr.......... . ftjl gl9f *i rft HtOM BoL*(* Ipl c*i WW LArfftATO<y SAMPtft f ". ~ t*trrtftf . . fw. V'jt4.,t*Mr L * Wtl^rUI .... . . . . ..... ... y ' * (hlirlkt V fc'iwWM*' IU" *fiv"*ri !.i piUi L p, IUt *jw-* . II It felO)l PROPUl-i vn--u.. SYMBOL SCH 5. 1423 MONTH OF . V jji 'I r.fik I hU ,417 | ,4?6 2?e r .!> 3-?B4 p.O'O 3.VP .6,700 3> . *0)4 . CV4 ; *xx 6.3C2 .109 .V? .C4T .'-o . Z.'j ; .Cvl -C-3T 1 .10? ,.C l ! o?7 ! .007 1 ,ov .127 . r,'0 .CV ..Nf. .''>2 ,??c 7W-- i,3rf *0ft0 ,?C: *r:i .''IP i .rbP. . ;'T79 11, "M ' ,"'V| 7^0V <',7 '/a Lsi 'w . Ctifafliltt Aai. lilt UlA>n1 ................ * HlillMil "*75" HONS 052114 ujt.doas. < eouip.t w*'- ;*' . . -. -.. . ............................. . flM*I Art&W 0 IMP ' m*9 CtOW)I/PlNn. jWT ' MTMQ CHkOAOplfHevU..... JaRACHLOP DIPHENYL . \-M\s.WIN' mi woei* # iu tStf PAAACHlOA DtPHCWl MtUiUH ( |* i*W,U*** j. HilffW ***< Upp'ln f .*** ?r$ PH 5t Af . jl ^ pfrl CMvml* If V rwNfwtfrt ___jli btw*r* toiCfMk PAKHt AND IMIPflM COM. H.llHtll W|UMr ......................... ........ ... ,, *, filM................................... M W . N tef Carton*. . . 04C Aldw ... *ltoi A HkVt*u rf.ft<t [,S*. D**MrM3w6tHf awta5 pseo in A IM|I )**l PwMat CmI II IM link Cn (tMf CttltMft . Ut# l " 'iff ItHiMiiiAWl)Mn| y 4> Mtalmift bt(fitoiy. [1 Oftklng brnnSoY) ___; Imtkn*4f*_ 'i-- ' Ollfdifiltf PRODUCT oiSTlUtO AR0C10R / I6ID ,, /44 SYMBOL. $CH-H9f...... .MO?lTHOFy>>^ IMS. . I LriuDO*. * r. TOTAL..* . . .... EQUIP, f |tatal [ Un'-W* M> fHinCtotti O HkcVItij l J*6M**M |Hri **'!* li **<!ftoftt . ri')Nw*Mf bwi tom N.ftfUrtBWBB fACKMIMOfMIfftNItMt ...... . . mim ............................ Cm........... ........... tw h+ jmbm..... *< e*rB*r. IfclBM*... ........... B W*M _ 'll twiSm r<. M*| _ ,h tom .......................... j.nmitoiikt . . ... 3M 1*1 HWwHhM*mil__*_**____. V toMfi '* 11 JIi. .......... .. H Uw toUlli j* U*r ICi ' 1} toMrtitaf I VtoifMftf tol>tU>lBptA|OMl Vtatawm tartt*T toMRtoty )ta*lrnf| Ik____ total* Aef*w*l ttattaa MibwDbI "" ' , thl})** _ MQNS 052116 HI hi !>. ,t.t 1P1AL * . . 0) 4 , CM* A*t`CiOft j? |I42 VjJ<J Al IML ue jtvu.ATB ,o> cnxc ^ryuou # iM2 M4 AlXtOH tMC y< pfc-i WiJKAU 1...:.a IT l.i'.kl flil.M *<<! vi.u>i lumi# fMl Hull I'M KMM. *M t-WW-lKC CQ$1 i Vl"iH l< lil*i It li r" III UI'M |i >>|< )>. |Mrt 14 CMbt>)( #4* V l|M fc* > l>< 1>J l'i Ubnf M> WhwlM'** II *( rqwl|>-4 PI<P Iam In tUpi lliVf ... m*i rwvmirud , ,P tnM>tr > ^ * l*b U*fcC*n 41 llbft till IflMli O |bAf I ft O IhIIiMDI * *. r lM* |<i(pp(Af fill tt-nmiiM* IntiMni) IhlfXlhlJ WmImm < >b PtHtntr# _ . . IMMIa A<ri>(>< tot ftMin# lhrMM) . Ww < *] /' i PRODUCT 0S7lieii ARuCmR 0 124? SYMnOL, SCH 6-M33 MONTH Of YU* 101>U Amotoif |j Prr lb. S.t, ooo /46 193 r* . 19 4 i.k . Off-'- <*< ... . '. 7 > / '/ `' 7 / !' e 70? 9.37/i .OfD .0;' #,77? b6<f? .72? .7U0 ,4t*0 C.3-. *0? ,7? .H' .c.y '/ .> , 3l'L . j 'i //' ! /j 7 / ' ./ ,i ' :. , O'Q * O' -o 2<X> ,034 .03 .100 ,IOv 1 .OUt .0' , : , - ` . - ' ' 3.4-7 3,tti i 2X ( ` /; '/ . ...i ... ; j IM'S VfWIH Ppimd* Ao-r-nt , '. / 1 ......... 1'T' ......... u ' !' Pm lb ' 07f. , *3.4 , `.>v 3 I.CVc' 4.S'" 13.167 14.3-U : -- mmiiiini An.fiiini Pr* lb / . ' 1' 1 . s i; :U\ ! '] 1' . i j. " ...... ......... --/ - 7 ' " / 1. * , I1 . ; . ; j; l! ii V .[ j . ;; 1 i // vO ' ' ^ . 1' .. : . a . j.... . _i ' . * 7V J . < Bulk 'V- '* 1 ; to l * I ' 1 * ! 7 II ' ' i i . ..---- .... ,, . i.............. r .' i ,1 , 1" : ^. ' /. 7' - - > . r r, iv i- ' / ''ll v /- ' MOMS 052117 > : ', icit. *** EQUIP. S4Ki5r-S' LnjPi IvW . . .. UlfWl - p |i .; < U (MM / 1148 u . |)4 MKLM LIMt ^||| Pllf/Wl tf* ftwt.UMr VilrtUI ' l,iMf r i |tHU CM* [l fit" [I I" **1 tip I, MK*4*.iu r^itWK tJ fclrriiilnf fcifriCffN'miM Piwi fc.Wi*** 90 OtftCCV VOfAKC (f InWHil' *lrf Vf* . '/IlfWHK_____ ___________ _ . ____ ____ If toMtotoini CpiTiuU pwoouct oistiueo AwaoR jTn YMBOL^ $Ctt -U35_ r_MONTH Of/^ * jji >i :>.33S /.d.sfrj, 11. PIS' pi.' jybA\,<0/KV yo/ .3 b ,/ry Vm: . /y/o\ 40 O'>^'1 f . '.* *> uji, h ot^ :.//! 7? 1/7. 3ft _/ii /<? /It'I *0,000 1,003 I l.06t ,013 ,0141 | 8.TW5 B.>., ,013 .010 ! e.<T0 .8to04* .660 .600 8.3T' .61 ,70 .81 ' .616 .34/ I' .063 .200 .046 .121 ,173 .046 ,136 .124 .131 .083 3.863 ! 3,40* ,200 ,304 I "* .070 t .090 ...6*8 j! j9 ,803! .868 4.766'4.371 13,834 ||I3,723 fftCXINft ftllft tXIPPlNQ COSl <th . - ||#H W>*f ................ ,, I . Cti .. >UBMe*t 6nm* ft! ._ fc.atkty..i._. ,ni Um *4iiUMf 'fl bftlCm PM. V)| ....... _ ,muM .. `. \I. W** Wtutk* III. #*! tNirafr ft ftMgt. , uMJp MlHtMsi. X, X NftlHmMet;ff *-h 41 (M*| hl tin It UMi CulMll |J *Mt *'. flit (fttHM*) I f(t|fi(ft| - tiniltmt In ....... 1.. hHmt___ . . (tyiftf totfRlor}__ o! r,T inn piwur (I ftmewt ...a.. :ri m /? if/ ... . T' /ppj - /='7 17777 .77.1:7 TKrtj; 1.' ."wylT'7>, '/vyr # ...........w...ll , .. , . it pH |i Pa(c(k<ed;,4 -/T/ts ' ;.fn| ___fJLi.Hl. t J>y V-, U., - ii\>-iS ` "* A Cjl-t. Cn -i HONS 052118 h u >X [Mil** [#. t toM ;fi uw {* III* eftn tk t* -- .... -- 141 tofc*_____ .............. iMU.r.f t!.lf. > IWtt . I A. . JhmbilhJuts&Cmifi(i__________ f X ***.. U'l ; * ton*** ..A* ... i)l um Wem ______ [ li UU C ItKl J l UW* Ul . ... I 0 *m*i*| ft wiMr| fl i'i tLi<S--sck*Lu5plAp [I VlulMtiM fnvtnterjf t . I 1. tftfftlftft tavtutary ' 1nnltitu|l'^rj JtBkltlf &> n'nf "1 lit-u Mitl ' ' _ ' F?-t V v 4f.irj,.-t.cv.rvii' .! MOMS 052120 HONS 052121 tLoat. , total . PRODUCT OISTJUEO AROCIOR 0 1262 SYMBOL __$CH 6J439__ MON7H_OF^^_y " ........ mofcMU ^ 8 ' br u. auoctt V. "/ INO" tr Lb. ft? lb. ,09 c*uoc AAoaoA # JI62 j 1409 AWOLOit #ii{Z V4 lM:;<.:.on l (lit IJ3-J-0V.U?.. It. VuI'M'K ........... 1 1 ........... i "' ' ........ ..'. i>' : " ` /C .. | -. ! .......... .'w ' ,: ' : rMo)tiT>n} Ct *th jU/ TO.W 1 :P . I. C02 1.0(2 .OiO ,00) ' >004 _. . ;; r b,s&3 2,309 .. J _ 1 . .. 1 ; ..............f. 1,006 ,05* __aP2A e**5t*i J>,33* .. .,1- j. // ........... . ' . . >&4 ,500 . . -w > i ... r>40 ,47t ................/ . . V .......... .V . / . .. *860 567 .............................,400 ,477 1 "i vim/ / 1.1 ^ *32 . i ,< . *0$ 2 ,' _______ O': . . , i.. .. _______ 1 ' . :~j.\t/nil . .,.030 y- _______ //:,, .i.oi 1_____ _1 !1 1.. .,.070 27? 122 , <65 036 , M6 ,060 > V,t "7,'&4TrX^r 200 .?7^ *000 076 ,130 _j.62kli0l.6_ V03 it)OV 3,852 4,fi Util *^DC*R ,** . f*" ' PRODUCT OtSTUlEO ARPCIOR / 1264 ,Jjp SYMBOL . SCH 6-M10. . MONlMOr^, - , 13 5 ihi$monm ; j . _ m*ibu 11 Amnimt (| Pel IV 8 Amoertit || Pull- | aoocn _ / torn A Amount |j fifth {[ f*t (ft. li r *** iMrlMl L! M*V 7 - filtrlel If If. - #*'' [ft.|*irt*W . t> Oil* 1 *K* *| W** < 10 f Itln Clolfc 10 Ilfrtrodr*6i furl Oil 11 WorMi^ ; ) UK>f*'M !|. I ft **<ftont. i> *...... '"* f m QumieHen _____ jj fttftfrft Cnnmilen MtCnotmte_ II PACKIHe AMO 0MIPPIN6 COST < ** . . P W*i ft 11)1 Mine lh Ukw M CmlttM _ .. .. 04 Qhttoyt ill (Met 04* Uh* H 1*1 C fei Olej .............. Hi Lim ' H (M*i IterlHf . ;H OiW. IlMiff 0 J III Atfi'tiinj___ r Met PtrMftf Cel! tzz-ti' 11 titof link tin ............ i| UJmt Cilidt 41 UM ICC . 0 tetfoMnj I WetyM*|......... Met SMpftint Co** Minlumm (nvenlnry ftntOf Initnlnty 1lMfMl4tA , flftllW#______________ Trill U AmmmI fo (M(ri| Inventory_____ Ahpotfrt if >m 'J >' ------- 11 fit IMIS MONTH Pocmei | Amount Pet U VfAA 10 OAK PMtnAl :i /Lo -rO -- --- <1* >q U ./o<f lo if' ./u-' 5w/( p-C-lji II ft i/.'/ hi HI MCNS 052123 If lit** j*T, IOTM- * , vtn *** CQ ,412 (IW6t AAOCLOR t 1166 Aoa. tint 14(2 A4W.WI f tlM> 1442 / 22I66 JM i*0UM UM* ^,,1,, tfshrltlt t/"' .'.UN* iitnUI ,,, (1k- 4W* . * |***f*"*l 11 Ei(<1i*dr*tFr1<m U IUrVI| fnvmlM Fl*rt l t"SnnsdrC/^*w*w_'M_#_* ....- tot *& ; fitioNfi ana iMtrrmc com ' IrMfte . > tow i itfi cm ' ,, .. ... . , n c*fc>i . * Hi lfc*r i V* to* ft. ftiy (.......... - l tow*tMtoH%* kiU* ")U\J <mv . h\Sfi 4 IW***' I .tin* f* 0 *W|* ..... _ ....... .... MIMIm tut I *w O' 1 tow 1wifc0> .. - 1 tow tKlnA i ton m t4ihln|tWilgMn| . lt|l 6*iI . ktlmiM Imtnto* Opttta| lltsilttlrllft ' .fi44*4 . . ........... . ............ ttfctfe AtciMMf F*f . 'u.. CH(A| tavfftto) if, topp< u,*. " ' fiat .1. C/.l- ,1 t 1} product oismuo Aftoaod f izce t~9 SYMBOL SCH 6-1442 MONTH OF lY/i-tj 103 5 ................................... / #' 6.486 MOMS 052124 ' ,u. ldos. * r equip. TOTAL ft I . ( K-Bii l!. - . i' fcptJtl................................................ t - 01 .............................................. - PRODUCT 01 STIUEO ARDOUR f 1208 8YMPOL SCK 6-1443 MONIHOT , Tf11 lu out (! Amount 1! Pm lb. |j ____ lUOtill Amount //"/ '/ ' 1B35 / ..I'U.l . . p. lt>. |i Ptflfc. .500, OW Ull $11 M9 jjpi c*vm AAOCLO* # 1168 UW.................. Lilt HYDRATE . CWtt AWltauf I'19 ' T. '/y. U . 7.. V , I,i40 I.3v ,oo;>: ,o^3 ,00 . 1113 311 notion # i I 18 ASOCUIA # I 168 AAOCl OR LIME . >'7' IH4 ` /./ 'ft > ^ ' j ,00 C.80S e,7/5 ox t'1 Kl, V*ti . ..,1,11.1.'. , *1 . Ilhni tMoul i*t - Mitnlit mil titp{iiiii I'.tut'Mh to nittr Cloth y ' -?:. aZJi . ;. v ..,/) .<^r i'-'-n .' ! ; '' ,|;i . 0^ i .oit l! :,ll> . ./:. / . .m 5T <-!/:/ / . <M . 1 - _n- /I >' . / . - / p i ,, 1 1 C,6(i9 ' .4*0 .419 #&oc- 0v>t .2' i 2 ' 0 267 . zrj ! r(M5 .046 fioir ! 11 Bto^hlrvf .................. 1 ..........> . ..' ij/ : 1 . - .ov* M- /a .> / iC?i>7. 1 ; .i : /' . .. j . .024 .Off) -OM .oa^ . ''/' / .. - 1 * / -/ ' |: i .MG .MG ; , 1!' ... ^ ............. : .. ,p2ij Ol'c j- <>.l ffinvftilon ' K - ,:1 17` ' ' . . - 1 1' MI* l'll<*t ..,1.. 10 bluett ,&FaI . y -. 7 ..jyi-1 C . 't ' i.w*nrr aiul tain ' .. . ,7- ' (.fTioiKpA tMitr<Cnttcri)a* . . m'-.T. : 1 llr ' ^, AA ! ' ' . tolitCoovmtnn j; / y -<(/ .! jj)- a : .:> IK|lt||tHlltl Cut Oulu ,1 -c.'i Vl.-..! / '.hi >y .-.-yy; . ................................................ -................. -yl; -------------------1 i! ..........i ;> ' t ii 1 - ;---------1,T1 i , 2i0 i i .075 -: .62/' .2-13 C>04 C'.j .513 .661 2,6:/i ' U.503 `).4C7 j PACKING AMO (HIPPING COST Cwh _ _ _ . . .. .......... liMt_____ _________________ _____ : lt|i- Cum . . ...______ ___ ____ _ > l.hM . _____ * l*|i C*r!Al __ 14 Carboy*______ ... . *# Lahir_______ ; 1i* **** ./'k... mii, >*.. l*k *lMtt . . ............. . (tariff Cfwip- * tidfi. , ^ lalil Pa<itiA| Cut fc,*|t l/ 7 " " , - Uifr-hnli Carl '! iiut" Cat iat 7 * HilfWhf ( Wrtfhlni ' -M^u tint Itiifflni Cut Ninlnmm InftMlty Oppntng _ If.nilrmdt* y,. tiUMo AeaauM far , (`.jwifrf at 1H1S WONTH_ _ . Pound! . Amount ''I............ rrf.::.:: 1 ...L \ J .... i I j.i.r. . y..? , . ~rxci >; Afnount Apith, / : ^ - V_ * / "m' / */ " / / 7. -. A . <s :V 5 r i -V- ...........y .<... ...... y/;hi ' 7-;! TTTmT '' W rrr-r- 1" " i ,,S !j 1 .1 jf V 1.. ' ____________,__-_____ _-__ -_pT___rn_ _.. . ..''77 / ^ |. y . > / li&!C4/-i____Z_0z7X..-.---- i'-U. ' --1 - ,<5/' >// . Y" XT' .:T /'/.' / 'I < ' y li . MONS OS2125 . _'i | I... J I/', HONS 052126 l PC*f> c ir.'Ai. ftl't. * EQUIP, f 1H(S MOUtM in,furl Pi PRODUCT OISTIU.O) tfi'.'UI** V ''*** svmhol SCh i> 452 mc'mtm of //"< k.->5 TJ**TOP*n ' r II\t Pe>ib. ` " BfOCH > *V,M " N'.ii ' P,rlH 4R \,h*iO nUKLXt ff Mk Z. . ArtvC t* / 5042 b Cl m 2: I'f.k.Bf. ft> &Hlt`PKt<! "Ok! /> Jl W. rv |H`* M8* M Poti*** Hit P<- " u Rin inri PbV'tf _ CV6*__~ *__ ry__ . __ __ " ' .1 lvt Itk lM**f__________________ __ ......................__ _ - _ _ ________ _____ _ UCm*<(). . ,, ________ ... ...... .............. .... . :... .......... _. ............ u.vs-%.. * -i fij.ini fcfiui* ..j.ut.'i - \f>t ii S.k.n$ Cum " 7'*~17 77 17_I__ ....'___ .... .. 7.. . 7'. 71 - ................... _ . . ... ............... . . . ................._ . . _. '......... - __ _ ...._ . -. "'1 ....................... .................."7............... 7.7 ' ' i U** Cm* ........... ...........__ ____ __________ _ . j_ . _ .. I**-** in" * v. , ,, / 77*77777777.77.7. !.. . i ___ __ ~ ,' _ ............. - ..." .................. I S* m*i>h C*i't P > l****pp i t BuN. *; . ~r. P, I.'-' i I^ ' <;1 2 --J ; tj HCNS 05*127 HONS 052130 tF9 mmj?* i LABOMTOW METHODS| SMOinCATXOM ABD tqoinmT Ii MthaM A, Plant Method* for Controlling production Of Crude irooXor* X. Dpeolfio Oratity t, toidity I, Aoftanlcf Point of Solid Aroolor* 4i Bold Point tor trodor* Hi60 and XX60 I, Cathode of Analyala for Aroclora or Vood tgr Control laboratory I. Botoo t. Acidity of Matilled ArooXora I. Dpeolfio Qrerlty of liquid Arooloro 4> Tandenoy of ArooXor #6666 to Conoo Bloating in ArooXor - Stoortao fitch llxtoro It Bold Point* for Arocloro #1X66 and 1190 6# Aoid Buubar of Crude Arocloro Tt CryatalUeetlou toot an Bon-Crystalllae Arocloro It Motillotion Banc* of liquid Aroclora 0, Total Chloric in Arocloro 10. Fra* Ohlorldoo in liquid Aroolora 11. four point of Arocloro 11, Loro on Boating of Arocloro XI, Color of ArooXor #6460 14. Coaffiolant of Bxpanoion of Arocloro 16, Dotornlaation of Treeatag lotato 16. Detemlnaticn of Banael insoluble In Solid Aroclora IT. Taooriiatlon Looo at 68C It. Hfhngrl in Cnidt Diphenyl or Dipbanyl Still Bottcno 1*. Dialoetrie Constant of ArooXora 10. RaROr factor of Aroclora II. Bealetlrlty of ArooXora 1. ArooXor #1164. Q.B. Conpouad Bo. 1476 1. Chlorinated Diphenyl, Crude* Aroelor 1116 I. Chlorinated Mphenyl, Crodo* Aroelor #1141 4. Oilorlaatod Diphenyl, Crude, Aroelor #1146 A. Chlorinated Diphenyl* Crodo* Aroelor #1160 5. Ohlortootod Piphenyl, Orodo, Aroelor #1164 T. Chlorinated Diphenyl, Crodo, Aroelor #1160 6. Chlorinated Diphenyl, Crude, ArooXor #1161 I. Ohloiinttod Diphenyl, Orudo, Aroelor #1166 MODS 052131 /co fjaaderd Bpeoirloatlgas (Soutineed} U< Chlorinated UfhNjrii Crude, Aroelor #1169 11. Chlorinated Wphenyli H.B, KU, Crude, Aroelor #6668 lta Ohlorin.ted Diphenyl* H,8. Ill, Crude, Aroelor #4066 Ui OUmluM U9> Bailor. Crude, Aroelor #6069 Ui Ohlerlnated Diphenyl, Distilled, Aroelor AtU It. Chlorinated Dlphnyl, Distilled, Aroelor #1249 16. Chlorinated Diphenyl, Distilled, Aroelor Attt 17, Chlorinated Diphenyl, Distilled, Aroelor #1261 16, Chlorinated Dipbmyl, Distilled, Aroolor #1260 16, Ohlerlnated Diphenyl, HltUlod, Aroelor #1666 60. Chlorinated Diphenyl, Distilled, Aroelor #1M4 61. Chlorinated Diphenyl, Distilled, Aroelor #1666 62. Chlorinated tliheol, Distilled, Aroolor #1666 Setor Quenohed) (tilled, Aroelor #1619 64, Chlorinated Dijlhmnyl, Cl,tilled, Aroelor #1846 (Constook 6 Veseott) 68, Ohlorlneted Diphenyl! 8.B. ids, Aroelor #4466 66, Chlorinated High Boiler, Aroolor #6460, Distilled 67, Aroelor Moisture Proofing Couponed fax #601 HI, Laboratory Test Iqulpnsat, Showing the Pieces Arallable Ter Transfer to 0t. Louis 60hs 05il32 >I010 I I. UMTtlCAL MTHODS A. nut Ibibvte (w OutnUtai rntuttv iwk.wbww mm faunoim woman wnn>. ctb n. lm hons 052i33 PUNT METHODS FOR CONTROLUNO THK FH0DU0TI0N OF CRUDE _ABQOLQR3 8PKCIFIC ORATIT! Hi* temperatures at whloh the pnltlii of liquid Aroolora ore taken vary with the vlsooslty or the liquids A natal oylladsr of suitable (1m to provided for oetahlng the osnple fro* tho ohlorlnstor. Tho sample, after hotbe caught, 1 ooolod (odor tho top to wlthlB about 10*C of tho taapersturs ot whloh tho gravity 1* to ho token. Tho hydromotor to tboa lnmorood la the liquid to e depth jatt sufficient to oovor tho bulb eod to hold la tblo pooltloo otth the loft hood while tho liquid la stirred vigorously with tho thoraioaotor It the right hood. Tblo stirring lo continual until tho toaporoturo of tho liquid lo one degree shove the desired gravity toaporoturo. At this point tho theraoaoter lo qulokly roaovod and tbo hydroustor allowed to sink gently to for to It will into tho eenter of tho cylinder of liquid. Tho hydrometer Is rood sod this reeding rooordod so tho grevlty of tho drooler. Tho gravities of AroelorsUlS, 114*, 1148, 1180, end 1184 sro token ot 08*0. The gravities of iroolors 1180 sad 118* sro taken ot 90*C. Tht following toblo shows tho Halts within whloh each Aroolor should bo finished. 1110 -- 1.11* - 1.11? 114* -- 1.848 - 1.880 1180 1.4*9 - 1.4*8 1184 1.809- 1.807 11*0 -- 1.889 - 1.88? 118* - No hydroaotsr (Must bo finished by festphai) 1233 Be sure tho sample la stirred well but osrefully la order to ovoid breakage. Tbo hydrometer ehould be rend ns qulokly as possible, slnoe tbs toaporoturo drops would give wrong rending. . ora HONS 052134 y jism Approximately 35 of the llqulA eroolor (or 30 gran* of a allA araalor) lo poursA into BBO banker. To tbla 100 oo of alooholtiaaal alxtura (furaiahaA by tha laboratory) 1 oAAoA. Tho mixture t* (ltratoA with K/lO oauatlo solution (aloo obtalneA from the laboratory), lefere tba titration ta otartoA a llttla water la aAAaA from tha tap. |Wi tha anA point la ranobaA tbe watar layar will ba ooloraA pink, Tba Mating sparetIon la oomplata when lata than g on of tha oauatle solution me requlreA to raaob tha anA point. ira MONS 052135 pormiiHo point or aouc aboolors Ball and Ring IMtM Preparation of tba Beanie Th temple obeli be melted and atlrred thoroughly, avoiding ovarbeetlag or laoorporatlng air bubbloe In the mnee not then poured into the ring to to to leave s alight aiceaa on oooltng, Blsoa tho Aroolore dhrlnk eonelderebly on oooltng, tha ring should bo vail fIliad, naarljr to overflowing. A llttla of tba axoaaa should ba drawn otar the top of tbo ring ot several polnta ao aa to prevent tba ooolad Aroolor from drop ping out of tba ring. In tba name way, tba aaoond ring la filled vltb a ntaaderd Aroolor of toon aoftonlng point, Tho otandord Aroolor ahould boro a ooftanlag within at laaat 10 to IB* of tba Aroolor being tooted. Tbo rla while being filled abould raat on a oloen oen lid or on a braaa plate wblob baa bean amalgamated to prevent the aroolor from adhering to It. The Aroolor In the rlnga ahould be fully ooolad and hardened before prooedlng vltb the teat, Prooeduro Add water (not above room temperature) to tho beekor until the onrfaoo Of tho water la t" above the plate holding the rlnga when tbo ring oupport la auapended In tbo beaker. Pleoe tba rlnga oontnlnlng tho Aroolor to ba taatad and tho etenderd Aroolor on tbo ring eupport. Plane ball on tba oanter of the upper aurfaoe of the Aroolor la eeoh ring, Buapond tba thermometer ao that the bottom of the bulb la level with the bottom of the rlnga and juat midway botveen tbo tvo rlnga. Plane boakar and appnretua on a B laoh round hot plate and beat. Tho temperature reoorded by tho thermometer at the lnateat the Aroolor touohee the bottom plate la reported aa the eoftenlne point. The booting la oontlnued until both Aroolore have dropped to tba bottom plata. pptva 1, The atandard Aroolor to run along with the aample under teat la order to oompanaato for varlatlona la rate of heating, dilution of Oyoerln, and thermometer varlatlona. t, Bensol la need for oleanlng tba rlnga and belle. S. Water oan ba uaed lnatoad of glyoorln for aoftonlng polnta P to BO*C. 4. Per aoftonlng point# above 100*0, well bollad glyoorln should bo uood. Tho uouol glyoorln lo not eatlefuotory aa at led to 150*C, It belle with loee of water while tha temperature remain# praotloolly oonotont. It la wall to have o eupply of blgb-bolllag glyoorln on hand to ba uaad oily for ooftoning point# above 100*0. b, Air bubbloa on tbo ring* end belli during tho toot abould bo avoided oe for oo poeelble. MONS 052136 S124 Fiem lit dtk o/ C. P MICHELS HONS 052137 '6f joamatjiw t uai p**crlptlon of Apperetu* Tb* r**pta*l* for tb* Aroolor 1* *-i/t z 1" (1m tub* ehlob HI MH Mbit* *t oa* *od, Tbl* tub* t* J**k*t*d bp pl*o* of **b*to* ppi trapped twit* around tbe bub* and 1* laaartad 1b *^u*r* tight IUH MU1* bl*h 1* lniulated ob tb* botto* bp l>*r of 1 Inoh *ktrH* fibre, Tb* bub* 1* bold la plea* bp a large tort. All of tbl* ln*uliUm U u**t 1b bb effort to k**p tb* Aroelor fra* tooling too rapidly Hi It U b**t to get additional lB*ul*tloa bp wrapping tb* *lgbt oubo* Httl* 1b t*l fter tb* aeapl* 1* added. Proatdur* Melt about 100 **. of tb* aa*pl* la bek*r OB tb* hot plat* Hi your it lata tb* tub* ustll it 1* fillet vltbia l-l/a" of tb* top. ft* Mttrltl Will probably orpetellle* lu* to tb* sold tub* *ad *111 bar* I* b* b**t*l o**r a ga* buro*r to **lt It agela. Wb*n It ia salted la**rt I Nitabl* th*r*0Mt*r (300-380*0) ableb 1* fitted *lth *ork to bold it la pleoa. Tb* bulb of tb* tb*r*os*t*r ahould b* fitted la tb* a*nt*f If tb* tasplt, ear* being taken that it 1* aot too aloae to tb* *ld* of lb tub*. If tb* d*tr*laatloB 1* *ed* on lisp or I860 tba tub* tbould bo h*at! until tb* th*raoMt*r rad* about 300*0 and It 1* pieced la tb* NbMtO* j**k*t and tb*B put la tb* bottl*. Seeding* oa tb* tharaonater Ire t*k*a at 00 attend lnterrel*. At flrat tb* traparatur* ulll drop rapidly (about t* bat***a reading*) but arouad *50* tb* drop *111 d*or*a** tad aauallp a polst *111 b* r*aob*d br* tb* drop will atop, and *111 titter *t*p ooBotaat for too or aor* reeding* or *111 start to go book ap. Ibe isrreet bold point 1* tb* point at ohtob tb* t*sp*ratur* r***ln* *onataat or 1b ** tb* tenparatur* start* to go b*ok up th* hlgh**t point 1* tbl* ri** la t*k*B, Tor *zipl*l >48, >43, >40, US, UO, 842. 830, tdt, >41*0 would be tb* *orr*0t bold point. 1b tb* * of 1188 or 1S8S tb* proeedur* la tb* *aae *ieapt 1*1 tb* tub* 1* b**td to only *00*0 inetaed of >00*0 after tb* tharsoMt*r It laeartad. tri MOWS 05213d JQSiSLJL * mmsikssm l. atthtto *t iwlirili tn imUn u oni kr tti uwntttr gfaa.aw.ou. goyar fwnofiai KfunnH WMM. ffitt m. HCNS 05il39 'it NOTES CO! ABOOLOB TESTISO A number of A.B.T.U, Methods ore used la tooting Aroolors, pjrtiae *: Tire Point Plash Point Tloooaltr-Capbolt Softening Point IP-92 Mt 0-08 D-3S The A.8.T.I'. directions ora exnotip followed for aush taata. Color. Lortbond. for color of liquid Aroolora, tha Lowlbond tllaaater with 1" ooll la uaad. Standard olla of tha National Patrol-- on Aoaoalatlon (N.P.A. standards) ora roportod to be no loneer erell- abla, Tha following ooirrerolon table la naodi N.P.A, Oplor Numbera 1/4 1/* 9/4 1 1-1/2 2 Loribond Analysis .6 1.1 l.T 2.4 S.O s.o tofl oo .12 .so 2.50 Dlalaotrlo Strenctb) Asm D a 117, No equipment he a boon uataiiaA at Anniston for Making this toot. Loop on Baatine; d houra ot 100*0. Thi0 toot to similar to M.t.W, That D-d exoept that otati lo Maintained at 100*0 and tine of holing lo extended to d hours. Thta teat la uaad on O.B. Material bar* aa speelfled. A 40 ea. sample lo uaad In the pleoe of SO C**- *a HONS 052140 /*3 DIRECTIONS FOR TEST NO.__ tHHt SUBJECT t Acidity of Distilled Aroclors METHOD:_____ haOH Titration____________________ (CO *, 1) (tmof the Aroolor n nl|)( late ECO tt ktikir n< 100 M of O.P. boBMBs addsd. After solution tei tern affected the sample lo titrated with .01 I alaoholla NaOH aolatloa, using 1 a* (about CO drop*) of l Mhsaolpfcthalela solution aa as indicator. Tba aod point la raaobad bao ths solution is visibly plak throughout. Rapid stirring should bs ussd While tha MaOB solution la being addsd. Tbs rsaalts ars rsportsd la mg. of >*0H par gram of soapIs. It la unusual for a dlatlllod Aroolor of tha 1*00 osrlss to require wrs than .5 oe titration, which la equivalent to .004 sold ho. Tba aleobdlo KaOH solution Is trsparsd by making up S so of 101 aqueous ceustlo solution to *00 as roluas with tBjS alcohol (ranaila SA). era HONS 052141 DIRECTIONS FOR TEST NO. ld-10- SUBJECT; Bpoelflo Orwlty ef Liquid Arealore METHOD: Wentphal Balance Oonaral Specific Brevity 1* determined by ueana of the Weatphal balance. Tka teapereturee at which tba apacific gravltlea ef liquid Aroolora are taken vary with tba vleooelty of the liquid. Tba apaclfiaetione far aaab Areolar ehould etete tba temperature far both tba Areolar and tba ustor te uhleb eoaperlaon ef gravity la aeda. In plant preotlee, apaelflo gravitiee ef trotlora containing up te B4$ ahlerlea era uada at Bd/dd*0 vhtla apaelflo gravltlea ef Aroalera containing dO-**,J ahlerlea are a>da at oc/oo*0. Spaelfia gravltlea of aay ef tba Aroalera any be mnde at ee/as*C by uaa ef the A.8.T.M, method far road tars, aapbait cemente, aoft tore pltabaa, aerial deelgnation D70-XT, 19X7 (deaarlbad le Bureau ef Btaadarda Mlaaallaaaeua Publication Be. 110, Staadarda aed Speoifleatlona for Beuaetallla Mlearala and their preduata, page IBS.) eetphal Balaaeat Similar to Bluer aed Amend Oatalog Mo. 1M90. Fluumet eaad uet have thermometer aeala te 00*0 but ehould not be eubJect te Injury by uaa at thia taaperatura. Oylladar: Pyrax glean hydraaaatar Jar l.B" l d". Thermometer: Oee thermometer ahlah baa bean oheoked for aaeuraey Of aeala In tba range need. procedure Plaaa the Weatphal in euah pealtloa that the piunmet la T - 0 laahaa abora the work bench. By mbna ef the leveling aerav, adjuat the Maatphal balanee to ebot naro reading with a clean dry pimanat in air. Buepend the ptamaet during adjuatnant In a empty ayllndar to protect tba epperetua front air currents. Heat the Areolar te be teated te a taaperatura about 16* higher than tba taaperatura at whleh determination la to be aada. Tar exaaple, If apaelflo gravity la mate* at dd*C, the Aroolor ehould be heeted te about BO*C. Than pour the heated Aroolor Into a elaan Pyrax ayllndar which haa bean warned by netting at edge of hat plate. The cylinder abould be filled with tba Aroolor te wltbln about 1 inch ef the top. MONS 0521*2 /7# fa** * DIRECTIONS FOR TEST NO. 14-10-S* j SUBJECTS METHODS Alloa tbs Aroalor to the ojrllnder to air oool until the tempera ture la about T degrees shore that desired, tbaa pi see tbe epllnder in a kot attar batb ablab la at a temperature about 6 degrees abort tba iaalrad taaiparatura. A litar baakar containing sufficient aatar to ta equal to or abort tba laral of tbe Aroslor la tba eplloAer la a setlsfseterp aatar batb. la aaaa tba Spccino orerltp la to ba taken at 80/*0*, a glpeerls batb about< ba substituted for tba aatar batb to arol< tbo aatar vapor aitb Ita oondenastlon on tba (aatpbsl beiaaea ablab la prooomt If aatar la uaaA at high temperatures auob aa 95*C. Vlthout disturbing tba adjustment of the ffaatphal ablab la aat to ree aoro with plmmaat la air, place tba epllnder eontalalng tba Aroalor la auab poeltlon that tba plumnet la immersed la Aroolor end add weights to the boaa of tba Veatphal aatll tba beam la again laral. Tba plmmat should not ba ooopletely Immersed aa aall aa about 1/k" of tbe euepeaelon wire end the plummet adiould not touab the epllnder at Of point. Stir tba Aroolor with a thermometer at frequent latarrala aatll tba iaalrad taaiparatura Jaat la raeohed. At thla point tba weights are quloklp adjusted until aqalllbrioa la obtained and tha reading noted. Baring obtained tba reading for Aroolor ot tba daelrad tempera ture, tba opaalfia grarlty la obtolnod bp dir1ding tblo figure bp tba reading vben tba plummet to Immersed la pure eater ot tba sane tempera ture. Tbo reading for water Is obtained la tba sow manner aa for Aro olor. Stnee tbo reading for water la eenataat, presided there are no errora In welgbte ar Vastpbal, this figure need not ba determined with aaab Aroalor teat. Tba figure for water whleb in used aa a eonatant eboulA, bowerar. ba abashed onaa a month or whenever graetoat sooursap la needed. Tba reedlnge for aatar at dS*C end 9*C are respectively ! ,WB and .MT*. I Oalouletlao ef Result Example 1. Assume readings aa followsi Veetpbal loading with plummet la air Veatphal reading withplmmset In Aroalor at 05'C loatpbal reading with pinnaet la water at 88*C Than ap. gr. at > 1.80*8 - 1.8*88 .86*8 Example t. Asawe readings as felloes i Vastpbal reading with pluanat in air aatpbsl reading with plunmat in Aroalor at 90*C Vastpbal reading withplummet In water at 90*C Than ap. gr. at 90/90*0 - 1.84S6 > 1.898S .987* Zero 1.8015 ,98*8 Zero 1.8438 .967* HONS 052143 /7/ M* * DIRECTIONS BOR TEST NO.