Document MML0dJ9ay2wLKda9r88O3Zynk
\'SlCG'1l36 CODE RT-695-D PKG__
1m
L2J2G
7 - 7LOT NUMiiR)
7'EST* WT. 2608* LBS*
.~ -
PROCESSES' . < )RT--695-D <G>
COMTYP JOB NAME TYPED BY: KLW STANDARD HRS._________
. ' ^PREPARATION NOTESt___ /-U/X? a'ti
V3
APPROV JJG 3/18/81
- EWK- 12/7/81 36RT695DM
TIM M ^
NON-BLEEDING-
AME: BON* RED DARK
USE | N-CODE 1 ACCT
LBS |
I LBS -
SSARY, CLEAN,. DRESS SPARKLER PRE- |
WITH 1 5t DICALITE FILTER AID-
I. ML
N FOR S 6 2-CHL0R0-4-AMIN0 TOLUENE-5 l
ONIC ACID
'I
TAIN FOR S 42 3-HYBRQXY~2-NAPh TH0IC ACID|
.. . . : .-
I
. 1 777--A i 740-C
1 I 82-C
1JM..
23* <73201 WATER INTO V-317
II
tJElGH O POUR IN SODIUM HYDROXIDE -
1 y. I
M__Z2._, J?s5I3a ! /? I 7-D .
URN ON AGITATOR 6 STEAM 6 DUMP IN FROM S 2! >*^-CHL0R0-4-AMI NO-TOLUENE-S-SULFONIC ACID I
1 740-C
LOT .3^2=,-
. 100% -Mpr
-3.%L
ggZl2> :
I i
J
1
KWRGH ON POSTAL SCALE 2-AMIN0-T0LUENE-5V<jk:FONIC ACID 6 ADD LOT _______
I. .1 f
1 584-C
i
8 l/DUMP IN ACTIVATED CARBON | 9 l/DJINP IN DICALITE, FILTER
I 50 AID' I 10
1 113-B I 777-A
50 TO
11 IXflEAT TO 214-216 DEG* F
WATCH FOAM
|.
HI JX15EC0RD: BYJl II__<
IF' NECESSARY ADJUST
| >-T*6 + -J3Y SODIUM HYDROXIDE
ASSUME 50%
l 1____
7-D I _____
112 k-StlR 30 MIN* AT 212-214 DEG* F, THEN SHUT I
i L~FF STEAM
WATCH FOAM
.
I
I i^NOTE RECORD : SPARKLER PRESSURE &JC-PSI i
| 1 _^"IF NOT ZERO, NOTIFY SUPERVISOR
1
(13 1-CtRGtiLATE 15 MIN DR LONGER THRU SPARKLER | |JB^TIL SOLUTION IS CLEAR '
i I
10V 5 1&2
| | .-MAINTAIN AT 190-195 DEG. F FOR S 15^
1'
1 | RECORD-: -HT/i:_DEG.F 6 RECORDEF^XOe G*F i
| | RECORD: STARTI^l TOTAL MINii.CLARlTYjdfiC. 1
100 |14 k Sn *1 (99G) WATER INTO V-TOO
I
3 115 U*?flN S--13 COMPLETE, PUMP V 317 THRU
I
I - \J8&mffLER* MAINTAIN V-317 AT 190-195 DEG * F 1
i - jvRECORDT STARlil^OTAL MINJL&
I
| I SAMPLE FROM HOSE* SHOW-TO SUPVR FOR OK 1
]I
' ;i '
''
!
MAKING INSTRUCTIONS: BATCH UNIT
EQUIP I I MENT j | PAGE 02 OF 04 CG 34 CODE RT-695-D CO)
-jr 317 16 UWfetf S 13 COMPLETE, CLOSE V-317 OUTLET 4
4 PUMP
17 L#i IN 7* <216G> WATER & HEAT TO 190-195
I, DEGJF
, .
I USE LBS
I I | l
---gg-g
ACCT LBS
317 118
CONI'D| 4 |.
Ix^dJLATE Th r u s p a r k l e r u n t il s o l u t io n is
#TAIN AT 190->95 DEG. F FOR S 19 & .
ORD: HT/dC,,DEG. F & RECORDER
RECORD: STARTCL4ITOTAL MI NZ1_CLAR *
I` ^
_
\
IS COMPLETE, PUMP V-317 THRU
-STWKCe R INTO V-100 RtJN.jC-5' (90G) WATER & HEAT TO 190-195
15 MIN THRU SPARKLER, PUMP V-317 |
ARKLER INTO V-100
MT, BLOW OUT SPARKLER INTO V-100
}
TO 165-170 DEC. F (TAKE 1~ QT. - SAMPLE) I
I'(WITH AGITATION ON)
I TEST FOR CLARITY OF SOLUTION:*-,SHOW 1 QT. I
I SAMPLE TO SHIFT SUPERVISOR FOR APPROVAL
1 (EXAMPLE OF ACCEPTABLE CLARIFICATION OF
} N-740-C IS AVAILABLE IN OFFICE TO COMPARE I
' WITH)
f
f IF S 23 IS OK,. CONTINUE WITH S 251 IF S 23-1
" IS NOT ACCEPTABLE, RECLARIFY THRU SPARKLER I
f IF S 23 IS OK, REHEAT V-100 TO 165-170
i DEG. F FOR -S 26
.
