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Ethanolamines/Glycol Ethers Tier 3 Procedure Section Number: Issue Number: Original Date: Revision Date: Title: References: 504 1.0 1 -4-96 Author: Larry Locicero E Series DEG/MEG Questionnaire E Series Glycols Fault Tree (503) 504. E Series DEG/MEG Questionnaire To determine the root cause of the DEG /MEG problem, answer the following questions. 1.0 is the Set points 1. Reactor Steam Press -- 475-485 psig 2. Reactor Outlet Steam Flow -- 1500-2000 Ib/hr Instruments 1. Steam Press Transmitter 2. Steam Regulator 3. Steam and Condensate Flow Meters u: 2.0 Is there a tube leak? Analyze all column overheads samples for water. If a samples is above 0.2 wt% H20 for T-l 10 or 0.05 wt% for others, there is a tube leak in either the reboiler or condenser. 1. Notify maintenance superintendent. 2. Shutdown system and prepare for maintenance 3. Determine location of leak by: Analyzing column bottoms for Ca High Ca means cooling tower water is source and the leak is in the condenser. Helium detector Add to shell and detect using ejector system not vacuum pumps Sample and analyze streams exiting the R-103, T-110 BTUs and T-110 feed coolers for water. Notify maintenance superintendent of problem. Print Date: 4/19/98 Page 1 of 2 Paper copies of this document are uncontrolled and not subject to update. The controlled version can be found in file \tsguides\Megs.doc. DO A 059116 CONFIDENTIAL Analyze all raw materials for water, if greater than amount listed below, this is the problem. Notify maintenance superintendent of problem. | Raw material Alcohol Catalyst * Oxide Acid Recycle Sample Location P-104 A/B D-106A/B Call Glycol II DV-102 DV-113 or Recycle stream Maximum H2Q 0.01 wt% 2.80 wt% 20 ppm 0.015 wt% Recycle streams<0.05% Corrective Action | *Note: Glycol II should run an analysis on their tank to insure there is no leak in cooling coil system. The condenser on the EO drum may be a source of water, but unlikely due to higher pressure in tubes. This can be determined via 1. A TOD analysis on the cooling tower water off the condenser or 2. Reduce CTW pressure and sample condenser water effluent for EO Print Date: 4/19/98 Page 2 of 2 Paper copies of this document are uncontrolled and not subject to update. The controlled version can be found in file \tsguides\Megs.doc. DO A 059117 CONFIDENTIAL DO A 0 5 9 1 1 8 CO NFIDENTIAL Ethanolamines/Glycol Ethers Tier 3 Procedure Section Number: 505 Issue Number: 1.0 Original Date: 12-25-95 Author: M. Jordan Revision Date: Title: T260 Operation and Trouble Shooting Guides T-260 Operation and Trouble Shooting Guides Click on double arrows in bottom right comer to flip through page List of Fault Trees - 1. Column Instability or Atypical - 2. T260 High Bottoms Color - 3. High Water in T-260 Overheads Page 1 Print Date: 4/19/98 Paper Copies of this document are uncontrolled and not subject to update. The controlled version is \tsguides\t260op.ppt. CONFTDEN T-260 Operation T-260 Unstable or Atypical Parameters (See additional fault trees for specific problems! ip, O <X oc Page 2 Print Date: 4/19/98 Paper Copies of this document are uncontrolled and not subject to update. The controlled version is \tsguides\t260op.ppt. CONFIDE- T-260 Operation o <c o o T-260 High Color (Note: Color is always caused by temperature, oxygen (air), or reaction unless you are adding a contaminated recv< Page 3 Print Date: 4/19/98 Paper Copies of this document are uncontrolled and not subject to update. The controlled version is \tsguides\t260op.ppt. DO A 0 5 9 1 2 1 CO NFIDFNTTAl. T-260 Operation HI WATER IN T-260 OVERHEADS Page 4 Print Date: 4/19/98 Paper Copies of this document are uncontrolled and not subject to update The controlled version is \tsguides\t260op.ppt. A 059122 CO NFIDENTIAL Ethanolamines/Glycol Ethers Tier 3 Procedure Section Number: 506 Issue Number: 1.0 Original Date: 12-25-95 Author: M. Jordan Revision Date: Title: T-120 Operation and Trouble Shooting Guides T-120 Operation and Trouble Shooting Guides Click on double arrows in bottom right comer to flip through page List of Fault Trees - 1. Column Instability or Atypical - 2. Steam Problems - 3 High MEG in T-120 Overheads - 4. High Water in T 120 Overheads - 5. High DB in EB Page 1 Print Date: 4/19/98 Paper Copies of this document are uncontrolled and not subject to update. The controlled version is \tsguides\tl20op ppt. uu A 059123 CONFIOE'My IA1 T-120 Operation T-120 Unstable or Atvolcri Pametof iS-- additional fault tree* lor specific problem*! Page 2 Print Date: 4/19/98 Paper Copies of this document are uncontrolled and not subject to update. The controlled version is \tsguides\tl20op.ppt. DO A 0 5 9 1 2 4 CO NFIDENTIAL T-120 Operation Steam Problems on T-120/E-120 Page 3 Print Date: 4/19/98 Paper Copies of this document are uncontrolled and not subject to update The controlled version is \tsguides\U20op.ppt. T-120 Operation High DB in the EB <n/ t<---jr o h- <r o Q Need to define what to check/do Page 4 Print Date: 4/19/98 Paper Copies of this document are uncontrolled and not subject to update The controlled version is \tsguides\tl20op.ppt. DO A 0 5 9 1 2 6 OONFTDFNTTAL T-120 Operations High Water in T-120 Overhead Stream Typical level for EB series is < % Tvpcial level for PM series is < % Page 5 Print Date: 4/19/98 Paper Copies of this document are uncontrolled and not subject to update. The controlled version is \tsguides\tl20op.ppt T-120 Operation High MEGs in T-120 Overheads (see Glvcol Fault Tree for Addressing overall Glvcol Problem^ (I\\ <_1) 2O' h- O Uj Q <X U. OO O2 <J Page 6 Print Date: 4/19/98 Paper Copies of this document are uncontrolled and not subject to update. The controlled version is \tsguides\tl20op.ppt.