___14-X0-98 SUBJECTS_______________________________________ METHODS._________________ i_____________________ _ BtStt X. Th* might* neat with th* Vaatpbal balaae* should h* eheekad t*rtoU*Ur h/ weighing aaeh an an analytical balanaa. t, Tba odjwatmat Of th* liquid to the azaet tanparatur* a**lr*4 la aoat laportaat. Da wt alia* to aool raflMjr.ul atlr frequently aaoogb to mlntala a anlfora taaparatura fro* top 00. bottoa in th* yltndor. NONS 05214* DIRECTIONS FOR TEST NO.________________________ Tendenop of Aroolor SMS to un Blooming 1 SUBJECT J______Arnnlar-aimarlmn Pi tab Mixture_________________ METHOD) wBWaoopilWitqii^irw Tnomm^ewitavwwdsw.e Bolgh out 10 groan or Aroolor 1565 and 15 grama of eteerlne tilth. Malt tba Aroolor la a beaker and add the etearlae pltob ia too i or throe portions, itlrrlig ell tbo tiaa and gradually raising tba temperature orar a period of rite to 10 minutes to 180*C to S00*C. Stirring la oontlnued at tbla temperature until a on1fora mixture baa bean obtained Tbla map require 10 alnutea or More. Tba pltob la added to tba awltad aroolor ao aa to avoid axaaaalra oxidation of tba pltob. Whan tbo mixture la unlfona and reasonably free Treat foen It la at onaa poured lato a mall salre tin (tba tin *" la diameter la a eonvealent alaa). Tba salra tin la aorarad and tba Mixture allowed to tool. fbea ooolad to room temperature tba tin la opened and tba eurfeoe of tba Aroolor-etonrlne pitab Mixture la "seeded" with arpetala, no seeding operation aoaalata almplp In rubbing the finger llghtlp over a aampla of Robartaon roofing nblob baa bloomed badlp or orar a prarioua teat aampla of an Aroolor-atearlae pltob mixture tbat la aorarad vitb blow ao aa to plek up a treat of tba blow on tbo finger--kip and tban linger printing tba new iroolor-ataarlna pltob Mixture ri tb the name finger. Oara mutt be taken not to plak up too auab of tbo white blow and trenefar It to tba w* teat Mixture aa the "aaad" map than be Mintaken for blot*. Tba aalra tin eootalnlng tba aaadad aampla la aorarad and la tban piaaad la a warm apeee at about 40*0. At tba and of three dapa tba eemplo la lnapaatad end If rerp dlatinat blow bee net daralopad tba aurfeee la rubbed over with tba ftngar tip ao aa to aproad the aaad arpatela tbat are already preeent orar tba ontlra eurfaae. Tba aampla la tbaa ra-aaadad la too apota aa befare bp finger printing with a finger that baa bean ltgbtlp rubbed over a aurfeee aorarad wltb tba blow. Tbo awplo la lnapaatad totea uaaklp for the appearance of blow. Tba blow eppoore flrat oo a alight dulling of the eurfooe, than aa a uhitiah pouder on tba aurfaea and flnellp under tba aleroaaopa aa Mhlte traaaparaat naadln-llka erpatala. Ia the eaee of an Aroolor with o otrong tandanap to blow tbo obit# ooatlng derelopa oltbln too ootka. In the osaoa Where bloom does not appear bp the end of two wwaka tba taata abould bo oontinuad to at least four weeks before a aagatiwa result la reported. Fire weeks la safer. MONS 052145 f?3 Mi DIRECTIONS FOR TEST NO,; ! SUBJECTi T<>noy of Aroelor IS&8 to Onuae Blooming eto. : METHOD i._____________________________________________________ l Ijotoe i The preparation of a hoaogeneoue alxture of Aroolor en4 ataarlaa I piteh free fron exoeeelre feaa when the alxture le ready to pour Into ; the eelee tin appnrently requiree none experlenoe, I The otearlne plteh le a "soft plteh" obtained Tram IIr. P. W. i Jenklae of Mellon Inetltute, Ptttnburgb, Penneylranle, for uee In the ; teet for Moaning. : ere I MOWS 052106 DIRECTIONS FOR TEST NO._____________ SUBJECT i Mold FoUt. for Aroolor* UM A U METHOD:____________:_____________________________ PooorlUoB of Apparatus Ik* NMflMli for tho iroolor to 4 l/l x 1* (loot tub* which too koto ooolod It on* mi, fhto tub* to JookotoA kr o ploo* of oobootoo papor wrapped tele# orou&A the boko aaA to lasorted to o aquar* elght-ox. battle oklok to laeuloted ob tho bottai by o layer or 1" oobootoo ftkro. Tko toko to holA la pleee by o tare* oerk. ill of tklo taoulottoa to aooA Lb ob offort to koop tko iroolor froa eDoling too rapidly oaA it to boot to tot oAAlttonal taoulatton by oropplat tko eigbt-oa. kottlo la toool oftor tbo eaaple to added. Froooduro Molt okout 100 pi. of tho oanplo la o koahor oa tho bot plato aaA pour tt Into tbo tub* aatll It la fillet attkla 1 1/*" *f tho top. Tho otor1*1 atll probably oryotolllao Auo to tho oolA tub* aaA will bowo to bo bootoA oror o pi burasr to Mlt It ageix. Whoa tt to aolted laoort o oultaklo thomonotor (800-900*0) oblob to ftttoA with * oork to holA It to yiooo. Tbo balk of tho tberaoMeter ohoold ho fitted la tho ooator of tbo aonplo. ooro bolag takoa that It to not too oloao to tbo alAo of tubo. If tbo AotarnlBOtloa la aaii oa 1189 or 1849 tho tubo ohoold bo batted aatll tho tbomono tor rooAo about 300*C and It to plaaot la tbo oobootoo Jeofcat oad than pat ta tbo bottle. Sob ding* oa the theraoaoter or* takoa at 80 out. latorrolo. At flrat tko taaperatura will drop rapidly (about 8* botoooa rooting*) but around 880* tklo drop will Aooroaao and aouaUy * yotat will b* rooohod Wboro the drop will atop, and Will wither atoy ooaotoat for two or more roadlago or will start to (0 book up. Tbo oorroot holt point to tbo point at whlwb tho taaporoturo roMlas ooootmt or la aaao tbo touporotur* atorta to go book up the htghoet point la tklo rise to takoa. For oxoaiploi 844, 849, 840, 886, 886, 889, JH, 889, SST. 948*0 would bo tbo oorroot hold polat, Za the oeoo of 1146 or 1846 the prooodur* to tbo aauo axoopt that tbo tub* to boatod to only 800*0 laatooA of 800*0 oftor the thoraoaotor to taoortoA. la all roadlago a (tea oorreotloa to aedo (unloao partial lwarotoa tharonwitor la wood) by no* of tko following formula: 6t*u oorreotloa K a > (1*4) I Factor for expansion of aoroury la glass .000185 M Length, expressed la dogroos, of the aoroury ooluan amrgant froai the bath, T Oboorrod thermo** tor rooting. t Moan taaiporatur* of tho oaMrgsat atoa wblob la found by plaelag o oaooad tbaraoaotar at the nlddl* of the exposed thread of mroury. or i MOMS 052148 r* 7 76 DIRECTIONS FOR TEST NO.__ X"14-36 SUBJECT; laid Kunbar of Oruda Aroclara METHOD: >0B Titrntlaa_____________________ Iwwtoi MiwIti 00 ptai of Arotlor la 00 O.P. bwwl aontslaad Is ISO *o biaktr. Ml 00 so of OOjC nthyl aloofcol SBa titrsts with 0.1 IbOB solution using 10 iropa of l phsnolphthalsln solution * lndlsator. Oafors storting tbs titration, s llttls dlatlllsd vatsr Is ilM; this susss ahnrpar sal qulskar separation of tka agusous layer fro* tha san-siuaous laysr. Oaloulsta tbs acidity Is allllgraaa of RSOB re quired par gran of saapls. On aooovat of tha strong Nam solution used for titration, tbs blank titration of tha raaganta nay ba emittad. Ilpa HaOH par gran saapls titration In aa x 00 art. of oaapla txaapls: If tha titration of 00 grant of oanpla la 1.1 so, tbs aoU auabar la found as folloaat 1.0 * 00 dialled by SO .40 Mgn RaOB par gran of droolor. ora HONS 052149 (77 DIRECTIONS FOR TEST MO. 1*-40-94 SUBJECTt Cryatalllaattoa Tat on Non Or/atalllna Aroolora METHOD t Bolutlon In T V A P Orada haphtha________________ ftroatdur* Ik* t*at 1* baa*d on the relitIt* laaolublllt/ of ar/atelllna Aroalora In naphtha. Velgfe *0 (ran* of powdarad Aroolor (prafarably find; powdarad) into * old* Month 8 onnaa hottl*. Add 40 gram* of naphtha and atoppar tightly. Slink* ontll aolutloa 1* aonplat* hot do not oaro to h*t*n Mlotion. Sot aald* for 3 da/*. If no ar/atalllaatloa t*k*a plas* olthln thl* p*rlod tha notarial 1* *onald*r*d o*tlof**torj. panhth* Itnlit matora and Palntara frad*. Initial boiling point ItHlI'T and and point WHHt'f. Obtainable tram nofford Oil Oonpanp, Biralnghaa, at lty par gallon. ar* HONS 052150 trm DIRECTIONS FOR TEST NO.__ 14-31-gC SUBJECT: Distillation Rang* of Liquid Aroolors METHOD: , A.8.T.M. DB0-00 With Modifications Tba apparatus, consisting of flank, aondanaor tuba, shield, and thermometer, la exactly tha seme aa described ndar A.S.T.M. test OTO60 "Distillation of SltuBisoue Materials suitable for Road Treatment". Tba aatbod la shanged to tho extent tbat thermometer readings are taken fbsn specified percentages (usually 10, 60, 00f) of Iroolor have bean distilled Instead of following tbe A,B,T.M. prooedure of weighing tba distillate between spselflad thermometor readings. In testing droelore 1*64, 1*48, 1*4E, eto., 100 ee of aanple are taken for taat and tbe dletlllate la reoelwed Is a 100 ee graduated cylinder, In testing Aroelor 1**0, 100 gas. of aanple la neighed Into the distilling flask and distillate reoelwed In a tarsd flask or beakar ranting on pas of e torsion bnlanoe with 100 gran saala. Procedure Tranafar 100 on of anapie (weigh 100 grama in tbs ease of Iroolor 1**0) Into tba distilling flask, Assemble apparatus as daeerlhed under 4.8.T.M, DtO-30. Insert thenaoawter (4.8.T.M. high distil ling 0-400*0) through cork Is tbe neck of tba flask so that tbs top Of tba bulb la level with tbe lowest point of janotare of tba Subuletura and nook of tba flaek. Apply heat to tba flask supported on two sheets of *0 wash wire gauss so that tha first drop ooaiee over Is from to 16 Blautee. Oonduet distillation at rate of SO to TO drops per alaute, Oolleet distillate In 100 ee graduated cylinder (or tared flask in esse of Aroelor lldO). When 10J( baa been collected as distillate, sots end reeord tha thenaoBeter reading. Repeat when 60 aad 90? has been oolleeted. for reeord purposes the temperature when first drop fells sad when eeah successive 10^ bee been oolleeted (up to 00^) should usually be resorded eves share specifications require only tha 10, 60, and #0readings. No corrections for emergent stem er pressure are applied to tbe tbenoneter readings. ere HONS 05ilSl DIRECTIONS FOR TEST NO. ____________ SUBJECT t *ttal CttiriM la Imliri' METHODi Fararlt* IUIm i mB| tHwttn uraocn fra^iak. curaiMtiw f Qwiu 1.1 i.o,. _ iai. t*. a. I. IW urn),_________________________ CUsriM la IrMlwi m; ka ky (utw of Ui M|ii altk aotla* iiraili la a krpiH'vr faalaa ny, artraatlag tw (uln altk aatar, aaltlfylif tka mW artraat rltk altria atlt, aat yraatyt- (Ui| tka aklarlaa ky admit* af aa aaaaaa af Mil* altrata. Itt* flltratiaa, tka axtaaa af allTtr altrata la ktonlul ky tltratlaa acaiaat yotaaatua tklatyaaata, aalas farrlt aaaaala* Mlfata aa latlaatar. aiwnt Tka faalea any aaat la tka Bargaar-farr Salta* M Sa. S far fl*aa Igaltlaa. A laaA faakat la aaai. Far lgaltlaa, tka kaak la aaayaatad UmH a l-a/la" roaai kala la a l/S* traaalta ylata. nta alleaa tka faalaa tay m aataaA tkraafk tka ylata fa* akaat */*" IfMtlaa la affaatad ky atraatly kaatlac tka katta* af tka faalaa aay altk tka fall flaaa af a Makar karaar far taa alaataa. Simf. i&tiaf Tka faalaa alrtar* la aata ay af akaat IS yau (aaa aatal aaaay) af tail** yaraxlta aa< 0.0 ta 0.S grata af flaaly yowdarat aaaa aacar, tka aaaaat af aaaa aasar tayaatlag ayaa tka nlfkt af aarkaa aoatalaad la tka aaayla. Tka raayaata akaall ka fraa fra* aklarlaa, a* a klaak raa aat aarraatat aaoartl^ly. Ska faalaa alrtara la tail alxat ky ylaalas tka lagratlaata la a a*all kattla altk rvkkar atayyar aat akakla? rlsaraaaly. WLft* f tryataiilaa tyya ara aalgkat la tka fat* af tall ytllata. Tkaaa ara yrayarat ky kaatlag tka Araalar aatll aaak a aaaatataaay la raackat aa till yaralt tnyflit It fra* a glaaa atlrrlas rat aate a tlaaai aarfaaa (a aa* tay]. aaak tray foralac a yallat. >haa aaal tkaaa yallata aa* ka ra*rrat fra* tka aarfaaa ky laaartlas a ayatala aatar tka*. .4 yrtaa ara aaat. Tka yallato ara kraakat lata tka katta* af tka faala* aay art tka faalaa alrtara ylaaat a* tay af tkaa. iftar Wgktaalw tka 1U, tka tkarga la raaty fa* faala*. Tka tryataiilaa tyya la valfkat la tka yaatarat fa**, .4 gr<*a kalag aaat. Tkay art akcrfat la tka aa*a aaaaar aa tka aaa tryataiilaa tyya. Llano MtOOLOBSi .SO ta .SO sr*a art valfkat ky trayylae trm a atlrrlas rataata flaaa af tkla kaalaykarltally akayat si***, aklak kaa kata Jaat yrtTlaaaly tarat, aat Altk rraalaa aa tka kalaaaa. It la aaaaaaary ta kaat tka *ara Tlaaaaa Araalara ta "trayylai" aaaalataaay. Tka ylata af flaaa tkaa aaally alltaa off tka kalaaaa yaa lata tka HONS 052152 /so yoga No. $ DIRECTIONS FOR TEST NO. >4~l-g< SUBJECT s_______________________________________ METHOD:______ __________________________________ The following queatttlea of ample, auger, and AgNO, or* uni for the reapeetlwe lUeriii ooatente: . w m-m BejC- wjt Uf. - o; Weight of Bangle .1# - .*0 Crane .gs-.so .as-.so .40-.41 " .40 -.41 * Anouat surer Aid>0, 0.0 SO .IB g.(l/* aaoop) BO os .SO g.(l eooop) BO e .80 g. " T6 .80 g. " 100 ee Procedure Fleet the faelon tap, which oostelne the prepared ample end fuelan nlxture, 1 the trenelte igaitloo plate end apply the full flean of the Maker buraer to the bottao of the futloe tup for B nlnutec. (OACTIOBl Do not oteod too oeer the fttelae during Ignition) Tbos renown the flam and oool aader the tap. Vbea eool reaowe aorew tap. Thoroughly rtaae the oup oower with water, oollootlag the rlDeluge la o eleea 400 oo beaker. Thea pleee the fwelon owp on Ite aide la the beeher end newer with a weteh gleet. 80 -- ?5 oo will bo la the beaker froa rlaelng the eap, ead thlo la oaffleloat to deeonpoae the ehurge. Renown the eup end rlaaa wall. Whoa deooapoeltlon it ooeeplote rlnee off eower-gleea ead Odd para EDO* with etlrriag, until eeld la preaeat la oeeeae to the extent of about 10 ee. (About 50 oo of aold are required.) Add exactly 80, (t or 100 ee of ateadard ellwer nitrate eolutloa froa e pipette (dopeadlag upon ohlorlae preaeat) and atlr to offoat coagula tion of the ellwer aitrato precipitate, niter with euotlon through aa aebeetee pad oa a 1.8" porferetod poroelela plate end wash beaker and filter 4 tiaee with aaall portloae of oold water. Allow the filter to drela eeupletely between waabtage. Trnaefer the filtrate beck Into the 400 oe keeker and rlnee the fleek twice, adding the rtnelnge to the keeker. Add B 00 of forrlo Iran indicator to the eolutloa end titrate with ateadard E0M8 eolutloa until a dlatiaet plak tint la Juet obtained. Calculation of Chlorine Content Subtract the wolwae of BOMS required from the woloan of EONS required to titrate the mount of atenderd AgWO, eolutloa need. Thle will give HONS 052133 tat Page So. * DIRECTIONS FOR TEST MO. 14-18-04 SUBJECT I________________________________________ METHODS_________________________________________ the roluae or sons equivalent to the chlorine la the ample. Multiply the voluae ao obtained by the ehlorlne value of oeeb ae of KOHS and llvlde hy the weight of anapie taken. far aimnlei Jr SO on of allrer altrata eolutloa la equivalent to 41.4 of EONS aolutlon and the value of 1 ao of X0N8 eolation la ,008770 cron Clj then If It la found that 0.3 gran of ample above a JONS titration of 10.4 oo tho pareent of ehlorlne la: U1.4 - IQ.4) _ .003770 * 100 - S4.0J 01 .8 la aaao the fuelon alxture or other magenta oonteln ehlorlne, the aaount auat ho determined end deduotad froo the ehlorlne found. Solution# Beaulred Standard MO. Solution! Shout 0.10 St dlaaolve 10.4 grena of ailvar altrata la aaoh liter or veter. Proteat the aolutlon froai light, fifty !aa of thin aolutlon *111 proolydtete by theory 0.175 gran of ehlorlne. I Standard ICES aolutloni Shout 0.06 St dlaaolva 8 great, of IONS In 1 liter of voter. 1 eo about .006 great ehlorlne. ;arrla Iron Indloetori Dae a aaturated aolutlon of ferrla aanoaluB altne. Pure Nltrlo Sold. TOit Stook aotd aufftaea proTldod It la eolorleae. It ota ho boilod la a booker until oolorlaaa If aeoeaaar/. ; Staaderdlnetlon of Solutlona Oelgh 0.8 and 0.1S gran yortlona of pure dry NeOl Into eopnreta 400 oo bookora. Sdd *80 oo of dlatlllod water to aeoh end 10 oo of pure B0> nltrlo void. When aolutlon la oonplete, odd 80 oe of etsaderd SgSOe aolutlon froai plpotto. Stir veil and filter through an aabeetoa net on a perforated porealaln plate, uolng auotlou. Saab filter and tr.nefer tbe filtrate book to tho banker la tbe aaao Benner ee when working with a aanple. Titrate tho ftltratea with atanderd K4MS aolutlon, ualag ferrla Iron Indicator. The ralua of SO *e of SgNOi aolutlon la tanna of HONS eolutloa la 'found by auhtraatlng the oo of XOSS aolutlon la titrating tbe 0.8 groa of M01 fraa tvlee tho uuaber of eo of KOMS aolutlon uaad la titrating the 0.1S grob of SoOl. HONS 051154 M* *o. 4 DIRECTIONS FOR TEST NO. 14-15-34 SUBJECT!. METHOD: Ifel* v*lu 1* ebeekad by titrating BO of igNO* aolutlon *44*4 to 400 eo of water an4 10 or pur* 80j( HMO* with KCMS volution. Tbio titration aboul4 agrea vary eloaoly (*1 0.1 oo) with the value found fro* the titration* of NaCl. The titration mat h* mada olovly to avol4 trainee* error. Sine* far* HeCl eontaln* BO.ttjC Cl fey theory, tb* value of the KONB la tera* or ehlorlae aay feo foun4 fey dividing tbe weight of ehlorlae In the NaCl taken fey the ea of IONS equivalent to the allvar nitrate required. E*aonlei Too 0.8 gran portion* of NaCl ahow IONS titration* of 13.11 ant 18.18 ae. Teo 0.1B gran portion* of NaCl ahov IONS titration* of 87.SB ant 87,84 oe. Tb* IONS equivalent to BO ee of dgNO. 1* than (87.86 * 87.84) -- 18.18 or 81.4 **. By tltretloa of BO oe of d^NO* agalaat IONS aolutlon, it 1* fount that 81.88 ae are required. Tfela *0-aa* vltbln .04 ee of the value obtained tram tb* NaCl titration*. The ehlorlae value of the IONS la then, .8086 x .8 divided fey 81.4 18.18 or .008770 gran* Cl per oe of IONS. 1b* ablorln* value nay alao b* ealeuletad fro* tha titration of 0.16 gran of NaCl. 0.6088 s .18 divided by 81.4 - 87.86 glvo* .003770 graoa Cl Bar oe of EONS. - J&iSi 1, 1b* fualoa material* bav* erploalva propartlaa If wrongly bandied; ooaaequantly ear* mat be taken to ua* aaf* proportion*, to aaeure a good mixture free of large lump*, and to properly aeat tha eover of the fualoa eup. Tb* fualoa mixture mat ha kept auay from eater or motet air, either of which may Ignite th* chore*. The fualoa mixture eheuld not fee ground to reduo* lump*. ' 8. Th* method aa daaerlked 1* not applleafel* to volatile organ!* oompouuda naleaa praaeutlon* ar* taken to avoid lo*a of annple during weighing. HOMS 052135 Fag* *0. * DIRECTIONS FOR TEST NO. 14-15-84 SUBJECTS, METHOD: I, Ob iMeut of the high ehlorlaa content of Mar of the Aroelort end the niU amount of inqtla taken, put eeoureoy ia required 1b weighing, treaafar, oat mixing of the oempl*. Tba pipette aa4 taratti for neeaurlag tba Blender* aolntloBa nuat bo vary alaaa to ovoid drelnege error*. 4. Faalaaa Bhlob aho blaok aarboa dapoaltaa oa tbs eovar and sl4a of tba fwaloa eup may or nay not give tba fall ablorlaa bobtent. If a aarboa 4apoolt la fanad, a aeoond faeloa ehould ba mode ualag a mailer aampla or radualng tba amount of anger la tba aharge or both. 5. Mixing the fualoa eberge by ahaklng after the aarew aap baa bean Irava 4oa any land to lneoaplete faaloBa. The mixing of tba aaapla with tba fualoa mixture abould bo dona la auah a vay tbnt tba aaapla la fully eoverad trlth tba alxturo. d. Tba teopernture at oblob tba ataadord oolutlona ora ataadardlsad abould ba aotad. la aaaa roam taaparaturaa vary from tblo taaporatura, appropriate volume oorraatlaaa abould bo auida. T. Tba fualoa mixture materiel* abould ba aaaantlally free of abloriao. The ablorlae aoatoat may ba datarmlaad by mnklag a bleak fuelon, that to, ottheut addltloa of eenpla, and titrating la the uaual aay. rive aa of *gMO* may be added lmatoad of SO aa. Tba EONS titration 1* than aamparad with titration* of 6 aa portion* of dgRO* oolutlon la Ilk* voloeo* of aolutloa and attrie oeld. are RONS 052156 '64 DIRECTIONS FOR TEST MO. 14-98-84 SUBJECT i Chloride* la Liquid Aroolore______ METHOD) Opalaaoano* of ttr txtraot with AgPO, Prootdur, Weigh bo graaa (. X gran) of mmpi* tato a 850 oo erlenoeyar ftMk. iM X00 00 of boiling hot we tor, etopper and thoroughly nbako for 8 to > Blanton. Oool In a watar bath. Dooant the voter leyer through a filter paper lato a 180 ao baaker. Ml 1 ao of BHO, and 8 oo of 0.1 M igRO, eolation. At the earn time oAA like aaouate of raogenta to aaob of throe 150 ao beokera containing (1) 100 oa of watar, (8) 100 oo of water 0.5 ao of atandarl .0868 M MaOl eolation and (8) 100 oo of water 1 eo of etandard MaCl eolation. Mix oontente of eeeh beaker bp atlrrlng. Pour invitee after Ixlng, ooapere the turbidity of the eeaple agalnat the turbldltlaa of the known eolntlona. A eaapla ehovlng turbidity lean than produoad by the 0.8 ao MaOl eolation (equivalent to .OOljC) ebould be reported aa .000. 8aai0.ee ehowtng turbldltlaa equal to or treater than the 0.5 00 MaOl eolation ebould be oettaeted ee eloeely eo poeelble from etandard MaCl eolutlona at D.B eo Interval*. 0.8 ao MaOl eolation 1.0 eo MeOl eolation 1.B ee MeOl eolation . * Bolutlona Required .001< Cl .Odtjl 01 .008j( 01 ate. Standard MaOl eolation, .0888 M, 1 ee .001 pi 01. Dleaolv* 1.84* graau pure dry MaOl In eufflalent water to aaaeure l liter. Stiver Mltrete eolation, 0.1 M (l.T). Dlaeolve IT gran* of dry Oliver nitrate la eufflalent water to naaoure 1 liter. 1 eo .01? ga. AgMO*. 1 ee la equivalent to .0055 ga. Cl or to 8.5 oo of the etandard .0888 M MaOl eolation. Motoe Doteminetlon of free oklorlde* 1* aeaally eonflnad to Aroolor 1854. The Method above 1* elaborated from ASTII Itothod D11T-91, Taatlng lleetrlaal Inaulatlng 011a, paragraph IS, Mineral Aetdo (ohlorldae and eolfataa). ere HONS 052157 DIRECTIONS FOR'TEST NO. 14-8X8 SUBJECT i METHOD i Four Folit of Aroalorc A8TM Wh-90 -- Cloud sad Pour Point \. The pour polat of e petroleum oil to the lowest temperature et hlib the Oil till four or flow when it la chilled without disturbance under definite prescribed conditions," The method of teat holoa folloae 101M directions mttlj except that observations ere made et Intervale of t*C laateal ot 1*1 aad reeulte ere reported on Centigrade eoele. A eketoh of the assembled apparatus la ettaobed. For details of apparatus aee ASTM D97-50. Bastte* Four the Aroalor Into the olean dry teat Jar to a height of t to t 1/4". laeert oork oarrrlag the teat thermometer and edjuat ao that the thermometer la la the oaater of the teat Jar and the begtaalng of the capillary la l/g" below the eurfeoe of the Aroclor. term without atlrrlng to a temperature of 4d*C la a bath at 48*0. Oool to >0*0 la an air or water bath. . Adjuat temperature of the ooollag bath oo that It la 8 to 14*C below the expected pour polat of the ArooXor aad maintain In thle range throughout the teet. Pleoe diOk (e) la bottom of Jaeket end laaert teat Jar (with the rlag gaaket, f, 1 lneh above the bottom) Into the Jaeket. Plak, gaaket end laalde of Jacket aunt be eleen end dry. Beginning at a temperature 10*0 before the axpaetod pour point, at aaeh teat thermometer reading which la oa even number, aerafully remove teet Jar aad tilt Juat enough to eeoerteta whether there la e movement of tba Aroalor la the teat Jar. The complete operation of removnl and replacement ahould not require more then S aeooade. If the aemple hea not eaeaed to flow whoa tte temperature baa reached g*0, place the teat Jar dlreotlr In a cooling bath of eultabla temperature. An noon aa the aemple la the teat Jar does not flow when the Jar la tilted, hold the teat Jar la a horlabntel position for exactly > seconds aa measured bp e atop watch. If oil shows movement, replace test Jar in ooollag medims end repeat teat at the next temperature t*C lower. Oontlaue testing la thle manner until a point le reeohad et which the sample abowe ao aovsmsnt whan the teet Jar la held borlnontelly for exactly 5 seoonde. Bote the thermometer reading at thle solid point. The pour polat la recorded ea the temperature gC above the solid polat. HONS 052158 figittl DIRECTIONS FOR TEST NO. *++y* SUBJECT:, METHOD: SsSa& Tba oaoling madluma utually aoaployad era ahowo kolav: Malarial Aptraa. Four Faint OoaXlac laita Loaar Unit far Madina teaalor IfttO *8*0 laa and fatar 10'C Araalar Uti 10*0 Xaa, fatar and Salt (Baci) - Araalor UM -*0 Cruabed laa aad aalt -1**C iraalar Utt HI0*0 Qaaoliaa aad aolld CO* -BB*C Cruahad loa and aalalua 0Florida aryatnla mtj ka caad far tamparaturaa doaa to HONS 0S21S9 directions' for test NO. SUBJECT! LoB* Of Aroolora I METHOD! * Hour* at 1BVC, IBTSt Toot Dft-30 BITIBPWI; too* o heating of oil na aanhaltlo erapound ism <*a*B*tlon Pdr-80. iPParatU* IwttM Pin! Fraaa 11*8trio Otob with rarolrlng (b to rpo) aluoiaw eh*If, liaor and teas* No. lttOS or aqulmlaBt. ftlHWwttn "iBTM Lool w Boot, IBB to 1T0*C", Th* thenooetar It loniii In front of rad lorol with tke rtTOlTlng *k*ir in sook * Manor tkot It M/ k* rood through tfc* dcmklo glee* window or tk* otob door. Botin* MahOW! OB. 0111 *tyl*, riot bOttOM, BOUlOOO OlataOBt box, daap pottorn, o* aodo ky Bnarleaa Cob Co, at Weigh w * rough koloao* okout BO gram* (_ 1 S*) of tho rail nixed ooapl late a aaauretoly torod boating Blab, lot otand until dlok and oontoata or* at rora twnparoturo, thoa weigh aaeurately. Plo# dtok lk os* of tk* rooooooa of tba rerolrlng ofcelf of th* otob whioh ka* kaoa brought to 1BS*C, than oloo* otob rad atart rotation of ahalf. Maintain *B OTOB toaparatura of 1*8*0 (388*F) for 8 hour* aftar tk* oampl# kaa kooa latrodueod and th* otob ha* again roaobad that toap aratura. Tbon ranor* aiuapla trim otob, oral and rooolgh. from loaa in might, oalaulat* th* loaa duo to TOlatlllaatlOB. s Notoa Barlag th* 8 hour kaa ting period the tmparature ohould aot wary or* tkah 1*0. ill taata showlag greater rarlatloa la toaperatur* should h* rajaatad. Ondar ordinary alrometanoa* a number of aaapla* h*Tlng about tho am dagr** of TOlatlllty any bo tooted at tha oaas tlaa. Saaplaa rarylng groatly 1b TOlatlllty ahould ka toatad oaparatoly. Whore oxtraaw eoewraoy 1* required aot aora thaa oa* a*ttrial ahould k* toatad at on* tlaa and duplloata waaplaa of It ahould ka plaoad alnultanaouely la the oran. All tost 1* oxaetly that daaorlkad under ISTV DB-BO which ahould ka ooBoultod for further detail* of apparatu*. The taat la dealgnad to *OT*r loaa la might axolualT* of water. If water la praaeBt, It ahould flrat ha raaorad by aultablo aathoda of dehydration kaforo proaoadlng with tho boat toot. HONS 052181 ora DIRECTIONS FOR TEST NO.