Document MJr00Kmj3yv5p0KOp7mRapEdx
PREPARATION NOTES:.
PROCESSES?
APPROVED BY
( >R014-A ' . <I> EWK 12/17/81
COMTYP JOB NAME: 32RC014AMI
TYPED BY: JMH
STANDARD HRS *
TIME
NON-BLEEDING
EQUIP MENT
NAME: "WATCHUNG* RED B
i USE I LBS
NOTE: DO. NOT START IP PRESS WILL NOT BE
i
AVAILABLE WITHIN 3 HRS AFTER MAKING,.MAKING|
SUPV TO REVIEW WITH P.fi. SUPV S RECORD:
j
PRESS WILL BE READY: 1______ M_
/ ._
<
P.R* SUPV__START MAKING..*__________M_____ /_._ _ _i
MAKING SUPV____________
I
N-CODE
ACCT LBS
NOTE: RUN IS* WATER INTO V-904* PUMP WATER FROM V-904 THRU DISTRIBUTOR, IF WATER DOES NOT COME OUT.OF ALL DISTRIBUTOR HOLES WITH FULL FORCE, NOTIFY SUPERVISOR-*
i I i I
RECORD: ______ BATCHES SINCE SPARKLER LAST i
i CLEANED* AFTER 4 BATCHES, CLEAN, DRESS
!
SPARKLER & PRE-COAT WITH 15# FILTER AID
i.
OBTAIN FOR S11 2-CHLORO-4-AMIN6t OLUENE-5- 1
SULFONIC ACID
I
OBTAIN FOR S35 3-HYDR0XY-2-NAPHTHQIC ACID j
INSTALL DV & CV RECORDER & CONTROLLER CHART!
NOTE: NOTIFY PRESS ROOM BEFORE .ROPING OFF |
AREA UNDER V 922
i
CLOSE OVERFLOW OUTLET VALVE FOR DISTRIBUTOR!
LINE AT REAR OF VAT
!
RUN 13" <1300 WATER INTO V^H? & HEAT* TO .
80-100 DEG F
'
ADD IN 2-3 MIN (DRESINATE X)
STIR 5 MIN i, RECORD: PH______ -<9*5-10*5)
STIR 20 MIN OR LONGER TO DISSOLVE FOR '4&
!
! i t I
130 !
777-A 740-C 253-C
Mi
530-A I 130
IN 37" C762G) WATER INTO V-922
;H IN V-926 SODIUM HYDROXIDE & RUN IN
YCAUSTIC SOLUTION)
M./2-_____ ,
TURN ON AGITATOR & STEAM & DUMP IN FROM S2
2-CHLORO-
LOT #10%
4-AMINOTOLUENE 3a ...........C...t.i
_ 12.
-SULFONIC .
ACID
... J.
DUMP IN <ACTIVATED CARBON)
UMP IN DICALITE, FILTER AID
HEAT TO 212-214 DEG F RECORD HT.^A^DEG Fi
fEC .DEG F WATCH FOAM* RECORD BY_3fr_.< + ) IF NECESSARY ADJ TO +BY I
SODIUM HYDROXIDE
ASSUME ! 0 %
5 0
i
.... }
LOT-______
COfliyp JOB NAME - 32EC01 4AMI PAGE 02
BATE PRINTED: '27/32
EQUIP MENT
I USE
N-CODE
PAGE 02 OF 03 CG 32 CODE RC-1 4~A (I) j LBS I
!
----- -- --------------- ------ ------------- ------ --------- ------------1-------- --- 1 ---'--------- 1
STIR 30 MIN AT 212-214 DEG F THEN SHUT OFF
SJEAM. WATCH FOAM., RECORD: SPARKLER
|
I
-RESSURE _??__._PSI, IF NOT ZERO NOTIFY SUPVRI
CIRCULATE 15 MIN OR LONGER THRU SPARKLER I
UNTIL SOL'N IS CLEAR, MAINTAIN AT 190-195 FI
FOR S20 * RECORD: Simi
TOTAL JEN--j L--;__L / CLARIT/____________
I 1
HT_( ___ DEG F, REC__/^l ,,DEG F
I
-I
MEASURE ^^^UNITS IN V-92S FOR S3G
(HYDROCHLORIC ACID) M,,./2=,,,_2,
28-B 557
68 < 669G) WATER INTO V-feU
WHEN ST7 COMPLETE, PUMP IN V-922 THRU SPARKLER, MAINTAIN V-922 AT 190-195, F, RECORD: STARTQTAL MIN_./Sa.__,,
,
i !
