Document Mn647GpKB4VdMmGX6yLY2x2x

y/v, #Lancaster Laboratories A division of Thermo Analytical Inc. Analysis Re Pll .w-imAdKavievaai LLI Sample No. TL 2795998 Collected: W 3/97 at 13:45 by SN Submitted: 10/ 3/97 Reported: 10/24/97 Discard: 11/24/97 CWK-BD-49 Soil Sample TCLP NON-VOLATILE EXTRACTION Chambers Works Soil Reuse Job #6015-08-06 Account No: 07032 OERS/DuPorrt Env Remed Services Barley Mill Plaza, Bldg. 27 Routes 141 & 48 Wilmington DE 19805 CAT NO. ANALYSIS NAME ' AS RECEIVED METHOD RESULTS DETECTION LIMIT UNITS 3329 3330 3331 3332 3333 3334 3335 nitrobenzene N.D. 0.0020 mg/1 hexachlorobutadiene N.D. 0.0020 mg/1 2,4,6-trichiorophenol N.D. 0.0040 mg/1 2,4,5-trichiorophenol N.D. 0.0020 mg/1 2,4-dinitrotoluene N.D. 0.0020 mg/1 hexachlorobenzene N.D. 0.0020 mg/1 pentachlorophenol N.D. 0.0020 mg/1 The semivolatile analyses were performed on a non-volatile toxicity characteristic leachate of the submitted waste. The leachate was prepared according to the procedure specified in the March 29 and the June 29, 1990 Federal Registers. A sample is considered to have failed the Toxicity Characteristic (TC) test and is therefore considered a hazardous waste if any of the semivolatile concentrations (mg/1) in the leachate exceed the following maxima: Total Methyl phenols 1,4-Dichiorobenzene 2.4-Dinitrotoluene Hexachlorobenzene Hexachlorobutadiene Hexachloroethane 200.0 7.5 0.13 0.13 0.5 3.0 Nitrobenzene Pentachlorophenol Pyridine 2,4,5-Trichiorophenol 2,4,6 -Tri chiorophenol 2.0 100.0 5.0 400.0 2.0 The limits are published in March 29, 1990 Federal Register, pp. 11845-6. QUALITY CONTROL REPORT SAMPLE MDL 1335 Arsenic 0.029 1336 Selenium 0.048 1746 Barium 0.0028 1749 Cadmium 0.0031 1751 Chromium 0.0066 1755 Lead SAMPLE UNITS mg/1 mg/1 mg/1 mg/1 mg/1 BLANK Batch: 972825705004 N.D. Batch: 972825705004 N.D. Batch: 972825705004 N.D. Batch: 972825705004 N.D. Batch: 972825705004 N.D. Batch: 972825705004 DUP RPD MS MSD 0 (1) 89 87 0 (1) 80 81 0 (1) 10 11 0 (1) 77 78 0 (1) 80 80 MS RPD 2 2 1 0 1 P.0. LBIO-62248 Rel. L146 LCS LCS LCS LIMITS LCS DUP RPD LOW HIGH 101 101 0 80 120 95 97 2 80 120 104 105 1 80 120 100 106 6 80 120 107 106 0 80 120 Questions? Contact your Client Services Representative Nancy Bornholm at (717) 656-2300 8V3 (E BVS B E R ACTL Lancaster Laboratories 2425 New Holland Pike PO Box 12425 Lancaster, PA 17605-2425 717-656-2300 Fax:717-656-2681 Respectfully Submitted Ramona V. Layman Manager, Metals/Leachates See reverse side for explanation of symbols and abbreviations 2216 Rev. 8/4/97 DUP050464922 Explanation of Symbols and Abbreviations The following defines common symbols and abbreviations used in reporting technical data: N.D. TNTC iU unthos/cm C Cat maq 9 ug ml m3 none detected Too Numerous To Count international Units micromhos/cm degrees Celsius (diet) calories milliequivalents gram(s) microgram(s) milliliter(s) cubic meter(s) BWIQL MPN CP Units NTU F ib. kg mg 1 ui fib >5 um/rnl Below Minimum Quantitation Level Most Probable Number cobalt-chloroplatinate units nephelometric turbidity units degrees Fahrenheit pound(s) kilogram(s) milligram(s) liter(s) microliter(s) fibers greater than 5 microns in length per ml < > ppm ppb Dry weight basis 'ess than - Trie number following :he sign is the limit of quantitation, the smallest -amount of analyte which ran be rehabiy determined using this specific test.' greater than parts per million - One ppm Is equivalent to one milligram per kilogram (mg/kg), or one gram pet million grams. For aqueous liquids,, ppm is usually taken to be equivalent to milligrams per liter ring/l), because one liter of water has a weight very c!ose to a kilogram. For gases or vapors, one ppm is eauivaient to one rniuoMer o` gas per liter of gas, parts per billion Results printed under this heading have been adjusted for moisture content This increases the analyte weight concentration to approximate the value present in a similar sample without moisture. US. EPA data qualifiers- Organic Qualifiers iricrgank Qualifiers A TIC is a possible aide!- condensation product S Value o <CRDL, but Dl 8 Analyte was also detected in the blank Estimated due to interference C Pesticide result confirmed by GC/MS iv) Duplicate injection precision not met D Compound quantitated on a diluted sample N Spike sample not within control limits E Concentration exceecs the calibration range of S Method of sTcwhe'd additions dvlSA; used the instrument Mr cak ulation i Estimated value U Compound was not detected N Presumptive evidence of a compound (TICs only! W Post digestion spike o.,t of control limits P Concentration difference between primary and * Duplicate analysis no! within c.ontro! limits confirmation columns >25% + Correlation coefficien; for MSA <0.595 U Compound was not. detected X,Y,Z Defined in case narrative Tests results relate only to the sample tested. Clients should be aware that a critical step in a chemical or microbiological analysis is the collection of the sample. Unless the sample analyzed is truly representative of the bulk of material involved, the test results will be meaningless. If you have questions regarding the proper techniques of collecting samples, please contact us. We cannot be held responsible for sample integrity, however, unless sampling has been performed by a member of our staff. This report shall not be reproduced except in full, without the written approval of the laboratory. WARRANTY AND UMXJS OF LIABILITY - In accepting analytical work, we warrant the accuracy of test results for the sample as submitted. THE FOREGOING EXPRESS WARRANTY IS EXCLUSIVE AND IS GIVEN IN LIEU OF ALL OTHER WARRANTIES, EXPRESSED OR IMPLIED. WE DISCLAIM ANY OTHER WARRANTIES, EXPRESSED OR IMPLIED, INCLUDING A WARRANTY OF FITNESS FOR PARTICULAR PURPOSE AND WARRANTY OF MERCHANTABILITY. IN NO EVENT SHALL LANCASTER LABORATORIES BE LIABLE FOR INDIRECT, SPECIAL< CONSEQUENTIAL, OR INCIDENTAL DAMAGES INCLUDING. BUT NOT LIMITED TO, DAMAGES FOR LOSS OF PROFIT OR GOODWILL REGARDLESS OF (A) THE NEGLIGENCE (EITHER SOLE OR CONCURRENT) OF LANCASTER LABORATORIES AND (B) WHETHER LANCASTER LABORATORIES HAS BEEN INFORMED OF THE POSSIBILITY Of SUCH DAMAGES. We accept no legal responsibility for the purposes for which the client uses the test results. No purchase order or other order for work shall be accepteQby Lancaster Laboratories which includes any conditions that vary from the Standard Terms and Conditions of Lancaster Laboratories and we hereby object to any conflicting terms contained in any acceptance or order submitted by went. DUP050464923