Document MJG0X1Xnv1og25E0XnZY8ver7
S.V. c*v*{f5}903
'CG CODE RT-880-D PKG
JAN 2 0 1982
A2J90
( DATE )
"(LOT NUMBER)"
EST, WT * 2522* LBS a PREPARATION NOTES:_____
D.V. 902,904
PROCESSES ( >KT-380~B (G)
TYPED BY; JMH STANDARD HRS * 9,3
APPROVED BY EWK 12-31-8:
TIME
NON-BLEEDING
EQUIP 1 BENT 1
----------------j.
! 1
NAME: UATCHUNG RED B
USE LBS
1 NOTE: BATCH MUST BE PRESSED PROMPTLY TO
j
1 CONTROL COLOR- DO NOT START IF PRESS WILL |
I NOT BE AVAILABLE WITHIN 3 HRS AFTER MAKING,1
1 RECORD:
i
1 PRESS WILL BE READY______M_____ , _____ PR SUPV |
( START MAKING____^,,M____/,,^____^MAKING SUPV]
II
| NOTE- NOTIFY PRESS ROOM BEFORE ROPING OFF T
l AREA UNDER V-922
I
ii
I NOTE; RUN 15* WATER INTO V-904, PUMP WATER I
| FROM V-904 THRU DISTRIBUTOR, IF WATER DOES |
( NOT COME OUT OF ALL DISTRIBUTOR HOLES WITH !
i FULL FORCE, NOTIFY SUPERVISOR
I
II
I N-CODE !
PREP 1
I 1 } RECORD:_____.BATCHES SINCE SPARKLER LAST
1
1 1 CLEANED. AFTER 4 BATCHES, CLEAN, DRESS
}
1 1 SPARKLER G PRE-COAT WITH 154 DICALITE,
(
I jU-PTLTER a id
.
f
I^MliTAlN FOR S11 2--CHLOR0-4-AMIN0TOLIJENE--5- j
!C ACID
I
E-S' JUafTAIN FOR S27 3-HYDR0XY-2-NAPHTH0IC ACID I
T INSTALL DV & CV RECORDER & CONTROLLER CHART I
777-A . I 740-C
82-C
ACCT LBS
RUN 12* (120G) WATER INTO V-Jj tv ABU TO
100 DEG F
D IN 2-3 MIN DRESINATE XX
1R 5 MIN & RECORD
9,5-10.5)
1 STIR 20 MIN OR LONGER TO DISSOLVE FDR S36
I ! 115 !
I I
99-A i 1 iS (
37' (762G) WATER INTO V-922 WEIGH IN SODIUM HYDROXIDE IN V-926 G RUN INI
jiVT TURN ON AGITATOR G STEAM G DUMP IN FROM S2 I
I I
J-DT,_ ,
41003
,1
( } 2-CHL0R0
tu
I T 4-AMINO
___ _______ ___ ;_________ _________ I
II TOLUENE - ____________________________________
i
I { 5-SULFONIC____________
I
i! ACID .
'
!
7-D 740-C
ViST
EOUIP-! WENT I
DATE Pk INTCD.
i 3/0.?
T * T USE !
I PAGE 2 OF 4?. CG 3' C0DEW-8S0-D (G) I LBS I
*"#***'
IN ACTIVAtED CARBON
UMP IN FILTERED
V-
_ ..EAT TO 2f2-214*DCt; F, WATC# F$}AM44
ie !
! RECORD: BY_.3rL_ MU#T BE +, ADj* IF NECESSARY |
^
SODIUM HYDROXIDE
ASSUME 50%
I_JL_
I STIR 30 MIN AT 212-214 DEG F, THEN SHUT OFF f
! STEAM HATCH FOAM! NOTE: RECORD SPARKLER I
! PRESSURE j5L__RSI. IF NOT ZERO NOTIFY
I
PERVISDR.