__ SUBJECT; c*>r of *fOttloy 5*50___________________ METHOD: Uvlboad Color of 1;I Solution la Toluol lolgli (on trip balenoa or equivalent) 50 grama of tba Aroolor Into a tarad 50 beaker. Add about 5 eo olaar toluol, warm aad tlr until tba Aroolor la dlasolvad. Plena baakar eitb oontanta on balanaa and add toluol until the total oontant of tba baakar la 100 grams (50 grama Aroolor and 50 grama toluol). Fill a ona-lnob Lonrlbond Coll with tbla solution and obtain Lorlbond oolor readings in tbs usual wap. srs MOMS 052162 f9o DIRECTIONS FOR TEST SO, ____________ SUBJECT: of Kipenaloa of Aroolora METHOD: Oaleulatloa fret Bp, Or, Data OOimOMT OF EPAM8I0S IF AROCLCR3 Average oefflalent of expeaeloa between to given toapereturee to ealeuleteB tram epeolflo grevltlee ao Betenelnea >7 experiment at thaaa teaperaturea. H--riLa for Aroolar IBM twraaa Oaoffleleat of expaeelon over range from *8*C to BSC. Bp. Or. at BS/BS 1.6316 (Determined) Bp. Or. at BB/BB l.BOB* x (Oaleuleted from above) Bp. Or. at BB/tB > 1.S460 a f (Determined) Formula i VfJHB------------ OOOBB8 a/ae/*C Tka formula la derived from l/ - l/y , abteh gtvea the Vr (be - m) abeano la volone par wait volmae from 880 to 08*0, divided by the amber of degreee la tba temperature renge, It la apt atrlotiy ao oureta baoeuaa tba eoafflalaat probably abeagaa lth tba ebaaga la taaparetura bat aey be ooaalBaraB aa approximate arerase eoeffioleat for tba given raaga. MGNS 052163 ora DIRECTIONS FOR TEST HO._________________ _ SUBJECT t Determination tf freezing Point* METHOD: Tlw method* below are tboeo reeomaended br Reernh Dent. **!* Point of PI ohearl (revlaed method) bmt; to 100 pi. of Diphenyl *r* ple**a 1b 100 oo Oriffln beaker and heated uatll tbe entire mean to aaltoA. Tha liquid ta atlrraA oltb aa Anaobutn (0*-106*C) thermometer. A reading la takaa abaa tba flrat oryatala appear. It auper-ooollag takaa plaea the temperature will rlaa Imaedletely after the flret aryatala appear and beoome ooaataat elthla one minute. Thla ia the laltlal freezing polat of the eaaple of Diphenyl aad la ao reoorAeA. ' Freetlnn Point of Aroolor* For loe-freezlng material* auah aa Aroolor 1X19, the reosmtiended aathoA ta aa followa: Seventy oublo centimeter* of Aroolor 1X19 are plaoeA la a 100 eo riffle-type beekar. Thla beaker la placed la turn la a 180 oo beaker. Tba 100 oo beaker la aapportoA by lta flared rim oa the rla of the larger beaker and beaga looaely la the larger beaker. Tbe boated beakera ara ao* plaood la aa loo aludge. laltlal freaala* Polat. The Aroolor la atlrraA *lth aa Aaaobuta thermometer (aeale 10 to 68*0) The temperature la reed every alaute aad eeeda of both g-ehiorodlpfeenyl aad 4-ehlorodlphenyl are added every alaute aatll aryatala begin to fora la tbe liquid. Tbe temperature at blob aryatala ere flrat eaea to appear le noted. Oontlaue the atlrrlag aad temperature readlaga at one alaute Intervale uatll a thin Blurry la obtained. In oaee auporeoollag takaa plaea (aa it often do**), a temperature rla* Pill occur after oryatale have appeared. In thl* event, continue the birring and teapereture reading* until t*o or three ooneaoutlve reading* again aha* decreealng temperature*. The htgheat temperature attained after aryatala begin to appear la taken a* the "laltlal freenlag point". In eaee of no aupereoollng with reaultantlrlao la taaparature, the temperature at *hl*h aryatala flret appear le taken aa the "Initial freezing point". Holldlfloatlon Point. The 100 oo beekar la thea removed trm the larger beaker end placed directly In tbe le* nludge. Teapereture reeding* are continued until the Aroolor baoonaa too tblek to etlr or util the bulb of the thermometer la expoaed. The lent reliable tempera ture le recorded a* the eolldlfloetlon point. HONS 052164 P* > * DIRECTIONS FOR TEST NO. SUBJECT: Peteralnatlon of frln Points (post'd.) METHOD J________________________________________________ ftmlM Point. The freezing joint of the Aroelor le arbitrarily tokos ee the Hereto or too "Initial freezing point" end the "eolldtflee- ties polet". The 'liltlel freesing point" sal the "aolKlfloetloa point" should he reported along elth the "freenlng point". Oheik. da s cheek on the Initial freenlng point the keeker nap bo raaored ftam the lee sludge, earned la the bead, while the dreolor Is otlrred with the theraoaeter, until the tenperature la g* to 4*0. below the Initial freenlng point. The beeker Is thea wrapped la a towel end held la the bead. Stirring ie continued tutoll the erpatele la the Aroelor Just Balt. The tenperature at this point la recorded aa the final Belting point. If oarafullp determined, the final Belting point nerves ea a ebook on tba Initial freenlng point and Should not differ hr aura than a fo* tenths of e decree at Boat tram the Initial freenlng polat. . If the Belting point eheok Is Bede, the average of the final aeltlag polat sad Initial freenlng point la taken as the cheeked Initial freenlng pointi biu 1. If sarefullr serried out and If the Aroelor la frequently seeded with both P~ohiorodiphenyl and O-ohiorodlphenyl, the determination of laltlol freeelng point should not require cheeking hy the aeltlag pelat aethod. Roeerer, the Aroelor la very readily enper-oooled eo that nnlese greet oare la token. It asy he eoeled several degrees helon ltn Initial freeelng polat hofare nryetelllnetlon starts. The result la that when oryetalllnation does set in the tanpereture rises hut the aaxlaua tempera ture lo aot attained and ehaerved Initial freenlng point le therefore low. t. It Iw for this reason that the 100 00 hooker In Jeoketed with n larger beeker during the determination of the Initial freenlng point. The Jacket serves to alow up the rets ef cooling and lasuren a more aeeurnte determination than the aethod whore the 100 aa hacker It pleoed direotly la the lae-aludge for tbs doteralaetloa of lattlal freezing point. S. On nooonat of the abort exposed mercury eoluaa of the Anschutz thermometers, eerreetlons of observed temperatures for wergent stem ere not ordinarily required. Under uauel conditions of test, this eorreotlon la halos 0.1*0. If conditions of test are such that the otea eorreotlon lo lorgo, the appropriate correction should he nede sad recorded as eorreoted tanpereture. Seale eerractleoe, if any, should always he applied. 4. Za the deteralaetloa, the stirring should he eentlaueue end the temperature readings made at one minute Intervals throughout the toot. The ehsnge from the voter Jeokwt to the loo hath should be made quickly without Interruption of the one minute readings end the point of change to the lae hath should he indiestod on the time tcapereture curve. HONS 052165 194 DIRECTIONS FOR TEST NO. SUBJECT: Deteratlnstlon of Rental Insoluble In Soil* droolers METHOD.-,_____________________________ Prooedura Crush about 60 grama of reals. Vslgk out 1 groia lato a tared lag aa flask, aid S8 so of bantol and agitata tbe flaak with a similar motion for a fa* mlnut#a. Than add S6 as more of beanol, sashing down tbs aids of th* flaak. Alla* to stand for 1 hour. Praper* a fs Oooeb erualbls with an asbestos pad Is the usual saner and dry to sonataat eelgbt. Arrange tbs eruotbl* for filtration hy sustion. Miter the solution through the sruslkls, using alight notion. Das about 90 as of bensol totransfer the insoluble materiel left adhering to tbe aid** of tbe flask end to vasb any adhering film of rsaln from tbs aide* of tba eruelhl*. try the aruolbl* and flaak Is aa ores at 109-U0C, tool and *lgh. Add to tbe *elght of th* Insoluble Material In the aruelbla say Insoluble matter remaining la th* flask. Report Insoluble matter e* peroentnge of original weight of rsaln token. issst 1. The method dsasrlhad shore la th* one used by the H. n. Robertson Company. era HONS 052 ley DIRECTIONS FOR TEST NO.__ SUBJECTt Taporieetlon Dow at 66*0 METHOD! The tut biloi ! (bit given to un by tho H. H. Roborteon Company. They oall for tbo 100 hour low at 160*F (46*0), Prooedura Malt nligbtly Bora than 60 grane of Aroelor in a aultabla oontainor, Ibeing careful mot to ralae tbs taaparatura higher than naoaaaary to maka tbo raala fluid. Four Into a tarot ahaliou glaaa oontainor (100 ailli[neter Fotri 4tab), aool to roan taaparatura and aalgh. Boat for 100 boura (4 4aya, 4 houra) at 66*0, in a drying oven provided with a ranting outlet for eaeape of volatile Batter. Remove froa tbe oven, aool to room taaparatura and revelgb. Report loaa in weight aa pereentage of original weight. KtU 1. On aooount of tba aaall vaporination loaa at 66*C, tbe welgbte Buat be taken vary carefully. It ia vary important in obtaining thaaa aloaa weighta that tbe Aiah and oontenta be at etmoepberle temperature when tbe neigbte are taken. I. Robertoon'a flrat deaoription of thla teat nailed for tba determination of loaa after SO, 100, and 180 boura of drying. From thla dota, tbay draw up curve a abowlng loaa egalnat tlae. Tbelr latent pro cedure ealle only for the loaa on 100 boura drying. era MONS 052168 I f9t j DIPHKNTL IN CRU1>8 MPHKNTL OR phumtci. stux aoTTQMs 1 . Procedure . Trenefer 100 to BOO greme of the aemple to 850 co beaker. " fllgti bedker.ind oontante on s rough balance to neereet gram. Warn bankar util aontaota ara Hauls than pour-100 to ISO grams Into a BSD ec distilling flask'slth 10 iaah distilling eolumn attached. Jtswelgh bSBker and aontahta, thereby obtaining by difference the might of sample used. Plaoe a gOO*C or 400*C thermometer in the top of the 10 Inch dis tilling coluto la ouch a say that the top of the bulb Is even with the bottom pf the aide neok outlet. PI still off t.ha diphenyl and collect In a neighed reealelngefleak until the thermometer r.eede B7S*C. Weigh the reoelrlng fleek agnln and esloulata raaulta. ' % diphenyl at, diphenyl 100 ' wt. of aample - Pour the reel due la the fleek while still liquid Into a oeeeerole or pea kept for thle purpoee. Hinee with hentol and allow to dry. PPftU0 'The distilling fleak la a A50 eo flaek to wbleh e 10 lneh column with aide, outlet near top la attached. The ooltnn hat Indentations to ineresae surface area. Aaheatos paper ebould be wrapped around the eoltmn. , A Kaker burlier ie uaad la beating the .flask. Slnoa a high bolllag point uat be ranched, the tranalte board or Ira. gauge on whioh the flaak raata ebould bare a bole nearly aa large aa the diameter of the fleak. The fleam may also be applied directly to the flaek without the uae of any trenelte board or wire gauge. If naeeaaary, aebeetoe paper ebould be placed at the top of the fleak. g 100 oe distilling fleek makes e oonvpnlent reeelwer tor the dlatlllate. RON5 052169 era /9 7 Diawmio 00H8TAHT OF AR00LORE Portaltlona Aar nlaotrlosl oonduotor upon ahlsh an alaotrloul ahare* on ha atorad ta an alaotrleel oondanaar. Cenaoltmaa (Symbol a) Aa alaatriaal oondanaar aan ha ohnrgad with a aartaln ouantlty af atatla alaatrlalty, eapandtng upon lta abapa and alia. Tkla proparty la kaoaa aa Ha aapaaltaeaa, and tba farad la tba abaolnta unit uaad, far aoaraalaaaa tba farad 1a aubdltldad Into tba mloro-farad--aynbol al (Oraak 1attar a), and tha mioromlcrofarad--eymbol aaf. A farad la daflnad aa tba aapaaltaoaa af a aoodanaar anab that oca aonlonb af alaatriaal aaargy 1XX produaa a patantlal tiff, of 1 volt batman ita tarnlnnla. A nlara-farad la .000001 farad and a alaromlaro-farad la .000000000001 farad. Tha ataroalaro-farad la tba only unit nnployad la Aroalor work. Tha dlalaatrle aonatant of any notarial la dafload aa tba ratio af tba aapoalty af a oondanaar asda up with a dlalaatrle of tba notarial ta guaatton ta tba aapoalty of tha aama, hating air aa tha dlalaatrla. A fraao-tbanaa-olaaftrla otan, faraad air, aarlai Ho. eci-dl, la Vaad far boating and maintaining tha Aroolor at 100*0, tha taatlng tamparatpro. Bolaa ara drlllad through tha alda of tha orac to aaecmodate tha tarmlnal landa. ftteitert S&touu* Thlaaondanaar la a Oonaral Radio Froalalon Oondanaar, Typa M-L, Sarlal Ho. 1109. Xt bao a flea worm gaar tarnlar ableh panel t a tba Mttlng of tbla oondanaar to ba road to a fraetlon of a mloromtoro-farad. Tba oaala of tba atandard oondanaar la dltldad Into tBOO perta by tha tarnlar aaplayad, and aanapttng tba flrat thraa hundrad dltlalona and Xant ana hundrad dltlalnna, tha aapoalty ahangaa tary uniformly vith ahanga of oattlng. Xa othar aorda It la aXaoat a atralght lino oondanaar bataaan nattlnga of froai 900 to tdOO dltlalona. Balow aattlog of 900 and ohota ItOO tha lino la not atralght dua to odga offaat anoountarad la ngagXng or dlaaagaglng tba plataa. Tha oondanaar ahould tharafora ba natd bataaan BOO and 0400 naaXa dltlalona (XdO-XdBO mt). HONS 052170 '98 Th* oondanaar li eupplled with It* gallbretlon abort shoeing alaroolaro-ftred aqulwalaneo of asela dlwlelone at aaoh 100 divisions. Aran this short, iba eooompsnylng ebert la mala, showing the aapaeltaaea equivalent for aaab possible aaala setting (rig. #-). Thla aondenssr la a UMltlpleplete variable air eondansar. Two auab aondeneere ara nod* part of the apparataa. Oaa baa a eepeclty or ISO anf, (Oeneral Radio SSdrgi laolaatlta dleleotrle) and tba other a aapaolty of 100 naif., and aaeblaa lta obrloua raaga of uaarulaaaa. Tba oondenaar la aouatad (looally) la a rsoteagular aatnl aaaa, apaa at tba top, and should fit aa oauglp a* poaalble. The rotor-ahaft aaaaa through tba froat plate of tbo boa and a stuffing boa, poakad with llbeatoa twine. Tba purpoaa of thla boa la to ooatala tha liquid aaapla around tba plates of tbo aondaaaar wblab ahould, at tha tine or tooting, ba eoaplatsly aubmargad la tba liquid (Aroelor) lalapalag PanSamar, ca) Thla aaa ba any typo of air aandaaaar with an sffeotlva aapaalty of 1500 anf. A Oaaaral Radio Type 148-1 la ueed. A tbraa plate aldgat lr aondaaaar la uaad la parallel with thla ooadanaar for warnlar effeot, Capaalty ftrldsa A Oaaaral Radio Typo 118 la uaad. Thla la tba main part of tha apparatua and furnlebea tha srme wblob aake paaalbla the balanelng of tha ayataa. A reeletuaoe box la provided la oaaneetlen with tha bridge and aaa ba uaad la either ara. A. 0. floureo. 0. Tha aouroa of A.C. la a Qonerol Radio pure nine wata audio aaalllator, type *15-8, and la fad by a 8 volt atorage battery. Aaallflar Tha aapllfiar aoaalata of two atagaa or audlo-fraquaaey aapllflaatlaa, using two O.X. S01-A tubaa, two audio traaaforaara, and A, I, and 0 batterlaa. It la uaad for aoeaatuatlng the null point or bslenae paint, Bwltabaa. 8w 1, Far aanaoatlag 8 wait atorage battery to audio oeollletor. I. Por oannaettng 8 wait atorage battery and "8* battery to fllaaeat and plat* or amplifier tuba*. . bridge 8, y*r piesing realeteno* box la either A or B ar of oepeelty HONS 052171 \*e / MOMS 052172 riSST AKFUTXXS TUBT JKPUTUCR TOKK SKCOKD JKPLXJTKB SECOSD AKPU7IEB 50BR ABC 1/18/32 4.5 TOlt# cihcpit Assvunxuurr or two stags amtutxer . TOa OSS WITH CAPACITT BHUXZ MOWS 052173 20f &mi* Tbs two storage batteries UHJ *r* Torfl autoooMlw betterls*. fbt " bsttery la Shy oonvsnlsnt 45 volt blook. fattaw Cbanwr As A.O.-D.O, rsotlflsr, Wootlnghouow, otjrla 376703, la uasd far kwoplng tbw to storage battarlaa wbargsd. 32202 Tba oooompsaylng airing diagrams atll mek# tha hook-up alaar. rroosdurs for Msssursmsat faat Oondanaar Tba dlffsrsno* Is espeolty bataaan tba pistes apabad and alosad mat ba dataralnad with aa blgb dagraa of sooureoy aa possible. la tbta taat air la used aa tha dlalaotrlo median bataaan the plataa of tha eoudaaaar. This aonatnat *111 not obnnge apprsolsbly during tba Ufa of the eondeneer, but It la adrlaabla to dbaak it frost tine to time, Tha taat ooadonaar la plaood In tba ores (at 100*0) and allowed to eoaa to temperature. This takas about BO minutes. Tba taralaala are aonaaatad to tha lands from tbs apparatus by Mans of tba leaps provided. Tha plataa of tba oondanaar ora than turned to tba alosad (maximum aapaoltp) position, Tba rotor-shaft will anoountar a atop pag. Oar* mat bo taken not to turn tba oondanaar plataa too bard against this atop, aa It Bight ba bant, thus giving a falsa reading. Meat, tba standard sondanaar la sat at araatlp 400. Tba two awltobaa oarrplng tba powar supply from tbs battarlaa are now slowed, and tbo tuning fork on tba oaolllstor la prlskad gently with flngar nail to start It vibrating. Aa this la dona, a loud not* vlll ba board in the boad-phonsa. Hast, tbo balanalag oondanaar, Oa, la turned until a minimum noise level la produced. This sola* level is further radusod by saving tbs raalstanaa soatrols and mldgot oondanaar alsultanaoualy until tba vankeet signal In evident. Tba system la now nald to bo belwBoed, both with rwepeot to tbs oapaolty, and raalatsnao la oath era nf tba bridge. Tba reeding on tbo etandard eondonoor (400) In recorded. Bant, tba taat aondanaor la turned to lta minimum (open) poaltton, until tbo rotor-aheft la preeeod against tba atop. Row, without touohlng tba balancing eondeneer or mldgot oondanaar, tbs standard condenser Is tnrnsd toward * higher setting until another minima, nolo* level Is roeshsd. Tbo fins bslonoo Is obtslnsd this time by varying tha standard eondanatr and renleteaoe dooadaa slmultanaounly, When s balanea la reeohod tba randlag la roeordod from the standard eondeneer ee before. Only these two readings (400 and tba last) wra nosaaaary for computing the oapaolty of tbo dlfforonao In position of tbo platos of tha testing sondsnssr. Tbe HORS 052k74* .1 2o3l |kll|t la roalatanoa MMinr} Is limaeterlsl. Tha aaeond raedlng alll It found to > about ISO ttrlalona htghar for the ISO aaf aondantar and Bloat 00 dlrialona higher for tka 100 nf eonSacoar. fko aatlra akor* prooadura la repeated, ualng tka oacood randlag for tka aaxt taltlol aattlng, ato. until tka rang* from 400 toBOO taala dlrialona la oorarad. laok pair of reading* la tkan tranalated late aatf a* town andar ealaulatloaa'', aad tka amallar auktraotad from tka larger to oktala tka ftpaaltaaaa dlfferanee for minimus aad maximum oattlnra of taat oonflapaar itlBB air a* thadlalaatrio medium. The dlffaranoaa thua found art erargad to (Ira tka aorraot aonatant for tho ranga oorarad. Tka Aroolor la poured Into tka aondonaar until It Juat oorarad tka plataa. Tha aondonaar la than plread la tba oran and allowed to ra ntIn thara too houra lafora anting tba taat, ao that It will oom# to 100'C, tka tooting temperature, Sxaotly tha aana prooadura la uaad a# la da tar si alag tba aondantar aonatant, azaapt that only tao determination* ara taka* a* akaak* kaaauaa tba Initial kalanoa rill k* aaporatad from tb* final kalaata ky 11 or*r btir tha uaaful aaalo aa tb* ataadnrd aondantar. If tb* flrat Initial ratting 1* 400, tka aazt Initial ratting ahould be aasaabar* near 000, ar parkapa #00, depending, of oouraa, an tb* aatur* of tka oukatonoo undar anamination. 41*0, tka original aattlng tan ka tho high ona profited the taat aaaganaar 1* at It* sintwin (open) aattlng. Iran number* glran abort ar* for oxasplo purpotaa and go not k*ro to bo uoot, but are mora oonranlant for oelaulotlont. MlWWilHH Ikon oondantora or* oonnaatod In parallol, tb* following formula Obtain*i <1 (total taptoltf) (tl a ) *um of naob In thin satkoi tba total oapaalty eon*late of Co Ox 0*. Stao* 0* otaf* oonotont, and 0* nan be found. Ox ean alno b* found by oubtroatlag tb* Initial 0* from tb* final Oa, 1th tba Initial and final aoel* raadtng at hand It la only aaaaaaary ta aonnult the abart to oktala tha oqulralant anf| tba amallar In auktraotad froai tka largtr to obtain tba dlfferano* In nmif. IMa glfferanoa, whan taken with the liquid in tb* eondenstr 1* dlrldad by tb* tanntant far taatlne oondanear (dlff. with air tn the tondaaaar) ta oktala tha ratio roforrod to In tha definition of 0.0., 1,0,, tka tlalaotrl* aonatant of tka material In quontlon. HONS 052173 2.03 fiauu Tlnel Ponding lattUI NffWIMI Conetent for tooting toadeneer B50 Therefore, D,C, 1076 4.SI b5o gli B194 400 mt (from ohort) 1194 BIS 1076 >Ct8 1. About TOO ee of eeaple ere neoteeery Tor toot. B. A hydrometer It provided for tenting the etorege bettorloo from time to time. 8. The bottorloo thou)4 bt dieoonneoted from the root of tbt ott wbtB oberglng. Jellure to do thlo *111 eoueo e fuot to bio* out. 4. Tor D.C. aoesurtmont the temple any bo betted to 100*C on t hot plete end then poured Into tbe eondeneer without eny loee In tooureoy. 6. A tover le provided for tbe eppnrttue end ohould be kept In pleot whenever the epperetue le sot In uee. 9. If there le eny "oneoklng" Bound In tho rtoelvtre the tubet ebould be tented by e reliable Redlo ehop. All eonneotlone end oonteete thould be kept et fret et poetlble from dirt end gretee. HONS 052176 FJf.. 5 KgpiVAUMOK OF !>OAU RJ-ADIHO IN MMF. FOR STANDARD ....xudms__________________________________ HUB' Iwt . --Jhl. -.. i --. To ffM flW tlM 400 * 899 HONS 052177 HONS 0521J9 MONS 052180 I POWBt FACTOR Chen oonOeneere ore uaod on A.C. circuit* there 1* as eaargy locc In the dleleetrio, Thl* lota arlatt through the reposted oyole of IkiDIH of olaotrlo flux through whloh th dloloetrlo It tekan by applied alternating yoltage. Tbit lott luoraeata oltb tho froquonoyj henoe, the frequency he a to be reported with the reault. It alno verlea with the taaparotura of tho oondenoor, and bODta thia alao aniat ha reported ra part of the reault, Tho "Power Paotor" la the ratio of oil anargy loeeee la a 41oloatrio to tho "opparoat power" la the dioleotrio. It la uauaily exjreaood la poroentaga, la the teat to bo deesrlbod the ataodard taaiporaturo uaod la 100*C, aad the atandard frequency la 1000 eyelet par aoeoad, Henoe, It la lot aeeoaaary to laeludo thoaa habitual eoaatnnta la reporting roaulte. ftiwor factor Determination laaaaueh aa tho eeme equipment la uaod for aaaeuring power footer aa dioleotrio eonetaat, the method will ba outlined, making rofaraaeo to that rethod. Inara tun The apparatua la the eeme aa that uaed la dlalaatrle eonetaat aaatureiwnt exoapt for the taatlag toll, A drawing of the eall la etteohed (figure ) It ooaalata of I eylIndore of the dlmaaalona ahown and la contained la an 600 oe Orlffla Beaker, la tha eccanty the booker eontaialag the eall la plaead la the oran la the neat ploeo aa tha dielectric eoietoat eoadeaoar, and la connected to the eaiae loada. Due to tha fact that tho toat la affootad appreciably by amall aawnatc of atray earroata, tk* 600 oe beaker la Ineuleted from tho Iron floor by maaaa of a gleet *1" atilt, upon Which It atnada, and tha laaor oleetrodo la auapended from a ring eland by manna of a gleet etlrrlng rod, peaoed through e oork, aid "hooked" ot tha bottom. Tha wire loop patting through tho wertleil rod of tho laaor electrode la hung on thla glaaa hook. mthcd of maaauromont HONS 052181 To neoeure the Power factor of aa Arcelor, tha teat oall la filled about two thlrde full of tha liquid, and the loodo oonuootod, oa la dioleotrio oouatont noaouromont. The ataodard eoodeaoer la oot on obout 1600 toelo reading and tha eystem brought to balooeo oo dlrooted la tha dklactrla oonatant procedure. Tho Co reading and alto the realetaaoo fooling ore notod. Tho oaa of the loada la dlaoonnoetad outaIda tha ewon, ere being taken to more the two ends oo little oo pooolblo from their lonnootod poeltton, end tbo oyotom again brought to balonoo by manipulating the otendarl oonlttuicf' e*4 realitcnee deoedee, The now rpadingw i e4 ft} are noted, 2.09 surn.wm Dm aquatloa for !