Document MLryVkeyZoZqykGqRqGK7nox

FILE NAME: Johnson & Johnson (JAJ) DATE: 1960 DOC#: JAJ035 DOCUMENT DESCRIPTION: Letters from Battelo Memorial Institute with Reports and Test Results J 9 B attelle M em orial Institute .5 0 $ K I 1 6 A VN UE C 0 LU M S I, 0 H I 0 April 12, IMO Hr. N t . unir Offici 6f Gnral Camiti Jehnsan nd M m m Mm BftmMiik, mm Jxy Bac* Mr* Werner ThU lattar port camiti ih Rotati* tali M i in ut Mbacatory In connaetlan Uh th prparation f ih pat*t application "Platy tele Banofieiatlan*. AM BltamM.In thit wpart nera airi mino Italian "Th fi li Mvi xp^nt w n nB io Batamln whsthar anlenlc urfaaa activa genti cibar thon th Aaroaolo, ! a or, nera affiativi In colettivi fiatatilo of platy tei* Font anisnlc magenta ara colletai for tha study* Thoco oro UatoB in Tibia 1* TABLE i* ANIONIC KBM&MTS STUDIED m as TraBa Hama Dopami ME Anatra 1216 Targltol P2B Igapan T Claaa or Paratila SaBim lauryl sulfata Alkyl aairis aulfanata SaBim Bft (2<*thyl haxyl) phoaphata A aubatitutaB aaiBa CjTHjpOOHtCHgJCaHolOsKa Main Vaca Oatcrgant, Biaparacnt, Mulalfylng gant Ootargant Matting agent* miai* Tying agant Datargant Booti on iho available flotation lltaratura, l i appura that too of th reagenti, Anatren L213 and Igopan 1, bava th am froula. Tha Biffar* ano btwain tha la that thay aro narkataB aa ponBara at Blffarant caneantratiana, Anatra 1219 at 10 pa* aant anB Igapan T at 31 par ont* Tha raaolta of tha axparionta in tha currant prograai, aa m il aa tha raaulta of aavan pravieualy rapmrtaB rparimntl, ara pmaantad In Tabla 2* Protected Docum ent-Subject to Protective Order JNJNL61JOOOOOWSO V* ao S c) S o ? 0 1<5 O 1 Feed S o lid s, Dowfro th Experiment % PH HC1 250 TABLE 2 SUIMARY OF FLOTATION EXPBtllffNTS WITH SURFACE ACTIVE REAGEHTS F lo tatio n R eoaents. lb/tcn o f flo ta tio n feed Other Ragents W eight Per Cent(b) P laty T le R e su lts, F lo a t lie ) M ineral C o u n t, per cent N o n p ie ty T alc D olom ite T re a d it O th ers 163(4) 7 .2 6 .8 BW 7 .2 4 .4 1.79 **-- 8 .4 7 .5 1.75 0 .0 7 - Doafroth 200 134(0 8 .0 4 .7 1.77 0.07 187(d) 7 .3 7 .5 -- -- 1 .3 2 - Aerosol OT 182$* 7 .4 6 .8 1.73 0.04 0 .7 4 - Aerosol 18 legi**) 7 .0 6 .8 1.80 0.04 0 .6 2 - Aerosol 18 328 8 .4 7 .2 1.38 0.05 0 .4 7 -- Sodiua Lauyrl S u lfa te - Anionic 329 8 .7 7 .0 1.37 0.05 0 .0 6 8 - Sodlu e Lauyrl S u lfa te - Anionic 330 8 .4 7 .2 1.42 0.05 0 .4 6 - A lk y l Aeide Su lfon ate - A nionic 331 3 .4 7 .1 1.42 0.05 0 .1 8 - So d ila, d l (2 -eth y i h exy l) Phosphate - A nionic 332 8 .7 7 .2 1.37 0.05 0 .4 6 - Sd k stitatcd Amide C n H s O M tO b Jc u u n jIh - A nionic 334 3 .8 6 .9 1.35 0 .04 0 .4 6 - T riaeth yl-n -d o d seyl a m e n i . ch lo rid e - C a tio n ic 335 8 .8 7 .4 1.35 0.05 0 ,4 6 - T rlm th yl-n -d o d ecyl e m a n i ch lo rid e - C a tio n ic 336 9 .0 7 .6 1.31 0 .0 4 0 .4 6 - O ctylaaiiM - C a tio n ic 337 9 .0 7 ,5 1.32 0.04 0 .1 1 - Octylaaiine - C a tio n ic 338 8 .9 7 .3 1.35 0.06 0 .1 7 - Hexedecyl D leth y l Aine - C a tio n ic 339 3e8 6 .8 1.36 0.05 0 .4 6 - S m t it u Manolaurate - N onionic 340 8 .4 7 .2 1.39 0.06 0 .4 