Document MM3jzgjrvogEXbd4gzvmyMO8x

: #R226 _ 081 ACUTE TOXICITY TO FISH (FATHEAD MINNOW) TEST SUBSTANCE Identity: ArefmeirxrteudretocaonstPaiFnOiSng, pFeCr-f9l5uo,roorocatsanaescuolmfopnoanteen,twhoifcFhC-m3a0y31a,lso(1b-e Octanesulfonic acid) (CAS # 2795-3-3). R30e3m1a.rkCsu:rrentThienfo3rMmaptrioodnuicntdiiocnatleots nituimsbaemriwxtausre2o. fT0h.e9t6e%stPsFaOmSp,le20is%FCdiethylene glycol butyl ether, 62.11% water, 10% ethylene glycol, 1.92% propane sulfone foamer, 2.02% polyoxyethylene monooctylpheny ether, 2.88% sodium octyl sulfate, 0.06% sodium lauryl sulfate, and 0.05% benzotriazole. sTthuedifeoslloonwiFnCg-i3s0a31n,aLbobrte2v.iaTtheedsseusmtmudaireysoafpmpullyttioplae mfiaxtthueraed wmiitnhnow incompletely characterized concentrationsofimpurities. Data may not accurately reflect the toxicityofthe fluorochemical componentofthe test sample. METHOD: Method: Not given. TGyLpPe:: NAocute static Year completed: 1976 Species: Pimephales promelas SAnuaplpyltiiecra:l Nmootnigtioverni.ng: Not given. Exposure period: 96-hours Statistical methods: LCs values determined by graphic interpolation. Test fish age: Juveniles Length and weight: Average length = 48 - 50 mm Loading: Notgiven. Average weight = 1.4 - 1.5 g (wet) TPeresttrceoantdmietnito:nsN:one. Dilution water: Aerated carbon filtered well water Dilution water chemistry: Not given. Lighting: Not given. CSotnocceknatnradttieosntssodloustiinogn rparteep:arOanticoen: Not given. Stabilityofthe test chemical solutions: Not noted. Exposure vessels: Not given NNuummbbeerr ooff rfiesphlipcearterse:pli1cate: 20 per test solution for one study. for remaining studies. -- Not given 002860 Number of concentrations: five plus a blank control Water cphHemriasntgrey(r0-a9n6gehosudrusr):ing the studies: 7.27.4 (control exposures) Temper2a1t-u2r2e raCn(gceon(t0ro-l96exhpoousrusr):es) Dissolved oxygen range (0-96 hours): RESULTS 5.0-9.2 mg/L (control exposures) Nominal concentrations: Blank control, 100, 250, 500, 750, and 1000 mg/L for two studies (7/6-10/76, 7/27-31/76). Blank control, 250, 500, 750, 1000, and 1250mg/Lfor one study (7/20-24/76). Blank control, 100, 180, 320, 560, and 1000 mg/L for one study (8/10-14/76). Element values: 96-hour LCs range = 560 -- 800 mg/L Element values based on nominal concentrations Remarks: Testing was conducted on a mixture as described inthe Test tShuebsftluaonrcoechReemmicaarlkpsrfoipeolrd.tiTonhealvoanleu.es reported apply to that mixture and not CONCLUSIONS The test sample 96-hour LCs; range forfathead minnow was determined to be 560 to 800 mg/L. `Submitter: 3M Company, Environmental Laboratory, P.O. Box 33331, St. Paul, Minnesota, 55133 DATA QUALITY Reliability: Kiimisch ranking 3. Testing lacks recordofmethodology used. There is a lack of characterization of the test sample. Test solutions lack analytical confirmation of the amountoffluoochemical proportion in the solution. REFERENCES These studies were conducted by the 3M Company, Environmental Laboratory, St. Paul, MN, 1976. OTHER Last changed: 6/26/00 002861 ' 740101 UATIC TONICITY WORK SHEET ENVIRONMENTAL ENGINEERING LABORATORY - Type Test___ 96 Hours = Sint, Test Organisa_Fathead Minnow bate started 7/6/76 Tine stareed____ 2200 om Material Tested, f 7% = 22 2 Avg. Weight 4g site_d.20m vate Completed 2/10/76 Plotced 16g, Tnaugll Dilution Water Carbon Filtered - Well Water = Cone. sur2v4iyvharls