/ obtataad bjr our laatruaanta lot r.t. 0a, - Oo to BaalatanOa raadlng aorraapondlag to 0o. *X * Milataaaa raadlng oorrtapondlag to Ooj. Ca,> Largaat raadlac (la aof) oa iti. ooBdaaaor, Oa * *allaat raadlac (la amt) oa atd. aoadanaar. f Droottoaor la ayolaa par aaaond. laaaala Obi * 1*00 aaala raadlng 935.0 oaf. Oa, * 1881 aoala raadlac 1184.9 Mf. Aj o 180 ohaa (raadlac aa daaadoa) Aa > 108 ahaa (raadlac oa daoadaa) r . tiiM - .it* .Kxm 11*4.8 - *88 .tt.juWaMo, * |gjw ,uV.juiM (allda rula) (1) Tha laaor olootrodo ahould to auapaadad ao aaarlp oa poaalbla la tbo aaatar of tba outar alaotroda. (I) If fc -- >i la aatativa, tha aaaaa tkot tha pooar tutor la aa low that It la withla tba lowar Halt of aasauronaat (.MjC) of tha apparatoa. la thla aaaa it la ra portad aa 0. (8) Tha aaw ganaral aotaa uadar dlalaotrta aoaataat alao apply to powor faatotp. mons 052182 f'ACi'op CULL rte. 4 i i > % i : a V HONS 052183 f*OWMK frtCrvK CC6U' SVtCAfJl tltr**. 14**0 T/t#<Xs 04/0C/ f~ HONS 052184 fpffp OMMIQAI- OOHPMI |y>PMTI01 py*HTMgg Hi JUT HONS 052185 -213 kbiamm or aroclorb ' Healatanoe (ormbol ). Obetruetion to alestrig now. The ratio Of roltege (I) to ourront (I) In a eonduetor or eloaed olrault. (R > t/j, Ohm'a Loo). The praotloal unit or roalotonoo la tha ohm. gloOtrleel Roelotlrltloa. The ourront nhloh floaa between two aonduotora lamileted fren oaoh other by a dlelootrlo to made up of two ooerponanta (1) that whloh flown through tha dlolootrlo ltaalf nd (g) that Whlth flowo through a ourfaoo film of mol aturn or ethar oamloonduatlng materiel (oil. duat, or foreign matter). Thoao oomponenta ara deelenated reopeotlrely oa "roltaae reolotlrlty" and on "aurfaoa roalatlvlty". Toluwa Boalotlrltr. Symbol p (Oraak latter "rho".) Alao aallad apoairio raalatanoo. Defined aa tha raalataaoo between two oppoalte faoaa Of a unit ouba of the aubetenoe. p where 1 la oroao-aeotlonel area and L la length of tho ourront path through tha aubatanoo. The jraetlorl unit of roalatltlty la tha ohm-oentlaetar (ohm-en.). Tha raalatlrlty of Aroolora la reported In multiplea of 10* olmr-om. A wolumo raalatlrlty of T3t k 10* oha>-am la equlrolent to aaylng that tha roalatanoe offered by the aubatanoo botwaaa two oppoeed parallel faooa of 1 aq. am. oaoh, pleood 1 aa apart la T3 % 10* ohma. Tollowlng tha yraotloo of the Oeneral Kleotrlo Company, roalatltlty la aeaeured with tbo aubatnnoo under toot (Aroolor) at 100*C. "Baalatlrlty" aa applied to Aroalora elwoye rafora to woluae roalatlTlty, Burfooo roalatltlty (ayabol 6, Oroak latter "81*aa") la defined aa tha raalatanoo between two oppoalte edgee of o aquara aurfaoa film. Tbo praotloal unit la tbo ohawem (between oppoalte odgaa of a film 1 am. aquaro) Jtb/l Where R la roalatonoo of a roe tangle of film of length 1 and breadth b. Meneuromente of aurfooe raalatlrlty ora applied to aoltd di aledtrloe rather than to llqpld. Tor moat meterlala the aurfaee raalatlrlty la much loner than tha relume raalatlrlty, Atmeapherle humidity oondltlona at tine of meaaurlag may frequently greatly alter tha aurfaoa raalatlrlty. era MONS 032186 3VHWWT or Rjwiatjyrrt gp AROCioia amp liquid dikmotirob - fiMlU-W t Method Uelng Otnaral Radio Typo &4V-A Megohm Meter Tli* megohm meter 1* eaeantlallp calibrated bridge with weouum tube toll ncter the hull Indicator, A blueprint le attached ehowlng the lreult dltgrea end the brief taatruetlen* furnlehed by the manufacturer for the operation of the megohai aeter, Heeletlvltjr 1* obtained bp aatahlag tk* woltege ooroa* the I* reeletor (aea blueprint) with that eoroee the A reel*tor. The raelateno* la megohm* la raed directly froe tha dial controlllag the'log arlthmotleally tapered rhaoetat B. Thla reading in aagohae ilwldod by 0.TD8 gift* th* opaolfla raolatena* in ohaa n lotyau. as, Tha acaeuramant* ara aad* with th* dlalaotrle under teat at 100*0. Tha apparatua la aultabl* In tha rang* 10,000 ohao-10,000 magohwy'ou. on. About on* pint tf aaapla la required. Apperatu* pettarlaa: Two 48 wolt Radio 8 Battarlaa, aerie* eonnaotad ar* aaad. Two 1,8 wolt dry aella, eerie* eonnaated. The battarlaa ahould ba taatad from tine to tin* bp naan* of a poakat woltmatar for radio battarlaa and thoa* battarlaa abowlng weak oalla (nor* than a few wolta below rating) ahould b* raplaoad. Bettaria* ar* uaad for a aouroe of woltog* to obtain tha daalrad ataadlnaaa aino* otharwlae the normal leakage surrant through th* dlelaotrlo would be naakad bp tha larger aurranta flowing Into and out of the taat leotrodaa with aaoh pulaatlon or Irregularity of tb* woltega. Teat Terminal* or Ilectrodeai Braaa nlokal-platad cylinder* aad* according to drawing Mo. M-1569865, moan ara* 101 *q. on., opasad .*84 am. apart, Ooplaa of thla drawing ar* attached. Than* tarminala ahould be raplatad *a raaulrad to maintain an awan aurfeoa fini ah. The alaatrod* aonatent (Araa/Langtb) for thaaa tarminala la TOE. So* "Calibration* of Ilactrodca" for darlwatlon of thla oonatant. Thaaa taat terminal* map alao b* puroheaad from th* Oanaral Uaatrle Oampanp. Th* olaotrodaa ar* planed on 8" diameter pyrex gleae plete ratting on tb* bottom Of a BOO Ml pyrex beaker to aomplat* th* aleotrod* aaaanblp, Th* apllndara ar* fully laaaaraad in tb* liquid dlelaotrlo under taat. Beating Oram A free* tharmo-alaotrlo oxen, foroed air, BO to 180*0, alt* IB" ( IB", aerial Ho, 6*1--41 la uaad for boating the Aroalor and taat aleotrod** to 100*0 at which temperature th* rcalatlritp 1* aeacured. Two holaa ara cut through the beok of th* owan through Wblob th* flexible wire* to tb* aleotrod** ar* Introduced, Olaaa tubing 1* uacd at th* hole* where th* inaulatad wire* eon* through. Inalda th* owan, th* wire* ar* aorared with poroelaln baada. The and* of the wire* ar* Joined to aoraw clip* te whlob th* wire* from th* taat aleotrod** may b* Joined when ready for maaauraoenta. . HONS 052167 Zt99*Mrt far Rcclatlvlty Hcccurcmcnt gjrtparttlop of KlaaVrodctl Before uae, tb* electrode*, gleac plctc, end beaker suit be vary aarafully el*n*d and dried, Clear flrat with nail bruah and benaena to ramora prime. Waah with hot dlatllled water, try ana waah 1b carbon tetreohlorlde aa<! try at 100*0 for at leaet ooa hour, for Bleeping after wet 1b Aroelor, aah with bestene to remove ell Aroolor. Then waah thorou|*ly with oleen eerbon-tetreehlorlde end Ary at 100*C for at leant IB mlButea. Do sot touoh with the ringere any aurfcoaa of the eleetroAee, flan plate, or baakar (whlah are to oona In eontaot with the liquid to ba teeteA) after the laat caching. ' filling of Elcatrodca: Beat the temple to ba teataA to 100*0 B*0, an a hot plate. Four tba eubetenee to ba teataA (Aroolor) Into the tried alaotroAa aaaambly until the liquid entirely oovera tba eyllBArtoal aurfaaea of the eleotrode with l/B to l/tn azoaaa. Cara muat ba uaed to make aura that the lip of the eontalner, fro* whleh the liquid la poured, la eleon. Tilt the baakar 1b auoh Banner that all air bubblee 1b the Aroolor will rlaa to the aurfaoa, Plaoa tha baakar (containing tho eleotrodee and Aroolor) In tho forced draft oran whloh la maintained at 100*0 *_ S*. llaaauraoMBta are Bade after about IS alnutee heating. Baadtnai Tha attaohad page glraa tha method for Baking tba readlnga with tha Oenerel Radio Type B4d--A Magohn Hater. Botea 1. Tha electrode* are centered ea aloaaly aa can be judged with tha ope. Kora exact cantering la not naoaaaary alnoa tha average apace between aurfaaea renatne aonatant. After centering, aara nuat ba taken that tha elaatroda poeltlon 1* not further dleturbed by jarring or by vibration from oven motor, I. noalatlvitlee of Aroolora era uaually maaaurod at the temperature Of 100*0 epeolfied by tha Oanaral Sleatrlo Company for tooting Aroolor ltS4. Tha uaual affect of temperature on realatlvlty la that If tha dleleotrlo oontalna molatura, tha appllaatloa of boat will reduce tha aolatura content and elnultaneouely lBOraaaa tba raalatlvlty. Is the oaaa of a thoroughly dry Alalaatrto, however, iBOreeec of temperature uaually bee tba raveraa affect. Prolangad heating of a dleltetrlo, if in exeeee or aafa or ooneer- vetlvo working temperature, la lnjurloua and tand* to bratan tba breakdown Of th# materiel by docompoaltlon or obeailaal obnnga. The Oanaral Electric Company apaalfiad that Aroolor ItSd after beating at 100*C for 9t hour* ahcll abow no laaa la raalatlvlty, B. Tha raalatlvlty af Arooloro 1* lowered by tha praaanea of polar lapurltlea auoh aa farrla chloride or bydroohlorls cold. Thaaa polar lerpurltlce affect tha raalatlvlty to a greater extant In the more liquid Aroalcra than In tha vlaooua Aroolor* (Rcfcrcneci B. B. Olcac). ,,0HS l. 4. The raalatlwlty or * Alaloatrla with aurranta lo waually loot than with ooatlnuoua ourronta, and daoraaaaa programItaly aa a rula with Inaraaaa la fraijuonoy, owing to dlalaetplo anargjr loaaea. g, 4)10 aaauroroent of realatlvlty by tha abovo aathod about 1 plat (470 *1) of aaapla la raqutrad. 4a Dupllaata >aaauramanta on ona aanpla abould ahaak within about S0^ ara HQNS 052189 ztr Itaferanaai Plalaatrla souse Maurorm or run<m dikuctoxcb Standard Band-book for Slaatrloal KSelaaaro, Oouraajr) Kloatrlaal Ooadaaaara. IgaUtlTltT I, Ota-,,. Paraffin IMatd Quarts (ordinary tanp.) Hit*, Madras or Baacal Mloa, Ooaada Olass (ordinary taaparatura) Bulbar Bakallta Oaglasad Poroolala (ordinary taaparatura) Msrbla IIQ0IDS 1 to lOOOO k 1018 0.1 to 10000 s 1018 10 to ISO z loX* 0.44 to U z 101* 10 to 10000 s 101* 100 z 10000 z 101* 0.8 to 5 z 101* 100 to 1000 s 101* 0.1 to 10 z 10* frsaaforaar OU i Iksaafonaar OU B Prttta Astral (karoooao) Osator OU *grl Aloobol Uaaaaft OU OllnOU hW, Platlllod *aalor U84 (100*0, BOO 7.) 490 Z 10* MOO z 10* 470000 z 10* 80000 z 10* 8.8 z 10 80 z 10* 1000 Z 10* TO k 10* 100 to 800 z 10* MOMS 052X90 29 tnimlilVwn it Us* prmt tlo* all produota art dram off lato ataal Imi for atorago prior to forthar proooaalag or ahlpamt. Thl* otthod Of harilin 1* Tory anaatlafaotory bacaua* of th* largo mount of (MM roloaaad, tsltu Za gmaral all ralma oa th* chlarla* or HOI llaaa arc lahrlaatad Haroo-dordatrm plug cock* with aoroood ooanaotioa* aad ndr** a Us* Uqwld Ub*i aro all lroa clip typo gate ralma. ill aqulpamt la tho ehloriaator atop la atool or iron. Tbo bottoa half of tho ohlorlnatora la laggod with t of Mp oagaoala. tho blowing taak aad aoltlag taak for aatorlala going lato iroolara #11M aad list ra lamlatod la tho aaao way. tho yip* llaoa froa tho too aoltlag taak* aad th* llaaa to th* blowing took aro atoaa Jaokotod* tho folloalag drawlaga of th* proamt chlorinating oqulpomt iioagsy thl* raporti Layout of Ohlorlnatora Magraaoatlo Layout of Chlorinating lqulpomt #0-dtS6 #0-ddU Th* following ralato* to th* waggoatad now plant aad It* oparatlm. th* proamt ohlorlnatora work wary aatlafactorlly. It 1* mggootad that tha praamt thraa ohlorlnatora ho wad In th* mm plant, aalta* th* roqalrmmta or* wary largo, aad It oas dacldad that a fan largor wait* oara prafarrod to a largor anb*r of unit* af tha proamt ala*. MENS 051995 Xt would bo Tory dtsirable to prorido oaoh ohlorlnator dtb It* Indlrldwal trap, Saab would swabla oaoh ohlorlnator to operate ooatlnuoualy a* Ita allottad Wowpowada. Tbo production of iroolars A169 aad 116S wold null tbo aawe aa at prosatt bat tbo production of tbo otbor Aroelors owuld bo twlco aa groat aa It ia at tha praaaat tlaa. Tbo SCI froa aach trap would than pa** to a oomob trap bafara paaalag to tha BC1 absorbing spstan, Tbaso traps aro of aa laprosad doalga aad aro arraagad to drain bp graHtp to a eatob tank or to tbo dlphsayl waasurlag tank, Tbo HOI fran oaoh trap than paaaaa to a Oonaaa trap bofera paaalng to tha HC1 absorbing apstoB. Tbaao traps art of aa teproowd daslga and arraagad to drain bp graoltp to a catch tank or to tha dlphaapl waamrlag tanka. Two dlpbawpl aoaaurlag tanka aro provldad and tha prosaat waiting tank for UN and 1160 It rooonaowdad as a oatob tank, this lnvolTta tbs Installation of sa additional pwap. Tbs prosaat tank la satisfactory for oao. If a now tank wart to ba lastallad a bnapod bottcn would baMocanwadad, Xt la aaawaod that gassouu oblorlna would bo available at St. Louis and tha vaporiser la onlttad. tha naa of a trap for oaoh ohlorlnator alapllflas tho piping to tho HC1 abocrbor. Tho HC1 goa obtalnod oontalaa a anall want of organic natter whloh ahould bo rswsrsd far tha prodnetlon of tha highest quality Ml. totet Item Products aro expected to bo atorod la tanka or bias In tho plaoa of draws aa at prosaat. This Involves tho Installation of aw additional pwap for tha blowing tank. MOMS 051996 3/ jurn eroo-lordatraa lubricated floe oooka will be used on all rapor llaea and all Iran (at* ralTae on liquid llnaa aa bafora. All tanka and trupa ahould ba lagged with t* of tBf aagnaala, Tba batten half of Via obiorInntore ahould ho la(fed aa bafora with I* of lif aagnaala, Tha plpa linaa to and fNa tha diphenyl aaltlnf tanka, tha catch taak. and tha plpa linaa froa tha ohlorlnatora to the hlovlni taak will ba ataaa jacketed. Buggeatad layout of Ohlorlnatora for at. Louie Bo-1404. S& HONS 05199? mm mi nmrm mma 32 The HI absorbing equlpnont 1 essentially the meual lUri sllloa absorbers in ofaloh ths B01 gas 1* diseolTed in nWr End lbs tait'UHfipttM. lbs Installation Is designed principally s a Mans af Aqodni of tbs HOI tfiioh la forasd In tbs sblsrlnstlon although, of oourss, tbs hydrochloric sold la sold Awrsr possible. Tbs HOI |ts Isa-ring tbs final trap sf tbs ohlorlnatlon equips**! la tarrlsd bp n > Iron pips 11ns to a bwrlsontsl 16* 0.0. * 40* atssl Arm shioh asrrss to asttls sat sons sf tbs or(*alo aattsr and solid lapurltlsa. lbs gas than passss throats s I* stssl pips to tbs bottao of a Tsrtlsal atool ooolsr and Altar 04* 0.0. a <7* blb mieh Is flUsd vltb oaks. A rlssr sf Ats lengths sf 6* bsll and spigot torra-ssita pips, approximately 10 A. high oarrlss tbs gas to tbs fused slllsa absiWOsrO. Tbs sonnsotlon bstssan tbs tarra-sotta pips and absorbsrs la Bads Ip tso langtbs of 7* 0.0. ball and spigot, sllloa pips faming a trap tlib drain Aloh loads to tbs pyrin ooolsr. Tbs H01 gas passss In sarlss tbrongb 15 sllloa sbsorbars rrsaged ona so top sf aach otfasr. At tbs top sbsorbsr aster Is aidad shleb floss oosatsr-currsntly to tbo gas sad is finally dlschargad as tydroohlorie sold fron tbs sllloa pips ooaasetlag tbs abeorbors with tbs tarra-cotta rlssr. Tbs hydrochloric sold floss through a ooolsr SOStl(tine of - 1* Pyrox tubas satsr Jacketed for 4 A. saeb arranged la sarlaa and la discharged Into a snail brick lined oatob tank or ben. Tbs pooled aeid than floss by rubber lined pips and Tairas to a robber lined steal tank sf 10,000 gallon oapeslly. Tbs gasaa lssTlag tbs tap sf tbs oilloa absorbsrs la oarrlsd by 0* tarra-ostta pips to tbs bass of a dressing tossr 18 A. high, oonetruoted of tarra-sotta ball and apiiot aaotlana 04* 0.0. the framing toaar la Ailed with ooke and la ssppllsd with satsr shleb trerflowe at tbs botten to a drainage ditch. A Duriron fan is loostsd at the tap of tbs framing tossr to pall ths gasss through the H01 abtorblag aystm tt sasss to bo praotlsblly lnposslbls to keep this sqnlpnmt H|bt sltb the result that bydrasblorls said of serious strsngtbs la apUlad star tbs tarloua piseas of sqalpnsnt. To protest ths stssl mppartlag struoturs and ths stssl squlpotnt, It Is coTarad by a hsasy asst of tar. Ibis aeons ta work rsry soil. HONS 051998 Yh* tydrochlorto add made It ;Un 1a color ami oontalaa ip-T1 aaeoai of organic Batter. Baaploe of this add hare already tWI rat to Benaeato Leboratorlee la St. ball far oxaaiaatlan. It l anderetood that It la planned to ooahlaa the BC1 from the ehloriaatlco of diphenyl oltb HC1 derlred from operatloae already eyentlas In 6t. Louie. Aooordlngly no plaaa hare keen Bade of BOl aboorMoc eqdpnaot far the It. Ionia location. St dll probably bo aooosaary to laotall acne typo of flltertaf epporatM to ram the argaalo laporlttoa In the BC1 before abaarptlan. A flM ooko peohlag elll probably oerre thla prrpoae. MOWS 051999 H0TB3 OK AHOOLOR DIsmUTIOB taPIFIBHT yor> ABQCLOBs to. inu. iaa. itid.iSdo. 1888. 1868. 4466. MM Tha fttlnlu not** ralata to the praaaut plant. Tho PMnt for tho dlttlllatlon of nil distilled Aroolora oxoopt 1868 and 1868 oonalato of a tbouus, pipo-otlll tppa, apparatus without a fractionating ooloan. rot Aotallod daacrlptlon tha following divisions olll bo uaadt Hafar to Drawing fo-6898. 1. Molting Tank 8. Xottlo 5. (Julnby Pnap 4. tlastar 6. Itu Trap 6 Oondanaar 7. Raoalvar 8. Blending Tanka 6. FI1tar Prana 10a Aotd Sarnbhara 11a Vaouuu Puapa 18a Hot Aroolor Circulating Sjrataa 19a Vllaon-Maualan Tapalog 14. Mlaoallanaoua . Tha salting or charging tank la or ataal S' alaaotor bp 8' 4aap with a l'l" aona bottos and holda 17B gallona, Tha tank la baatod bp a atnpla ring gaa bursar on the cona bottos. It la filled fron druna lifted Into poaltlon by a abaln hoiat, and la Hoctorgad through a 8 !/" (*t* Taira and pipe Into a funnal eontalalng a 40 saah atralsar. Tha tank In lagged with 8" of laglo-Plober Oaaant Mo. 66 and la fitted alth a tight ataal aorar eeaoeotod tlth an exhaust fas to provost anoapa of flaaaa Into tha la lettlo Tha kattla la a apllndrlaal steal tank 86" la Alasatar bp 8' high, sat TsrUaallp, alth rounded top and bottos, alth a distillation aherge capacity of approxlsatalp 17S gallona. The lead of tbla tank has ooaaeetloas for tha oharglag pipe, vapor, drain fron foas trap and superheated 11 ;uld fron tha heater, Iba abarglng pips la 1 1/8" ataal pipa Jacketed to allow circulation of hot Aroolor 1148. Oloao to tho kottla lo a 1 l/t" karoo Kordatros lubrloacad plug eoak. MONS 052000 Jf Th* npw pip* ! 4* and 1* eoasaetod by a flaapa MMNttfll to til* aoaal wtil pip* laadtop to toa foa trap. tha drato froa toa foaa trap 1* a oa* laoh pip* toadtop tonaph to* boad to vltbto ca* toab *f to* bottoa of to* MU*. Th* 11a* oarsrytop ouparfcaatad liquid froa to* haator **U la t* atoal pip* )>ek*M for hot Iroolar, Am 1* vat pip* oloaad by Paroo-Pordatna nln on to* (Id* *f to* 1*111* a**d for ebtr|li|i Ihto 1* a fetoby lo. P iaok*t*d aorM pap alto a oapaclty af t( pallaaa / atoat* drlvaa at 1P00 MX by T-balt drlva fna 1*!. fetor. th* pop la rad by a t 1/** Jaekatod pip* 11m (to to* tottaa af to* kattla. 1 *t**l (*t* wl l* loo*tad In toil 11a* slow to to* tottl*. th* paap diaobarpM thra^i t 1/** Jadntoi at**l pip* hl*h 1* r*du*d to 1* J%m\ War* It t*n to* baattop Mil> thli *M*l*to *f li*li*al oail *f 1* ito*l pip* I* dluator (to pip* MUr) MitHl| lb taiMt *aoh tom apprortitoly 1* (to to* afar, th* Mil i* pl*o*d to * qyltodr&Ml J*ok*t Md 1* b**tod bp ferfM* tabwtto, too rU|, to* pr***wr*, Mltipl* ]tt p* b*r**r dMki par hoar sapaelto, th* *oil 1* jataal to to* pipM lwdtop to Md frM th* k*ttl* *p pr*aad Jotot mloaa, it a abort diatom* tb*** to* aalaa, !/ pip* alppl* 1* mld*d to th* pip* Milt th* alppl* to clM*d bp a d*m o*aa*ator aad pint* thl 1* Md to oto Mt to* hMttac ooil bp raaovtep to* piac *ad alloatop to to am Mt to* liquid m it raahM tot* to* mouW aqulpaaat. a 1* to*rt*d to th* Ito* dlrwtty b*for* It atm tbi* la a dov&M aada *f 14 ra aanal mtal. It la 1m*Ud m to* top *f to* kattl* aad to rpo**d to to* vapor lto* bitoiai to* kattl* aai aoadaaaar. htmallp it to *pltodrto*l to top* IP* to tttta *ai to blph. th* tour Mr* 1* *l*o *f aoaal Mtol to to itomtor aad tto hl0i bavtop a **ld*d omr aad a ***U*p*i lavar top* *p*Vmld*d to to* ba** *f to* oatar abaUt it to* oaatar *f tb* b*ttaa *f to* f*m trap torn to 1* plpa laadtop to tototo 1* *f to* bottoa of to* kattla. Tb* vapor lto* eoaa**ttop to* f*aa trap to to* k*tll* vapor flaapa 1* *f 14 pup* aoeal a*tal 4* O.k, hi aatora to* f*M trap toapmtlaUy fair laohaa fre* toa bottoat HONS 052001 the ratar? notion that laparted to tha vapor tends to asperate the dark oolored entrained liquid ahioh flam under tha lunar oora, through tha ana Inch plpa back to tha kettle* Bio vapor pnaooa froo tbo loan trap through O.D, flangod aonal plpa ohtoh la oannaatad to tha oondanaor by too *0*flangod alia. dll flangoa of tha foan trap OBsanUy art ooldad to tha plpa. Bila la a It ft. lagth of I l/l* aanal plpa nutloaod by i Jaokot of 4" otoal plpa. 1 rodaelng flauga oeaneeti with tha flaafad alia at tha lnlot. It lnollnaa at approxlaataly 46 to dlaoharga Into tha alfht cyllndor looatod an top of tha receiver. Tha light oyllndar la of Pyrax glnaa 1 l/f O.C. * T* X.S. a T* long aot In too grooved atool flangoa with rranoh typo Ooetie laad-aaboatoo gaakato. f. laaalvar Thla la a ataal tank 10* la dlanatar by 56* doop. Ita oalll, botton nd oarer aro llnad with aonal natal, 1 ana laeh galvanised plpa lino laada froo tha botton of thla Toaaal to tbo klaadlag tanka. 1 dona of alfht laeh ataal plpa 4 l/t ft. Htfi la voided late tha top of tha reoeivar* thla dm la 11aad throughout with aonal natal, tha tap af tha dona haa a t* aippla aaldad la Otloh oaunacta through a oroaa to tha vtount puap line* aaroury gauge and oonpreaaed air aupply. tha dona la for tha purpaaa of coaling tha roper la*ring tha rooalrar and radaolag tha atopyaga of tha raeuaa llaa by aubllaata. twa galvaalaad Iran tanka 60* dlanatar by 46" deep are aaad far Handing, tha produet la traaefarred fran tbo racHvar to tha blaadlag tanka by oaopraaaad air. tha Handing tanka are aqulppad ulth * Lightning* agltatora for nlzlag. this la a It laeh bras* plate and fraaa Sporty praaa. Filter cloth backed up by Whntnaa la. 1 filter paper la uaed to tract all liquid droclera. tha praaa la haatad by fear alectrio trip-heatere, tvo an aaeh aids, droolar la feroad through tha praaa by an Obardorfar lo, T braes harrlng-hana, gear pomp. MONS 051002 I 3r M laid flarebbtrj taring dlatlUatlon a mJX UKXBt of hydrochloric acid la fornad by dnooupoaltlon, nhloh aut bo acrabbed oat to prevent damage to the raeaae paf> f* aorubbere atool Tt* hi|h by (4* diaaotor fillad with ooke aoakod with tOf oaaaUo aoda aolatioa ara placed botaoao tho eyetan and tha racoon poop. Theae aro arranged ao Out they ay bo oaod alternately, to permit cleaning without Interruption to diatillatloa. loroally tha eyetan ia oadianatod ty a Bheelar three atage Tubejot Taonaa Poop. 1 Darina notor drlraa reciprocating racmaa puap la alto laatallad for aarrlee rhanoror oar anall boilar ia that doaa. U. lit irwlar fil,rnaleUng Irif' Aroolor U4| ia oaod to boat rarlooa potato of tha ayatao. Thla la haatad by *aa ia a tank 14s dlaaetor by C4a doap and circulated by a t/i Anerlcan March CaatrlfUgal Poop, Hot iroelor la aappliad aa aoadod to tho falloalag pointai (a) faeketed Uaaa ftta kattla to Qoinby pap and tna ooil to kottlo Pocketed charging kettle S Wily pap jidwt Suiaby poop pnoklag (land Jacket Thia hot oil oiroalatiog oqalpMat rith lta open hoatar la of a type rilloh ahoold not bo installed ia a aoa plant. Thla ia a air point reoording pyranetar. Too pointa lath ara oaod at tho Inlet and outlet to tha ooll, one in tha foaat-trep aad one la tha reoelver, *Vaby fyoda* (tbarnooouplaa) aro aaod with thla lnatrunant. Ui Brnnuwi Oootao Bo. * gaakota node of eopper and aeboatoa are oaod an all of tha flanged Jolnte of thla apparataa. MOMS 0S2003 33 The discharge part of the Qulatp punp ie connected te * tee ehloh la turn oonnecti to the 4*8**** ** pipe leading te the heating eoil and aleo to a f Iron plug-ooofc dhlah serves te drain oft ittU battens or reildae. The preaaut practioe la te MNMtiti approxlaatalp BW lbe. of still botteae and th te aetatala thla aaowt bjr periodically drawing oft the oalowlatod (OcnaalaUan over thla valee, It la tron*ly reooansaded that a grew-off be looated te the aide of tha kettle eneh that BOO lbs. of atill bottoaa etll be autoeatloallp maintained la the kettle. froooaad Float It eould be possible te nova the preaaet vaousn UatUllef equipseat te lt louls aed operate It, as at present, producing bath 'liquid* aed 'solid* Arodere with a oapeolty of approxlaatalp S,000 lbs. per dap. If, however, there la the prospect of ae teoreaaad dauad for distilled Aroelora, thee It is suggested that the pressat ettU be lastailed at St. louts, equipped as aboa* te Drawtef le. Bo-1400 for the production of 'solid' Aroolors, and a aew still be lastalled with a ainlnea oapeolty of 10,000 lbs. a dap of the 'liquid1 Aroolors, as shorn le Drawlat lo. 6o-*405. It Is warp dealrabls to keep the 'solid* aed 'liquid* iraelara asperate throughout their aaaafaeture. A snail antnat of osataaleatiaa of the 'liquid* Aroolors bp 'solid* Aroolors will sarieuslp iapair the quality. This la partioularlp true whae the fV-fllvM-it aatawial is orpstalllae. Whaa the ease still is used far both solid <asd liquid aatarlale It Must be cleaned very oarefullp das ~p*--p ewer free aee product to the other. This eleaaiag eporatiae ie tiae oonsuulag aed area with tha greatest of aare eeeaslanal oaataaiaatioa will ooour. eaiae !.]. etati (Drawing le. 8o-t*0e) arJuUrn JHt The snip ahaeges suggested to perult the use of the presuat still for 'selid* Aroolors slang area the Installation of a Fartte-dreear hattar, or equal, with punp, wto., for tha hot Aroelor 1141 to bo trsulatod le tho pump Jacket, pipe Jaokota, ealtleg taek, aed sndaeear Jacket. Thla rsplaoaa tbs erwda outfit le usa at tha praaaetl leprowaeaet of tha ealtleg taek bp tha ess of hot Aroelor boa ting colls la tha plaao of gas sag a naohanleal ulxeart battar design of gorwbber far raeoeal of Ml frsa tha gaaaa galeg to tho Teener puepi addition of a 10,000 lbs. blending tank for 'solid* Aroolors aloes. MOhS 052004 39 Tha danlfa of thla (till la abow la Draolag #Se~tdOE. Thla lruil| ahova tba ganaral layout aad principle featuroa. lo detaila af thla atill ban beaa prepared. The eeaeatial ohaa|ea propoaad for thla atlll aa oaaporad to tha proaaat layout arai ! Tha om of a 40,MO lb. atort(a task feeding tha aeaewrlag tank aad atill, roplaatag tha proaaat meatiafaotory hnadllag of aatorlala la draaa, t. Tha wo of a atoaa hoatod <"Hy ottrrod aaaaurlag taak raplaolag tha proaaat gaa hoatod watlrrad taak. It Tha uoo of an lataraal foaa trap la tha atill kottlo. 