Document MbJYLKVn1Oz2gXaaxLNL4jaM
Rollins EnvironmentalSsn/lcesmoInc.
P 0. Box 609. Deer Park. Texas 77536 (7131 479-6001
1 BILLING INFORMATION
2 PICK-UP LOCATION
HO 4zz<}4-
WILL BE ASSIGNED BY RESfTX).
PPGcompany namf Industries, Inc.
AnnRFRsP* 0. Box 1000
city Lake Charles
rtatfLA
7IP 70601
contact Jere Clark
phone*?:8 ^91-4215
companynamf PPG Industries, Inc.
AnnRFSR P- 0. Box 1000
city Lake Charles
^statf
zip 7060
CONTACT Mik" HUb"
ANCNf318 491 485
3 MANIFEST INFORMATION
4 GENERATOR INFORMATION
rnkiDAkiv kiaup PPG Industriss, Xtic>
..repair lad-008086506 TMrin 99922
AnnnFRS
P. 0. Box 1000
city Lake Charles
^statf
contact Anne Corbello
phonf
namf
zip 70602
namf
318 491 4364
Gerald L. Perry
TECHNICAL CONTACT Shift Superintendent 'emergency CONTACT
PHnNF318 491 43 PHnNF318 491 43
5 GENERAL INFORMATION
GENERAL WASTE DESCRIPTION
Trichloroethylene and Perchloroethylene Heavy Still Bottoms & Cartridges
Production of Trichloroethylene and Perchloroethylene
PROCESS GENERATING WASTE
QUANTITY RFNFHATFD
2000 lbs
UNITS
PER
year
TIME
FREQUENCY OF REMOVAL
18_____
NUMBER
TIME(S) PER
year PERIOD
6 SHIPPING INFORMATION D OT HAZARDOUS MATERIAL'
IS YES
Q NO
TEXAS WASTE CODE NO
992030
DOT PROPER shipping name
Hazardous Waste Solid, n.o.s.
DOT HAZARD CLASS
____________________ DOTID.NO. NA 9189Hn
1 pound
USEPA HAZARDOUS waste NUMBERfSt
K030 and Polychlorinated Biphenyls
REASON FOR the ABOVE CLASSIFICATIONS)
Listed Specific Source Hazardous Waste 40 CFR 261.32
HAZARDOUS SUBSTANCE
Chlorinated Hvdrocarhons
CONCENTRATION 40-fin?
HAZARDOUS SUBSTANCE
CONCENTRATION
7 SHIPPING METHOD
CD ENCLOSED VAN
0 OPEN TOP VAN
TANK TRUCK
CD VACUUM TRUCK
CD DUMP TRUCK
TANK CAR
ED FLATBED
CD ROLL-OFF BIN
8 GENERATOR'S METHOD OF COLLECTION
DRUMS TYPE / siz^0T_21-C/55t^L
OTHER SHIPPING REQUIREMENTS OR INFORMATION
D DUMP BIN [D CUSTOMER DELIVERY CD OTHER_____________
.OTHER.
DITIONAI DATA ATTACHED 0
EVERY ITEM ON THIS WASTE OATA SHEET MUST BE COMPLETE
CHAMPION BUSINESS FORMS -- Form No U
(SHADED AREAS FOR RES USE ONLY) nnr nd SAMPLE NO.
ROLLINS ENVIRONMENTAL SERVICES UNIFORM WASTE DATA SHEET
(SCHEDULE A)
RF.S SAI FR FXFC- It CONTRACT NO.
RTRFAM NO HO-42294
A. GENERATOR INFORMATION
11. Goeeinieeirdaituofr Nivamec.: ______ PPG INDUSTRIES. INC.
? Terhmral Contact: 4 Emergency Contact 6. Generator USEPA I D.:
WILLIAM H. COOPER, ASSOCIATE RESEARCH CHEMIST,, Phone No 318-491-4250
SHIFT SUPERINTENDENT
SAME (Title) 1 Title)
5. Phone No. 318-491-4340
LAD008086506
7. Generator State ID.:
N/A
8. Disposal State I D.:
TWC ID 99922
B. PICK UP LOCATION 1 Company Name:
PPG INDUSTRIES, INC.
2. Address:_____________ COLUMBIA SOUTHERN ROAD
8 C ity-
WF.RTT.AKF,
4 Rtate- T.A
S Zip Crvte- 70669
8 PickuD Contact:
CHARLES PARNELL, AREA FOREMAN. ENV. (Title)
7 PhnneNn 318-491~4858
C. MANIFEST INFORMATION
1 Company Name:
PPG TfintTRTRTFQ
2. Address:
P 0 BOX 1000
3. City:
LAKE CHARLES
INC,
4 State-
LA
5. Zip Crvte- 70602
6. Manifest Contact:
VICKI CORMIER. ENV. SECRETARY
D. INVOICE INFORMATION 1 Company Name:
2. Address:
PPG INDUSTRIES. INC. P 0 BOX 1000
7 PhnneNn
318-491-4831
(Title)
3 City:
LAKE CHARLES
4 .State-
LA
5 7ipC.nrte- 70602
6 Invoice Contact:
GINGER BUSBY - ACCOUNTS PAYABLE CLERK
(Title)
7 Phnns Nn 318"491_4526
E. GENERAL WASTE DESCRIPTION 1 Name nf waste- TRICHLOROETHYLENE AND PERCHLOROETHYLENE HEAVY STILL BOTTOMS AND FILTER CARTI
2. Process Generating Waste:
PRODUCTION OF TRICHLOROETHYLENE AND PEREHLQBOETHILENE
3. Quantity Generated:2000 LBS
Per^EAR
(Year/MonW)
F. SHIPPING INFORMATION Yes No
0 D i EPA RCRA Hazardous Material
2. EPA Hazardous Waste Number(s):
tp 3. Disposal State Regulated Material 4 DOT Regulated Material
__________K030, NAQ1RQ ____________________________________________________________
5. State Waste Number: Generating State: Disposal State:992030 6. Proper DOT Shipping Nam*- HAZARDOUS WASTE SOLID, N.Q.S., ORM-E, NA9189 (K030 AND CONTAINS
POLYCHLORINATED BIPHENYLS') RO
7. DOT Hazard Class: QBMHE _
8. DOT UN/NANo.:____ NA9189
9, RQ (lbs)I --
G. METHOD OF SHIPMENT.
.
1. (3 Drums: Type/Size:------- DOT-21-C/55 GAL~
-.