7 - S o rtita li Nonolesirate IM lyoxyethylene D eriva tive - N onienlc 341 9 .6 6 .7 1.39 0.05 0 .4 7 - Secondary Aadde o f Laurie Acid - N cnienic 342 9 .0 7 .0 1.32 0 .0 4 0 .46 - Nonyl Phenyl Polyethylene G ly co l E ther - Nonionic 343 9 .0 6 .6 1.31 0.04 0 .44 - d o le Acid Plus Sodino d e s te - A nionic C o lle c to r 3 6 .3 3 4.4 6 4.8 5 9 .0 6 9 .7 7 0 .8 7 0 .4 9 3 .0 7 0 .8 5 6 .5 6 9 .3 70.8 7 1 .0 7 5 .6 88.1 7 1 .2 7 0 .9 7 7 .2 7 2 .8 7 2 .9 8 2 . 7 6 .5 95le ) 96 98 98 >97 <99 >96 >97 >98 >98 >98 >98 >98 98 96 >97 99 99 <99 99 >98 <96 HW 4 l 1 >2 >1 >1 2 <1 <1 <1 1 >1 >1 >3 >2 tra c e tra c e <i tra c e i 4 tra c e tra c e <1 tra c e tra c e tr e e a tra c e tra c e tra c e tra c e tra c e tra c e <i <i tra c e tra c e tra c e tra c e o i tra c e <1 O tra c e tra c e tr a c e tra c e tra c e tr a c e tra ce tra c e tra c e tra c e tr a c e tra c e tra c e tra c e tra c e trace tra c e tra c e tr a c e tr a c e tra c e tr a c e tra c e tra c e tra c e tra c e tra c e tra c e tra c e tra c e tra c e tra c e tra c e tr a c e tr a c e tT sce tra c e tra c e tra c e tra c e Per Cent, , D olom ite 1CJ 0 .4 0 .2 0 .5 0 .3 0 .9 0 .4 0 .6 0 .8 OJ 0 .2 0 .3 0 .3 0 .2 0 .3 0 .7 0 .3 0 .3 0 .3 0 .2 0 .2 0 .5 0 .9 (a) F lo at 1 Is fro th removed In fiv e ndnutes. (b j Assad'en flo ta tio n feed (c ) Calculated fr a , 00a a ssa y . _ (d ) See "The P hysical C oncentration o f Ita lia n No. 2 T ale by F lo ta tio n -- in v e stig a tio n o f F lo ta tio n Reagents" S a tta lie Progress R ep ort, January 31, I960. (e ) This Is a corrected fig u r e . The fig u re show la the Anuary 31, 1940, rep ort as 92 per c a n t. A recount (in d u p licate) as nude o f the product and shoeed I t to be 95 per cent p la ty . ( f) See "The P hysical Concentration o f T alc Ores--F lo ta tio n o f Ita lia n No. 2 T a lc " , B a tta lle Progress R ep ort, Ju ly 31, 1959. c. 0s 1 f I B a tte llo M em orial Institute Ik* H, Lt temar 9 April 12, 1940 P a g e ______________ Hm mult i ItAMkMti 499 t MS intimi, n v u lii that ttna # H h m almi m vtfttf im M m m tent m Im im ttll A lM M iA l til f 9 fBMrlll M M *Mt M M lM iV l Iti ly MMMMt tint 4M tu* |lM MMlt M fM4 til AtMMtlt M l Ant*i 1219, ftp H llM M * li MMM 9i i Hm iM ** my I 44*9 jmrt Mt n y Him tm 4m M m iarnffteinit Mint f Hm m M it iM W tttn fu i t i tht btelMbl wlHi Hm Aim n Ii m m i m 4 Ut tlM Hm* Mapanti# 4 In M it i Hm dinit* t t m i lMf M Hm n ln U m fiM m Um u n to ti liufftiU M i it Mld tow tMiHiHMiMd Hm Ntffit ip yU iitl {* Hm Am m 1* Hin t)M MMlt itm Ibi nnrtowt win antani Mipwt m m in U iM ii to tel mtin tow Httol Hilt toM M tln U y w to tateshma* It I m Ii Im m * mto to pHtocad Htk ltoltto amt *f Mitianal litonttoy auk In ml* to Mito m m Um nf tto ayt t* to toiltoto In Hm mHIm IIm * Oteaa Hm M >totil Mt pfwtemly AtmlMdi m i Unit it tolto MrfMM m Hm w tn it i n toitoto totototo Hm fi!