4. A B/too faekooa Thap raplaolag tha Soraar Typo felaby I# A aora oaapaet aad bottar deaigaed osedaaaar. I. A bottar deaigaed raoalTar paralttlac dlaehargo by a poap rathar thaa ooatpreaaed air. T. A bottar deaigaed aad aora ottYealeatly looatod Icrabbor for 401. C. Too 10,000 galloa bleudlag tanka aaad aolaly for . lltjuld* Arodora. 0 Skprovod Taatllatlag ayrtak JSftl tv-- HONS 052005 laosL ACTUM 40 Areolar lo, UN la the prodaet dlattlled fron chlorinated diphenyl with ohlorlae oontant of at?. A brlaf hl*tory of than apanttcu mold poteUf bo to ardor* The firat dlatlllatlcaa ooro aad* 1* --all atool pot* flrod by |tli A aattafaotorp product oaa aad*, tat ther* m anoh daoonpoaltion olth loo yield. To laprov* tbi yield, o oast oooatroetod a mlt eaulrtlmg of a ooat iron pot vlth tillok aidoa aad botton. The laalde of thla pot oaa cooplately aaohlned ao that tha heavy pin type agitator ovoid aooap althla l/l* of the wtlro Interior aorfaco. firing one dona with go*. Thla orraaganont lnoroaaed tha jrlaU tat carbon Wldlag ap and adhering to the ahell ovoid vary often atop thaagltator* Thla atill oaa aeon abandoned la faror of the praeaat type of dletUlatlon oqalpnant ahloh (are higher reooTerlea olth creator aaao of oporatlon. Tha praaent atUl eoaalata of a atool pot olth a lanadar on the lnaldo of the ahall. Thor* la a drain fire* thla lanadar to tho flekor (feaeorly to tha qomohla* tank)* The pet ha* a renewable oerar olth a vent. The firing la by g Tha mggoetod plane for a non plant aa ahona an our OraoUf #8c-t407 propot** a tank* lagged and heated by olroulatad hot all or ono of tho iroelora* for rocalvine tha batch fron tha ohlorloator*. tatorlal trim thla tank ooold bo fad to a flakart fron ahloh m alarmtor oonld oloaato to aa overhead b&a. Tho above draotag dm a bin of. 80,000 lba. oapadty tat thla oaa b* varied aooordlag to operating ahhadal*. ' Tba fUkod natorlal ooold flow to tho etlll pot, rnhlah real* aa a platfora ooalo and fron mhleh tho enact oelght for a oharg* 1* dotoMUod* Id a alallar mgr, lino 1* added either fron o tag or alallar devie*. Aa alternate nay of charging tho otUla eould b* to rm In aaltae credo fron the hooted (torag* tank. 01ao* the ehlorlnator* raquir* 40 boor* to prodao* 7,800 - 0,000 lba* of ornd* and tha *tlll* have about tho tana capacity, ton* of tho oroia ooold b* atorad hot for oboat 40 booro. Credo 11St oad 1180 bold olltfitly abam tha netting point dooenpoaa to aaea ntait, Whether thl* aaenat of daocnpofitlcn ooold bo approolabl* or not la not kaom. HONS 052006 4/ i CmwiIm of tho liquid onto ehlortoatod notarial Into lltkn flat(hod product or flaked oolld font a* rapid!/ aa possible loans Via aoat advantageous procedure. Iftor a ohlorlaator batch la juapiil Uto the storage teak the flaker would be atarted. la rapid!/ aa stills booaao available ooltoa notarial would bo na Into then natU all liquid orudo waa oxhauatod. Btllla would than bo charged with naked Mtorlal. The atllla filled with a batch arc elorated aad eoova/ed to a (teal setting UUod proforabl/ with Insulating rofractorlaa. these Insulating refractories arc especial!/ adapted to such batch operations because ef their lew eapaelt/ far heat, firing aa/ be tp aa/ fuel, uae that whleh is cheapest aad aoat oonraalant. The notarial dlatllla out aad is naked an a chill Mi Area ohlah it paaaea to an dewater and eworhead pecking bln. In these operational off grade product cones off at both the atart Md at the end ef a batch rat. Zt la aactuary to dlwert this off grade notarial Area the chill dteal. for this purpoae we uae e anall vwssd with speut. thle dawlea deneote the off grade product end (reranta it reaching the toll! abed. it the and ef the run, the pot with ode, line, ato., le lifted Area the catting ad ranered to an area afaara it eaa be MMt olMfttdt ill aanatruetlen aaat ba tight o that a ilntan ef duat aantaeta tha operatora. Tha roen houalng thla equipment ahould be wall ratilated both beeeuae the etllle ere hot aad aa aa extra safeguard against. duet. Operators la oaataet with aueh duat na/ develop e aewero fora ef donoatltls. Theae eperatiena aa abova deserihed are far Aron Ided. Tha bateh requlrea aleae patching to prerat off-grade products atklag with the good predaot at tha first and last wf each dlstlllstUa. Thle splitting la antlrd/ dependant an tha operator, hla oare aad wlaual observations. iaothor factor eoaplleatlag eperatlono le the enddon doooapooltlaa ttot poemra at the and ef the dlatUlatlen. The gar evolvvd ----tot largo anoints of sold forming vapors aad alee eoae ef the tototoar IMP ae at external/ fine!/ divided dust ehleh le dlaoelered ant decided!/ eeld, Ukrti aade to collect thla duat aad rework it hove not been euoceeaful. Our operations at proaant are to discharge thses dsoanpeaitien produota through an arheuater and late the ataosphere. Such a procedure ta e aere populowe eapnaaltp nl/kt areata a aulaaaoe. HOMS 0S2067 4Z A batter aatbod ta daiirod far olMaine the ooke and Uaa rooldaa aat of tha pat*. At tba praaant tlaa tba laua( tightly, adhering mi la chipped out with Wi or dlaledged by pounding m Dio pal* tha atlll pota aoala aad dlatart aa a remit of tba ml <ar aad ara battarad by tba cleaning aparttlaa. lat(li| tba roeldae baa baa* triad bat did aot faollltata tbalr rwwil. Paoaat dlatillatlaa baa bate oonaldarad bit oartala aaapllettleaa praaaat thaaaalwea. lha olaaalng af aaob a naaa atlll aaald ba a aarlooa problm, far If dlatlllatloa aara oaxrlad aaly to tba palat ahara tha raaldua would roa oat, tba recovery aaald ba la*. Tha aatarlal nKUm readily tad op air laakaga maid fildAgr eauaa a atoppaga bp tha adUiaad aatarlal. Then too tba bald palat la wary oloaa to tba boiling point andar radnood Bata oa waoaaa dlatlllatlaa aa dant by tba laboratory ara aa fallown- laid PaUt af Batch #1M Ohargo llald SM 0 Mi 0 BaaldBa U0 total BlatlUntlaa TUo : I4l0 * MB <B = It *las. or It (^ala Aotnal IwOu Corraotad for lat graa (appro*,) lftth m m MS 1 ut Id0c til tM HI tM tTB 148.1*0 et.r tsi.l 187.1 tM.t m.t ala. T.i 7.8 7,8 7,i 7.8 Paoaapoiad at aad, eaalag owar dark. Sharp rlao frae Mi ta C7V*0 with llttla oealag awar. Oar layout, aa ahoaa aa Drawing So-EAOT aakoa ao prowlalaa far altbar gaaoral vwatU.tlo* of tha dopartaxot or for tba eaUaetloo ad fhrthar praoaailag of tba product dlaobargod fraa tha atlll at tho aad of tba ran. per gaaoral roaa vaatllatiaa ww Mild aaggaat dlao ar prtptllar faaa. Por tba coilactio* af tba flaw daata, doeoapoaltlaa yrodaata, ata., wa aaald raoaaaaad hooda, daot-wurh, aolloator, oto,, aaaaootad ta aa aknit faa. HONS 052008 45 (ha oholsa of a oollaetor for tblo. aarvieo to Hfftwlt aaa. Tha aatorlal la acid and tha {laam of partlolaa appraaah that of foe partlclaa. Wool aloth la qaloUbr dagtropad. To oa It aaasa 11*alp that tha aaoooaafnl oollaotor 111 ha a aerab towar, tha Mtavftal oaajbt la thla tooor oooia that to raaadcad to laprora tha plaid* M>/Jfw*t HONS 052009 44 Drawing i Ugrnt It pin of tha abort plaata la Am aa This layout thorn a building 00 ft* add* by 000 ft* ll alth loading piatfoma aad ollniyi oa tha alda. Tha building Anil bo Of firn-pnof oaoatruatlao alth tha aartoua oolta aoperated bp flra walla. Thara aqr bo approrad doera U theta flra mUi bat batter arraagenant mU bo to bare tha flra walla without doora bat alth aoeaaa to the eerloua rooaa through doora loading fran the aide piatfoma and wolkwap. Tha handling of bataano vapor at high taapernturar ad la aquipnant find otth ge, tha dletUlation of converted graduate bp dlreot flra and tha atoraga of thoao prodoota olgbt aaaa to oautltuto a dooldod flra and eocploalau haaord. Thaaa ganger! art aver proetet bat tha euulpaaat la ao designed aad aparatlaaa are ao arranged that than haa naaar boat aa explosion and oolp a foa nail flroa In old oqulpnnt Allah haa' alnoa bean nplaood* Pvwahtbe paat too poan.aad with equlpaant aa laetallad, than haa amr baon o fin or aacploalaa* The layout aa Am m Drawing #8c-t40t la arrangad to kaap tha fallowing In alad* naawlp* (1) The bausaue food tanka, tdilah hold ooaeldaaroble beaiaot, would bo In on laoletod building, whan If a fin did oeour, tha d- niigo would ho at a alilon and oo damage ooold oeoar to the precasting oquipaant. The aala atoraga of booaol would bo looatod at a aafa dlatanoa fna the feed taoka or alaa wader grwmd and oo protected that daanga would not oeoor If o flra took place la tbo faad tank houaa* (t) Tha oeovertar wnlta an ahaun in ana and of tha building and la auoh a nap that antra malta oaa ba inatallad la aa additional bap of tha balldlng aad tharabp rwadllp adalt af ftore mpaaalaa. Capacity of an# nalt la >|M Iba. diphayl par dap. HONS 051010 4f (8) The Xaatruaant and Control Soon and the Mphaayl ad High Boiler 8torag# are adjacent to tb oouverter unite, tad the epuca allotted la tha cantor of the building should ba aaplt m for future and largo production* (4) The chlorine,tore aro shoe* in a rather large rooa la Alch considerable other chlorinating oqalpaant eoold ba laatallad at a future tine. Iqalpaeut ahoaa dotted oould aanbla tba production to ba doubled. Should the oquipamt ahoeu dotted ba Installed with twloo the oopaolt/ of tba preaast oqulpawt, than tha ohlorlaatlag oapaolt/ could ba three tlaaa that of the preeant oblorinctara, each lth It? ou separate trap, (for capacity aaa Schedule under ahlorlnstera) If a production, graotac than that of throe tlaaa throe ahlorInn tore with aeparate traps aaa be forenoon, than nore building space ahould be allotted to the ohlorlnatora. A OhiAl whaal la shone la tha ohlorlnator rooa. Ihle would flake either diphauyl frou the atoroga tanka or olao oavtala of tha ehlorlaeted diphenyls from the ohlorlnatora, for either (tiler requiresante or future proeoaalag. (t) lb# dletlllatlan equip*ant for the various Iroolowe are thorn la too building aeotlcuo and sdjaomt to the ohlorlnatere. The apaoe allotted would provide for a production of ISO,900 lba. Aroclor #1M, 100,000 lba. Uquld Aroolora and 90,000 of aoUd . Areclora, othor than ltdO, par nonth. Zf largaw produetloua aro now faraaaan, than groator apoca Aould bo allotted. Future expansion oould aloe ba attained ky inatolling aqulpnant la the (rehouse Saotlcu, and than building oddltlanal Warehouse apaea an tha and. (6) Tha BC1 abaorbera and atoroga for Marlatlo laid aro ahoan outeido of the building and(ppoalto of tha ohlorlnatora. Other locatlana would bo equally aa good and It night alao ho deelrablo to pipe tha BC1 gaa to existing abaorptlow aqulpnant. (7) 1* have kept In alad, atralght lino production with n natarlala awtorlag awe and of the building and being ptrooaaaed In a Una and finally arriving In the Warehouse, SMIUit We have bean advlned that thla aqulpnant will probably bo icetilled In an existing building ahan dlnanaiana are unknown to ua. Thla study la tharafora aubnlttod In tha hop* that It night bo of aalatanoa la laying out thla oqulpnaut la /our preeant building. n/lv V*v HCNS 051011 HONS 052012 ffpxaauat-i BOTB OX D1PHMTL AMD DI7HXHTL DWIYATITEi FLAXTB OPBU1TOI, iS IT MBIBTOX BY j. l. wnmvm r. x. izujiXB 'opbutixo mpjRTMHT) Tto Draolaxa Rafarrad to la Thla Sootloa ayai nwnnr O-MU -- Dlytoayl nut -- Dtagrauatla now Shaat of Fraaaat nut aussumBuux OHM -- Macraaoatla Layout of Oklarlnatlat IfliaHt mmmwK Xo Brawtaga MOOMB MO. IBM 0-Mlt - Layout of 1M0 flut HM - Layut of Badgar stlU HONS 052013 47 urancnu or Hma it ruction at sun cannon oovm run tainot, mui Hftaql 1* folyaarlaatlw produet of llmol reealtlaa M the beatlaf af laaael tifor to t*nportura* wad NW< {(> (mU 1* aooeafealad by tho Ubaratlea of ooo solo of lydrogw for oooh aolo of Mphaoyl yrodsood aooerdlac to tho folloolag rwotlwl o o ** OO Mphaayl produotloa lo oloo eeoeafealod by fbrthor folyaarlaatlw prodaate wd aom doooafooltlw yieldlag ortho, Mto ood parailpheaylbwawa, tetraphaayl, tor* aad oarbw. Tbo jdold of Mfhwfl wd forowt of ooavaralw to hither felyaera la a diroet fwotloa of twporetara. tha waofbotare of Dlphwyl M practiced at tbo tv*na Chmloal float la Jaaiatoa la abow dlacraaatieally by drarU* >o. Min attaabad, by aotaal photo*rayhJ of tha afalpawt wd la doaBribed aa folloaai Iwaal la tho aaly tw aatorlal required for tho prodaotlw of Mphwyl bat It la oaawtlal that a faro baaaol ho lead, fhla aatorlal la beaght aador tha ataadard ayoolfloatlwa of tbo harrott Owfiay far Xadaatrial faro faaaol to ddob baa bow addad tha foUevia* apeolfloatiw for Foealag Folat. tha freeala* polat aoat aot ba balao 4.dC, toot to bo aada la aooordwoo alth tho aathod of >. . ttaal oaf.* tha ftawta* folat foolfloatlaa baa bow foaad to bo tha aoat valuable toot la dotaralalag tho fuality of Iwaal i faat nfrlaiM baa abow that layarltloa la Iho Baaaol toad to doaroaao tho yield of dlphwyl, laoroaoo tha perowt^e of higher falyaora wd loaor bolUa* alia. HONS 052014 Thaaa laparltlaa tin shoo la tha naoltlag Uplwgrl wl mm (Mill la tbi Iroelwi tubaaquMtip aada teas It. Xt U iIn ftroafl/ oaapMtod that danaatltla Bong the opartton la oaaaad tjr laparltlaa la tha hansel. Inal la raoalTad la task aara. Zt la slaailal with a #HB iaatM pasp asd pooped ttm|k a 1|* llaa ta 10.000 (alias atona task looatad ikon |wwl, no fW tros tho dlphasyl halldLp. Ala task la aqaippsd with ataas Mila ta prerast fraaalM la sold weather. Hms required (aruatka tasaal la pMpedfros thla storage tank with a lj* flJdag pap throagh a ateas-Jaokated, lagged, 1|* Hat to asa at fear TB0 (alias fast lw~fl--"'***' __ Ieasel la papal from asa af tha foad tasks aslac IaatM U asp (hiah (lwaa a llaa prMaara of OS - 00#. (krapk a !/* #Utt (ehatta loartlag kotasatar. Tha flow la wplatad to IK (ills^aar through a haad aparttod l/d" nil*. Iho llaa man aftor laarlag tho oaotrol valve la 00# gdaga. It* llqald hansel la than lad throagh a oaata haat vaporising aall, laaatad la aa aaxllUr? ataok to tho dlphaspl .salt, asd asargaa IMS thla Mil at a iaaparatara of 1U - 1W0. asd a proaaura af n# goag*< It 1* that lad to tha #1 prahMtar pot, ahloh la a load hath pat hMtad prlaatpallp hjr tho oaato gus fW tha ft prahMtar pot asd tha oaswartar pat, huhhlad throagh tha laad asd aihaaatod oat tho tap. Tha usd tasparataro la bald at 400 4M0C asd tha salt aopar laaraa tha pot at U0 - *T8C asd a praaawra of H#. Tha vapar la thas lad to a aaoosd prohMtdhg pat rath la alsllar to tho first mpt that thla la a find pot asd la aaaratai m m to salatata a laad tasparataro of fWfi - TM0. Tha salt vapor loan* thla pot at a tasparatan of U - M00 asd a proaaoro of Id#. Ip ta asd Isolating thla aeoaad yrahMtlag pot than la pnetloallp * oooranlao to dlphen/1. Thla la panooolp avoided hooasM past sapor! son haa ahoas that asp llphapyt. fanaad prior to tho loot or aasrartar pot tasdad to fats higher polyseTM Md oarhas abas pat throagh tha oosoartar rt, 49 tftar liwln tho nm< ynkMtw the nftn ara frt UfM|k Wii flml load Mk pot m11i4 tha ooovortar. U flrod pat aad tha load toMaraturo la Mlatalaod at X>0. Tha It kmt Iwtm tha oNNrttr at TU - TIOOO and t mum *f #. fiw dm aatlaoad twd tmpiiaturaa aro oorroet aad ara takm Mk TUaaa --1 fpada throagh Imparttaro milt tmariad la tha load bath* lka vapor taa*orataraa ara alao aoimrod iltk *Uam> mil nda tat ara alx ralotlvo la that tha toaporotcuro aalla ara loottad la tha dlaahaaga plpaa aboot It* atm tha tap* at tha pata aad tha taaparatara aa aaaanrad la lafltaaaoad tgr radlatlaa, talma af goa floo, ata. Aftar laarlag tha ooarartar pot tha taparV paaa throogh a trap ahara aar load lawyawr ar oarboa la droppad oat and thaaoa to tha fraaklnmtlag aalma. dt tha top af thla aolma tophi ogaator la aparatad la aaah a amir aa ta ratara dll af tha dlphoapl, high bolUag mtarlal aad part af tha mooaaartad boaaol book ta tha talma fraa ahlah it la dlaohargad at tha bottm throagh a ataaa>]acfeatad 11m to aaa af thraa TdO galloo bom toaka. tha taoparttaro at tha top of tha oolam la aalatolaad at T to KdO tp aaatral of tho atollag oatar flaw throagh tha daphlagmtor. dftor aaparatlaa of tha dlphaopl, high bolllag mtarlal aad part f tha baaaal, tha raaalalag momrartad haanol vapor aad hpdrogaa la paaaad throagh too aaadmaaro oharo aabatmtlau/ all of tha baaaal la iwdaaiad. Thla la rotamad to tha food taki aad . rtmaad* Tha Ipdrogaa aataratad olth boaaal Tapar paaaaa oat af tha laat aaadaaaar ta a malar, ta throagh lata altazaato ahmbora of a Plttabug toatradryar Coapoay, aotlvatad almlaa atlaarbar. lara tho boaaal la aMaoihad, tha hpdrogto paaood aa throagh aad oaotad HONS 032016 50 fun amzau. vmm Hjhmji ft Aroolor ft*U41 l*rt, DaralojMat ftaildlaf right. hMptnhtnyl ft imlw WUb( ilrldad lato thraa taction* ftp fir# till*. Ooorartr wit and ehlorlaatora la lift taction, Crude ripbeajrl aeliaetlen and dlatUlatlc* oaotar tactics, frMtwt atorage la right Motion. MOMS 052017 if rbnm, mourn mU low* ootUlM hi Hi !n(n fnr drlreo tjr | U, 4, 8. oxpletioe proof Motor. (blooding rot# 1,(00 gollo##. (or boor, fabpod throogh too laeh 11om< MOMS 052018 A? hsiol matron n* an l* jus Mto taf. Mfllar ! f*d tot molt toot fVt ij MOMS 052019 53 MMOb itouoi ,MO U<* (writ to* HwUr. 18* 8 MOM M. HONS 052020 *4 unoi romoi laid' ** ink ood for hudllof bwool to wit food toako. Too wprldht plpoo ooao u w aatl-ayphoo dorloo. MOWS 052021 roM. TOSt) UU I . Tao liUa & * WOaUaa rtfM miM art wwVy ***** k**1 uSim fro. bwiol atm and *ai Uaaa OOoneoUd io Uotrogr/ar abaorbara. Mgbanjft mli faad rm i* ** * r flrat faa* tank Jwat laalda gata. HONS 052022 S6 WHMfc NMD NMlag tram loft to rlht. wLlt^T15T JR** r*>r4 lt JJ5*,f'*** Mowo IUm halw toMittut MtnUn, Owtor Brow oolot fotoatloaotor. r*oHf rtUl o4 ehlorlaotor t*poroturoi. Bight J"** *l*Ml ^ MV witch i fhntto Kowrtlac Miol flow itUf Bight VthliM Tonti ft Motor rofUtori tMMi | 7urH* u*~* MOMS 052023 I Dxnona kit ItM m tok ()* la fontrows! aiod talp u i br-P* tortUg topping ad, Obi la Mtwral Haw:la* ooll tei bwiol mor'liir, "frod` ai'tii if mnooliltlM lwrt wit through thl* tok. fpor Ihw thl* Nil lad mUet ewtir pot hloh 1* #1 pnboitir. H*1**' *> to lift pot ihlob la #K prihMtor ind the to right pot ahlih 1 tho ooarirtor. th* ippinto* (hom la thi foriground 1* uporlaaetal iad 1* bot port of thi dlphagrl wit. HONS 032024 KHflta nzt top riot ohofllaf #X prohootor orator, ft prohootor loti, Bad oonvortor right. trtroai right thomt load trip. Boat plpo oat top it ttU trop (ldiu|U lato bottoa rt froctloaatlat li. tho m Lboh Uaoo ohora oomlng trom tho toy* of ooh pot oad aoalfoUod lato tho horisontal 1$* Liao aro roloooo llaoo aad art wad for otnallolaf pot prooouroo Bhoa ohottlai do aalt. Iota MLdod oovoro oo #1 prohootor and Load trapo. HONS 052021 59 wiura. wtr IMUmUn mIw it lift. V^kUiMter < iwdmwi m Upw fUtfin. HONS 052026 60 tman wit ' : . Brtmo ridfct Won top of fr*oUootl oolno. *4*t oootor Woo* (nUifwWi Caodmeod produot ritam to ooXmb. (oft enter ood estme loft ibon beetol oondeaetro. Oondonood produet returned to food took*. Vpper pipe oeooeetloei oro ooollag outer. HONS 052027 6/ tamms) umbu mmo** uk*,b HONS 052028 ___ ____ i toh Bailor ioporttlaa Th* mmUot of th* Banaol. Plphaoyl, Blgh Bollor alrtur* collected la tho auap tonka la don* in throo atop* sail* thro* till*, rial iwuLCUll IUi atill oonaiat* of a borlaontol tank h*at*d by tubular atow ohoat ualng atoau at 110 - US# gag* proaauro. fhi* tank la oranootod to a fractionating oolcan oqulppod with a ooll typo dophlo(aator and a tubular eondoaaor. Th* produot oollootod la th* aiaap tanka la puapod to thl* atill vary eight hour* through a If* Oould oantrlfugal puap and th* atill bollod down one* la oaoh *4 houra. Th* bonaol which la dlatlllwd out la return*d to tho dlphanyl wit food tanka and rouaod. Th* roaldu* r**alnlng la th* atill eonalatlng of > - lot Banaol, Plphanyl and llfh Bollor 1* tbaa duwad Into th* Dlphiyl atlU. Wniti atm Thla atill ooaalata of a ortleal tank, a fractionating ooluaa paokod with lj* Br*g*at Bplrala and a laekotod pip* typo oondanaer. Th* tank la aqulppad with a aubaargod typ* Kua**y e*ntrlfhgal pop Uhloh elroulato* th* dlphaoyl - high hollar alrtur* through a ga* flr*d ooll h*at*r and back Into th* task. >ll*on-laul*n Pyod thoraoooupl** located la th* tank, at th* lnl*t and outlet of th* heating ooll and la th* ooluaai hand, oono*etad to a Brown I*oordlng Fot*ctlowetr aorr* a* ooatrol* for thl* atill. Th* oharg*. whloh baa th* fallowing approxlaat* oonpoaltlon Banaol low bolllag hydrooarboa* Biphenyl Sigh Bollor. Tar* aad Carbon si B. t *% >. r rax B. f ltd b. r B0C 100 1B0C ucc l?60 (approx,). 1* rva by gravity froa th* b*aa*l atill to th* diphenyl atill. l*w boat 1* applied to th* *oll until th* r*aldual bwaol haa dlatlllad. Thl* 1* rotum*d to th* auap tank*. Th* boat la than lncrea**d and 0*U*ctlo of tb* dlatlllat* la pan* b*gun, Th** pan* ar* aad* of HONS 052029 galvaulaad Iron and neaaurt II* t 4T* a }*, th# ftrit pu eontaint tha In boiling hpdroonrboai and la known aa *haada*. Thlf anountt to approxtaatalr CO# par ahaiga. When tba potentioaatar lndioatae that tha balling point of diphenyl baa been reaahed, tha delivery pipe la awung to another pan and haat end dephlagaator regulated la auoh naanor aa to dietlll teohuleal diphenyl of M.80 or higher fraeelng point. The and paint of tha dlatlllatloa la oarrlad Cfi - KW abewo tha boiling point of diphenyl to laaura aa oonplote renoval aa poaslhla. for thla roaaoa aoaa Sigh hollar will ha dlatlllad over lato tha laat pan, thla la knoua aa tha *talla* and thla aatarlal, along with tha "baada1, la raaarrad for tha production of iroolor SMS. tba raaldua froa thla diatlllatlon la knows aa "oruda high hollar* aad la althar puwpad to atorafa, dram out la druaa for etortge or duapad into tha High hollar Still far auhaaquant dlatlllatloa. |<ah hollar till thla la a noma atlll and la af tha nano geooral daalgn aa tha diphenyl atlll axoapt a raoalvar, trap aad wnouun puap hart baaa addad. tba raaldua froa tba diphenyl diatlllatlon haa tha folloolM approxlaata ooapoaltloai Biphenyl Qrthodlphanrlbaaaaaa CotadlphenyibeaBeno Paradlphan/lbaesana Tetraphanyl, tara and Oarbce 1.0ft t.O 10.0 M.O M.O Baoauaa af tha high boiling ranga af thla aatarlal (MOMwO) It la aaaaaaary to waa waeuun dlatlllatloa. tha ho11lag raiya at (0 aa la raduead to tufi - BW tba oherge la run by frarity into tha high hollar Mill, tha toaparatoro at afclab It la duapad la above Ita boiling point at tha raduoad praaaura (CO aa). tha alraulatlag puap la tharafora alerted and tha eharge allaaad to aoal to approximately 1TCC bafora tha Taauna puap la (tartad. A dlfforantlal af SO^C bataaau tha ialat aad outlet af tha banting ooll ladloataa eetlefeotory alroulatloa. Shau tha tenperature haa droppad to 1TS0 tha waouea KONS 052030 G4 mum If atortad aad th* toaparatura ( Dm aharg* drop) rapidly to 1*00 (t ahioh toqparator* th* raaldual diphenyl dlatilla. than th* t*p*r*tur* *f th* ooluaai toad Indio*to* that *11 tto dlph*nyl 1* dlatlllad lb* vamrai to r*l***d usd to* raaldual dlptoajrl dram from th* raoalrar. Dietillation to th*nooBtino*d totil approximately tQf if th* arl<U*l Cher*# baa ditlU*d. |hta to datoralaad ty raltaalaf th* vaeuua periodically and neaaarUg th* eoalaeta f th* raoalvar* da axpwlaeoad operator pan Jadf* thla and point %olto aooaratoly by ohaarrlag th* fl** of dlatiUat* through th* *lght glaa*. th* dlitillatioo to thi (toppad aad th* diltillad high hollar draan trm th* raoalrar Into p*n*. Th* ttill raaldaa* eonalattog principally *f tar* aad aarhaa to draw cat aad dtoeardad. Juylh TV* dlptoayl wit ha* a rapacity if 10*000# todtetoal tlphaapl par Math. \ MOMS 052031 Cf TIU MOM firoa left to ri<ht. 0round floor. Benaol reoeloer froa doorber thro* erode dlpbm/X op took*, wtdoraoatb flatfora Jaat lliem* bio lo dlphaojrl Otui tank, right, high bollor otlll tab. Oa platiorn, Baoeol atUl with fraotionatlng oolvan and oondonoor on eooood flafcfoxa, Foreground, diphenyl roadj for HtUn. MONS 052032 6>fo fTtU IBiTSB OOIU Ufi OM* el***4* >* U 'JLmS ell for eoU. . * fir* ^ HONS 052033 a>r MIUH) DIPIHflL OOUBCnOH HONS 052034 wmm nm rot norao eolgrotiDd (hoi* high boiler (till. HONS 052035 UOB BOU.IR CT1U l*ft * (till tank iIwiIh <riw to MtaMifW %jf hui; fiof! tn otr, fretlrtlt Mloan. llfht e*nt*r, lol*r. klfht, !> HOMS 052036 to CIIKMICAI. COMPANY, Diphenyl Operating Record ending 7:00 A. M........1*11........... 193 S Unit No. *.... No. I SHIFT FOREMAN bf B .M B ....# .. ... L_ M ......# m M # _ uo SI ___ m .1* MS a W____ m. M # . M Jl., J 1X7 u _**... in B . . M M.I M _# .. . J* H JL_ 11 w___ 1M 0 * ITS____ 41 - it in _ ... n M 44 , u us 49 10 m 1J N -ft* K> ttteMnl JR m... .. J.. -J*-- . 