_
2. Bulk: Type/Size:____________________ _
3. Other (Please be specific): __ ______ __________________ __________________________ ____________________ 4. Transportation Requirements:ENCLOSED VAN;^ 046297___________________________________________________________
Page 3 of 6
nm cn Am o<-v- *
Turn Page and Complete Paa
Stream No. HO-42294
K. REACTIVE CHARACTERISTICS Yes No 53 1- Explosive 133 2. Pyrophoric
Yes No
51 5. Air Reactive
qa 6 Reactive Cyanide:
13 7 Ro^rtiye Sulfide
51 3. Shock Sensitive
3 8. Oxidizer
53 4. Water Reactive
9. Other
L. ELEMENTAL ANALYSIS (Total Metals required for memorable waste; TCLP or EpTox Metals required for landfill waste.)
Total/Units
Total/Units
TCLP or Eptox/ Units
1. Antimony 2. Beryllium 3. Copper a. Nickel 5. Thallium 6. Zinc
NA
NA 9.9
11 <2.0 31
mg/Kg mg Kg
mg/Kg mg/Kg mg/Kg
7. Arsenic 8. Barium 9. Cadmium 10. Chromium 11. Lead 12. Mercury 13. Selenium 14 Silver
<; 1...2 1 mg/Kg 46 / mg/Kg
< 0.5 / mg/Kg
9.1, mg/Kg 7.3 , rag/Kg
< 0.2 1 mg/Kg < 1.2/ mg/Kg < 1.0/ mg/Kg
/ /
/ /
l <
/
Additional Requirements for RES (TX) Inc.:
15. Manganese 16. Potassium
28 mg/Kg NA
17 Silicon 18. Sodium
NA M.
Additional Requirements tor RES (NJ) Inc.:
19. Molybdenum
___________ 20. Vanadium________
'<
M. TCLP ORGANICS "" nn47-Tetrachlorethvlene. D046-1.1.2.2-Tetrachloroethane, D030, -1,4-Dichloroben2ene D037 Hexachloroethane, D036-Hexachlorobutadiene
N. DISPOSAL CERTIFICATIONS
1 Is this waste excluded from direct land disposal by land disposal regulations that are in effect on the date of this Waste Data Sheet?
3 Yes
No
If yes, describe which restriction(s) applies to this waste. (See 40CFR268 and 40CFR761.)
2. Under 40CFR268, can this waste be landfilled directly or chemically stabilized and landfilled? Yes KEl No If yes, completed RES Certification Form must be attached to each Manifest.
3. Under 40CFR268. should this waste be incinerated? 3 Yes No If yes, completed RES Certification Form must be attached to each manifest.
4. Additional information_________________________ _________________ ______________________________________________
l hereby certify and warrant that the information supplied on this form and on any attachments or supplements represents a complt and accurate identification and description of this waste material, its constituents and its known or suspected hazards. I further cer and warrant that this information is the result of an analysis of a representative sample of the waste obtained and analyzeo accordance with testing procedures of the U.S. Environmental Protection Agency or by the application of knowledge of the proce
Page 5 of 6
aES-50-*19 Rev. 12/88
Turn Page and Complete Page 6 (tor PC8 Itei
-------------------------------------
3.1-701
WASTE ANALYSIS REPORT
Sample
Environmental Laboratory PPG Industries, Inc., Lake Charles, LA
- StJ/Js
,/Lr/lr,' iJhii
-&orr> fer/T*'
rLocation of eSaammnpllae Sample Collector
- Me*JtlCS Sft// Bd4v>*S
Corner ef ^
- ^ aM^s
Scte****
"Sample Method/Device -
^rJo /Sc**/?
Date of Sampling
- lifnjTZ />ir
Date All Analyses Completed - dlJa/jtq Report submitted by:
d*rkj)p
------------------------------------------------------------------------------------------ -------------------------------------------------- Ifct*--i_______ L*lL3.
ANALYSIS RESULTS
Cast Faitnun
Corrosivity : ^ - `t/A
Rssctivity ' N/A
EP Toxicity
C A - M/A
Othsr Psranstsrs (1C nsadsd) ( ) - N/A
MD tJwe.
Revision 1-18-89 F. A. Corbello
RoHim Environmental Services rm Inc.
P O Box 609. Deer Park. Texas 77536 1713) 479-6001
FPG File 505.6.89
1 BILLING INFORMATION
2 PICK-UP LOCATION
AnnRFSR
P 0 Box 1000
rnv Lake Charles
STATF LA
zip 70602
contact dare Clark
phonf 318/491-4215
COMPANY namf PPG Industries. Inc.
address______ Columbia Southern Road
city Westlake
.STATE LA
zip 70669
contact Mike Huber
phone 318/491-4858
3 MANIFEST INFORMATION
COMPANY NAME PPG Tndustries__ Inc^
AnnnFRR
P P Box 1000
CITY. Lake Charles
STATF _... LA 7IP 70602
CONTACT. Anne Corbello
phone 318/491-4364
5 GENERAL INFORMATION
4 GENERATOR INFORMATION
USEPA i d LAD-008086506 two in 99922
name Gerald L. Perry
TECHNICAL CONTACT
name Shift Superintendent
EMERGENCY CONTACT
phonf318/491-4370 phone318/491-4340
GENERAL WASTE DESCRIPTION Trichloroethylene and Perchloroethvlene Heavy Still Bottoms and Filter Cartridges
process generating waste Production of Trichloroethylene and Perchloroethvlene
QUANTITY OFNERATEn
2000 lbs
UNITS
PFR
year
TIME
.FREQUENCY OF REMOVAL.
18
NUMBER
. time(S) per
6 SHIPPING INFORMATION
DOT HAZARDOUS MATERIAL?
H YES
O NO
TEXAS WASTE CODE NO. 992030
DOT PROPER SHIPPING NAME __ Hazardous Waste Solid, n.o.s.______________
year PERIOD
DOT HAZARD CLASS
D O.T. 1.0. NO. NA 9189
USEPA HAZARDOUS WASTE NUMBERfS). K030 and Polychlorinated Biphenyls
, RO 1 pound
reason FOR the above CLASSIFICATIONS) Listed Specific Source Hazardous Waste 40 CFR 261.32
HAZARDOUS SUBSTANCE
Chlorinated Hydrocarbons
CONCENTRATION
40-60Z
HAZARDOUS SUBSTANCE
CONCENTRATION *i
7 SHIPPING METHOD
Q ENCLOSED VAN
Cl OPEN TOP VAN
O TANK TRUCK
D VACUUM TRUCK
CD DUMP TRUCK
TANK CAR
13 FLATBED
ROLL-OFF BIN
8 GENERATOR S METHOD OF COLLECTION
DOT 21-C/55 gal
DRUMS TYPE/SIZE__________
Tan1<
OTHER SHIPPING REQUIREMENTS OR INFORMATION _________________________________
D DUMP BIN D CUSTOMER DELIVERY1
O OTHER______________
.OTHER.
ADDITIONAL DATA ATTACHED ST`SAMPLE PROVIDED
GENERATORS SAMPLE NO, Lab LogJ817 - *
' *1- -
EVERY ITEM ON THIS WASTE DATA SHEET MUST BE COMPLETE
CHAMPION BU8INC88 Fn>
*-- wo. 00
SL 046300
Yes No
Generating
5. G Disposal State Regulated Material 6. State Number: T.Annnsnftftsnft
Yqs No
7. Ci DOT Regulated Material 8. DOT Shipping Name:
HatarHnns wagfe
9. DOT Hazard Class:___ 9 PGIII 10. DOT (UN/NA) No.:
NA3077
Destination State _ Waste Code Number: 992030 ______
(contains Trichioroeti -solid,.n.o.s. and DadiLuitetliylijng
11. RQ (lbs.):. 1 lb
G. METHOD OF SHIPMENT 1. 0c Drums: Type/Size: _ DOT 21-C/55 gal
2. Bulk: Type/Size:.
3. Other (Please be specific):___
4. B Transportation Requirements:.
Yes No
5. 3 Customer to Transport
Enclosed Van
Yea No
6. IS Truck Scale at Customer Site
CUSTOMER REVISION: Signature _ Page 3 of 6 res-50-419 r v90
SL 046301 Date.