'
TO 16" < 15900
NV-
EAT V-100 TO 165-170 DEG. F .
RUN IN V-324 HYDROCHLORIC ACID THRU DIRECT
1 LINE AND RINSE IN
M__.3---.
L^TTft 15 MIN AT 165-170 DEC. F
1 ADJ TO 50" (4970G4 AT 34-38 DEC. F
| RECORD: TEMP_20--*#EG. F AND IF NECESSARY H30X330
[ ADJ TO 34-38 DEG./F &
RECORD: . TEMP^j/.___;DEC* F . ,v
I ______ I
1
45" (4320G) WATER INTO V-10T
I ON AGITATOR AND< STEAM- AND DUMP IN
GANESE SULPHATE
-..,L
P IN BARIUM SULPHATE
.
0 .150-160' DEG* F AND. STIR s . ..
.PH (5.0-5.5) '
PH. ABOVE 5.5, ADJ TO PH 5*5 OR LOWER
ULFURIC- ACID ^
-ASSUME 78%
_____ : . PVUtjjujLjl ' ;
'
^OTE: IF PH TJELQW. 5.0> DO NOrADJ; UPWARD
n 6l d FOR S 58
p-1400 | |Li25&- I,
r 1'
1 . sjm-w. 1
r -* ISL.I-
.j
-T.rfK; 1 .' I
336-B [ 65-A I
27-D
140 250
r:>s
DUP050061087
MAKING INSTRUCTIONS.:BATCH UNIT
&3UIP 1
1
-MENT I 1 PAGE 03 OF 04 CG 36 CODE R.T-695-D <0) I
1 '
' 40 *k"R,UN IN 47* (1610G) WATER INTO V-322
J
Ml ywn&H AND POUR IN SODIUM HYDROXIDE .
I
______5ldi3JL i 142 kmJMP IN FROM S 3 3-HYDR0XY-2-NAPHTH0IC ACID I
&*,,
1
r.. j.
USE LBS
./:'V';;L
------- --U
. 1--
feW*H 1-HYDROXY-2-NAPHTHOIC ACID ON POSTAL f ,
t l>i0SLANCE AND ADD LOT /gLJ&X--
I
| 44 L4?EAJ TO 70-90 DEG* ^F
,. '
I
145. L^Cn- IN BLANCOL N IN ONE TO TWOMINUTES
1 27
146 IsWHP IN -TETRASQDIUM PYROPHOSPHATE 6 STIR 5 18
i iJaH OR LONGER TO. DISSOLVE . *
I
| N-CODE | ACCT
I LBS
1~
I
I
I *' I
7-D 470
82rC^;
l b 1 1:80-0.1
.1 '| 1 567-B -l f 479-D 1 I1
|T
27 8
^ 313/ 147 KtStlGH SODIUM NITRITE 6 POUR INTO
i j^rOR $ 50-
____ '
:m<P ) I
,.. ___ \_
1 725-A f 365 i
1 "1
: '322 .. .10
-448-T ADJ V-322 TO 65* (2240G) AT 77-80 DEG* F. I
1 1 & RECORD: TEMP_JV.1_DEG, F
I
-W^l SLURRY TRISULPHffStrSOAP D WITH 30 GALS
I 160
WATER IN DRUM. POUR IN AND STIR 5 MIN.
|
I
1I 1 |.
I
j I 39-A I
1
116
IN N-725-A FROM S 47 AFAP. INTO V-100 I
1
STIR30 MIN AT 36-38.DEG* F MAINTAINING . |
f
"CR, +KI /
l --1
RECORD: TIME STARlj..t.CR___ ll.KI,,_l__ i
1
- . TEMP,,_^^LDEG. F
II
NOTE':
,1
I (1 ) IF CR-, KI-. ADD 205= *AS IS* INCREMENTS! .
I }
HYDROCHLORIC ACID .
ASSUME 32ZI______
RECORD: CR______ .<+), KI___ ___<+)
I
| (2) IF CR+, KI- ADD 204 "AS,IS* INCREMENTS!
I SODIUM NITRITE .*
ASSUME 33% I_______
RECORD: CR___ KI__________________< + >
I
TEMP___ ___^_PEG. .F
I
COUPLE V-322 THRU UNDERSURFACE DISTRIBUTOR i INTO V-10 IN 904110 MIN (USE 9/1 6/.ORIFICE) !