41.... .. -49 ... in ..... W M u. 1 40 41 in DEI. A VS--Coooe OTAt HONS 052037 MONS 05*03 MOMS 0SSQS9 piPHUttL PUN'f PAII.T RtPOBT FOK_fcj rfuotloftt techniool Dlplien/1 Orude Rifh Boiler fcUl Metilled High Belter Ifydroehlorioi' t4 * HONS 052042 . ;$ UTUVU worn m m wmnoi or m uraam. nit flow Voter AmwomoIw lHorilai Veaordiw Tetwtloaeter Ymperitari Oootroll at lamart lut Suafo Pohstti loertlnf X/V, #UtV Wllaw lit Pyod* ( Iron - oonitaataa) Villon laalw I Polat fipalof Brow* Tolat Wilton Kaolie Potwtloewtir ectuatiac lurltu lillitor Co. Motor valvii. Coabuitloa l^laeerlng Co. U|k fninri (tc#) Vobllac Tank-O-IUter UWr a aarafol ohook bM ba>io oido of tha varlow sootrol food llaw, food pwp. ralewe lino*, water llow wd othor equipment the gw bumnra in 11*btwd wd thw loot twperatmre la the foto broupht op to operetta* temperature, lUi requlrw approximately la houri. Buriat thl* period tho (took ooatalnlat tho bwaol vaporHer ll doled oad tho produeta of oombwtiw diaoheiyad through a aoparete tak. Thli ll done to prevent overheating of tbo vaporiaer coil. fbw tho Ijnta hai rwobad operating teapereture It la awapt oat ttwniUr with tuta dloxldi to w to mm tap traow of air wd void wplwlvo alxtarw of air aad bwaol. Iftor thlo precaution tha boeiol food pom lo otartod aad tho flow of. bwaol atartodthrotyh tho wit. Tha tpwt humor gww arc thm tumod through tho tack --tnioiop tho bwaol traporlaor tad tho waito boat willload. Tha rato of hwool flow la thw gradually raiiod aad tho whole ayatw brought lato aqallltrlw at a flow of approximately HO gallwa par hoar. _ dew la a raverial of atortlac It. Tho product* Of iwhuatlw art wt off tho vaporliar 0011, tho bwaol flow la atappod aad tha food pwp abut dew. Tha ayatw it fthw awapt wt thoroughly far tw alawtoi with aarbw dioxide to laiuro oeuplete rweevil of bwaol, Tho raloaio Haw at tho top# of the pota are thw opwad ta afuallw tha pot prewurw, car* beta* takw to opw tha ooavortor roieeao, tha ft prahoator ralewe, and the #1 prehwtor roloaw la tbo ardor awod to avoid blow back of load. Tha HONS 052043 74 ft* It than abnt ttt and 11 tha rint doua It to be for tar extended tine, *11 water and *ta 1* alto afcat off, nf -tha Uataadmr a pleat of tfulaamt la a two ohtaber activated olenina adaorbor a*ad for resowing bensol from tha hydrofea produeod la tha awafeeturo of diphea/l and alaa for aolleetlaf tho banco! report laaulaf fro* tin wtnta af all food aad eolleetloa tanks, tha ohtaber* ara equipped with pip* ooll* aaaaaetod throigb two wap Ttlwaa to flats aad satar, ftu-lai the adaorblaa period eoollaf satar 1* turned through the aolla shlla durlm tha re-eetlTatlea period ataas la tuned through the oalla. The operating period* ara alx houra, during whlob tin* adaorptloa la taking pl*o* la ana ohaabor while re-aetiwttlae la bolag acooaplltbod la tba other abasbar. The teaporatarw af tba adaorblag ohjab*. la bald bales N0C, tho re-toUrtUon abasbar la batted aa bet a* poetlbl* with US# ataas for flwo hour*, then eooled to balsa tfiC durlag tho alath hour. ettne Stfftmltfoa Epreaast dljhiayl. salt la operated with a tlaa efficiency of 7Jt , Tba prlaetppl factor eaaalaf last eparatlsf tlsa la aarbos foisatlto. (bta la Indio*tad bp ehaagM la operating preature* aad occur* seat frequently la tba following ardari 1, Oooaaaeek* fros aessartar to trap and frea imp to oolwa, aaat be dataad bl atsthly aad require* about four houra, Ip&r* footMooka are oarrlad aad oaehaafad, I, OoawtrWr dlatrlbutor pipe. Moat be cleaned or changed taal-aaaaally. dpere dlatrlbator carried aa band, Changing require* about olgbt boura, I, lo, I prebetter. Runt be oletaed about aaea a peer, tba oarbon foraod 1* eery bard aad dasat aad It la aaoaaaary to altber ohlp It out or burs ost vltb oxygen. HOMS 052044 77 Oihtr futon oocaalonally oaualag loot oparatlnf tin* aroi Milrltator ftilan duo to |lf broakK* and ladle*tod by ehtaa* la oporotlaf prooouroo or roluoal ooerorolon. Thomoeoupl* itU foliar* luo to Tlbratton *al Indicated I7 loakoi* around the oonnootlen at the top of the pot, food punp f*Ur* duo to wow In th* yuap to mob an antoat that it fall* to dollror th* a*0*00107 pro*our*. fot failure indloatad by load ruanlAf out th* firebox door, Iheofar a pot la opened It 1* aooooUal that th* load ba nooourod and any aoooooary nake up added, th* aeahanleal action of tha roporlaod banool pooolnj through tha nolton load oauaw paoooge f thl* notal iron os* pot to another oal from tho oonwortor pot to tho load trap, th* proper depth *f load in Bo, 1 and Bo, t prahaatara la 4S* and in tha oenvartar it", tha aunp tanka and faad tanka ar* Tonted through tha leotrodryer. Oooatlonally thaaa llnaa booooM plufted oaualap back proaauro an th* tanka ar booking up of tha diotlllod bonaol, It la noooooary to elaan thaaa rant llnaa uhanarar thlo aaonra. Baaaal naad far Mpbanyl Mnufaetnra la boufbt nndar tha fallow ing Ipooiflootlour1 (dll Cawarolally Par* Panaal. UK tha Tlolbla talar ahall not ba tutor than n notation of 00K fa. nf potaaalua blehrout* la on* liter of untor. Conpariaen 1* to bo nad* In laatlor Tuhaa * 10 00 alaa. M.mi.itai Th* product ahall dlatlll frau atart to dry nlthln WK. flthla ahlah dagraaa ahall ha Includad tha Vna bollla* point nf fura Bonaeat (W.PO.) tha nathod of dlatlllotioo ahall ba In aooardanaa with nathod g-4, l*an, 2nd. Inf, Oban. lOjlOOd (lOlt). isMJUh th* uooh ahall net ba darker than Bo, 4 Barrett Colarlaotrlc Soalt, teat In aooordaao* with dlraotlon* for toat fourn, lad, Bag. Chon, MOMS 052045 nliM protect (ball awtali u firaa wU< iMlWf ||--**r ^Pacific Orrltjr at U.l0 ahaU ba bataaw IT! aa4 iMi |htnm teat ba aaaantlall/ traa ot Ij0. Tr--'f fcl,t Itraailii polat auat ba act balav 4>t^C. Taat la wmmihi with Mtbod af V. . Itacl Oatp. HONS 0S2046 79 * * lumcron or amxsom Irodor If mm w**d to Itiifutf Of riOwiMM prodwot* at , Th* phyfioU proMrtlo* wry fro* a light aobll* ell to laa and Mt-tqrtililM aelld* dapaadiag opoc (ha dagraa af ohlorlaotloa aad tha ooapofltice ot (ha raw aatorlal. Itralght diphatyl ohloriattod yield* a llaald product af iaeroaalag rl*oo*lty w to aad laoladlag Iff ehloria*, dbaaa (hla (ba /laid la a arratolltfla aolld, Itralght high hollar aad Urturai af dlptoail aad Ugh hollar ahlorlaatod yield product# of Incraaflog vlfoeolty ap to aoe-cryttollla# raala> A raaorloal ayetaa af eoaoheUture ooala(lag af four digit* ha# b**a dwwolopod far llaUfylng (be warloo* Aroclora. Tha flrft digit daaotoa (ha rat aatorlal aaad far (ha ehlorlattice, the flgara *aaa* ladleato* 10Cf (aehaloal Aipheayl. tha aahead digit daaotoa ahathar ar pot (ha prodast la dlftlllad. the flgara *et* ladloatlag wadletllled. (ha flgara *(ao* iadlcwting dlatlilod. tha la*( too digit* laaeto (ba approxlaet* paroaatoge of ehlorlao aeatolaad la (ha flalabad product, tbara are ewworal arbitrary larladeat froa th* abor* aeaaaolator* aa follow*i 1. drodlara IMS aad 4485. tha foraer la th* orud* froa ableh th* latter la ahtolaad by dlatlllatlaa. tha *(artlag ra* aatorlal aoatalaa dff dletllled high hollar aad gff toebaleal dlpbaoyl. tbla 1* ahlarlaatad (a Iff ehlorlao. I, Areolar* 1050 aad 5450. th* fexa*r la th* erode froa ahlob too latter 1* dlatlilod. Th* atortlag raw aatorlal la 1O0I1 dlftlllad high hollar. T*l* la tolorlaatod to Iff. I. Aroolor CMS* fhla la m ondlftlUod product, the ftartlng raw aatorlal eeaalata af Iff arada Ugh totlor aad rff toohalaai dlphtoyl. tbla la ahlorlaatod to Iff ehloriae, tha drooler* ar* aot pur* oahpwdo hot or* aixture* of (wo or aor* ooapound*. loweror( froa (heir ehlorlao ooatoet (hoy aty ho aatuaod to haw* th* followlag ooapoaldoat HONS 0520*7 30 Arotlon 114* and itU 1140 IMS 1104 1104 1100 1000 114t 1000 1100 1100 1100 1000 4000 4400 1000 0400 - 01*74*1 0i*j81T UMd O&tSjttU Xht mfutr* af iroeloro la dlelded lato tao operation*, vial lha ahlerlaatlan of tba ra Material* to emit drolort. The dltlllation of the erule Aroelor* to flalahod product*. JUlClBA&lfli fkl* operation la thorn dlafNMkblMUr to drawl* >* 0-MU, by attael photograph* and la described aa follow*' the re* notarial* aawd la the Manufacture of the tooelor* are priaoipally tedalwl Mphwayl and Ohlorla*. gone fee *f tho drooler* royolro erode U|h boiler or dlatlllad bleb boiler m will bo ahem latnr. to* lato atooa boated neHln* tanka. 144*14 ahlorlao la reooleed la olaglo elt tank eara whloh are ImmI fron the nenefecturor, 0o additional atorog* la profiled bat ehlerlaa la aaad directly fron the taak oar* after beInf peooed through a nrerUar. The eaporlaor eonalata af aylladrleal taak aeetalalaf wetor. boated tj ateaa, la ahleb la Inaerawd two 10* a 40* oylladert. lha llgald tUertae la brought la ftoa the taak oar tbroafh a X* llna and Manifolded wo aa to food both cylinder*, Veporteetlea af tba liquid take* plaoe and tho gaeeeu* ehlerln* 1# llioburged fra the cylinder* through 1/0* otxpantioe rale** into 1* line* to manifolded that any ohlorlnator nay bo fad from either eayorlaor. Proaour* gnagoa or* wood to aoaaaro tho ohlorlao flow. MOMS 0520*0 The Ohlorlaator* are thru tjrlMrlnl iUl Wiki| U fit U|b k; I ft. dlaaetor, Tho** bin flanged oenvex twin and bottom*, fttf m nUtl to bolt their depth with Iron tnW lor oetolyele. Ami in eoolooed la oa troa obeli *7* la dlaaetor, A oao laoh oo11 far ateaa wad wator extend# around tbo loigth r ootel/it chaabor boteeaa tbo two ahalla, tho apedaf botwooo each tan la approximately two laoho*. A two laoh llao load* froa tho bottow of o*oh ohlorlaator throu(h a Oould centrifugal puap to tbo top of tbo ohlorlaator, tblo la for olrealatloa of tho charge darlac ohlorlaatlow. la tbo ooworo of tho ohlorlaatoro aro lalot llnoa for ahargla^ hydroohlorle add dliobargo llaoa, olroulatla( llao* aad wont llao* for aao whilo charging, Tho hydroohlorlo add llao* froa lo. I aad lo. I ohlorlnator* oatar a ooaaoa llao leading to tbo hydrochloric add abaorptloa lyatoa, lo. 1 ahlorlaator, which la waad for lldt aad lldt dleohargo* It* add through a trap aai tbaeea lato tbo ooaaoa add llao beyond lo, I ahlorlaator, tho required charge 1* weighed and dumped lato too aoltlng pot, aoltod aad paapod to tho ohlorlaator. tba ahlarlaa flow la kept lew at firat to prerant looal awerheatlng aad dlpboapl eubllaatlon, Tbo olroalatlag poop la atartad after toning aa the ohlorlao. At tba daaaltgr af too charge laor#***, too ohlorlao flow la laoroaaod aatll too pawoowro reeebeo too aaxlaua ahowa la too table, Tbo boat of reactlaa af ohlorlao aad diphoayl la ao groat that ooollag wotor la Meeaaary to kaap tot toaporatora within tow required llaito. Tba maxima toaparatoro ahowa la too table lo that aeoeeeary to laawe ooaplot* raaatloa and to kaap tho eharge Molten, OarlH ohlorlaatlow aoaw aatorlal la oarrlod wat af tba ahlorlaator with the lal |M bp aotralaaeet, foaming or aubllaatloa. Tar tola roaaaa, lo, I aad lo, I ohlorlaator* are aower waad elaultaaeoualy, oaa tohg aaad a* a trap whlla tho other 1* la oparatloa, timber oao ohlorlaator being waad for oryotolllae Aroalar* ha* Ha oaa trapping a/atoa alaoa ooatoalaatiaa af aa/ of too other Arooloro with ary*tell would render than wealeable, A ooparato trapping a/atop for each Oblorlaator would laoroaoo too aapeolt/ V/ oao third, Tho overage aaouat of trapping* la If of tho flalotaod betoh. When oaffloloat haa aommulated, it 1* uaed for tho HONS 0520bS naaufeetore of Ull *r UN, or for ony of the Aroelora if no trappinga fro* tha leet too are pramti la chlarlaatii^j Aroslor eontatnlng high bailor particular ear# mat bo taken to alainlet fanning. A* (urfaea teneloo of thla atarlai la apparently higher than that of diphenyl, therefore a higher Ohlarlaatlng teaqperaWra will reduoe foaalag tendency. Ohlorlaa Mat not ha fad too rapidly at loo teaperatore. faaplee ara takao fron tloa to Uaa to datarolaa prograff of tha ehlorlaatloe aad aaar tha and oxime oare Mat ba takao to praraot everrvnalag tha aad poiat. lowwrer, an experienced operator oaa flalab to apaolfloatlooa with great aocurecy. lhaa ehlorlaatiap la oooploto Irodara 1141. 1154, 1140, 1141, 4045 aad 1646 ara pooped to tha blowing tank, Thla tank la equipped with ateas oolla aad perforated pipe for eoopreaeed air. lealdual hydrochloric aold la Uao eat haro the hlowiag period oarlaa froa fear to teelwa boora, depending ea tha iroelar. Thoaa that ara to ba ablppod aa orod# aura glwaa tha aaxlaua porlod Ofalla thoaa to bo dlatlllod art glvaa the alalMau ihao apaolflad by tha nuetoner that aay of tha ligald erode iroolore ba ahtpped aa tush, they ara given epeelel treatment with foliar'a Barth and hydrated line and than filtered. Ifter blooiig, the natarlal la draws dlrooUy Into nhlpplng oootainara or Into 50 gailan drun for ntorngo preparatory to dlftiilatlon. droolora 1155 end 1151 nalt too high to ba blow no ara drana dlrwotly fron tha ahlorlnator late open top droM. Thaat enidoa Met be dlaebargad fren tha ahlorlnator on rapidly aa noaalbla in erdar to prevent freealM. Thin ndlbol of dleoharylng la dlnagreeabla aa wall aa haaardooa to tha oporatora and oould ba greatly improved by tha lnatallatlon ef flaking aqolpnant. the following table and ohart ahova tha operating faetora lavelved la tha produetien of aaeh drooler. MONS 052050 um not UM 1300 1300 UM UM " ion MM w*-ri 30-00 M00* M - Moof *T-M r XT 3M r 37 1 r M UD 3B uo XM 5,900 Opodflo OmoUT UtS - 1.(49 49^8 w 4,000 Moelfio Oraolty 1.4U - 1.UT 40*0 to T,000 OpodAo OMiMr *** - 1.50T 8C (*) Vf6o# M- T M uo UO 7,900 VoBlfle Poorly u* - UM () tfOOOf M-B T M IB 3M 7,M OKooiflo tofttgr 1UB - 1UTO SOcPO (o) t^ww# V K - 40 UO 3M Offico mad xwa* IB - 190c (4 Moo# 40- 44 0 V 3 6 0,000 Bold MM BO - nfio (8) 2-SQf * 790#ejtxQ) 3M m 7,900 koftaaltat Mat Borrott Tl - 8^J <) tvana3#HuEMmM*> 3M 7,900 OoftokSkf MM ktarrott Vp - 00C to 1,000# - < B UO B0 7,000 kftMt Mat knttt UO - ltfio U> (IS CMlikU* ft) BftUM U|k poTSf (3 Bt w| fidy of Itow (UolHtM nit to WO,COO 1W. (3 Am* flnrl'W-- aro tikM V tk, jjrar with Igdrwtw of itlMt* Hop. Ik* fltol lllii ro iftoitowl If tko oootrol litowtwy with tko Iwtftol Hoi--oo. (S) Ik* *toU Mot* U tfcot yolat tk tko fT--laf xtkfo ohm tho Md otooo tko ehormctoriatio Is Am tt test of HI jitnl71--tilit (l) Bo NftHki fttat lo dotaNted la tko plmt ty tko Onraott Bat aotkoO, tko aotorlol total iriokHl ky ooapoolaak o&tb a rWaflott of taoooa ooftoalaf ptat. $o$^ooo aovooo 279^009 ln^oo 27%fOO 189,000 XttpDO Xtf^DQ HONS 0S2051 Cb 'k 052052 ',1*\*> U '*<-jty. '* okuhum homo* *, and r* r t liquid oMwln* 41ebM|Ug UUn. Oeotr o*r U < kydroeblorlo eM loading UUm. HONS 052053 36 CHUMUkI VAFOUUK lot atar tank oosULnliy two T*jx>rllag yllndara> tiqu14 hXsria* M la through dirt trap at laft. Oaaaow ohlrUi dlaohaiyad thru Mpanaton iiItn at to> Vppar praaaura cat** Mad far controlUf ehlarlaa flaa. MONS 052054 8f QHU>UliTOUI Tb* thr** ahlmrlaatora and thalr circulating puap* it* ihom, th* Trtlol Uai mUrlng th* ohlcr- tnatori awr tb* bcttoa *r* ohlorin* Th* bolted pUt*t permit distributor r*pl*oBmt* X* th boiground ewi b* ** th* bottom* *f tb* to diphanjl ltlnr tank* and th* puap* **d fir ob*rglng th* ohl*rlator. MONS 0S20S3 86 OHLORXMTOM Uft Chwrg* Hln* twk, 0Bt*r - Ohlorlnator*. rlfbt - CWorln* Tiforlitfi HONS 052056 . tor nn or obwmiuiom IbMI obuyliv llM| bjrdrooblorle sold |M dUohMyo lino, and olroultUnf lino, Foro*round ibwi oklwln# oil fold, Ohlorlno plpo bon ontori** ohlorlnotor Ooat top, ortondo to boUo of eblorlnAtor but 1* wlr Utod la t distributor troublo. HONS 052057 pisobajom OaU>Rl*ATO fwag :?*"! & 41##h*r|*a *w P"' ^ <U|trwl opvrttloB. sssr^i u ss. - w*> HONS 052058 I I 9f CHLORINATION RECOUP klor No. Batch No. Chlorinate)- No. |trve<l by _ flmi . itltbtd by Time Time _UUO PM Date 3$ Date JJMi Jl*l Hour* _|j __ Weight of Bntoh fa_____ _________________ mfMM&aa/i____ :_________________ I ' Vapor ' Book ' ~"En9 PoTnt ' Vap. ' Bock ' IM Point Rise J Temp. J Preen,] BstolT' ]' BV3T. "] Time J Temp. ! Prose. [ KTcK I"5l<HY' MM l' J I` .i .. . t. .r,, MONS 052059 xw laU Mwwn lace ear aol af hydroohlerle add 1* produced for every aol of chlorine need, prowleloo Met be aede for the collodion of this by product. The eold |M peeee* tram the ehlorl*iore downward through trap, thenoe out of the bdldlag through e twe loch pipe to e cecoad tree et the ebeorptloa eyetwa. tram thle trap it pteeee throi^h e coolly tower to Tltreowll ebeorbore. Theec ore thirteen la suaber pieced one ehowe the other, Veter enter* the upperaoet ebeorber end floe* oouaterourrent to the gee, Mfficteat water being added to produce lroe eold. The oondeneed acid paeeat through a eerlee af eee loch Pjrraa eoollag tube*, thane* to a >0,000 gallon rubber llaed teel atorege tank. Jap wnebeorbed gee paeee* froa the abeorberd to a drowning tower, the weak add abeorbad hare being run orer llaeetose to the fewer* Approximately Mf of the add produoed It reeowered and abeorbad when atorege oepaclty It ewtllable. loewwer, thle le Halted to the atorege tank asailoned ehowe and two 1,000 gallon taak ear*, a* Mh af the add pad* la waetod, Should Sale* warrant tueh, the reoorary would ba aubetantlally lacreaeed bp pupping the teak add froa the drowning tower to the abeorbere* )a the whole the ehlerlaatlea preoeae five* practically ao trouble, A faa iteae af aeintenanoe ere llated below In the <order af the frequency of their ooowrrenoe. 1, Dletrlbuterfl the perforated plate ef there Met be replaoed aeal-eanuellp a* it aerrodee through la a dx to tight eonthe period. t. The Heroo-dordetroa Talwee ea the ehlorlae lines enut he replaced once or twice e year due to leaky etwee. I, The Crane waiter ea the waporlaer are equipped with regrindable aeeta Which aunt be reground eeol-annually. HONS 052060 93 nrDMxmoiao acid tun boa* TitraaalX ebaorberi, ooka packad drowning lover. 10.000 iiUm rubber ilnad acid storage tank, kuu teak at lafi 1* tar K>Be. eold oarbo; ehtyaoatat Iota also gravity rubberlined llaa far tank ear loading. moms osa'oai lift III HYDROOHLORIC ACID RKCOVm Fortran Myof*__________ Oparttor Mwm Data f^fuAL 94 ifiH liU h lrilfll V ' 1 pi.Ullatlon of tha Bruda IimIbu All ef the Aroolora exoapt Aroelor IS66 ore dletlllad to fin) abed produete. feo different type etUle or# need, Till 1, dtnoepherie, oo-frctlooatl*g, uaod for production of drooler 1**#, I, feovun, Circulating, Ooll looted Typo, wood for production of oil other drodore, AraoXtr 1169 PUmUUai The dletilletlou of thle produot hna reeolved Itoolf into vary elnple operation after hoving peaead through rather oonpllooted dovaloynent period during obioh oevarel typae of dietllletlen ooro triad, drodor XM9 lo the Moot highly ohlerinatod diphenyl having the epproxlnate fonralo OuffGU, It Malta ot approxlnetely WE0 aod hao a dlatlllatloa range, at etMotpherie preeeure, of 400 * dtooo. dtteMpte to veonvM dlotlll thle product foiled due to the greet tendency of the Material to euhlle, The foot that ite boiling poUt voder 1 i M preooure vary eloeely approaehoa ite Belting point render# the doolga of e eatiefactory veeuun (till extreMoly diffieelt, Matlllatiea at etnoepherle preeeure ualng a oleeed retort equipped with oa ^itator and dleehoxgUg the vapor through e peeked oolvnn vara vBaatlafaetory heoauoe of lav ylelda and the diffieulty *r raMoviog the etill botteau, dtteMpte vere Mode to eubllna the produot by poeolng a eurront of air over the oarfaee of the boiling liquid and ooll acting the mbllaad produet in a duet collector, Thle Method gave fairly eatlefaetery roaulta but vae dieoarded due to nipenee of Uietalle^ tlae end oeit of operation, doothor problan ahioh preaantod itaalf in th production of thle Material vae Ite phyalool vendition after dletUlatioa. Collection In pane vith the rvaulting elov aoollng gave large hard eryetala Aleh the euetoMr found Inpooelhle to grind to tho deelrod fineneee of one half nloran. *ons 0520h3 9C tlr aubllaetloa and alao dlatllling 1bto a wUr quenehlj* tank with iubaequeot drping of the quenched product gvvs a product of tifotoi7 phpaloal ohzraoterlatloa. The latter m diaearded hovavar la favor of tbs flaking abeal which la uaad at praawt. Tha distillation aa la Bov oarrlad on la above by parts of draaliy fO-tIH, bp an aotual photograph and la daaorlbad aa folloval Cgulpaant * Tha aquipuaet uaad In tbla operation oonalvta of four ataal pota Id* In dlanstar x 41* daap, vhloh ara uaad alternatalp in two aultabla fira brink, ataal jackatad esttlnge. Xaalda tha pota la voided a ataal ring or gutter approxlaatalp IP* from tbe button, tbla ring aarvaa aa a oollaotor for tbo diatlllod product vhloh la oondanaad on tha aldoa of tha upper part of tha pot. Tha dletlUate la dlaohargad through a abort plpt aat In tha alda of tha pot at tha ring laral. Tha pota ara aiao provldad with aultabla oorara bald In plvoe bp 0 elaupa. aatlag la aoooanllahad bp gaa flrad through a four ring* lot proaauro, uultl-jat burnor uanufaoturod bp Tha Purfeoe Oonbuatloa Ooupanp. Iba dlatlllata la collected in a pan vhloh faeda a 14* dlanetar a Id* voter cooled flakliy vheel rotvtlng at 11 tfl. Tha flakar la anoloaad bp a hood which la eonneetad to a ftaynond duet oollaotor equipped with atalnlaaa ataal tpolonea. Tvaiparatura la uaaaurad bp Tpod tharvooouplaa ooanactad to a tllaon-daulan Zndleatli* Pproneter, 1 llroooo azhvuat fan la uaad to eloar tha atlll roon ef funsa liberated at tha and af a dlatlUatlao. MOMS 052064 hn hundred pound* of Arcelor UM and twenty fiv# pound* of hydrated 11** or* weighed out ond charged into the distillation pot, A g*sk*t of Mboito* ropo 1* pXoeod around th flange and th* ooyor put on with 0 elupk, Thli eovar 1* flat *te*l plat* with a six inoh pip* IK* high w*ld*d la It* Mntar, The pot 1* sow liftod Into th* aattliy with * ehln-holt fanl tb* hood oonnaotad to th* exhaust fan nai Into pofltion evwr th* pip* la tho oorr, fh* delivery pip* 1* lwvgthwatd to reach th* fl*k*r r***rvolr to a *l*owa and alppla, A thermoooupl* 1* pi*cad 1 th* material through tb* oov*r and boat 1* applied, fhlla heating th* terlal to distillation temperature tb* flu* 1* allowed to eovar the bottom of the pot, Whan dlatillatlon (tarts, th* flu* 1* raduoad *o that It l*ek* two ineh** of touching th* bottom. If thl* if mot domo tho ehargo will boll avar into th* oolloetlni rln( and |1t, black material on th* flakar, tb* old** of th* pot abor* tba collecting rime met a* a ooodanaar for th* distill*t* Thao the tenparatura of the material raaoh** 400C dlatillatloa 1* lanlnwt, Tb* first of th* diatlllat* 1* generally blaek ae this 1* oollaetad la a swell pan ln*arted through a door la th* hood, Thl* 1* withdraw when th* atreu olaar* up. Th* material oaugbt bar* 1* re-dlatilled with a subsequent batob, Tb* flakar and dust oollaotor ara both startad the aoaent dlatillatlon atarta, Tba average tin* for haatlnc to distillation point 1* on* hour and distillation also consumes on* hour, Tba distilling rang* of thin Aroolor 1* 400 - 900, Toward tb* and of dlatillatlon th* oolar af the diatlllat* again darken* du* to dooomponltlon, Th* operator wuat watch for thl* and nnparat* th* dark material from the nhippabl* product. Thl* m*t*rl*l 1* *l*o r*-dlatlU*d, Complotlon of dlatillatlon 1* marked to tf>*t In known an th* blow*, This 1* a rather vlolant abwilltioo af dark oolored aubllpsta Whiob 1* strongly old. It* probable ou la auddan decomposition af warp high boiling chlorinated residue Whiob releases considerable hydro chloric aeid la a short apsoo ef tin* saualng subllnatlon. Then thia scour* th* fir* 1* linsdiately out and th* exhaust fan tartad. Th* blew laats about five minute*. Than It oeaaa* th* pot le lifted from the setting, plaeed la a water filled paa an a oarl, rolled Into tha yard and allowed to cool. MOMS 052065 Ibt lUll Mltwi h a aistur* of otrlM) HrtliUi 4eoapoaed ArOclor, hydroohlorlo eeld and o*lola ohlorldt, Thle alrtwe altog* rather teneolouely to tb bottoa of tho pot. It* reaovel it WMpUiM ealy by Inverting tho pot and baamerlai Vlaoroualy with *led*e*. Thla it *o***hat 4*glag to the pol betooaa. to Improved type of pot thick v ellatoate thlo pounds it bo* holag tout, I*oh teeaty four how produotlee of flaked drooler and tb* hit ooiifht to tho oolloetor it aired >i thoroughly u poaalble to order to ohteto o an1for* oolor and paofced either to tOO lh. Used hurlap bag* or 400 lb. eleeV barrel*, ae the ouetoaor dellre*. The (re*tot portion, boaeeer, la chipped la b^e. penealtr Tb* above deeerlbed Ittt etlll* here a ooaiblned eepeolty of 1,000# per t4 bow dap or 100,000# per Booth, Deeratlae Mffloultlaa I. The ftwar ao* to see iw sot deelfaed for thia aerale* aad haa too loo oapaoltp, to aplta of great ear* the pan ever flew oeoealooelly. thla *u*t be oollooted aad ro-dlatlUed. I, dale** the delivery pip* fro* the atllla la kept hot dwlag the h**UB| Period it etopa p wlian dlatlUation aterta. Thla seoeaaltatea oieenlag It *lth a rod. (. If for any reaaon a oherge 1* brought to boiling and then alleoed to oool without dletllltog. It 1U d*oo*poe* ben reheated and tb* raoovery *111 be lou. HONS 052066 99 S tuoautoi i*e nmumci left thoot eyolont dutt oolleotert. 0totor. aiiUlUUw pot la (M fired atttlaf . Mht, nucliv* rail thoolnf dltehargo of product, laat bohlnd tho fliJclxf roll oan bo aooa oooond lUU. Tbeoa too art opartted altfcrottoly. Ui]t plpot abort ftlUt load to ao oxbauit fan* HONS 052067 /Oo PRODUCT LCl_BKg<iL^ .ARfipl-WUjS-L. SI IU NO,___ I--------------- BATCH NO.--10841-------- POUNDS 1163 CHARM'D HIM MAI rIII ai._JW09 JtB it. i, . PRl'MUN OR OTF-COl OR___ POUNDS si iu bottom:;______ f|------- ------------ pounds pnr run on orr-eotoR_J____________ fiw *Ufrt--------------- f:H: OIST. stadtcil...JlU BIST, endfo,____ ||M--------- DATl JtlTrM oPtRAion_____ Xttzkov___________~ 0 4 0SHIFT N .