Trim Penn
D"*>
Stream No. HQ-42294
K. REACTIVE CHARACTERISTICS (check alt that apply)
Yes No
1. 13 Explosive
Yes No
6. Q Reactive Cyanide:
mg/i
2. 3 Pyrophoric
7. 3 Reactive Sulfide:__
3. 13 Shock Sensitive 4. 3 Water Reactive
8. 0 Oxidizers (specify): 9. Other (specify):___
!J' ' U
5. 3 Air Reactive
--t ELEMENTAL ANALYSIS (Total Metals and TCLP metals data are required for incineration waste streamsTCLP metals data ijfo, required t
landffirmaterial. For liquid wastes with less than 0.5% solids, total metals (in mg/kg) x density of wasteftoto/L) = TCt results (in mg/L).* (Record data for all that apply).
Total Metals: mg/kg mg/L
Antimony (Sb) Arsenic (As) Barium (Ba) Beryllium (Be) Cadmium (Cd) Chromium (Cr) Chromium VI (CrVI) Cobalt (Co)
JUJL
<1.0 <0.3
<0.3 <0.3
QAUNK UNK
ppm (Check appropriate unit)
Copper (Cu)
UNK
Lead (Pb) Manganese (Mn)
3.8 UNK
Mercury (Hg)
<0.09
Molybdenum (Mo)
Nickel (Ni)
<(Ui
Potassium (K)
Selenium (Se) Silicon (Si) Silver (Ag) Sodium (Na) Thallium (Tl) Vanadium (V) Zinc (Zn)
<Oi3 1.5
TCLP D004 - Arsenic____ D005 - Barium____ D006 - Cadmium _ D007 - Chromium.
(mg/L)
<0.2
<0,02 <0.03
<0.04
TC Level ______________ 5.0 _____________ 100.0 _____________ 1.0 ______________ 5.0
D008- Lead. D009 * Mercury _ D010-Selenium D011 - Silver___
TCLP (mg/L)
<0.1
<0.0002 <0.2
<0.02
*N.B. - EP Toxicity Characteristic data are acceptable until 9/25/90, or 3/25/91 for small quantity generators.
TC Lev
M. ORGANIC TOXIC CHARACTERISTIC WASTE (specify EPA waste code and TCLP results (mg/L) for all that apply, see instructions for list).
-------D--0--2--8-------------------- -----3--.-5---6-----mg/L
---------------------------------- ---------------- m,, g. /L..^_____________________________ mg
mg/L mg/L
mg/L mg/L
mg
' v|
mg
.mg/L
mg/L
mg
N. RECOMMENDED TREATMENT METHOD (check applicable box)
1. Q Incineration
4. Direct landfill
2. Incineration with chemical stabilization and encapsulation of residues
3. Chemical stabilization and encapsulation
5. Underground injection 6. Chemical treatment 7. Other (soedfv)
JQJ - .-.nlioR
________________ 1____
O. CERTIFICATION
-fig
l hereby certify and warrant that the information supplied on this form and on any attachments or supplements represents acomplete and accura identification and description by the generator company of this waste material, its constituents and its known or suspected haz^ds.
Signature Date: April 10, 1991 ,,
Title,:. Env. Control Spe Me
* CUSTOMER REVISION: Signature. Page 5 of 6 RES-KM19 Rev. 7/90
Sb 046302
-f M <nft
Turn ffcge and Complete Page
8
SQ8 Environmental Laboratories
E9008-038
? RESULTS - TCLP TOXICITY VOLATILES
SOS ID I 29008-038-4 PPG IDi 1327 P/T Heavy Still Bottom* Date Extractedi 8/11/90 Data Analyzed! 8/13/90
A
8
Ao
?
S
S
Concentration in ppb (ug/L) in TCLP Extract
1327 P/T
Method
Heavy
Detection
Still Bottome Limit
Benzene
HD 5.0
Carbon Tetrachloride
197 5.0
Chlorobenzene
HO 5.0
chlorotora
346 5.0
1,4-Dlchlorobenzene
41 5.0
1,2-Dlchloroethane
3,562
5.0
1, l-Olehloroethylene
88 5.0
Methylethylketone
HD 10.0
Tetrachloroethylene
105 5.0
Trichloroethylene
60 5.0
Vinyl Chloride
HD 10.0
TCLP Hank
HD HD HD HD HD HD HD HD HD HD HD
Blank Detectlo:
Limit
5.0 5.0 5.0 5.0
5.0 5.0 5.0 10.0
5.0 5.0 10.0
surrogate Standard Percent Recovery (at 0.050 ifa/L)