CORD'- START_fer__TOTAL KIN,,^Lt __
I
S 53 COMPLETE STIR 15 MIN
l
RECORD^ DIAZ0^2i__X-): BASE._!!_<+)
I
I PH^ji_<7*0-8.0) TEMP_fc!LDEG. F (60-65 F) I
I NOTE:
-1
| (1) IF PH IS. 5.,0-7.0, WEIGH AND DUMP IN 1
I
304 "AS IS* N-7-D DILUTED TO 30 GAL
I
| AFAR SODIUM HYDROXIDE
ASSUME 50% | _______
| (2) (FOR PH ADJUSTMENTS USE ONLY DILUTED I
>>r N-28-D AND N-7-D)
1'
Wh I ADJ TO PH 9.0-9.5 (SEE ATTACHED PH ADJ AID)!
.'I t HYDROCHLORIC ACID
ASSUME 32% I
(1) IF PH IS- 6 5-7.0, WEIGH 404 AS IS
1
,|
N-7-D POUR INTO 50 GAL WATER (1/2
1
1
FULL) IN PT 6 RUN INTO CV 100 IN 15
1
1
MIN & RINSE IN BTj STIR 5 MIN 6
1I
I|
RECORD: PH ^ fIi:L.___<9.-9.5)
1|
AW* A&f.Ur. ~P$&
57-A 1____ 28-A Ui:___ 725-A I___
fr
7-D | L___ 28-D 1______
DUP050061088
EQUIP I
EQUIP WENT
I . USE
USE PACE 04 OP 04 CG 36 CODE RT-695-D (0) I LBS
N-CODE I ACC1
N--CODE ACCT LBS
1 0
2) IF PH IS 7.0~7.5v WEIGH 35* AS IS N-7-D I .
I
11
POUR INTO 50. GAL WATER <1/2 FULL) IN PT & l
I
CONT
RUN INTO CV 100 IN 15 MIN. RINSE IN PT. I
|
STIR 5 MIN 6 RECORD: PH____ ____ .^<9.0-9.5) [
I
3)' IF PH IS 7.5-8.0, WEIGH 30* AS IS N-7-D r
I
POUR INTO 50 GAL W,ATER <1/2 FULL) IN PT 6 !
|
RUN-INTO CV 100 IN 15 MIN. RINSE IN PT.. ' I
|
STIR 5 MIN & RECORD: PH____________<9.0-9.5) I
I
4) IF PH IS 8.0-8.5, WEIGH 10* AS. IS N-7-D |
|
POUR INTO 50 GAL WATER <1/2 FULL) IN PT 6 1
|
X RUN INTO CV 100 IN 15 MIN. & RINSE IN PT. I
!
>
STIR 5 MIN & RECORD: PH___________<9.0-9.5) |
|
5) IF PH IS 8.5-8.9, WEIGH 5* AS IS N-7-D |
|
POUR INTO 50 GAL WATER<1/2 FULL) IN PT 6 i
I
V fe , % fc
RUN INTO CV 100 IN 15 MIN. 6 RINSE IN PT. STIR 5 MIN & RECORD: PH_____ __<9.0-9.5)
"IF PH IS ABOVE 9.5, DO NOT ADJUST
j 1. I
I I I
RECORD: PHj/i:_SODIUM HYDROXIDE ASSUME 50Z j_______l
NOTE: ADD N-28-D IN-5* 'AS IS* INCREMENTS I
I
TO APPROACH PH 9.0-9.5 THEN USE
1 .I
LESS N-28-D HYDRQXHLORIC ACID
JI
<CONCENTRATED N-28-D 6 N-7-D AND TOO LOW |
COUPLING TEMPERATURE CAUSES MASSTONE TO
I
i
TOO LIGHT)
*I
SHUT OFF AGITATOR
t
11
S SSSS SSSS'SS 3S S'SS:
107 INC S S3 HEAT V-107 TO 210.-212 DEG. F J
12 UT OFF STEAM
I
TE: IF NECESSARY REHEAT V-107 TO 210- J
r2 DEG. F PRIOR TO START OF STRIKE
I
PUMP V-100 INTO V-107 IN 70-75 MIN.
j
V-107 TEMP DROP TO 200-205 DEG. F
1
i^ORING STRIKE THEN MAINTAIN AT 200-205 DEG.|
iX^FUR BALANCE OF SjRIKE WITH AGITATOR. SHUT I
IN V-100
, /X
U-RECORD: STARTCL^__T0TAL MINjLLSL
I
161 U4SREN STRIKE COMPLETE, HEAT TO 21.0-212 DEG.FI
162 KSTiR'15 MIN AT 210-212 DEG. F
^
163 kFLOOD TO 180-1901 <182400.
? ^RECORD: PH_2*.y___ <6.5-7.2) AND STOP
fj *
AGITATOR
-
I I I l
iI
fi il
START
FINISH
OPERATOR
i.i i i.
ri
7-D I _____ '""T
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' DUP050061090
DUP050061091
11 DUP050061092