__. k_TM M_jM 10 *oo A ,11. -p,M. POUNDS n MAIFR IAL ATItR CENTRIFUGING--fet**** POUNDS ___________ *W( U MOMS 052068 fo/ ItamJBiatllUUfit ill af tin dlatlllwd Aroelore except 1(49 are produced la a nnia lUH, thla operation la ehown bp drawing 0-4868, by a photograph aad la daaorlbad aa follow*i Iqulpnect * The equlpeont uaod for thla operation oocalata of a baatlqg tank, wood for aalttag or war*lag tha otlll ehnrge, ahloh dlachargaa Into tba naln atill kettle. Thla atlll baa a capacity of approxlnately ITS gallona. tba aharga of Aroolor la alroulatad Aron tba botton throi^b a bo. > Qulaby yunp to a gaa flrad beating toil aad beak Into tha top of tha kattla. tha wapor la dlaohargad through a aotiol natal foan trap to a nasal natal alngla tuba aondanaor. tha eoadanaad produot dlaohargaa through a alght glaaa Into a nonal natal llaad raoalwar. tha aotlra ayataa la ovaeuatad to 1 through SOJf oauatla aoda aorubbara bi a thaalar tbraa 8teg* tubejat taouun fuap. i Borina loobanloal Taouun Punp la provided aa atand-by equlpeant. Ihaa aaadad to prarast freealng of th aharga undergoing dlatlllatloa Aroolor 1140 haatad by gaa la alroulatad through tha following Jaokatad part# of tha atlll aat up. lino froO atlll tank to Qulnby pap Uia fron boating ooll to atlll tank Chaigl^ lino alnhy panp Qulnby puap packing gland tha dlatlllad Aroolor la tranafarrad fron tha raoalwar to althar af two fit gallon galwanlaad blondlng tanka whara aawaral batehoa ar nixed with Pullar1a oartb bafora paatlng through a It* plate and fraaa (parry f11tar praaa to flnlahad atorag*. tanparaturaa art naaaurad by Pyoda eonnaetad to a tlx polat tilaon laulan tapalog. too polnta aaeh art naaaurad at tha Inlet and autlat af tha baatlng ooll, aat In tha feaa trap and ona In tba raoalwar. Par tha aaka of Urerlty, Aroolora U4t, 1(48, 1(54, 1860 and 1(6( and thalr oruda honolaguaa will ba referred to hereafter aa *llguld Aroolora*, while Aroolor# 1(68, 4665 and 6460 and their oruda honolofuo* will ba roftrrad to aa *aolld Aroolora*. Tha fomer nra HONS 032069 ot ell. etrlolly lieuIda, but thep are Mill* Belted and. therefore, B*p be (0 detained, The llguld orude 4roolore are delivered to the Badger (till to bungad drum# and tha aollda to opaa-head (ngli for ohargUg* tha bungad druae ara draw up by a ahala-hotat to a pletfom and the bung pi*cad euer tha lip of tha charging tank. Bum and vaat ara renored and tha drua heated with a gaa flaw. Boating la not aeoaaaarp far Hit and Utt to lut uaather, but all nu*t be heatad to alatere Tha aclld droelor* ara broken out of tha drone Into a box and Chorallad Into tha charging pot. d teaparatura cf 100 * 160 1c aufflalcat far charging tha llfulda but tha aollda anet ba heated to 160 - 660 to beoone auffiolaatlp llnild to prevaot fraallag uhlla ahaorglng, fhla operation la carp crude and affordo aonaldarahla roon for lnproranent. A bot-oll apataa for haatlne tha ehajgtog tank could ha anieh nora efficient and alaaner than tha open gaa flana no* needi Op# paroant of bgdrated line la added to tha aruda droolor* in tha ohirilig tank. Thla aautrallaaa anp reaidual add and proranta eublisitloo of farrla ohlorlda uhlob uould dleoolor tha dlatlllatoa Vbas tha atlll la cold before charging, all jaoketa ara ctmad dth hat drooler froa tha alroulattog apataa. If a aolld drooler la to ba dlatlUad, a anall obarga af lldf or U48 la flrat circulated la tha atlll at atnoapharlc pretcure to baat tha apatan thoroughly. Thla la punped out Jnet bafora tha charge to ba dlatlUad la readp. to dropping a charge a 40 nalh aoraan la placed ovar tha funnel af tha charging line to take cut Boot cf the line end cap foreign Batter that B*p ba la the aruda. St la extreaelp Important that no foreign Batter gat peat thla aoraan alace tha etaaranaa batuaan tha aoret and tha barral af tha Quiubp pulp la axtraaalp na*ll and It 1# therefore aaallp atallad. ' fuat before ebnrglM, the Qulabp puap la atartad and a lea flana applied to tha oollo. Kan tha charge la circulating, a* Indicated bp a lea teaparatare dlffaraotlal (So - >00) bataaan tha Inlet and outlet or tha aoll, circulation of hot droelor to all ^acitta but thoaa around tha ftulnbp puap packlig glande la atoppad and the Jacket# grained, the gaa la non tuned on full and the apatan evkeuated. Motlllatlon froa a oold apataa atarto to three to flue hour* after charging depending on tha drooler being dlatlUad. Tha lag batuaan batohee la 10 to 46 alnntaa( HONS 052070 01*o* the arude charged per bateh It 1.000 lbr, aad the reoorery 0T0# only 10 lbe, af ettll reeldue will bi left fro* tab batch. Thl* it aat auffleleot to maintain elroulatlrw, whloh requires at least 100 Xbt. Thtrafora, tha first thraa tr four batobaa are aat rue to oowpletlon to that olroulatlow nay ba aaiatalaad vhlle reeldue la aoounuletlag. fine# tha eapsolty af tha resolver la only 1.(00 lbe, tbaaa flrat batehai oust ba (pllt, tha reooiver enptled aad distillation resumed altbaut reoharglog, Bubsequwt batchat ara blended with tha awl; ocaa to that tha ooqpoaltlan af tha Whole will ba walforw. Daring IIetillatlen tha tenpereture af tha fat* trap eolBoldee wary eloral/ with that af tha Inlet to tha toll wntll near tha tad Whan tha temperature af bath tha Inlet and outlet laoreaee rather rapidly while tha feat trap temperature ranalna nearly aanataat. than a spread af 00 10 between tha tom trap and Inlet la attained distillation la complete, Tha above la true af tha liquid Aroclore, aad droolera UM and HW> Iroolar 44d6 aeaalfta af Mixture af dipbamyl aad distilled high hollar ablorlnatad to tBf and haa two dlatlaot toUtat mfii. Tha ehlorlaatad diphenyl dlatlUa flrat and will aolnalda with tha Inlet ae above. After thle haa dlatlllad tha Inlet aad outlat temperatures will lnereaae and draw away froa that of tha foaa trap and tha itreaw af dlatlllate will fail wff. da the taaparature af tha llfuld Inaraaaaa that af tha Taper la tha faaa trap will lnereaae until it again approaches that af the Inlet, laothar apraad iadloataa tha and af the dlatlUatloa. than dlatlllatlan la aoaiplata the valfe on the vacuun llae la eloaad aad tha (paten wonted at a point beyond tha reoelvar. 1 aoeeured erode charge af IT* in tha eherglag tank la aov dropped and elroulatad wntll tha reoelter la enptled to the blending tanka by means af aowpraaaad air applied through a valve In the vaouua line aver the raoalvar. Distillation la aat reruned. Tran tine to tine axoaaa atill raaldua mat be withdrawn froa the kettle, This la dona by partially opening a plug valve an tha dleoharge (Ida af tha ftulahy at tha oomaletlsw af a rua. By using care 1 this operation alreulation will ba nalatalnad through tha oo11a While draining. louever, If tha valve 1* opened too vlda the notarial In tha eelle will eerboalae wMeh naoaaaltataa drawing all raaldua# and renewing tha wall. HONS 052071 t04 Vbea th* rttU litoti t*k*e out *f operation th* punp le that Itm for * fow nlnute*, rdn at th* l*l*t to th* ooll* oloaad ud a want plug 1* th* ooll* epwaad oo that oigr tutorial ranalalag U th* ooll* *111 k* poll*! through bp Taouuou th* otlll r*ldu* era ooo puupod out and o snail charge of liquid Aroolor dropped aad alroulatad for on boor, th* latter 1* don* oo that th* puaip *111 rua fraelp h*n nxt used. Other*!** th* high naltlng otll! rldu** U1 fr**M to th* puop ood oaoa* It to *tlk. for distillation of th* liquid Aroolor* th* eendmnr Boat h* ooolod *Hh water to offaot eoaplat# ooadonoatloh, latar 1* need latamitUntlp bar* oa needed. Thl* aaod la Indleatod bp flashing* la th* tight |lwi, Whloh 1* * spraying and broke* *tr*aa froo th* gltobaig* Up. then Oolld Aroolor* or* keh( distilled th* ooado**r 1* lagged and atoao la used la th* Jaokot* lowavar, *rn the** till flaoh during th* early stages of dlatlllatlon and ooo* eollag 1* aeoetiarp. thl* la aoooopllh*d bp nlxtig tator with at***. do naationad obota* all drooler* bat UW or* bloan to blending tank* to Innr* Mlfnaitp. Th* liauld Aroolor* or* treated with of dried Pallor** earth, boated to lOC^-lt^C and fllt*r*d thrwigb th* |p*rtf proaa lata thirty *r fifty gallon galenalaed dnaw ahiah ar* asad a* ohlpplng oootalaara. Aroolor* 4485 and dddO an bl*nd*d bat aot tnatod with Pallor' earth also* they a*lt too Ugh to b* filtered la Aho_ breae, th*#* or* drank eat through dlapor dloth Into golrwlaod ire oontalner*. ilno* th* oat* binding took* or* wood f*r both Ugald and Oolld th*p awt b* aerefalVy dean*4 of Puller* earth b*for* u*lng for 4405 and 5450 aad that b*for* ttlng again far th* llguld* swat b* eleened agele. droolor IMS 1* groan glrootlp fro* tb* r*o*lw*r into galeaalaod In* paa*. After thl* oolldlflo* it lo broken oat aad poekad in laok barrel*. After dlatlllatlon of th* latter drooler th* noaltar eovor Mot bo ranorod aad thl* r(**l thoroughly (loaned also* a oaall anouat of thl* Aroolor alway* ranaln* and oontanlnatloa of th* other drooler* with this would vender thaw unsaleable. A separata raoaiwar would b* wf gnat nlw bar*. IwaUlf .MOTglUldl 1. line sludge Settle* to th* botton *f th* Obergleg tank aad sonatina* plug* the outlet. This dalap* oherglag and If th* anouat *f still raalduai In th* still It low thop nap frees*. t, Fraatlag of th* otlll rooldu** nap nault froo several aauaaai HONS 052072 *. flea ohar*lng u noted ebor*. b. foreign uttar euob Iron shewing* U th* Oulaby puap Whloh will (tall the form, o. Oredual **r in th* barrel of tbs Qulab/ pimp which reduo** the op*olty thereof and thereb/ eauaee e*rbonl*tlon la the eolla. 4. Power Interruption Bear or at the end of the run whoa there la nothin* in the etlll but high aeltln* realdua*. then dietillIn* the eolld drooler* power Interruption* at an/ tine durla* the run 1* serious, a. Drawing etlll raalduee ao rapidly that the flow through the eoil* 1* low enough to oauee earbonleatloo. then a freeae oocur* due to foreign setter la the puap it 1* generally naeeaaar/ to re-condition the p\aap, asking aew ecrewe and ro-grlndlng the barrel* Thle job ooeta approxlaetel/ #100.00. In addition, all line* to and froa the puap auat be taken down and oleaned out. in/ etlll reeldue left In the kettle generally fteye aolten long enough to allow tble to be drawn off a# a liquid, goat Interruption* of thle kind her* been traoed to puap failure, and the nee of a eetlffaotory type ef oentrlfugal puap here would ellalnato a great deal ef trouble froa thl* eouroo. If e power Interruption ooeure It 1* aooetlaei poeeible for the operator to prarant a fraeee by drawing all the aeterlal froa the etlll through the value at the puap dlaeharge. Bowtrwtr, the reeldue* harden wary rapidly and the operator met work feet. I. If the eolld Aroclore, particularly IMS, are allowed to enter the receiver too hot they tend to eubllae end nolldlfy at the firet eonetflotion in the veouua llae, thue eeuelng low vaeuva. It It difficult to entirely prevent thle elae* It 1* eeoeaaary to keep the dletlllat* aolten, lowever, mob tely free thle aourea vlll be prevented If the operator eloane out the fittinge at the head ef the dew after each betoh. d. Du* to gradual ebraeion it la aeoeeaary to reoonditlon the #uUby puap onoa or twieo annually depending an the continuity of operation. The following table ehov* the footer* Involved In the distilla tion ef the various drooler*. MONS 05/073 1588 USB UK mo UK UK 4485 5480 MO - 18S 100 -U5 100 -uo US -ISO US-350 500 150 ITS XJXO 1-5 Z000 1-5 1,000 1-5 \jxa 1-5 1,000 1-5 1,000 1-5 1,000 1-5 1,000 1-5 uo -- no sa-aos 500-550 50.-588 510-545 5S5 - 5TS 850 -- 555 9T5-907 550-580 ITS-404 no-no BatQafwfi 555- SSQ III48IIM iso- an uuMpi-- p. ol r. __________ UMSU/to U5*/to os -or o-or l^KOK/K os - or UOOtl^t 3-485 0 0^*0 os - or os -or 190* C-JL P. OS - K n-T8*e. 5j. 88-80 115* C 8je. 80 - 88 048--1% Par BTr *,000 # i^ooo l^jOQO 5^000 J^OOO 5,000 1,800 Op. Or. - Hwtfii ftwitr . p. - Bold PW*t s. r. -- Wtvbi PWaA HONS 052074 9Of /O? MaMao CantoInare Toouua dlatlUod Aroelore art packed la the following typea of oontolnorei liquid Aroolerel X. IB gauge OaXwaalaed Iron Druna - SO gallon eapaolty, tej` dl*. by M.-V'd* high, with I* bung d V** want In hood. f. 18 gaugt OtlTanieod SnuBa - SO gallon eapaolty, lui length and diaaotor ee aboro without bung* but ulth If* lf-bolt eotor la hold. I, IS gaugo Qalranlaed Xroa Druae - SO gallon eapaolty, 18-1/4* dia, by 19.1/4* high with U lf-bolt oover la hood, ao bunga, droolort 448S and MBOi X. te gauge Oalvaniaad gtaal Caai M gallon oapaolty, X8-1/4* 0, t>. by S6* high altb lach friction toy. Aroolor lHil X. Slack barrele altb Xlaara. fble Aroolor la ehlpped both luap and pulverlaed, oaa euatoasr requiring tha lattar. The Billing la doaa la a awing banner will. Thla operation la wary dlffleult la wara weathor .tinea tha Aroolor taoda to aoftan and etiek duo to friotlon la tha 111 la addition to tha abort, aaaplea and Xaaa drua ordara art rapaokod la t, 4 and aa. aerow top bottloeg ant plat, oao quart and ana half gallon friotlon toy cant) throe and fire gallon friotlon top wood-eboethod ana and fire gallon oquora wood-boxed aerow-top aana. da attaohad tabla glvat the weight eapaolty of aaeb of thoeo eontalaora for the dlfforoat Arooloro, HONS 052075 SOQ Diraran md 4jou>* axmw comiwa Qtrmtm > 0*1,8 0*1. I 0*1. 10 0*1, 80 0*1, m 0*. M 0.60 0*1. 1/0*1, Hound Hound fquar* 0*1Yd. 0*1*0, 0*1Yd, Blck 8t**l 81ek frndmrt Cun .... jBm, ,gn. 0P -- Prm..item. C*a 0n Oral 8*rrl ^ul uu 5 80-80 80-80 MO 800-876 INI ft 8 80-80 m ft m 1 80-89 60-80 80-80 650 800-800 876 500-800 mo 8 80-80 IMI ft n 8 80-80 80-80 80-80 400 800-800 800 600-800 IMt 8 80 to 800-850 INI 8 80 to 400 4M( 8 SO to 800 M(0 8 80 to 800 M85 8 0 to 1141 4 8 80-80 80-80 8*8 600 1141 ft 8 80-80 80-80 800 UM ft * 8 10-80 80-80 00 UtO 8 80-80 60-80 600 lilt ft ** 8 BO-0 80-80 00 Mfhwjl 8 18 u >71 MOMS 052076 /09 bjjdoeh mu a for dlfUUlM *11 Aroelor* axoapt UM, loft boloo - Qalaty elreulatlnt pM*p< ~ Oa* flro4 oo11 beatar. loft Motor - till tank boln* loaar part of foa trap* *i*t oaotar abor# Condonaor, Baloa - Taem trap* and aorubbar*. M|H froduet raoalTar* HONS 052077 no MOMS 052078 /// or-RsTioj' o? Biuwj't pnu ir*or Ho. |*M So. _____ "> _ JU tatbee Chsrgofl .........if.'................. fWiJi Mt'd.___ IptLlMl.-------}nn<i 6UU Bottoms .. ............ petllletion Started f, B_ Det Operator _ .... Shift Ho. . j Prom A). MOO Pit To iiioo r~r~ p._j5*Ail'- -&............ *,.,,*.,,*plhljaa rged j B.No., __Aro.__ __ Reed. > ! Botch f Urum 1 Irurn f 1 Checked t . .?. 4-. .A14h>..j ._?&. Jj. ..'W&V.. i.... ?/. _ I i*i~ '1- N*j- Wi - pfo| --... --41.. ...*.. ; i: it I U-4-*4'Wt......... * ti -IU--ii ^ -*f**t. -........ ...a.. . . . . . . . -*!- . I ... A _ .. . J .L. -*rI H Mi,, 3: .11. JM UH.leVejj. MGNS 052079 Drnian did aaoook oruunw tom Tha attaohwd oiytnlnation chart how> the Ban aicoiir/ for opartln|; tha plant whaai la fill operation, Bndar tha Coda It la MCMMI7 to hart at liMt four lan for oaah Job. that* Ban work at followat hift l Ihia t Ihift I thurv Trl,.. fat. .fun, Mod. Tuta. Had. lan - 4 Ian- 4 Ian I 'Man - X Mas - T Han - 1 Kan - 1 lan I Kan> 1 Ban - 4 lan * 4 Man - t lan t Ran t Man * V Ian- t Ian - > lan I lan - 4 lan - 4 Ian - I Thla llnaup holla for tvo woeka, than tha ahlfta ohanfa foraard, mb fi taking tha placa of nan #4, oho haa baan on floating shift, nhllt an #4 taken tha aftarnooa ahlft, Ion #1 and ft taka tha aldnlfht and dap ahlfta raapectlTeljr. fhla (Iran aaeh mb an ararage of 41 houra par oaak ernr as tigbt-waek period, hut tha Internment ohaxaoter of thaaa oparatlona pamlta bringing tha aoaraga down to 40 houra la tha aourat of a pair, for oontlauoua operation It would bo noeoaaarp to hart aoro experienced oporatora to hoop tha ooarage down to fortp houra. All dap ahlft Ban am kapt to fortp houra par weak abac poaalble, but narar abort fortp olght. MiU fhla Ban lo In eharga of hit ahlft on dlphaapl and orudo aroelor production. |la dutlea art u follooat 1, loo that aufflcloct honaol for oporatlon la kept in food tanka, ( hegulate foad to ooorortar unit, I, Taka hourlp aaaploa of diphanpl-bennol aolutlon froa oolian and dotomlna dlphacpl contact, bp dlntlllatlan, thua ohaoklw oonreraiMi. 4, funp diphenpl-bannol aolutlan to banaol atlll and dlatll tha honaol 5, Operate dlphaapl atlll, 4, Operate high-hollar atlll, 7, gee that oonrartar unit taaperatura* art oorraet, I, looord all data on dlphaapl operation oa thorn on tha attaohad Optratinf data ebaat, P, farfara anp aalntananoa that ha la oapahla af and which doaa nat bare to ha raftrrad to Via Plant lalatananea Crow, fhla iaoludet ohenglng dletrlbutora whan naoaaaarp. MONS 052080 ns Ob* operator only i* aao*****? whan tb unit U ramlag awoothl? |*i to* Ban Ohould Barer b* left aloe* pb thla Job. For tht* reason Ik. anil and th* chlorUntor* or* oparatad siwultanaouily whan poMlbla, Chlarliiater Qnaratfcr 1. Puap raw ilfhajtl to ehlorlaator. I. lagulat* oblorla* flo. I, Im that ehlorlaator ianparatur* 1* oorraot. 4. Rak* danalty, hold point or *oftwolnf polat dataxwlaatloo* to a*o*rtal prograaa of chlorination. 4, fiap ohlorlnatora when bateh 1* fialahod. I. Oporato hpdroehlorle oeld plant. 1, fill aold tan* ear*. 0, deeiet wait operator whanawar naadad, 1. liiilt with, or perform aaall Baintananoa Job*. irinr IMH Opantar 1, la* that aufflelant orudo Aroolar 1* ala*?* on hand to keep Kill operating. (Thl* 1* th* Out? of th* 4*? hlft nan). t. Obaif* waiting tank ablob auppllaa erud* to otlll. t, trnnofwr finlahed hatohao tram raealwar to blandIn* tank*. 4. fill shipping oontaiaar* with finished Aroolor* and otor* fIliad oontalnor*. I. Kaap pr*Bl**( around *tlll and aeo***orlo* elvan. Balwar* 1, Charge Bolting pot with diphenyl for chlorination, ti Pro** owt diphenyl fron pan* after dlatUlatloo. I. Peek diphenyl for (hlpnaat, 4. Padk and ator* erud* iroelor*. I, ftandlo orud* Aroolor drua* for distillation, I, lalp fill aarbor* with kydroohlorle acid. T. S*ap praaltai elaan. MONS 052081 ft4 tradar AH88 Owritor* laa that atlll oharga* *r# broken ap, rairbad eorraotly ltd Cbarfad to tho (till*. Th* day oparator ho* too h*lp*r* that ohz*a* for oil thraa phlft* nay to broken out on th* day *H1ft. It Qp*r*t* atlll* and fl*kr. |"l*h on* lalfar* of Onaratnr* to hgr. lilt, tho operator* la dltill*d Aroclor*, both b*d**r and IW. M|a to doTMop wnn typ* of doimotltlo. At that tin* oonttUtion faellltl** in both operation* nor* no*t Inadequate and th* mb nor* oxpofod to du*t and Aim fron th* hot drooler*. Iorar, **r*ru of th* >w had boon anbjoot to th* tut axpofur* for thro* poor* prorlou* to thi* and bad tafforod so 111 *ff*ct*> At about th* **m partod th* olootrloal proportion *f tho dl*tlll*d Arool*r* bocui t* fall bolo* ipoolfication*, tbarofor* It ** umm(I that *o* lapurltfi hlthorto not proaact, no* e*u*to| th* trouble, Xv**tl*atloe ror*al*d that th* banaol thon la ua* Oontalnod approolablo fuantltl** af paraffla, uhlab ubn pyrollaad with banool produced at/ran* a* an iapurtt/ la th* ilphauyl, Vhan tb* diphenyl at* dhl*rlaat*d# *kyr*a dlehlerldt **l al*o f*rud< Thla oonpound 1* txoatdiafly anitablo, giving op hydroohlorl* aold wrj readily, to* th*orp developed fro* th*** finding*, and alaot eortalaly bon* oot bp *lrouMtano*| *** that th* atyr*o* dleblorld* ontorad tb* r* *f th* akin with Aroclor Taper and finely divided duet oboro Jt d*oo*po**a, Tb* aold forBod noted a* an irritant! lafootlon a*t la and th* afcla d|**a* rowltod, tola *p*olallt* oaro eoneultod, but our* of th* dlioai* ua* found to b* alo* and dlffloult. th* oonpany b*oaa* involved in an oipocilva litigation ainoa ault *a ootorod by tb* naj orl ty f th* m *ff*et*d< A* a remit af thla trouUa th* follovlag pr*o*uti<mary na*ur** oar* taken, 1< All affaotad B*n oar* renovod fro* th* *p*r*tl*n end a* nn *ub*tltut*d * rapidly a* thay aould b* trained. It Adequate Vantllatlen faollltla* *r* installed, HONS 052082 I, A eoaplata ohaofa of elaan elothlr* aaa and atill la furnlahad to tosh Ml dally. 4, toaala, aoap, aloohol and oold crou ara alao furnlahad, taeb u if raqulrad to rub hi (ici, nook and ini with oold eraaa bafora join* to fork and to taka a thoroufh bath and rub klaialf with aloohol aftar work. I, Tha Ban ara axantoad rafularly by th Plant Pbjralelaa. I, to wan who ahowt a tondeney to daHaatltla la mplojoi In tha Papartaent. T. >414 apaolfioatlona wara aat wp for banool ao that thara could bo no raooourranow of atprana. la a raault of thaaa praoautlona thara haa boon ao rooecttrraoea of daraatitia anon* tha oparatora. HONS 0S2083 PrPHE'tfYL ffMD /7OCiO OPSP///ZPT/ON CHfi/T* sc/rcjersce* is/r/tzen. foa&*#.Yx n : ptp*en*i unit ' 5>otrot. 'cnt *t* tut. sh. CfiCOKiNPTOJt OraetmoK k>s fit/t ffMtOtfir i ; /rue ficrg \e* m Miroturi; j--------- -------------SriCA Mumt 9/r.<3*rr ! 1263 orererot 'vntrtt 9fit.sJtr \n*0/m.pB<>* '>aryfit>rrr-#*c ozz '<1*03-0*1 OKC0t\ ) Fmtrrt/ffinee /f*zz\ * zrwo ! \eott/f Orazrro\ t &*? Jtnrr mer 1 A- nto Nmv | HZ*SJtS i D/rr &rr Ozny\ SzzzfiPBt i u'/tzaron-ztetztoX Dor Shot 9*V } ' Jjrmo*rtfPN 1 . ncero I ; O/ry Szt/rr Ozvr MOfcS 052084 M& NOXMO, OABKKTS AND OTHKB A0CH590HE8 V8KD 1* DIMS)XL AND ABOOWN BANUFACTUiA flaati* lit. 1 OwniHttl fiQBMr Allmtai MiteSuUt&t Him 1. Baphlagnatlng Colons lead and Bottoa t. Daphl*gntor and Oondanear Flan*** Bonaol Still flanga* 4. Mphenji Still flanga* I. leotrodryar Cooler and Oondanaar Flanga* I. Sigh Bollar Still flaocaa T. Flanga* on Ohlorlaatora and trap* ti Badger Still flanga* l*hn*-B*n*lll* Citrlaae - Stria flT la Baoaal Snap* la Ooll Qland* an laetrodryar la laad* aod Bottoa* of Daphiago*tor and Oondanaar la Otlaa Baad on kaoaol Still la Oolnan Baad an Dipheajl Still 4a Oavar and flat* an leotradryar la Oalwn Baad an ligh Boiler Still la Ohlarinator Baad* and Dlatrlbator flan*a* Ta Iran flange* at bell* 00 Sal Ooolar (Ooattt la, t Ooppar Aabaeta* Saalcet* *r* raoonnandad a* raplaoanent* at all the** paint* except T and 8.) HONS 052085 N6 Dilated libeltoa Bona 1, BeHlagrot and Bloving Task Covers t. Tatar Bland on lei Cooler I, Oyllndar Beads on Chlorine Vaporiser 4, Cover Qaakota on ltd* Distillation foti I. Oorar on Badger Still Charging Pot Congoaition Paoklae - Manhattan Buhhar On. 17 Olaaa Oaqgaa on Toad and Buw Tanks I. 0>Bonds so Ooolar Tubas - Bol flent lai^nt Aabaatfti Jaakat Tana /64S - flountr 4 Tana larduare UnJ. 1, Bsads OB Isnsol Btill Btoaa Ghost. Anatelaaa Boaa 1. Beoeivar Cover on Bigh Bollor Btill stau-N>TiUa W-JmUXjQgJtaoXlat . . I. Csatrlfagal Poops Bandllng Orudo droolor and Diphsa/1 I. Jaarloan Barsh Centrifugal Puap on Badgor Btill lot Aroolor eiroulating Boston. light jar on Badgar Btill Ibaorbors and Coka Tonars - Bol Plant fttttlJu&tt l. Dust Oollaotor flanges and Cons above Oollaotlog Barral t. frap Oovar os Bigh Dollar Btill I. Oovar oe Badgor Btill Baoaivar iahn Crtpa Stela ISO Matain," V*1H 1 Dulnbj fmf packing (Badgar Btill) fltrlstt Mir. litilrtaf ,. . X* 0ra* fttgrisdftbl* lil ?!** cm Oblorlxit Ttporiter oba and Bata Taira Itana other than thosa alth ragrlndabla seat, Planetar HONS 052086 Coke 1. Toaers at Bol Plant t Bold Trap* oa badgar Btill HONS 0520J BEAT BALANCE OB fW*OIt MUU , CONVERTER BNXT HONS 052088 . BUI 121 i teat od the 6 Pot load bath Diphenyl Unit woe Bade oo lay . 1856. Ihr purport of this test a to uncertain pertinent foots regarding the host bnlanoo oo tho basis of presont operations. The faots to be broocht out by this test ware desired to supplylag data for the design of o Bare offioient dolt. The test lasted 6 hours froo Pi46 A.l, to 5l46 P.M.(Hay , 1086) sod the followiog determinetions wore Bade, It Oas Consumption t, Temperature of the Ben sol at various points Teaperoture of the lend in the pots Taaperr.ture of the side walls of the Unit ot Various points Teupert.ture of Combustion Oases I, Anounts of Bensol fed end returned end production 4. Braesurer in the various pots. tbs sttsohsd Print gives s oleor ploture of the heat balance showing the heat distribution sod tho tooperatureo of the gases at lnportant points. Toe efficiency of the Pnlt os operated at Annintoe Is 45.8Q. based on t consumption of , eu. ft. of gas per lb. of processed Bensol. It other words 46.8)1 of the total heat content of the gas is found In the gssss leavine the converter. The figures weed for the theraal properties of Bcarol ere based on the formula given 1b Perry's Bnodbook on the bottoa of p ge 649. lo data war evellablw to check the formulai 1. Cir ConsOTPtloB Converter pot - burnere on and off Preheater Mo. P-6 * s s Preheater Mo. l- * continuous Total bow heating value of gaa Total beat In gas 674.0 ou.ft./hr. 660.0 * MiL 176.0 HONS 052090 60.9 t cal./ou.ft. 1,161.940 lb,cal,/hr. fiX i. ImbwAiitv. Hecured Beniol leering Vaporiser Preheater fX *H Converter bond Breheater #1 * it Converter 156, 870 625 720 417 By aeana of Tapnlog 720 845 After checking the Inatranents nnd on the bed* of the requlrenente of U( beet balance, the following toeperetare* eere ohoem for the bmeol it rerlour point*. Bwoeol Fend Beoeol leaving Teporleer * entering Preh*(.ter #1 * leering lend Briber.ter #1 * * Breheater i\ * entering BreHester ft * lenvlng leed Preheater ft * leering Preheater ft * entering Converter leaving lend Converter * leering Converter ftenctlon oeeuieed to take piece 9 5C 186 1M (2 drop In plpo) 417 570 564 (8 drop In conn, pipe) 710 650* 622 (6 drop In oonn. pipe) 851 750 780C The reading of the Tepelog et thle point nor S25C, but war found to be la error. lenperature of coaburtlon gsaee before and after the raporleen Before 860*0 % C0,, e.S 0, 9.82? (80? Exc. Air) After 2660 Imunijrjwa Mi Mim.lt fraSwsMSB Aeounte of beneene fod returned proeeeeed 881#/hr, 607 2(4 Broduote Peecured 228 91? Biphenyl ft U.B. 9? Beneene Hydrogen (onlculeted) Beneene oarrled by Bydrogan(Celo.) Total Broduote neaeured ft oalo. Bnnooonntod for 208 20 5 25 268 28#/br, HONS 052091 Thor* one * well leak on top of the converter ehlch eight exp] (iIn the dlffereaoe. 4. frerWP# Item th height of the lend Id the 5 pole the proesure oan be calculated. fit height of tho lend one not aetrured but Uke from operating data. Top of Converter Vrei aura of Converter 80* of lead Calculated 1 lb. ,16.8 lbe feWJKlfl 1 lb. It top of freher.ter tl fr&pnuro of Vreheater #S 45*of lead 16,8 16.6 At top of frohMtor #1 Frepruro of Frohonter #1 47" of load 84.7 1M 87.0 Treasure of fead line 65.4 40.0 Tue teaper>.tur of the Beniol leaving the Vaporizer ear 156 oorrerpondlng to 68, b aboolute or <5.1 gauge. There le probably a Mall error la the tampert tare rending and parbapa alao In the height of the lead an reported. TVl/J 4/18/86 MOHS 051092 TYPE S44A MEGOHM METER *R-El 4I-MfEttM#4 II *MA *R 4t i 1w04onA P-* 0144 1 4*4 ll<ISSO 40 A lIN<.(Kft*A. A. f II mO *A ItlH4<'IINOOlMA MMstRMurrs n the abboci or ciriciTiKE m imAnow ronmcLs 1. Iutill kitUrUi or pomi^ppl; ualt tod tuboo aa doacrlbod 1b ooooapanflng laftruottoa book, pogo t Ifcrw OB-OFF itllob W OB oad volt about too alautoo for tub# to t op boforo bogiaalaft aBOouroaoBta. 9. OosBoet nbMB roolotor to 1* toralsolo Mfctni the "blgb-potor- 1* tiro oo abort oo pooaiblo* Tio or throo iBoboa la ootlofoetorp. 4. 