1327 P/T 1Heavy
Blank
1,2-0ichloroethane-d4 Tcluene-d8 4-Bro*oflurobanzene
89 %
84 % 87 %
86 *
103 X 104 %
HD den taa Hot, Detected at a level afi'v* the method-detection llmit
Member of thctoa Group (aoMMOMfMMawnwMwica
8
QS*eOSeSq8eStt8>008e>QieeqfOOSeS08SOtOOS*SOS*SOS*SOS*OOSeOSe80sf
SL 0A6303
bGS*SijS*SGS*SGS*SGS*3QS SGS*SGS*8GSSGS*SGS$GSSGS*SGS*SGSP'>SSGS*3GS*8G8*8GS5GS*SGS
iainn
SGS Envir nmental Lab rat ries E9008-038
9
ian
in i9n
Cin3
i9n
RESULTS - Sample IDs 1327 P/T Heavy Still Bottoms SGS ID: S9008-38-4
Qin
9
in
TCLP Metals
oin
-- Date Extracted: 8/13/90 Date Analyzed: 8/17/90
Concentration in ppm (mg/L) in TCLP Extract
i9n
a
in i9n
oin
> EPA HW
TCLP Metals
Result
Blank
Method Detection Limit
i9n Oin
3 3
D004
> D005
Arsenic Barium
ND ND ND ND
D006
Cadmium
ND ND
3 D007
3
3
D008
Chromium Lead
ND ND
ND ND
3 D009
Mercury
ND ND
0.2 0.02 0.03 0.04 0.1 0.0002
i9n O
(A
ma
in
ia9n
in i9n
3 DO 10
Selenium
-3 D011
3 n
Silver
/>
3
n
Total M ta^s
n
* Date Analyzed: 3/14/90
ND ND ND ND
0.2 0.02
Concentration in ppm (mg/Kg) in sample
O m
i9n O in
9
m O in
9
m iDn
3 V) 0
Result
Blank
Method Detection Limit
in
* Antimony
ND
ND
1.0
am m
Arsenic Barium
ND ND
ND ND
1.0 0.3
<3 in in
Beryllium Cadmium
ND ND
ND ND
0.3 0.3
3 imn in
Chromium Lead
0.4 ND 3.8 ND
0.3 0.5
a Mercury
in in
Nickel
a Silver
in w
Thallium
ND ND ND ND
ND ND ND ND
0.09 0.5 0.3 1.5
a m
in
3 ND denotes Not Detected at a level above the method detection limit.
w
in
a
imn
am
9
in
9
main ia9n
in
9
ian
in i9n oin
ia9n
min n in i9n
a
in i9n O in i9n ain
ia9n
in in Oin i9n
a
in
a in
9
ia9n
in
in a
i9n
m SV 0*6*0* |
9
in
a Member of the SGS Group (Soewt* ofwaM m sunmtMncai U)
O
80S Eftvtronnwntai LaboritortM
MlSULTS - TCL? TOXICITT 8SMXV0LATZLHS
E9008-038
SGS ID. E9008-03B-4
PPG IDi 132? P/T Heavy Still Bottoms
Date Extracted. 8/28/90
Date Analyzed. 9/01/90 Concentration in ppb (uy/L) in TCLF Extract
o-oreaol a-creeol p-creeol Creeol 2,4-Dinitrotoluene Haxachlorobenzene
1327 P/T Heavy aSlll SatSPHff
MD MD ND MD ND HD
Blank MD MD MD MD MD MD
Method Detection I
10.0 10.0 10.0 10.0 10.0 10.0
Hexachlorobutadiene
ND
MD
10.0
Hexachloroethane MD MD 10.0
Nitrobenzene
MD MD 10.0
Pentachlorophenol
MD
MD
50
Pyridine
MD MD 10.0
2,4,5-Trichlorophenol
MD
MD
2,4,6-Trichlorophenol
MD
MD
Surrogate Standard Percent Racoverv _Lat 0.200 mo/H
50 50
2-Fluorophenol
Phenol-ds
2,4,6-Tribroaophenol Xitrobenzene-d5 2-Fluoroblphenyl
Terphenyl-die
1327 P/T Heavy
asm Bgy&gag
13 % 10 % 17 \ 13 \ 14 a 10 %
&ia&&
20 % 19 % 33 % 38 % 37 % 21 %
MD denot a Hot Detected at a lev 1 above' the method detection limit.
m a rin e *
------- f ITT----1 HrfTT - 1 -1---- D1)
100 O0toa8Ot*0O8*iQSSO0*saS0O88Q0.8OttQ00O0*Q80Q8SQS>8Q0*0ai0O8e^
6305
RauMs
LAND DISPOSAL RESTRICTION NOTIFICATION foer 40 CFR 268.7)
.INSTRUCTION: Complete Part I. Check and complete Part.IIor Part III-Complete md iim Part IV.
1. Generator Name: PPG Industries, Inc.
EPA IJO #.* LAD008086506
2.
Atfflrexs:
P 0 Box 1000
3.
Citv-
Lake Charles
State:
LA
/UbUZ Zio:
T. RES Reference# fBR/HO/L/W/MO/OP): HD477Q4
Manifest #.*
5. EPA Waste Codes flint ALL code* for this stream and all relevant aubcaterories- -see reverse side of this forml 2
F025. D039. D040____________________________________
6.
This stream is (check on*) *
wutwtUr ( <1% total organic carbon and <1% total suspended solid* ) * nonwastewater
If wa*twater, consult with your Sal** or Customer Service Representative.
PARTII: Wastes Subiectto Land Dtsoosal Restrictions (It th* waata i* non-haaardous or *"n*wly Hatad waste" idantifiad in Part
III below. comoiata Part III rather than Part II.l
x Pursuant to 40 CFR 268.7,1 am notifying___ RES(LA);___RES(NJ):X RESfTXl:___ RES of LA;___ OPC;___ TET that undar the above
RES Reference and manifest number*, I am shipping to you a waata idantifiad by th* EPA waata cod*(s) and subcategory(ias) listed in Part I above, which is subject to the EPA Land Disposal Restrictions, as checked below.
A, Check line 1. 2. 3 and/or 4. as applicable
I. Treatment standard, as checked by me in Attachment 1, which I am enclosing, for _____FOOI;_____ F002; _____ F003; _____ F004; ______ F005; ______ F039.
2. Numerical treatment standard(s) specified in 40 CFR 268.41(a) (Table CCWE), par Attachments.
y
X
B.
3. Treatment atandard(s) expressed as specified technology(ies) in 40 CFR 268.42(a), for which th* required technology, per Attachment S, is _____ INCIN;______ DEACT;______ ADGAS fb NEUTR;______ IMERC;______ STABL; or, for PCBs, x Incineration in a TOSCA-parmitted incinerator (RES(TX) only).
4. Numerical treatment standard(s) specified in 40 CFR 268.43(a) (Table CCW), per Attachment 3.
Also check one or more of the following lines if applicable
5X 6.
7.
A D001-D011 waste which (a) ______ does (b) ____ does not meet the definition of a "California List" waste (see definition below). If (a), I have also checked th* "California List" section of Attachment l, which I am enclosing.
Treatment *tandard(s) with a "capacity variance" until ___________ 199___ _ per Attachments, as I have checked on
th* enclosed Attachment 2. Th* waste (a) X does (bl
does not meet th* definition of a "California List" waste
(see definition below). If (a), I have also cheeked th* "California List section of Attachment 1, which I am enclosing.
A nickel or thallium "Calfornia List" waste (see definition below). I have checked th* "Calfomia List" section of Attachment 1, which I am enclosing.
8. A specific extension or variance (other than a "capacity variance"), as I have checked on Lin* H or I of Attachment 2 which I am endaeing.
_____ _ 9-
The waste already meets all relevant treatment standards. I have signed th* required certification on page 2 of Attachment 2, which I am enclosing.
10. This waste is a lab pack. If it Is an "Appendix IV lab pack" or an "Appendix V lab pack", I have signed th* require certification on page 2 of Attachment 2, which I am enclosing.
PART Iff:____ Wastes NOT Subject to Land Disposal Restrictions
Pursuant to 40 CFR 268.7, I am notifying_________ RES(LA);___RESINJI: RESITXV. RES of LA:___ OPC: TET that, under th* abov reference and manifest numbers, I am shipping to you a waste which is non-haaardous and/or identified by th* EPA waste code(B) listed in Part I above. The waste is not subject to th* Land Disposal Restrictions because the waste is non-haaardous and/or consists only of one or more of the following EPA waste codas listedaince November B, 1984: D018-43,K064-66,K088, K090-91,K117-18,K123-26,K131-32,K136, U328, U3S3, U3S9.
PART IV: Authorized Representative!