* TJMMf*** Unti ni M UM ll tolto MttM tint M li M fatty id typa wttotto| m m toW to ttto m Im iitlfitiM Stotot taaomte m m d m totanUy to M f HmI* toftolto l i u to to Ml m ttiH U tol Hmm na dun in tkl a* TAKC a CATIONIC* MUONIC, AH>ANXQNfC U U D U SIISI Td ito-- Anp*atf 12 Mmm nMHM 14 to H 1m 21 ito ta y a Txfiti m Cl nr temute____________ lym ItlaitofiHHUlMyl --inti tklMrtda totylntoa towtoiyl Htothyl Mini savMtei M l tnHtw nantlMnt pdyMh itoylM tortvatly* A Mndny mid f lamrie iato tenyl ytoayl y d y a tto lM flycal atte otite MSdMedl* M ito Catlani m Mittente # Antenl* Naiii Hi totttof afartt, dt*tnt 6llaatar clltr tenlatfylA mt tetttof tntt dtotomto tettino t i Mteatnit tttef fast CUften rotocttv# O rdsr JNJNL61_0OOOO1482 . B a tte llo M em orial Institute U . K . L i * * * P a g e -JL _ d P U 1H * Ix p w W t# te M a r n i m i U i * t t a y u u l i i - t N 4l M l tiu ikNMU> U r f f M N ttH i S* litlMi M2 l | k l f M i w t f f a# pat m i I tha fia ta ti * f i U h p U ty te U M tM i f M t i t l p a v m W i M f t t M U T f M y t M t mm a tta in I tha teM hei M m M m U I l a lp atal H t 1 . h lapHribu t M h In whiah Aavaaal 1 1 w * Mi 4k * l | h t m w t i y te F l u t 1 h 4 l Th* niy uyeriewit In ihl ul* 1* chicli U * im i t i w n ntt u tia fu tu y m 4 ) t ft U a uniti* f Ule u l i M rallM lu it mm ml Th* #**th ytM ui f*t ffiito w t 943 cmulnM haut 1 a Mt 4*1M it* Ml i M lt m tfcitk MMhllh p**tl*U* M U ll Mah afin lttly m M nt h lattai i p ltty. Ih* anelati trm thla uM m * h fell* U ) Slava tat iwtM t km b*tn fami end th*n u y ha uny au< that an h m* Ukaat&valy* !* Mua th* ta t in t tatti* pf ul*tiyiataHl pu aaat platy til * (3) Th* t**fut* ivi*# ami fc*m U h* nutufttl in thla tMy f 4 m Italian Na* t tal h u ll n u b* itim i m l a t fu la tal* vu uh * Ma Mulatta* n a at aja* tai Mata tba a ip itiii *f th* u n it o ) I* aa nah m ili ( I) lh* autant a h u ll ha ttM I Ma Manu af any D nftniki Ihl a M t U m la Sapatlatnt 990 ta 949 inalati** huaai* ihn M l MP th* pa u iaaaly aptt tai m k i U llfcfa lu 4 m haai aapetUwite* au ani* ani M iai a m M mU m a l tha Accanai* litk n U n i r Afhdj |a pi^|wI * nm|uL* U ) Uhm au tant* U U am ha m i Mm I f u m* In uy nm ptlt-plant au (0) Tha mpaitoanta ahaufti ha unflanadl hy lapMuta latta <) Ih h u t w ttu ia * mW ha au lu tad *ith aalatian ta tha* u t pu tan f f u l. k p u tlu f 4m laalnf a u iriti In tha Battalia apart *tha Myalaal CM untutlan atf Ita lia n i . a Talc by fitta ti --In vu ti* af M autlaa aatanta" Jhnaaay SS 140, m a lu i M In U i u thla lattar apart al m pattai M m . Protected Docum ent-Subject to Protective Order JNJNU1JKW 001483 / B attello M em orial Institute far. II. !.. m m i P a ge_JL _ M* IHO mut in n i tk Nlta**t far H* Minati al altlaaal aaataftt far Ita ftalati af pUty ti*i K i tiUy# attar aafaata M tih Urvaatlfata Ma taaMwil *I#M a w all a aaaa batta*. ft w a ii la maawar tMR n W tyaiaa a anwli u n t--pmiiaala i l r l . f M i ** Iha rifiati nata an tha iabarattty aat 4aaa*iba la tfcta apart m m m M In Battali lifcwalaty Baiata I M Ma. I86B pay* ta IO, iMlaalvt Ma wm ba pia ta nana* any ptatian that yaa any bava tafitaina thia m A . V a ty tM A y y a a M f MCUb b a a ll it . aa* a . H. AaHtan (I) V * ! Chi l i Protected Docum ent-Subjw t to ProtectW . orttar JK JN L81JW 00014M