8ot oootroi knob (ohecb-owmib-cbjwoi) to emou V 9. Tura 900 APHBT kaob until golTOBoaotor roado Boro. If tbo 0 or adjuotaoat to liooff^tliit, oieoootva H or o- ttUin plekaf proboblj jroooat la tbo roolotor. If tbo aaro drift# otoodlij la tba dtrootloB, tbo fraooBoa of bopaoitaaao fa tbo takatn roolotor la loatol. la oltbar oooo, rofor to tbo jroooduro ftroa la tbo lootrar- a boob, pogo 4* . ' . .. 6. Tura oootroi ksob to OP0ATE aad odjaot OLTIFLIHt rrtWb aad OHIO 4U1 fw Mr* r**41at of idtaint*. T. Roo< r*l*tMO* fa Mfoha* fra. 1000(90 01*1 *d tb* WLnPllR W. . 0. For mott **ur*t*. Ittoialiitlooi raehaok tb* falvaixmlMr Mr* 1* 4 U< ft (bo*** . . . MGNS 052191 2/9 ** i . . Sabalauoa til* HBOOaB Mai a4 r*4 ah* rattalt 1* T. 10. If Mm MOLTlFLIffi ia U tin 100 ar 1000 F*ltloa, aulUfl; malt %j 1.00 If as aaauraay graotar than lof la laalral. for ratmR iworjutioh ui thk mamoorit* booi HOMS 052192 \4 HV HI C6T?S0 SNOM WOTIOI t II. RUMD triCiriOATIOIS mil CB1M10A1 OOMMJTC HSMOTIM WAMMBU HONS 052194 Standard specification The Swann Corporation Code No.__i40Ulrll5.4-_l_______________________ Gnd.^--AJL -PggOttP.4. Igi. 1476_______ --------------- Date Authorized 4/4/55 Supersedes Specification Dated________ Tolerable Limits Typical Value IN Swann Ohamleal Ooapany ahall tut eaoh 3500-pound batoh of 01476 Mia far sblneent to Plttaflald and ahall forward their teat data tfrteblerastein. t two-quart advenes eaaple for our Laboratory analysis Ika following art tha ehealaal, vhyeleal and eleotrloal apaolfioetlons lUth auat ba nat by the Swann Onealoal Company j . .1**Burn Paint ( 90(iSdlSi^6 bwttr fywaaattaflremi un*.A8&15MO0D(B-Wef7e-r5re0Td) te fear Paint P-97) Blgher than 350*0. 46-49 aaoonds 8 ayboIt Universal. Olor (SPA) USB Natbod S laidity UPS Matbod H--- 616) Ofclerldea and Balshates (ism D117-3D Iraporatian at 100*0. for 6 bourn (OB Satbod H-5955*) Laaa than 1. Ltaa than 0.01 ag. MaOB/gn or aampla Kona Laaa than 0.4JC Distillation Rang* (iSM D-*0) 10JA Point 50* Point lability 90S Point Tbara ahall bo no llbaratlon of oblorlna or oblorldaa aban tba notarial In beatod at 100*0 In glaaa vaaaala In aontaot with air for parloda of at laaat ona aonth. riaad Oblorlna Oontant Bseletlvlty at 100*0 undar S00 ToOllta .0.(Bleotredes-brewlng "b-'155?663) Aging Obaraatariatloa at 100*0 rer 96 boura in air 53 05* Oraator than 100 z 109 ohn/en3 Mo leas In raalstlvlty ovar original valua. Nalaatrla Oonatant at 100c 4.15 - 4.35 (Matbod H-3955871) blalaatrla Strength (4S1X D-II7-3I) Mot leaa than 30.0 kilovolts Approved by______________ Chief Chemist AA pp..r.o...v..e..d' *by_ Sales Manager MOWS 052195 Approved by Works Manager Authorized by_____ Chemical Director Standard specification OF THE SWANN CORPORATION ProductWlMi*4J?lphSSlX_Sffli*Code No.._l4OU0ilU9 Grade: 0 m Control Tftt B * HitOry Tfttt --:Date Authori*ed_?*?i!--i?/-?3/3 Supersedes specification Dated---------------- ---------- *_ Tolerable Limits Typical Value 0 8p. Or. at 65/65*0 Waatphal t i Ohlorlna 0 AolO Huabar, 14ga KaOH/ga 1.13*6 * 1.1576 - HONS 052196 Approved by__ -_________________________________ Chief Chemist Approved by Sales Manager Approved by--____ Work* Authorized by----------- ------------------------------ --------Chemical Director 2Z4 STANDARD SPECIFICATION OP The swann Corporation Ptoduct :__0W.Srla**4 _Dlj?h*nyl, OwA*------------------ Code No_140U0raU2------------- (Jude:. Afoulo? 1142------------- -----------------------------------------Date Authorized-?* fttj_-12/23/32 0 * Oontrol Supersedes Specification Dated_____ _______________ 1 m Heitor? T#*t Tolerable Limits Typical Value ( 6p. Or. it 65/65*0, Vtatphal 1.373 - 1*378 I f Oblorln* - 0 Aol4 Number, Ms* HaOH/ga - 0 Oontaalnatloni Dlpb*nyl Crystalline Aroolor Bon* Bone 42 i. 0.5 %ioved by__________________________ __________ Chief Chemist HONS 052197 Approved by-------------------------------- -------------------S*le Manager A|>|>rovc(l by_____ _________________ _____________Authorized by---------------------------------------------------------- Works Manager Chemical Director zzr Standard Specification or The Swann Corporation MlH. Chlorinated Dlphtnyl, Orate__________code Wf. 140110-1148 finrtf* Aroolor XX48________________________ Date Authorised Tent. 0 * OOAtloX Ttlt 0 m Hittpyy }0gt Supersedes Specification Dated_____ Tolerable Limits Typical Value 0 Bp, Or. at 65/65o, Vaatpbal 1.438 - 1,440 1 i Chlorlaa 0 AftlA Buabar, Ugm BaOB/ga - 0 Ooataalaatloa; Dlphaayl Bagatlva Crystalline Aroolor negative 48.4 - 48.5 Approved l>y____ Approved by. Chief Chemist Approved by MOHS 052198 ~Sa1e Manager Works Manager Authorised by--------- Chemical Director Standard Specification OF THE SWANN CORPORATION Mud Ohlorlaafa Aroolor, Oruda__________ _Code No.___ 1401X0-1150 Mr AmIuf 1150___________________________________ Date AuthorizedJdltj 15/ 2}/}C 0 Control TOOt Supersedes Specification Dated------------------------------- B * Hlotory TOOt Tolerable Limits Typical Value t 8p. Or. lit 65/6500, Vaatphal - I $ OhlorIna - 8 Add Kwrtar, Mg NaOH/p 4- 0 Oontlnatlon: Dlphanyl Hagatlra Cryatallin# Aroolor N*gat It* 1.45 - 1*455 - nuved by. Vprevcd by____ Chief Chemist Approved by. HONS 052199 Sales Manager Authorized by__________ ______ ____ __ rkfmiral Dirfclor r................. ................................. ... ......................... ~ ' 117 Standard specification or THE SWANN CORPORATION -orl, Qhlorlnatod piphanyl. Orudacode No________________ 14PllPril54------------ *^JLroolor A154 jl - Control Tost j. Blstoxy Tost j ______________ Date Aulhorized--TSnt . 1Jt/Z$/3 2 Supersedes Specification Dated------------------------------- Tolerable Limits Typical Value L Bp# Or. at 65/6500, fcctphnl 1*554 " 1*559 jl i Chlorine If ieii *ub*r, lie> >aOB/0i e Oontaalnatlont Diphenyl 1 Orystnlllna Aroolor i lagntlv* Nsgntlva 54.J to 55.8 Improved by______ Chief Chemist MONS 052200 Approved by------ Seles Manager farmed by--___ --_____________________ Works Manager Authorized by---------- Chemical Director ZZ6 STANDARD SPECIFICATION OP The Swann Corporation Product;-OhlerlHAttA -DlpbUUFlj -GtUdfl ____ --Code No.. 140115-1160 Grade:___ilO(ln ll60Date Authorized--Tent. 12/25/3 0 Oontrol Tail B History Tost Supersedes Specification Dated_____ ________________ Tolerable Limits Typical Value 0 #p. Or. at 90/90*0, Vaatphal 1.613 > I.618 H 1> Ohlorlne - 0 Sold Muster, Mss HaOH/fea - 0 Contaminations Dlphsnyl HogttlTS Crjratalllna Aroolor HegatlTa $9*9 to 60.3 .12 to 1.29 Approved by. Approved by MOMS 052201 Chief Chemist Works Manager Approved by----Authorized by___ Sales Manager Chemical Director ZZ9 Standard specification or The Swann Corporation product :_Qhlerlnat*4 PiyJayl_Cni4*________ code no___ U0ll0-ii6g_____ Or.d.:_-jtoOlr_ll62______________________ Date Authored 0 m Control Toot ' Blatory Toat Supersedes Specification Dated Tolerable Limits 5* ,_______________ Typical Value Bp. Or. at 90/90*0, Vaatphal 1.657 - 1.64s ft Chlorine - Aoid Buaber, Mgn XaOH/gn - Contamination: Diphanrl Hegatlva Crystalline Aroolor XogatlT* 61.7 - 6s. S6 _ - HONS 052202 Approved by------ .------------------------- ----------------------Chief Chemiit Approved by_______________________ _____ ___ Sales Manager Approved by----------------------------------------:-------------- Authorized by__________ Work* Manager Chemical Director ISO Standard Specification OP The Swann Corporation Product 0hlorliit4J>lpb*PllJCn^----------------------- -Code No------------14 0110-use _ Grade -- ArooXor 1166 Date Authorized _!/J/M-- 0 m Oontpol TWfc g m History Toot Supersedes Specification Dated------- Tolerable Limits Typical Value *0 Bold Point, 00 H Ohlorloo, % 0 Coatoalnatlon: Diphonyl "145 165 - Bogatlvo zohangod from previous spoolfleatlon. x57 6736 MCNS 052203 Approved by. A. B. Porto r_________ Chief Chemiet Approved by R. B. Colo Work* Manager Approved by .Botort 8 Wotherly Sale* Manager Paul Logua Authorized by---------- Chemical Director Standard Specification or The Swann corporation j*rt L, gwutoCode M,, U0U0-U69 l - Control Toot i- BUtonr not ------------------------------ Date Authorized___ 7/3/34 Supersedes Specification Dated._i*/o/3t__ Tolerable Limits Typical Value 10 Hoi* Joint, 0 I i Ohlorln# 0 Oonto*lnntiont Dipbonyl 885 - 850 Begat *40 68.8 *0bns*4 from previous speolfleati on A. B. Gorber Approved by. Chief Chemist B. B. Col# Approved byWorks Manager HOMS 052204 Hobart S. Boatherly Approved bySales Manager Ptul IO0U Authorized byChemical Director JCJHL STANDARD SPECIFICATION or THE SWANN CORPORATION Mct . Ohlorlnntoa DlphonjItHB Mix Crnle No___I401l0-t?6^ ante--Aro olor -*565 _ 6 Oontrol Teet B * History Teat -Date Authorized-Tent iB/ej/j* Supersedes Specification Dated- Tolerable Limits Typical Value 0 Softening Point ,<?, Bnrrott B Softening Point,C, Dj6-*6 B f Chlorine 0 1014 number, Uga NaOH/ps 0 Blooming Tost, 5 maeka B ions at l6}0, D&-17 B Bp. Or. at 5/50, D?0-*7 B f Iron 78 * 3 - Ne gatlr# - 79.4 70.0 64.9 0.3 - 1.0 3 1*733 .11 Aroolor *565 la tbs pro duet of chlorinating Onids High Boiler and Diphenyl (45*79) t 5S 01. A|i|irovcd by Approved by Chief Chemist Works Manager Approved by Authorized by HONS 052205 Sales Manager Chemical Director Standard Sopr ecification THE SWANN CORPORATION l'roducl :JBfeiOJCinjl ted Dljpfe9M.it Hg.|llx_.CrUfl9_Code No._____140110-4065 Grade.. ArOOlOr40>5... 0 - Control Test H - El8to 17 T#8t - --Date Authorised.. - -7/5/54 Supersedes Specification Dated______ Tolerable Limits Typical Value *0 Soft Point, Barrott, *C Std. at 76 _ *00 SB * Chlorlna 64 - 64.6 >10Id Nubbar, Hgn laOH/fpa 0 Contamination: Dlpbenyl Begativa Crystalline Aroolor * 77.0 64.5 .42 Aroelor 4065 Is tbs proauot froa ohlorlnatlon of a mixture of dlpbenyl and distilled high boiler (60:40) to a Barrett softening point of 780c +, 2. z0banged froa previous spoolfieation. Approved by--A* r .................. Chief Chemist HONS 052206 Approved by Bp_fesrt .6 WSStharlj__ Saks Manager Approved by------BiJRi i?Pl?------------------------- Authorized by___________ PWl Works Manager II .. _______ Chemical Director Z34 Standard specification OF THE SWANN CORPORATION product Cridc :_.^ATDOlOr -5Q6D.__________--______________ ___--_____Date Authorized 0 m OQDtlOl T#it g m BlPtOry TPSt Supersedes Specification Dated--------------- .------ ------- Tolerable Limits Typical Value 0 Boftanlng Point, Barratt, C 118 t Tant, B Jf OhiorIn - 0 Bold Humbar, Mgn HaQH/gn - 0 Oontanlnatlom Diphanyl KagatiTa Crystalline Aroolor Negative U7 59.9 - 60.t z.t Aroolor 5060 la dlatlllad High Boliar ohlorlnated to 60% 01. MONS 052207 Approved by___________________ _________________ Chief Chemist Approved by------ Sales Manager Approved by------------ Works Manager Authorized by____ Chemical Director Z3S- STANDARD SoPrECIFICATION The Swann Corporation Product:..fiklMlftfAsftJBlphsnjlj. Matillad ----Code No. U0111-1242 Cr.de ----------------- Date Authorized___ 7/5/34 -___ 0 OOlltrol too to Supersedes Specification Dated./3/j*_. vMafc ara to fee aada on avary lot* Tolerable Limits Typical Value 8p. Or at 65/65*0. Waatphal Bp. Or. at 25/25*0., D70-27 1.368 .005 Lovlbond Color, 1", Tallow #510 Tour Faint, oO., 97-iS Vlaooolty at 98.900, 988-26 at 54,1*0 37*8*0 0.1 > 0.5 50 - 53 Dlatlllatlon Ranga, P20 lat drop, *0 lOf % 28t 310 - 315 335 - 345 Ooaff. of Rxpanalon Flaah Faint, 00,, D92-24 lira Folnt, 00., 092-24 * Loaa on Boating at 165 0., #6-27 Rafraetlva InAax, 20*0., D-llno 0 gold Viaibor, 1191. Va0B/fn .01 Mar. Baalatlvlty at 100*0., SOOrDO, 01m-on Rlalootrlo Oonatant *t 100*0., 1000 ops. Faoar Factor at 100*0., 1000 apo. 1.6269 - I.6285 100 to 300 z 10? - 4*94 to 3.0 z01iaDgad from >ravloua apaolfloatlon NONS 052204 Approved by--Ai _..Qarbjy________ Chiel Chemist Approved by Robart s Waatharly Sele, Mti.|er Approved by___ R. B. Oola Work, Manager Authorized by. . Fll lOgua ....... ........... Chemical Director 23C STANDARD SPECIFICATION OF The Swann Corporation product :_0blOXlnat94 DlskMUl, JJiatlllad_____ Code No.___ 140111-1*48_______ Grade:_____ASBS.l9. JU4(L 0 - Oontrol TOat -Dole Authorized------7/3/54 Supersedes Specification Dated__l?/r3/3^______ 1 - Blttorr Tatt Tolerable Limits Typical Value 0 By,Or. at 65/65*0, Vastyhal BSp.Or. at f5/*5o, D70-*7 1.435 1 .005 1.459 0 Oolor, Loribond, 1", Tallow #510 B your Point, o, 097**8 >6.6 B Tiaaoaltp at 98.90 36.6 >0 Viaaoaity at 54>40 Tisooalty at J770 73 * 80 83.9 *18.0 B Tlaoh Paint, *0 193 B lira Point,0 B ft loss at l650, 6-7 0 Bold Busbar, Men BaOE/en 0 - .01 .005 B $ Prat chlorides B Distillation Bang*: D*0-*8t lot drop,*0 104 M504 *Ohangad fro* pretlou. speolfleation. HONS 052209 Approved by__1, J3.JI*xfcer Chief Chemlal Approved by_Ba JRa-fi&lfi----------------- Works Manager Approved by_ Hobart 8. Weatherly Sales Manager Authorized by--------____________________ Chemical Director Z37 Standard Specification OP The Swann Corporation a 1011-1*49 m-itsi__________________ Aroolor 1M9 Grade:-- .Aroolor .1851---------------------------------------------------_Date Authorized______________ _______ Supersedes Specification Dated_____ _______________ Tolerable Limits Typical Value Aroolor* 1849 and 1851 or* sot likely to b# uii dlreotly In the future but only by blooding 1848 and 1850 or 1850 and 1854 roopootiToly. Tbo tost* to b* ndi on th*ae Arooloro, homer produood, aro tbo aone as for Aroolor 184&* Bpoolfloatlon limit* oannot bo laid down until history Is obtained. I I Approved by . --.. ____________________ _______ . Chief Chemist MONS 058810 Approved by----------------------------------------------------Sale* Manager Approved by. Works Manager Authorized by. Chemical Director X3 Standard Specification or THE SWANN CORPORATION ,,*rt Ohlorlnatad Plphanyl Platlllad -Code Nn U0Ul-Xt50 Aroolor lt50 f * Oontral Taat I * Hlatory faat -Date Authorised-- Ttnt. Supersedes Specification Dated- Tolerable Limits Typical Value (Spi..Or. at 65/65*0, Vaatpbal llp..OOrr. at *5/5Cr D70-J7 I So>llaarr, loTl&na, 1*, Yallov ^510 ITlaooalty at 9h8.9*0 inaah Point, nc, D90-04 I nra Point, ao, P98-t4 lioaa at 16$ao, #6-1? I Poor Point, ao, 097-06 0 laid Innbar, >4* iaoi/ga ijTfrao Ohlorltaa 1 Mat Illation Panda, D80-|8t lat drop, *0 W# 59* .01 Max. 1.446 j8*3 B#o* 97 BM* 3IS 6#Oa 190 - 196 Koqi at 340 0OO4 a A|rproved byApproved by Chief Chemiit Works Manager Approved byAuthorized by HONS 052211 Sales Manager Chemical Director 233 STANDARD SPECIFICATION or The Swann corporation I'roducl :_GJlorlnat*a PlpMnjl., Planned___ __ Code No__ 140111-1262 Grade 1...... 8*2*lLl*6*____________________________________-Date Authorized.. JMSk ......... 0 Control Tost H - History Tost Supersedes Specification Dated__ 11/23/5*___ Tolerable Limits Typical Value H8p. Or. at *5/*5C, D70-27 0 Bp. Or. at 90/90*0, Wsstpbal 1.631 .005 *0 Lorlbond color, 1", ysllow 510 .23 - 1.00 0 H P A Color H Four Point, *C, D97-28 H Tlsooslty at 98.9*0, 1)88-26 88-98 H Plstlllatlon R*ng, D20-*8t lat drop lOjf n Bad B Oosff. of IxpanaIon B Los* at 163*0, D6-27 B Hsfraotlv* Indoz, t0*0, D-llne *0 Aold Huabor, aga BaOE/ga 0 - 0*01 % Ohlorln* B % Fa* oblorldaa *0bangd froa prorloua spool float Ion. 1*648 - 1.638 1*633 ~ 1*638 0.4 - 1.4 34.9 - 38.0 91.3 -103.0 |:1 .48 - .56 1.6501 - 1.6517 *0048 61.4 - 61.5 HONS 052212 , A. B. Oorbar Approved by_'_----------------------- ---- - ---------- Chiet Chemtdl Bo B* Colo Approved by _ . _. Works Manager Approved by_ Bobert 6. Voathorly . - .. . .................. ........... Sales Manager Foul Lofcue Authorized by............... ... Chemical Director STANDARD SPECIFICATION or The Swann corporation Mud :_BfelXA8*te(LMpMSTIj JDisliil* 4___ Code No. l4QlU-64____ Me drooler lt64Date Authorized--------^ Q * CO&trOl TOOt | ^ JtlOtory Toot Supersedes Specification Dated_____ Tolerable Limits Typical Value I Bp.or. ot *5/5C, D70-*7 0 Dolor Lot1bond, 1, Tollow 510 C Softening Point, Borrott, *0 1 Softening Point, V)6-i6-*0 I f Loot ot 163*0, P6~ft7 0 Add Vunber, lev BeDH/g* drooler IT64 lo In ozporlaontal stage ohoro roqulrenente oonnot bo epeolfled. If further produoed the otove toots ere deslroD, Approved by--_________________________ ________ Chief Chemist Approved by-- Approved by Works Manager Authorized by______ HONS QiZZIZ Sales Manager Chemical Director Standard Specification OF the Swann Corporation Product JUcUlllA_______ Code No....... 140111-1*68____ Grtdc : 0 * Control Tiftt I - HI*to 17 Mat ___________ --------------------------- ----- --------Date Authorised 779/51 _ Supersedes Specification Dated____________________ Tolerable Limits Typical Value 18p. Or. at *5/*5eC, Pyoonoaater If to** at 16500, s6>t7 t Aold Nuaber, Mg* NaOH/ga *0 Bold Point 6 Color t 1* oube not groator than .05 Max. 135 - 160 8 tandard 1.804 * 1.811 .15 - .4 140 - 155 xOhanged from previous specification. MOMS 052214 Approved by___ ____ 11 Q^rbe T Chief Chemiat Approved by Re R. Colt Works Manager Approved by____ Bobtrt s. Waatbarly Sale* Manager Paul logue Authorized by______________________ ___ . Chemical Director TWZ Standard Specification OP THE SWANN CORPORATION Mud Chlorinated Diphenyl, Plat Iliad____ code UP111-1*69 Me A*S> 9l T 1?69 W#teijiuenell*aDate Authorized___________________1/9/34 .. - 6 * Control TOSt Supersedes Specification Dated--IZ/Z^/^t_____ 1 - History Tost Tolerable Limits Typical Value B Bp.Or, at 15/250, Pyonomatar ' Blata at 163O0, d6-*7 % Hold Point, VO 0 i liolatura at IO5OC *25 - *55 0 - 1.0 1 Molftuta Ttatt Pry 10 grams in no1 Bture dlah at 105C for 3 | bourn or longer. *Qhangad front praaloua a pool float! on. MONS 052215 Approved by------------------------Chief Chemist Approved by--SPA---------------- ------Works Manager Approved by-- hsAy-- Sales Manager Authorized by______ ?ftnl __lPgUft--------------~ Chemical Director 24S Standard Specification OF The Swann Corporation ProductDiphfnyl PlatllladCode Mn U01ll-l8iq__________ Gr.dc : _ATttel0r Tfil9----------- --------------------------- Date Authorized- iMt. Supersedes Specification Dated__ ___ ______________ Tolerable Limits Typical Value Bp. Or. at e5/5*0, Waetphal Oolor, I/orlboni, 1, Tallow #510 rraasiog Point, *0 Flaah Point, 0, D98-*4 lira Point, C,D92-24 Sadlnant Ald nunbar, agm PaOH/cB 1,15 14.0 158 177 iona ,005 All of tha above ltana ahould ba determined on every batob until history la obtained, Aroalor 1819 la a autaotlo Blztuxa of para S5Jl and ortho 75S ohlorodlphenyl. Approved by____ Approved by MONS 052216 Chief Chemist Works Manager Approved by__ Authorized by____ Sale* Manager Chemical Director 244 STANDARD SPECIFICATION or The Swann Corporation Chlorinated Diphenyl, Distilled___ __Codc Nn 140111-1848 Grade AXOJdlPJT _l8d8#- Cfilllft IQA _4W00tt------ Date Authorized--ISUt.* -U3l (M^ontrol Teat Supersedes Specification Dated___ ________________ Tolerable Limits Typical Value 0 Distillstlon Bangat D20-28T but oorraoted tor anergant a tan of tbaraoaatar. lot drop, *0 10)( M 0 Bold nunbar, apt NaOH/*n 0 Color Lowlbond, 1*, yallow #510 0 Sp. Or. at 65/65*0, Woatphal $: $ 1.453 Aroolor 1848 la a Biddle aut from the distillation of Aroolor U48; it is a firaotlonal portion of Aroolor 1248. Approved by_.~---------------------- -____ __________ Chief Chemist HONS 052217 Approved by. --------------------- ----------- ------------Sales Manager Approved by. Works Manager Authorized by_. . Chemical Director 24* Product Standard Specification op . The Swann Corporation HB MixCode No____140111-4465___ Grade:_AJOOlOX 445Date Authorized_3#llt H/ij/jl 0 OOBtWl Toot Supersedes Specification Dated------------------------------- | m Bli%0V7 T#t Tolerable Limits Typical Value S BgL. 0 Lorlboad Odor,!*, TiUwl$10 0 Boftonlng Point, Barra tt, *0 1 Softening Point, 0, DJ6-16 I Ooofft of Ixpanolon I % LOOO ot l6j0, Vb-tf B Bofraetlvo Index . 0 Aold Hunter. Men Hoce/m 0 0(7* toll loot Ion Toot (Boo tolow) 4.3 - 6.4 71 - 76 0 - .033 Mono 1.71C - 1,716 *8: IT' TO*J :ZS. *.7 'W5 .006 .03 drooler 4463 lo tho product obtained froa distillation f AXOOlor 4063 Which lo a nixtuzo of 40S dlatlllod High Bo 11or iM60S Diphenyl chlorinated to 64.1 to 64.6^ chlorine with Barrett oftealag point of 76 to S00 (Ooaparleon standard rained at 78). Avoolor 4463 lo designated no "Ooal Tar Basin, CloarT In orroopondanoo and on ohlpaonto to H, H, Robertson 0o Onrotalltoatlon Tooti Tvanafor 3O-4O grams of oanplo to 19> 00 bookor, hoot to 10060, add a alnuto traoo of powdorod iroolor ltoo aa aood oryotalo and maintain at 100*10300 fbr M tours, At ond of thlo tins It should bo no tod whothor tho wood iryotalo havo grown or hav# dloappoarod. Approved by____ Approved by__ Chief Chemist Works Manager NONS 052218 Approved by____ Sales Manager Authorised by-------- Chemical Director Standard Specification or The Swann Corporation Mw,,ChtortMlt High tlirco* Nn M0m-546o _ Grade ^.ig<|w.546p PlotllltdD.le A,,thorieed._.. flfti. l*/?3/j* 0 m OOtttrOl Iflt Supersedes Specification Dated_____ _____ _________ B Blotory mt Tolerable Limits . Typical Value 0 Uittani OoXor, 1", Tallow tjlO B Bp. or. at 5/*5o, B-70-17 0 Baft. Point - Barrett, 0 B Soft. Point - D56-|6,0 B Ooeff of Expansion B Loot at 16300, d6-*7 0 held UlMfhor, MSB NoOR/01 B Bofraotlvo lades 0 Crystallisation U* iroslor $460 lo Dm product frou tbi Alstlllstlon of Aroolor 3O6O which M die tilled High Boiler Chlorluetod to 60 01. OrpetollUetloa Toot OnU1 further eoneldoretlon le elves to this toot, transfer 3O-4O frou to a booker, ult does, then Mlstoln ot 10u-105C for one week. Note If there lo any tosdesoy toward crystallisation, xxonlno dally. Approved by__________________ __________________ Chief Chemist t Approved by_______ Works Manager Approved by___ Authorized by. HONS 052219 Sales Manager Chemical Director *4? hoiBtt Standard Specification OF The Swann Corporation Nr, I40U8-501 Grade: i /joi - . .............. .. _ ------ Date Authorized__ JLO/4/54 -- Supersedes Specification Dated............................ ........ Tolerable Limits Typical Value Softaalng Mnt U.8.S.M.) fwrol Ylaooalty at, 98*9*0 58.0*0 45 iiwbIi tax 5OI la a alxtura of Aroolor 4465 - 96)! and Paraffin (540) 44. A|,|>ruvcd by. Approved by__ Chief Chemist MOWS 052220 Approved by________floW+rt 6a fMthtrly Sales Manager Authorized by______ masisL* Ui. ummwt ns* wirrni nun omuoAi. octait iwsowai im MONS 052221 2+f fjOaSBACT AHOOLOH IQVIPHKHT ran Bpoolflo Ororltp jmimL ArOllBblO to bo OOBtt to Hloo't Arnilablo 8t htvki Vootphol balanoa Ihibbord bottloo Ororltjr Joro Opoolol hydroma tor a lot aitjr Pro* Ohlorldoo Dolor Rottotlrltp Hit. liil* TiNHhir Hobo Hobo Nogolan aotor CoUo Hooko Ooadoaooro Bbloia Tbornomotor Lorlbond oolorlMtor Vlaooolaotor Iffuz roooptooloo Tbemomotoro Wolootrto Oonotont Honor Footor ItlK Toot Looo Ob Hooting Oron, Serial Vo, 681--41 Mlo otogo amplifier Audio ooolllotor Roolotoaoo box Bt4. sir ooaioBBor Bolonolng oondoBaor TerBier oonlonoor Oondenoer soil S otorogo bottorloo Oroa tbenaometar Same oo D. 0. Powor footor ooll Bobo oo roolotlrltp HONS 05inz Oroa with rotating oholf Thermometer Tour Point Ohlorlso Hobo oxoopt thermometer a Parr bombe end tlgbtoalng rook Jtro TMT . eft. Pi. Halt Pt. Iltrlti Iax nh pt. IfBMM High Seller fAO EPi-J. ____________ _ .XBSBBBL Available te be not to Pot Available 1--------------------- A.8.T.H. eaaembly Barrett eaaembly II.O.A. thermometer Refreotometer Cleveland opes eup aaaambly ant thermometer Barrett diet. equipment. Praasiae pt. thermometer laah teat atendarAa Tlgreaux oolumn era HONS 052223 MOMS 052224 schdu!,! or nuanos MONS 052225 cuauuumnft S. flUMb ft*' Woot - Dm UU SUfraaoatlo flow Ant SI. --ML m---ton l*|Mi UlteiUii IUn(i Abort QnmA fwad*Ham far Storafa Task A roo ftHt iroaad Food taak c-esao C-MSX MM MM s-msi bfNt ii of Aw* lu ImkmIM ImoUm h' InrttiMttat Colon A Tru Brisk boor k Buroar OiiUiii Datail of Shall Datail of Itotk imohi mmi nMi Btroatkral (tool Strcotural Stool fCMdlttlAI Floor OrotUf k IwdnUlii bU Fltttac* far FTootlo--tint Sul-- Qaa rlfUl for Barman if, auttsaumam Bamaal StlU - Aaatmbl? * * - FrmottoMtlaf OolMi k Taako * * Stnotoral Stool Support Siybaogrl Still - Aaaaotlr a - Altantieo to protaot Still a a - BooMgr Fuap k Sopport a a - Baotar a a - Stool Sopport a a - Altantlao* C-Mt e>mo MM 0-8SW 0-8BS4 0-6SOC M(N o-wr fl gig, 0-WSB K6M 0-MS1 MM e-twe 0-6SS7 0-SSS7 0-4F4S C-65T4 C-SS70 o-srn 0-SSTt C-SS78 MASS MOMS 052226 141 litlir IUU - iliNtI; * * * - Pu*p A Support * * * - kli fioUti Boot 1 * * - tap Prlro iMd Houalag * Kotor Boon * * - IttU Body * - KUoaUaataia Oaatliga * * * - tap Shaft. Poaa trap and Staaa doll - SttU Support * * * - Oolvan A lioilnr t. Piping a a . RMtar a - btwelon to Baatar Support - (Ueelvor A Sight Olaat a . Oanaral Layout Lootrodryor - Oanaral Layout awmxafl mnm 1 m mmu Layout - taa 1SU aitlag Pot Stool Supporting Structuro tantUatlug Rood f $ Qhlorlaator A Pittluga Magrauuatlo Layout 101 gbaorbora - Layout Boo. 1S8S * * Poo. 19*9 *0,000 Oallou gold Tank a a .a a a a fim, * - gold Cooling Ootla a * tank for (Irk gold Stool Stagra A Tooora t t * - Talk Oar Loading Station 0-0400 0-0481 0-0402 0-0480 0-0484 0-84*. 0-0480 0-0487 0-0488 0-0489 0-8490 0-0491 0-049* 0-005* 0-0058 0-0469 0-0865 0-5598 0-5599 0-0598 0-0599 0-0400 0-0850 0-085* 0-8585 0-6608 0-85*0 0-0587 0-0591 0-0417 0-0457 0-0458 0-0408 HONS 052227 VI. PlflTULlUtH KmUMUT VOUUB Still (Badjar) - Gwml Layout II - Blandl&f Tank a * - Tubajat Support a * - Xonal Foaa Trap 1268 Still - Oanaral Layout a - Battlug a a ,, ?ot - Rayaoad Dust Collaotori a Exhauat Faa 8 Ductwork - Hood for Flakar C-68SS 0-8078 0-6489 C-666S C-8889 c-am B-6118 -81*4 0-6478 C-67S8 ITD/Jw t/tl/M MONS 032228 HONS 052229 UR or run Boinn*i n obi AT mzevm. totm THAT WHICH IB AVAILABLE fOB TRAR8W TO RABT BT. lOOXBf ALORQ HT8 APMOIIIUTS KI0HT8, 0OBTB,BTC Hi 0. T, ooutm wqmkmbc mpajhvixt Botloi> ar f*Uow|Bwiol axndiiaB iqviyMot Cgtitrtw Obit Imntiti Mimt ChiorIntin* Bqlpaat lirliUc AoM nat NttUtt OqotpMNt HONS 052230 HOWS 052231 MOMS 052232 *3~9 MOMS 052233 sa