Signature__ -----------__________________________________________________________________ Date
Print or Type Nam*
William H. Cooper___________________
04-11-91
Title -------------------- Environmental Control Specialist____________
NOTE: A "California List" waste, is (a) a hasardous waste containing Halogsnated Organic Compounds at a concentration of 100* mg/kg or
mg/1, or greater; or (b) a liquid hasardous waste (including free liquids) having a pH equal to or leas than 2.0 or containing any of th*
- following materials at a concentration equal to or greater than specified: PCB's, W ppm; or (lnmg/1) tree cyanides, 1000; As,300; Cd_lDO: O 600;
Pb, 500; Hg, 20; Ni, 134; Sa, 100; Tl,130.
~
L 046306
1
ADDITIONAL NOTIFICATION FOR FQ01-F0Q5. FQ39 AWD CALIFORNIA LIST WASTES
For Part H. Lina 1 of th* LDR Notification (FOOl-FOOS. F0391
This waste muit be treated to meet the followinc treatment standard* (check the appropriate line): _____ F001 _____ F002 _____ FOOS _____ F004 _____ F008
WASTE CODE F001 - FOOS ipent solvent*
F001 - FOOS spent solvents F001 - FOOS spent solvents (Pharmaceutical Industry Wastewater Subcatefory) FOOS
REGULATED HAZARDOUS CONSTITUENT
WASTEWATERS CONCENTRATION
(mc/l)
NONWASTEWATERS CONCENTRATION
______ fnw/1)
BJL-S____ C C W E
Acetone
n-Butyl alcohol Carbon disulfide
Carbon tetrachloride Chlorobensen*
Cresols (and eresylic acid) Cyclohexanone
1, 2 - Dichlorobensen*
Ethyl acetate Ethylbensen* Ethyl ether Isobutanol Methanol Methylene chloride Methyl ethyl ketone Methyl isobutyl ketone Nitrobenaen* Pyridine
Tetrachloroethylene Toluene
1, 1, 1, - Trichloroethane
X. 1, 2 - Trichloro-
1, 2, 2 - Trifluorethan*
Trichloroethylene
Trichlorofluoromethane Xylene
O.OS S.0 1.0S O.OS 0.1S 2.32 0.125 0.66 O.OS 0.0S 0.0S 5.0 0.2S 0.2 O.OS 0.06 0.66 1.12 0.070 1.12 1.06
1.06 0.062 0.06 0.06
o.so
S.0 4.81 0.06 0.06 0.76 0.76 0.126 0.76 0.0S3 0.76 5.0 0.7S 0.06 0.76 0.33 0.12S 0.33 0.06 0.33 0.41
0.06 0.001 0.96 0.16
TAB
Ccw
1, 1, 2, Trichloroethane
Bentene
0.030 0.070
7.80 3.70
Methylene chloride
0.44
NA
R_E Q U I R E D
METHOD
2-Nitropropane
INCIN
INCIN
FOOS
2-Ethoxyethanol
INCIN
INCIN
For F039, a* indicated on th* reverse side of this Attachment
For Part II. Line 6. 6. or 7 of the LDR Notification (California Liatl
This waste must be treated as indicated below if it is (a) a D001, DOM, DOOS, D004, D005, D006, D007, DOOS, DOOO, D010, D01I,
or subject to a "capacity variance*, -- ni meets th* definition of a "CaliforniaList* waste; or (b) a liquid haaardous waste >60 ppm PCBs.or >_ 134 mc/1 Ni, or >_ 130 mg/1 TI. Check the appropriate line below,
x
j[ _____ _____ _____ _____ _____ _____ _____ i_____ __
HOC >.1000 ppm: incinerate in a RCRA incinerator
liquids, PBC >.50 ppm or: incinerate in a TOSCA/RCRAincinerator
liquid, pH .3: Neutralise
liquid, free cyanides >,1000 ppm: *
liquid, As >.500 mc/1: *
liquid, Cd >.100 mc/1: *
liquid, Cr >.600 mc/1: *
liquid, Pb >_SOO mc/1: *
liquid, He >.110 mc/1: *
liquid, Ni >134 mc/1: *
\~
liquid, Se >.100 mc/1: *
liquid, Tl >.130 mc/1: *
-
--
Treat to below California List concentration, or to non-liquid form.
SL 046307
ATTAC ENT 2
LAND DISPOSAL RESTRICTION NOTIFICATION
EXTENSIONS. VARIANCES. EXCEPTIONS
For Part II. Lin* B-6 of the Notification Form ThU wuta it (check one):
A. Soil or debrit contaminated only with tolventt end/or California LUt watte*, from the following Superfund Site: (thit variance valid until November 8, 1990)
___B.
Soil or debrit, contaminated only with tolventt and/or California Liat waatea, from RCRA corrective action order or permit
requirement (attach a copy of relevant EPA order or permit provision) signed bv
on _____ (thin variance valid until
November 8, 1990)
----
___ C.
Soil or debrit contaminated with watte apeeified in 268.33 or 268.34 for which the treatment standard it bated on incineration,
per Attachment 3 (thia variance valid until August 8, 1990 for such watte* in 268.33 and until June S, 1901 for *uch watte* in 268.34).
D. Soil or debrit contaminated with waste* specified in 268.3S for which the treatment standard it baaed on incineration, mercury retorting, vitrification or wet-air oxidation, per Attachments (variance valid until May 8, 1992)
__ _E. A waste specified in 268.35 (a) --per Attachment 3 -- orK071 (variance valid until Auguat 8, 1990). ___ F. K048, K049, KOSO, K061 or K052 (variance valid until November 8, 1990) ___ G. A waste specified in 268.35 (e) -- per Attachment 3 -- (variance valid until May 8, 1992)
For Part II. Line B-3 of the Notification Form. Thia watte it:
___ H. Subject to a case-by-case extension, pursuant to '40 CFR 268.5, granted by (attach copy)
___ I. Subject to a treatability variance, pursuant to 40 CFR 268.44, granted by (attach copy)
SL 046308
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ATTACHMENT 3 - p. 2
630^ 0^
ROLLINS
X m, ENVIRONMENTAL SERVICES (SHADED AREAS FOR RES USE ONLY)
DOC. NO..
RES SALES EXEC: #.
ROLUf ENVIRONMENTAL SERVICES UNIFORM WASTE DATA SHEET (EXHIBIT B)
STREAM NO. HQ-42294
A. GENERATOR INFORMATION
1 GeneratorName: PPG Industries. Inc. 0 Pun?ha<sinn Contact- Gerald Clark, Manager-Purchasing Dept.
-- a technical Contact- William H. CooDer - Env. Control Spec*.