,| |
,-RUN 90 s (2600G) WATER INTO V-90?-*
DUMP CALCIUM HYDROXIDE IN AND STIR TO
SMOOTH SLURRY
'
WEIGH- SODIUM HYDROXIDE IN V-926 MJZsJ,
RUN IN 6 STIR F0RS39
1I
1 550 1 542-D \i
7-D I ... I
550 199
WEIGH IN PT FOR S32 (SODIUM NITRITE) M_______ \a&2u
;
j
| 725-A
368
WHEN S20 COMPLETE, STOP PUMP 6 INSERT V-922I
FOOT PLUG '
I
RUN IN 10' <209G) WATER & HEAT TO 190-195 F|
CIRCULATE 15 MIN THRU SPARKLER PUMP V-922 I
THRU SPARKLER INTO CV
'j
RUN IN 5" <1040 WATER & HEAT TO 190-195 F
CULATE 15 MIN THRU SPARKLER
PUMP V-922 THRU SPARKLER INTO CV
WHEN MT BLOW OUT SPARKLER INTO CV
''"'POUR IN CIGEPAL CO-630)
63
HEAT TO 165-170 DEG F
I
RUN IN N-28-D HYDROCHLORIC ACID FROM SI 3 IN!.
*ST;5 M I N
1
ADJ TO 45' (4266G) AT 32-38.DEG F USING.ICE 1&&X330
ECOR:
STICK
I
RUN IN M-725-A SODIUM NITRITE FROM S23 AFAPi
'<5-10 MIN) & RINSE IN PT STIR' 20 MIN AT 32-38 DEG F MAINTAINING
I i
+CR, +KI. RECORD: CR_j7tE,,,.C + ) KI__jrT_( + ) I
NOTE; <1) IF CR-,KI- ADD 20 'AS IS*
(
.INCREMENTS HYDROCHLORIC ACID- ASSUME 32% f________
RECORD : CR______ <T> KI___ __( + )
i
(2) IF CR+, KI- ADD 20$ "AS IS'INCREMENTS I
SODIUM NITRITE
ASSUME 33%
_______ I
RECORD: CR_______< + ) KI_.)
979-D
28-D 725-A
63
* Ur
DUP050060821
_____ CQMTYP JOB NAME = 32RC014AMI PAGE 03
DATE PRINTED: 7/27/82-
EQUIP WENT.- v;S " ---f.
CV 9
CONT
PAGE 03 OF 03 CG 32 CODE RC-14-A
<I)
J^BOMP IN BARIUM SULFATE * DUMP IN FROM S3 & STIR i MIN
3-HYDRGXY--2I- NAPHTHO'IG ACID
| ADD FOR MAINSTT&AJINING 33;2-38 DEG F THRU S40 4 RECORD'VOL.
I -USE 1 | LBS .|
470 |
I U__i
I-- ___J
ii*X330j1
N-CODE | ACCT K LBS
65-A i 470 253-C -U055
57-A.
<9^ 2arl^7 | mH 37* (363G) WATER INTO V-1 & ADJ TO |
i JX90-110 DEG F
i
j-SCi ADD 6 STIR 20 MIN OR LONGER TO DISSOLVE FORI
S44 (STRONTIUM NITRATE)
|
90*2--
11
! ADD AMMONIUM CHLORIDE TO V-
4. 712
[ I
iI I 246-B,Ej
i* I
712 .
228 j 16S-A 1 228
CV WITH V-?0^AGITATOR ON, IMMEDIATELY COUPLE I
V--903E-THRU UNDERSURFACE DISTRIBUTOR INTO CV|
(54-60) MIN. MAINTAIN CV AT 32-38 DEG F. |
NOTE: OPEN ..VALVE 1 TURN. REC8f?D: . STARTZ&Bm. TOTAL min ./L--
| J
b a s e_i .<+)-#ia z o J!!"<'-) i
5) -
I
______ _________
0 ADJ TO PH 10.0-10.5 4 |
RECORD: PHJKUj L SODIUM HYDROXIDE ASSUME SOX
I | d6J
I'lR 3 HRS. HYDROCHLORIC ACID ASSUME 32% I
I I
; 7-D I -JZ28-D |
TEAM EJ&&T,V-921 INTO CV FROM S3S
|
ECKD PPHjg> ( 10.0-10.5), IF PH IS BELOW 1.0]
1 ' v'
SODIUM HYDROXIDE
ASSUME SZ>%
i
. 7-D
ADJ TO PH 10.0-10.5 & RECORD PH. I
OCHLORIC ACID
ASSUME 32%
|
cAM EJECT V-.921 FROM SS INTO CV
I
il
28-D I.
I
GH IN DRUM h POUR IN (OCTANOL)
I 25 I .588-A ! 25
m\ HE3.*& 193-i 95 DEG F.J^'70-75 MIN 6 RECORD |
J^fT.yX-DEG' F, RE C ,, tfjSLDEG F
.|
STIR 15 MIN/A2^T93'-195 1DEG :F. RECORD: START /Z!/w
j I
LQOD TO 180^190" < +/-18,000G)
1
RECORD: PH_52>V?,5-10.0) IFBELOW 9.5,
|
ADJ TO PH 9.5-10.0 RECORD PHSt ASSUME 50%j
TFPH IS ABOVE-10.0, DO NOT'ADJUST
1
7-D |_X.
STOP AGITATOR
-
I
!
WHEN INSTRUCTED BY PROCESSING HALFWAY THRU |
PRESSING DUMP IN & STIR 5 MIN STOP AGITATOR!
AND RESUME PRESSING.
I
10
5S8-A
10
FIN
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