1
CIRCULATE 15 MIN OR LONGER THRU SPARKLER 1
l UNTIL SOL 'N , IS CLEAR. MAINTAIN. AT^-i 90-1 95 I DEG F FOR S24. RECORD:
TOTAL MIN_34L^- CLARITY.^*-^-----
I, i i
RECORD*:
f & RFC
F
I *' -a
N-CODE
} i 3-B 777-A
7-D
I ac c t i LPS
I---------
fuse 4
]Jar\ LEIGH SODIUM NITRITE IN PT-1 FO i
WEIGH SODIUM NITRITE IN^DRWI FOR^j!^ ^
i WEIGH SODUM NITRITE IN DRUM FORf S5> ~~~
j j
MEASURE
UN ITS IN
HYDROCHLORIC ACID
M_._/____
I
\ RUN 1* <______G> WATER INTO V-_&&&- . ~7
TE USE CV IF MTY, IF CV NOT MTY USE V-904|
j WHEN SI 8 IS COMPLETE', PUMP IN V-922 THRU 1
I SPARKLER, MAINTAIN V-922 AT 190-195,M& F. I
I RECORD: START^:^& TOTAL
I
l 725-A 1 .375
jfc_ 1
725 -A 725-A
2S-D
1
1 1
1 J
44 44 557
___ ,.UN 63* (1648G) WATER INTO V-902 lArT WEIGH SODUM HYDROXIDE Iff V-926 & RUN IN
i _^r
m | DUMP IN FROM S3,
I \ 3-HYDROXY
-
. '
1 | 2-NAPHTHOIC ACID
1 ADJ TO 70-90 DEG F & STIR TO DISSOLVE 1 .I
I- I
zJ\
>1
!?:
922 I WHEN S24 COMPLETE, SHUT OFF PUMP & INSERT |
7 , | ^^Hf-922 FOCT-PLUG
1
0&AI RUN IN 10* <209G) WATER G HEAT TO 190-195 Fi
! I CIRCULATE IS MIN THRU SPARKLER*
1
I ! CIRCULATE 15 MIN THRU SPARKLER.
I
iI
-
`' I
./CV} 8
PUMP V-922 THRU SPARKLER INTO *W4YCV
922 V-j
RUN IN 5" (104G) WATER & HEAT TO 190-195 F 1
CIRCULATE 15 MIN THRU SPARKLER.
5!
-:7^r--N.
904/CV [.s Tj l Tp l 'MP V-922 THRU SPARKLER INTO V
/CV
10 IZ&n WHEN MTY BLOW OUT SPARKLER INTO V
/CV
1. i 7-D ! 473 82-C I lose
DUP050110371
PATE PRINTED: i/13/82
EQUIP | MENT \
PAPE 3 OF 4 CG 32 CODE RT-880-D (G)
*/CvUsPl DISSOLVE ALKANOL XC IN 20G WATER AT 135-145
' 10 rCONT
i FJiATER FROM HOT WATER MIXER IN DRUM t, POUR
r HEAT VfiTOl/CV TO 1<55`-*f?0 F FOR S41 r ' --------- ---- ---- --------- ------------- -WHEN S28 COMPLETE, MEASURE TRISULPHOIL SOAP D IKjCALIBRATED CONTAINER,. SLURRY WITH 46G WATER IN DRUM 6 POUR INTO V-902
j STEAM EJECT IN V-921/W* FROM SB
F'T-2
RUN SODIUM HYDROXIDE INTO PT M_jJL., J^j5t%
i: d)J- TO 20* (72G) STIR 5 MIN OR LONGER F0R-S57
USE LBS
"2(0
W.*
105
N-CGDE
ACCT LBS
133-B |
I
39~A I
1 l
105
7-D <
1 NOTE: IF N-740-C SOLUTION WAS PUMPED | * DIRECTLY FROM SPARKLER TO CV AT. I S'S 23 :6 24, OMIT S'S 40 & 41
CV 140--T RUN 1* (95G) WATER INTO V-
13 'HH5*t IF V--904 IS USED, PUMP V-90'4 AT 165-170 F
I | THRU UNDERSURFACE DISTRIBUTOR INTO CV AFAR
! ! (12-15 MIN) MAINTAIN 165-170 DEG F
ECORD: START___ ___ _____ TOTAL MIN____________
RJJN IN N-23-D HYDROCHLORIC ACID FROM S22
fN 12-15 MIN.