R Fmernencv Content:
Shift Superintendent
^
8. Generator USEPA I.D.:
LAD008086506
lTM'>
a Phone no<318 s Phone No (318 7. Phone No I318
i 491-4215 ) 491-4250 >491-4500
B. PICK UP LOCATION
1 Company Name: ? Address (not P C Box):
3. City:
Same
Columbia Southern Road
Lake Charles
4. State:
EA7(5602 5. Zip Code:
R Pickup Contact: Flf^n Carbon- Env--Asss-i Sl-snr-DertvarTyps ' (I ide)
7. Phone No. f 318) 491-4325
C. MANIFEST INFORMATION (if same as "B", wnte "SAME" but indicate Manifest Contact below if different)
1. Company Name:
SAME
? Address: P D Rot 1 nflfl
3 Citv:
Lake Charles
4. State:
R Manifest Contant- Vicki Cormier, Env. Secretary
LA JTiBo)
5. ZiDCode:
70602
7 Phone No. ( 318 \ 491-4618
D. INVOICE INFORMATION (if same as "B" or "C" write "SAME" but indicate Invoice Contact below if different
1 Company Name- SAME
P. A. d.d.ress:
SAME AS ABOVE
3. City-
4. State:
S. 7ip Code:
R Invnire Contact:
Ginger Rushy, Arrf . Payable Clerk ' (Tide)
7. Phone No l 318 ) 491-4526
E. GENERAL WASTE DESCRIPTION
1 NameofWaste: Trichloroethvlene and Perchloroethvlene Heavv Still Bottoms Cartridges
? Process Generatina Waste3onQuan.ti*t.y G-enerat.ed,:
Production of Trichloroethylene and Perchloroethylene
2200 lbs.
Per Year
(Year or Month)
F. SHIPPING INFORMATION (check all that apply)
Yes No
Yas NO
1. n EPA RCRA Hazardous Waste 2. Wastewater or 0 Non-Wastewater 3. 0 n TSCA Waste
TSCA
ommn
Waste Code: 9920^0
4. All aDDlicable EPA Hazardous Waste Codes and subcateaories includina Characteristic ("D") codes: F025/D040 /D039
Yes No 5. H Disposal State Reaulated Material
Generating fi. State Number: T.A nnOftORA SDR
7. S DOT Regulated Material 8. DOT Shipping Name:. -Hay-arHnn.c; uasfp,
9. DOT Hazard Class: 9 PGIII 10. DOT (UN/NA) No.:
NA3077
Destination State
Waste Code Number 992030
(.contains incmoroetl
flnliH.
*s * and Rsi diloi'OeLliyltJifc!
11. RQ (lbs.):. 1 lb
Q. METHOD OF SHIPMENT 1. Drums: Type/Size: _ DOT 21-C/55 gal
2. Bulk: Type/Size:
3. Other (Please be specific):___ 4. 0 Transportation Requirements:.
Yes No
5. 3 Customer to Transport
CUSTOMER REVISION: Signature.
Enclosed-Van
Yes No
6. S Truck Scale at Customer Site
SL 046310 Date.
Page 3 of 6 res-kmiq r. 7/90
Tum Pone anH rVvwniAto Pano
Stream No. _ HQ-42294
K. REACTIVE CHARACTERISTICS (check all that apply)
Yes No
1. C? Explosive 2. 3 Pyrophoric 3. 3 Shock Sensitive 4. 3 Water Reactive 5. E? Air Reactive
Yes No
R PI jg Rearrive Cyanide:
7. 3 Reactive Sulfide: ft. PI Oxidizers (specify): 9. PI n Other (specify):
mg/lmq/l<
-L ELEMENTAL ANALYSIS (Total Metals and TCLP metals data are required for incineration waste streams.TCLP metals data eve required fi landfill material. For liquid wastes with less than 0.5% solids, total metals (in mg/kg) x density of waste (in kg/L) = TCL results (in mg/L).* (Record data for all that apply).
Total Metals:
Antimony (Sb) Arsenic (As) Barium (Ba) Beryllium (Be) Cadmium (Cd)
(H mg/kg mg/L n
_<1 .U____________ <1.0 <0.3
<0.3 <0.3
Chromium (Cr) Chromium VI (CrVI) Cobalt (Co)
CXrA UNK
UNK
ppm (Check appropriate unit)
,, Coooer fCu)
UNK
Lead (Pb)
3.8
Manganese (Mn)
UNK
Mercury (Hg)
<0.09
Molybdenum (Mo) Nickel (Ni)
<n.s
Potassium (K)
Selenium (Se) Silicon (Si) Silver (Ag) Sodium (Na) Thallium (Tl) Vanadium (V) Zinc (Zn)
<0.3 1.5
TCLP D004 - Arsenic
(mg/L) <0.2
TC Level 50
DOOa - Lead
TCLP (mg/L) <0.1
D005 - Barium D006 - Cadmium .... D007 - Chromium
<0.02 <0.03
<0.04
lOOO 10 5.0
DQ09 - Mercury D010 - Selenium D011 - Silver
<0.0002 <0.2
<0.02
'N.B. EP Toxicity Characteristic data are acceptable until 9/25/90, or 3/25/91 for small quantity generators.
TC Lev 5 0
5
N. RECOMMENDED TREATMENT METHOD (check applicable box)
1. Q Incineration
4. Direct landfill
2. Incineration with chemical stabilization and encapsulation of residues
3. Chemical stabilization and encapsulation
5. Underground injection Chemical treatment Other (specify)______
O. CERTIFICATION
I hereby certify and warrant that the information supplied on this form and on any attachments or supplements represents a complete and accurat identification and description by the generator company of this waste material, its constituents and its known or suspected hazards.