pH vpmo 48 hrs Survival pH bpoom Sur72viavharls pi bpoom Su9r6vihvrasl pH ivpo0 era] 10[75g] 100 Frelce]too file] too [12s ser |a7 too[72]5=2] too[72 ss 100[zzlaa]100 [zag] zo |too[72]0]too J1a]4a] veo Jze[da]tooJia] o|too[750]loo[71]4s] Ao Juolaz]do fad] LLogo olo] ao[laa] zo ldo] 0lull Average Temperature 2(C| 2] | ! Leg, Caleulation ' EEE EE ` Em EHm TE e : MEeM e foe Ee 8 & na S Ss HEEEEepana z EEE EEE Tr a He HE EERE = EEE EE g BoE ThE HEH HH h soo EHH LH HEH (HEH 4 10 20 30 40 S50 60 70 8 90 100 % Survival - 3 002862... id 740101 ENVIRONMENTAL ENGINEERING LABORATORY -_ AQUATIC TOXICITY WORK SHEET Type Test___96 Hours-- Cine Test Organisn_Fathead Himou MwaeteirigalhTsestefdLfo5-CGs-8oB350nlSeuobnvy 2 Date Started 7/20/76 Date Completed, Tine seated 2tzom noses eso Dilution Hater Carbon Filtered - Holl vater 7/24]76 620 well 2CEs pe ssB hes p 72ThesRI, se nes vo Conc. Survival pH ppm Survival pH ppn Survival ph ppm Survival pH :pp ems] 100 [13058] 10[ales] 100 252]100[225d ougll_teo [21] 52]100[z0]50]100[telso] roo[elas] : oo |"too [1]53]100[z]So]100 [rola]too [zoe] 0 |wo[ro]s2| 65 [ofag] olela] oTI ooo |too [rolse] 0leglas|o[+]o[4] \ clasTelsol 0 ales] 0 [47]od] Average Temperature SC . Comments: Torlamd Wine dg Yk Solute ESET EE f . Cg, Calculation Hi : CE ne E eae S eee g ESEEEEEE EREey @ imme yg 8 Eee Hana aa i < -oiBiEEmLLL EB BREE HEE EEE EP F e EHEEEEH Hoe PH h E eE nHs H H @ ( FE Hi on HHH 4 10 a0 100 LELTLITTTTT 30 1 do SoTdOE 70TTT TaTT saTSa0 % Survival -002863"i ' 740101 ENVIRAOQNUMAETNITCALTOEXNIGCIINTEYERIONRGKLASBHOEREATTORY -- Test Organisn_Fathead Minnow we. weighs LS Date Started, 2/27[76 Date Completed. Tine Started 3 300PM, Plotted Lig Dilution Water_Carbon Filtered - Well Water Bemted) ASitge_S ou Zz] 76 zoornl) eral 10g [ial 67] toeFale]ipo Ta] soo riled] 24 hrs 48 hrs 72 hes 96 hrs Cone. Survisval pH 0pp.m 0 Survisval pH bpp.m 0 Survi%val pH Dpp.m 0 Survisval pH 0pp.0 M=eafolio]ve ross] 100 furlsal roo Jrolcd eo |too [0]60]100 fro[c2] toofrolsoltoo [ze] ca | 100Jpalso] ao [ro]So] go fiolag] 60[ilag L020Luo litle] Tecleol 0141 0 [HF] Average Temperature d 2) 2 . 1g, Calculation Een R====s=cs=cc TITEL] FELT 8 Ee Tee THEE eE e ne Sooper LLL 5 BFEEER F fridilicnn [EH EH @ i Ha ET THT Fp TIE Ei HEY a8 Belin g s EngSniEn Ll TEE H HT E 2 FEE Fr nds IE Le ELH ER HEE s gE FH Ii ithe ETH cir TH 2 Prvanns0nsusnn 10 2r0edS3A0 ER4E0DNRENSo Bian e0470)0PARR)8KnaR8unuan100 m + Survival 002864 , ! 740101 ENVIRAOQNUMAETNITCALTOEXNIGCIINTEYERWIONRGK LSAHBEOERTATORY - Type Test___96 Hours = SAMI, "Test Organisn_Fathesd wimow Material okCagal by, ave. Weight 158 sik Som Date Started Tine Started RL0/z6 2 000m Date Completed. Plotted Log, Dilution Water_Carbon Filtered - Well Water (Pepinf f-14-16 a oy L Gone. 24yhrs Survival pH bppom 48 nes Survival pH bpra oSuwr72vivnaels pi bopeo 96 his survival pi 0bp.0 owe] pyTrsfee]too Fa[salvoo Jado] oo [ralsd tceoug"ll0|wtooo[[1r0o]]62]]to0o [1z00a5a2[] Vvo0 [zo] [role vio \oo fiolag] rola 220| eo [2660] 00ledlaq|too|zo[as]loo|agldd] to | wo Juoea|QoJenldu| So Jrelas]so ealad Camlolol o [ETolf[0] erage Temenenaee 2FC] oomentpse TWALAL 150 D2 Ug pac tl 2 v SL pe syCalculation fn OO SEEE EEE TT THERE th Taree Ee soiree] HFi ree ee T EEEEER TRETII a ae 5Sem FEaELnETLn REEH r ae $ Enel Hr HET LE pn Re : 0 am4 S =< 2 5 r sq0E10EE20: 310 40 so e070 soTH90EE100 % Survival 002865