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AR 286 -- 0200 BIODEGRADATION (BOD/COD) TEST SUBSTANCE _-- Identity: ArefmeirxrteudretocaonstPaiFnOiSng, pFeCr-f9l5u,oroorocatsanaescuolmfponoanteen,twhoficFhC-m2a0y6CalEs.o b(1eOctanesulfonic acid) (CAS # 2795-39-3) Remarks: The 3M production lot was not noted. The test sample is FC2d1i0.e65tC5hE%y.lsenoCeduirgulrymecnootlctibynulftoysrlumleaftathtieeor,n,1i7.n6d0i.5c0%a9tp%eoswliayttoiexsrya,et4mhi%yxltueurnreeeoam,fo1n0.o.2o9c82t%%ySlPupFihteOonSny,el f1eot5ah%emre,r, 0.06% sodium lauryl sulfate, and 0.05% tolytriazole. cThhaerafcotlelrowiiznegd scounmcmeantrryataipopnlsioefsitmopuarmiitxiteusr.e Dwaittha imnacyomnpoltetacecluyrately reflect the biodegradability of the fluorochemical componentofthe test sample. METHOD: Method: Not noted. Type: Aerobic GLP: No `Year completed: Not given. CIonnotcaucltumt:ime: S2o0urdcaeysnot given. RESULTS CBhioecmhiecmailcaOlxyOgxeyngeDneDmaenmdan(dCO(DB)O:D): 510-DDaayy:: 20-Day: 390,000 mg/kg 24660,,000000 mmgg//Ll 470,000 mg/L CONCLUSIONS No conclusions given. Submitter: 3M Company, Paul, Minnesota, 55133 Environmental Laboratory, P.O. Box 33331, St. - ATA QUALITY Rmeeltiahboilditfyo:lloKwieidm.iscThhreaniknioncgul3.umSitsundoyt lparcokpserdleysccrhiaprtaicotnerainzdedr.ecTohredrsoefits hneo 001696 characterizationofthe test substance purity nor analytical measurement of the test concentrations. REFERENCES S-- R -- `The studies were conducted by Pace Laboratories, Inc. of Minneapolis, MN at the requestofthe 3M Company, Lab Request number G1358, 1989. OTHER piesa Last changed: 6/26/00 001697 ire . " . Nes, nc. REPORT OF LABORATORY ANALYSIS i Minneapolis, Minneso Coralville, lowa Novato, California Leawood, Kansas May 12, 1989 Mr. Wade Schell 3M Environmental Laboratory 935 Bush Avenue Bldg. 2-3E St. Paul, MN 55133 File: xsy - Dear Mr. Schell: Enclosed 1s the reportof laboratory analyses for samples received 03/14/89. If you have any questions concerning this report, please feel free to contact us. Sincerely, Pay Gully Susan D. Max Director, Sampling and Analytical Services Enclosures : ) -_-- 1710Douglas aM DriveNorth OMinneapolis,MN55422 OPhone(612) 544-5543 001698 pace. . Xz KS,x inc. REPORT OF LABORATORY ANALYSIS 393M5EBnuvsihroAnmveenntuael Laboratory BStl.dg.Pau2l-,3WN 55133 PMAaCyE1P2,roj1e9c8t9 Number: Attn: Nr. Wade Scheil Off`iWciens:sapali, Minnescta `CToeramipvai,leF,lolroiwdaa 8903145L11esa, Kansas 61358 DDaattee SSaammppllee((ss)) CRoelcleeivcetde:d: PACE Sample Number: Parameter IINNODRIGVAINDUIACLANPAALRYASMEITSERS BBlloocchheeniiccaal] OOxxyyggeenn DDeemmaanndd,, CBhleomcihceanlfcaOlxygOexnygeDnemaDnedm(a2n)d, 0B3y/C1l4i/e8n9t Units CCaarrbb 0150 DDaayy((11))mngg//LL Carb 20 Day(1)ng/L mg/kg. 069430 069500 069510 MOL Gl3SR-) G1358-2 G3SE-3 24000 24000 91000 400000 46000 260000 2540000000 764800000000 437500000000 740000 MOL Method Detection Limit 1710DouglasDrieNorth200cMuinntncepsppoornltiMysNe,nc5 loye5Ph4 one2 612)2544-0 8843 (001 699 . . MPra.geWade2 Schell REPORT OF LABORATORY ANALYSIS PWaAyCE1P2,roj1e9c8t9 Number: OffMiicnense:apolis, Mnnesc Coralville, lowa 890314A5o1i1uarid, Kanass PPaArCaEmeStaemprle Number: IHINODRIGVAINDIUCALANPAALRYASMIESTERS Chemical Oxygen Demand(2) Units MOL 069520 Glass mg/kg 50000 370000 MOL Method Detection Limit am @ mBCehiteohmciohcedamslic#a5ol0x7y.ogxeyngednemdaenmdanwdaswpaserfpoerrmfeodrmeIdn methods #508. - in accordance withstandard accord-ance with standard BaThypeprdodivaretedactmcesotunhptoeadriovnlieosdgiioienns..thiAsllreapnoarltysweesrewoerbetaipneerdforumseidngbyEPmAeororotuhnedrer B os ruarson Inorganic Chemistry Manager --_-- er -- * 1710DouglasDriveNorth 0MinneapoliMsN,85422 0Phone(612)544-6843 ee le TooI 17_ oS b