Signature
Titift- Env. Control Spe<
Date: April 10, 1991 _
-CUSTOMER REVISION: Signature. Page 5 of 6 res-scmis dm. 7/90
SL 0A63U Date. Turn Page and Complete Page
s o a -a a a
3Q8 Envlronmontml Utoofitortoa
89008-038
1
RH8ULT3 - TCLP TOXICITY VOLATILSS 808 IDi 89008-038*4 PPG ID> 1327 P/T Haavy Still Bottoma Data Extractedi 8/11/90 Data Analyzedi 8/13/90
Concantration in ppb (ug/L) in TCLP Extract
4
a
i
1327 P/T
Mathod
Haavy
Dateetion
Still Bottoms
Limit
Banzane
ND S.o
Carbon Tatraehlorlda
197 5.0
Chlorobenzene
ND 5.0
Chloroform
346 5.0
1,4-Dlchlorobanzane
41 5.0
1,2-Dlchloroethane
3,562
5.0
1, l-Dichloroathylana
88 5.0
Methylethylketone
ND 10.0
Tatrachloroathylana
105 5.0
Trichloroathylana
60 5.0
Vinyl Chlorida
ND 10.0
TCLP Blank
ND ND ND ND ND ND ND ND ND ND ND
Blank Datactlo
-Limit
:i5.0
5.0 5.0 8.0
5.0
5.0 4
8
5.0 10.0
5.0 5.0
10.0
aurroflata. Standard Percent Recovery (at o.ose mo/L)
l,2-Dichloroethane-d4 T0luene*d8 4-Bromofluorobenzene
1327 P/T Haavy mil B9.wi
89 % 84 % 87 t
Blank
86 % 103 \ 104 \
s
ND dan ta Not Datacted at a leval al> va th* aathoddeteotion Halt
EPA WASTE CODE
LAMP DISPOSAL RESTRICTION TREATMENT SUBCATEGORIES
SUBCATEGOIUES
COMMENT
D001 D002
Ignitable liquid* 10 % TOC or > Ignitablc liquid* < 10 95 TOC 1gnitabl* comprMMd gases Ignitable reactive* Oxidicer
Steel corroaive*
Alkaline Acid
Pr 261.21 (a)(1) Per 261.21 (s)(l) Per 261.21 (a)(3) Per 261.21 (a)(2) Per 261.21 (a)(4)
SAE 1020 cteel corroiion rate < 6.3S mm/yr Per 262.22 (a)(1) Per 262.22 (a)(1)
D003
D006 D008 D009
F025 K061 K069 K071 K106 P06S
P092
Explosives Water reactive* Reactiva sulfides Reactive cyanides Other reactive*
Per 261.23 (a)(6),(7), (8) Per 261.23 (a)(3U3),(4)
Per 261.23 (a)(5) Per 261.23 (a)(1),(4) Per 261.23 (a)(1)
Cadmium-containing batteries Other
Lead acid batteries Other
Low mercury High mercury High mercury, containing organics
(not incinerator residues)
High mercury, containing inorganics (including incinerator or RMERC residues)
< 260 mg/kg Hg 260 mg/kg Hg or >
260 mg/kg Hg or >
260 mg/kgHg or >
Light ends Spent filters/aids and desiccants
Low sine High sine
Calcium sulfate Non-calcium sulfate
< 15% total sine 15% total sine or >
Low mercury High mercury
Low mercury High mercury
< 16 mg/kg Hg 16 mg/kg Hg or >
< 260 mg/kg Hg 260 mg/kg Hgor >
Low mercury --residues from RMERC Low mercury -- residue* from incineration Mercury fulminate, high mercury --
incinerator or RMERC residues
Mercury fulminate, nonwastewaters -- not incinerator or RMERC residues
Original P065 less than 260 mg/kg Hg Original POOS less than 260 mg/kg Hg 260 mg/kg Hg or > Original P065 leas than 260 mg/kg Hg
Low mercury --residues from RMERC
Original P092 less than 260 mg/kg Hg
Low mercury -- residues from incineration Original P0S2 lass than 260 mg/kg Hg
Phenyl mercury acetate, high mercury --
incinerator or RMERC residues Phenyl mercury acetate, nonwaatewatere --
not incinerator or RMERC residue*
260 mg/kg He or >
U151
High mercury Low mercury -- residue* from RMERC Low mercury residues from incineration
NOTE: TOC = total organic carbon; RMERC = mercury retorting
260 mg/kg Hg or >
Original U151 less than 260 mg/kg Hg
260 mg/kg Hg
260 mg/kg Hg or >*
1
Use these lines for additional EPA waste code* and subcategories, if necessary :
-p. 2-
SL 046313
1
ADDITIONAL NOTIFICATION FOR F0Q1-F005. FQ39 AMD CALIFORNIA TJST WASTES
For Part II. Line 1 of th* LOR Notification fFOOl-FOOS. F039)
ThU waste muat ba traatad to maat tha followinf treatment standard* (check th* appropriate line): _____ F001 _____ FOOJ ______ F003 _____ F004 _____ F005
WASTE CODE
REGULATED HAZARDOUS
POWIUTVENT
wastewaters
CONCENTRATION
------- Lmt/n
NONWASTEWATERS
concentration
--------
TABLE
C C WE
F001 - FOOS spent solvent*
Acetone n-Butyl alcohol Carbon disulfide
Carbon tetrachloride Chlorobensen* Cresols- (and cresylic acid) Cyclohexanone 1, 3 * Dichlorobensen* Ethyl acetate Ethylbensen* Ethyl ether Isobutanol Methanol Methylene chloride Methyl ethyl ketone Methyl isobutyl ketone Nitrobensen* Pyridine
Tatrachloroethylen* Toluene
1, 1, 1, - Trichloroethan* If 1, 3 - Trichloro-
1, 3, 3 - Trifluorethane Trichloroethylene
Trichlorofluoromethan* Xylene
0.OS S.O 1.06 0.06
0.16 3.83 0.136 0.66 0.06 0.06 0.06 5.0 0.2S 0.3 0.OS 0.06 0.66 1.13 0.079 1.13 1.06
1.06 0.063 0.06 0.06
______________________ TAB JL _E
CCW
F001 - FOOS spent solvents
F001 - FOOS spent solvents (Pharmaceutical Industry Wastawater Subcatefory)
1, 1, 3, Trichloroethan* Bensen*
Methylene chloride
0.030 0.070
0.44
REQUIRED
FOOS
2-Nitropropan*
INCIN
FOOS
3-Ethoxyethanol
INCIN
___ For F039, a* indicated on the reverse sida of this Attachment
0.59 S.0 4.81 0.96 0.06 0.7S 0.76 0.136 0.75 0.083 0.76 5.0 0.76 0.96 0.76 0.33 0.135 0.33 0.0S 0.33 0.41
0.96 0.091 0.96 0.16
7.80 3.70
NA
method
INCIN
INCIN
For Part II. Lin* 5, 6. or 7 of th* LDR Notification {California Listl
'ihmVT *>1fW
This waste must be treated a* indicated below if it is (a) a D001, D002, D003, D004, D005, D008, D007, D008, DOoT! DOIoLdOU
or subject to a capacity variance', - mi meets th* definition of a `CaliforniaList' waste; or (b) a liquid hasaidons wwa*ssttee...>SSOO..ppppmm PCBs.or >_ 134 mf/l Nl,or 130 mf/l Tl. Check th* appropriate line below.
r, V , - .VXt
HOC >.1000 ppm: incinerate in a RCRA incinerator
liquids, PBC SO ppm or: incinerate in a TOSCA/RCRAincinerator
liquid, pH <_3: Neutralise
liquid, free cyanides >, 1000 ppm: *
liquid, As >.500 mf/l: *
liquid, Cd >.100 mf/l: *
liquid, Cr >.500 mf/l: *
liquid, Pb >.500 mf/l: *
liquid, Hf >.130 mf/l: *
liquid, Ni >.134 mf/lr *
liquid, 3* >,100 mf/l: *
liquid, Tl >. 130 mf/l: *
..
Treat to below California List concentration, or to non*liquid form.
SL 04631*
ATTAC 2NT 2
LAND DXSPQSA] j RESTRTCTION NOTIFICATION
BIOWS a--.VARIANCES.* EXCEPTIONS
For Part II. Lino B-6 of the Notification Form Thii wut ia (check onej:
.A. Soil or debria contaminated only with aohrent^ and/or California List vuti, front the following Supetfund Site: (thia variance valid until November 8, 1990)
___ B.
Soil or debrie, contaminated only with eolvente and/or California Liat waatea, from RCRA corrective action order or permit
requirement (attach & copy of relevent EPA order or permit proviaion) signed by.