TIR 5 MIN '
ADJ TO 45* <42520 AT 32-38 DEG F
47X3301 ' 57-A
RECORD: TEMP_^-C1 F, STICK _______ "
RUN IN N-725-A SODIUM NITRITE FROM SI9 AFAP (5-10 MIN) & RINSE IN
I
I STIR 20 MIN AT 32-38 F MAINTAINING +CR>
57-A
+!< ! FOR S54 RECORD j TIME, START"
CR "t___( + > KI ___( + ) NOTE:
I-
| 1) IF CR-, KI.-, ADD 201!: AS IS" INCREMENTS
RECORD: CR_j^( + ) KI_.___< + )
HYDROCHLORIC 'ACID
ASSUME 32%
J8-P
| 2) IF CR+, KI-, ADD 203= "AS IS" INCREMENTS
RECORD: CR_,,_,,( + ) KI_____< + >,
f
SODIUM NITRITE
ASSUME 33%
______ i 725-A ! ___
DUMP IN CALCIUM CHLORIDE
I 1i66 i ' 20-A i 1166
DUMP IN STRONTIUM NITRATE
255 I '246-B,E| 255
DUMP IN BARIUM SULFATE
L 52 i 65-A | 52
ADD FDR MAINTAINING AT 32-38 PEG F DURING sfcmSOj 57-A
OUPLING
i|
T POUR IN N-725-A SODIUM NITRITE FROM S20
)
J
j FOUR N-725-A SODIUM NITRITE FROM S21 INTO ! J^V-902 \pT\ DUMP IN AMMONIUM CHLORIDE & STIR 2-3 MIN
228 | 165-A
MB:-:.
IMMEDIATELY COUPLE 902 THRU UNDERSUFACE
I ! DISTRIBUTOR INTO CV IN 18-22 MIN. J'iA.If;
I ! CV AT 32-38 DEG F. RECORD: STARti
TOATL HIN,,,
INSTALL 5/16* ORIFICE IN UNDERSURFACE
f UADDITION LINE
WHEN S54 COMPLETE, STIR 30 MIH & RECORD:
I I TVASE jtL-- Tt > DT.AZO..jfc._( + )
5 ,.0-6.0)
DUP050110372
DATE: PRINTED:
: `-y
2QUIP i riNT |
*6 OF 4
I USE j M-CODE I AC
CG 32 CODE RT-830-D (GJ i LBS I
I LB..
N-7-D FROM S39 THRU 5/S &' ORIFICE
flNSE IN RECORD:
JjIN <40-50 MIN)
>0 MIN '& RECORD: F'H^y 7 (7.0-8.5)
BELOW 7.0 AD J TO
WITH
3NLY. RECORD PH__Js&sf_ ASSUME 50%
SODIUM HYDROXIDE IN f>924 & RUN IN ASSUME 50%
i.5 MIN & RECORD :^ASEj^_< + >
Jfar-C-O PH__
9.0-9. 8)
BELOW 9.0 ADJ Iw rH 9.0-9.8 WITH
I N>-7^0NL^. RECORD PH___ __
TIUM HYDROXIDE
ASSUME 50%
MEASURE I OCTANOL IN CALIBRATED CONTAINER ^ POUR IN
i^a -HEAT TO 193-195 DEG f IN 75-80 MIN. RECORD T L.START_______
U&n RECORD: HT________DEG F i, REC_______ DEG F.
166 | STIR- 60^MIN AT^193-195 DEG F. RECORD:
II
\&y\ AFTER^20-'f:riN SM STIR
RECTO;
r ' PH.,,_&*X__(8.8-9.3) 63<n IF PH J^OW 8.81 ADJ TO PH S.8-9.3 WITH
RECORD PH_________
j d iu m HYDROXIDE
ASSUME 50%
COMPLETE, FLOOD TO 180-190*
?-18,000G) STOP AGITATOR
I
i ID 37
7-D 7-D
7-D i 588-A
3'
f WHEN INSTRUCTED BY PROCESSING AREA HALFWAY
THRU PRESSING
1 <1) DUMP IN I OCTANOL
,,.
I (2) STIR 5 MIN
I <3> ADVISE PROCESSING TO RESUME PRESSING
10 588-A
10
/" 1
ESS'
"U
i 6
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