(thia variance valid until
November 8, 1900)
_C. Soil or debria contaminated with waate specif! iad in 268.33 or 268.34 for which the treatment atandard ia baaed on incineration, per Attachments (thia variance valid until A.iuguat 8, 1990 for auch waatea ia 268.33 and until June 8, 1991 for aueh waatea in 268.34).
mD. Soil or debria contaminated with waatea apeciQiied in 268.35 for which the treatment atandard ia baaed on incineration, mercury retorting, vitrification or wet-air oxidation, per Attachment 3 (variance valid until May 8, 1992)
___ E. A waate apecified in 268.35 (a)--per Attachment 3 -- orKOTl (variance valid until August 8, 1990). ___ F. K048, K049, KOSO, K0S1 or K052 (variance valid until November 8, 1990) ___ G- A waate apecified in 268.35 (c) -- per Attachment 3 -- (variance valid until May 8, 1992)
For Part II, Line B-8 of the Notification Form. THa waate ia: ___ H. Subject to a caae-bycaae extenaion, purauanl to 40 CFR 268.5, granted by (attach copy) ___ I. Subject to a treatability variance, pursuant to 40 CFR 268.44, granted by (attach copy)
on
SL 046315
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ATTACHMENT 3 - p. 2 -
^VQiiai*>os*t09*iai<iat*i
o
SQS Environmental Laboratories
RESULTS - TCLP TOIICITY SEMIVOLATILES
B900B-038
SGS IDi E9008-03IB-4
PPG ID. 1327 P/T| Heavy Still Bottona
Date Extractedi 3/28/90
Oat* Analyzed. o-creaol
9 /01/90 Concentration in ppb (up/L) in TCLP Sxtr
1327 P/T Heavy Still Bottoaa Blank
Method mifittgn hlML
ND ND 10.0
a-cresol p-ereaol Craaol
HD HD 10.0 HD HD 10.0 ND ND 10.0
2,4-Dinitrotoluen
ND
ND
10.0
Haxachlorobenzena
ND
ND
10.0
Hexachlorobutadiane
ND
ND
10.0
Hexaehloroethane ND ND 10.0
nitrobenzene
ND HD 10.0
Pentaehlorophenol
NO
HD
50
Pyridine
ND ND 10.0
2.4.5-Trlehlorophebol
ND
ND
50
2.4.6-Triehlorophejol
ND
HD
50
S-tjadird Percent Recovery (at 0,200 na/Ll
1327 P/T Heavy
SU11 Bffttan
Bleak
2-Fluorophenol Phenol-dS 2,4,6-Tribroaophen^l Nitrobenzane-d5 2-Fluorobiphenyl Terphenyl-die
... *it. HD denotes Hot Detected at'a level above the nethod detects
j SL 046317
a M*ra**f of th* eoaoraup (laMUMMlumMMi
;*SGS*StfSSGSSGS*SGS*8GSSa$Sns*SaS*!U3SSGS*8GSSaSSGSsar 'GS*SG8*SGSSGS*SGS 8GS*8GSi*n
Ctni
SGS Environmental Laborat ties B9M8-38
(A
a tn
tn
O tn
CA
RESULTS - Sample JDt 1327 P/T Heavfy Still Bottoms SGS IDi E9008-38-4
Ci (A tn
TCLP Metals
Ci tn tn
Date Extracted: 8/13/90 Concentration in ppm (mg/L) in TCLP Extract
CA O
Date Analyzed: 8/17/90
ca
v> O
Method
tn EPA HW
TCLP Metals
Result
Blank
Detection Limit
(A
a
in D004
Arsenic
ND ND
0.2
Ci tn
tan
tn tn
a
tn
tan
tn
(A
a
D005
Barium
ND ND
(A D006
Cadmium
ND ND
D007
Chromium
ND
ND
0.02 0.03 0.04
tan
tn tn
D008 D009
Lead Mercury
ND ND ND ND
0.1 0.0002
Ci tn
CA
D010
Selenium
ND
ND
D011
Silver
ND ND
0.2 0.02
Ci tn tn
Total Metals
Date Analyzed: 8/14/90
Concentration in ppm (mg/Kg) in sample
O (A
in
(3
v> tn O tn (A 0(A
01 O tn (A o <A
<n 0 t*n tn
a (A
(A a tn 01 0 m tn O tn (A
t
Antimony Arsenic Barium Beryllium Cadmium chromium Lead Mercury Nickel Silver Thallium
Result
ND ND ND ND ND
0.4 3.8 ND ND ND ND
Blank
ND ND ND ND ND ND ND ND ND ND ND
Method Detection Limit
1.0 1.0 0.3 0.3 0.3 0.3 0.5 0.09 0.5 0.3 1.5
ND denotes Not Detected at a level above the method detection limit.
0 (A
Ci tn CA 0 tn CA
o
tn CA G CA CA Ci
CA
CA
c
CA
CCA
CA
CcA.
CA
CA
c
CA
CA r
CA
CA c
CA t!
c
0
0
Cu
4
cCl
b b C bi b C b
0)
".
0 (*A
(A
0
A-
Member of the BGS Group (Socww Oanwate CM Survamaneat
0*6318 SL
|
c t
RES ADDENDUM TO UNIFORM WASTE DATA SHEE*]|
rCy^WQ additions or change 1 1 Bhang a have been made
A. GENERATOR IlfFORMATION
1. Company Name:
2. Address;
0. feavt
3. City: l_c3We-
10O O
4, State:
5. Zip Code:
B. REFERENCE RES UNIFORM HASTE DKXA SHEET 1. Lab Reference Number: ^/BR/DP/W/L (Circle One): List Number:
2. Waste Description; \ , PiaRc,.
Fu_Tgg.^_________
"7P6^-)0c *"
REVISION TO RES UNIFORM KA8T1 DATA SHEET CHEMICAL CONSTITUENTS SECTION I AND EPA CODE
SECTION F JVP-P1W>Wr*T*
ffpft ujfea>r& CODES - /?oa*5, DQA?,D039
CONCENTRAT DN
ci)j-OKr*/*i flipRccafi**) {tow
jgnactMwoEnttrta 1,1,0.,A*
^HmaiMiFwiETMNe
/ ~A &.
EPA
.CODE.
CONCENTRATION _LEVEL/RANCE ^S*fauraaETHA(ft -LrAA-
CLtS-Ufo.
EPA CODE
ADDITIONAL AMENDMENTS OR CHAIN IKS (IF ANY)
REGULATORY STATUS
r^T^YES
{ 1 NO
yes
im n
EPA RCRA Hatardoua waste Tsca Vaste
Ft INFORMATICS (SECTION C, D AND E) VERIFIED BY (CHECK BELOW)"
1. cm
2.
Analytical Testing (Please Attach Analysis Results)
Knowledge of the Process Generating the waste (analytical data may t requested).
CERTIFICATION
I hereby certify and warrant that the information on thiB form, any attachments t
supplements, and on any current active Uniform Waste Data Sheet applicable to this wasi
material represents a complexa and accurate identification and description by t)
g n rator company of this was1:e material, its constituents and its known or suspect:
hazards.
- SL 04631'
ASRALD io.~PE-R.1Lj
SIGNATURE:
TITLE* ^Ai>..gj^ttCft%>KveiTMw QX30rfcrwj -SPScxAixst
DATE:
nr