Document MJ3rq1Vpzk7Nq46d7QBxaBL3V
INTER-ORGANIZATION
FROM: D. C. Hidinger DATE: June 21, 1974 SUBJECT: Vinyl Chloride Monomer Testing
PERSONAL
The testing program to determine the -vinyl chloride monomer content of various PVC products produced by the Chemical/Plastics Division has given these results to date. Please note the changes in sampling procedure and calibration curves which are being made in the course of the program to achieve greater accuracy.
UCU/elo
DISTRIBUTION:
W. D. Coder' W. C. Douglas (4) G. J. Frisone M. G. Glenn R. W. Laundrie D. H. Markusson R. K. Ritzert H. P. Schick L. Scott P. A. Taylor A. J. Urbanic J. A. Weber
Attachment '
. C. Hidinger
! GENC 20856 BETTER Service 1$ Our Business*
OEWC 20857
SA-IPLi :.J PITP-Olo-
Tj3
2dC
?axuci
04 Sight Shield GTft Part PU.5105 Injection Molded
.Soloing Compound
miJtTrncTi3h
Lot PlolUT
ftOUJCTIJI ATo
deceived. SAT/Tti
Stapled
5/lii/Vi
TROT
ddsa
Scdulneji fVC UJ19 Schuljnen PVC 0319
I S..1PLJJ. AT
| Akron
I
Akron
V
LATd 5/17/71.
5/17/71.
Page 1 of 1
AP- Jlill CnLAlIoo aA.AG-4
1*S *
ppta
1.3 3 3-5 PP
1.1 ft)*
v3: oj*L.jabK_O-.--------P-H--J-IU--C-r---------
ft 3-1
.lollovtn od M Cist Expondad aiM Upp*r
3-2
ILirtT IFICaTICK 3-1-20567
^urOCTIQh EATS
5/7 - S/dm
Ag*d 1 weak * t anbUat
TOL3PO
etZSIN
3kln 55A5 Mtrrlnol 5051/Pliovle H-90 Fact 50/50 FPCc5U/filOTlc .1-90
r
3.1 HEE AT__________ ' UTi
A*ron
5A6/71i
? loll ?pa V1ML
CHUtiHS XXiQfcA
1.1 * 0.2 ppa
0.2,0*2 + 0.1 ppft
OENC 20858
i
5A.-lPLi HO, uc
IOC
las
Ur uo iiin ui
pmeuct
Liquid Plaatiool ad (waive
Unflnlahad Procuct, Soft-Toucb Apparal
UtapLcMBtod nuttwl
inis dealn iteain Soi't-Toueh Apparal
AfcApDiO
-------------------------- --------------------------------------
naiii I3.ti
! PaaiiKxiai cats
assm
-
sm6U
50 .tarrtnol 5051 25 (Urvlnol 53 2$ PUovic H-90
Factor/ Orbar aj5<*, ;cw3<J3?
SO Harvlnol 5051
25 Hanrlnol 5 3 25 Pllovic H-yo
50 Xanrirvol 5051 25 Harvinol 53 25 Pliovio .1-50
L-0131Q35 L-ti-MWP-T L-160062
Hanrtool 5051 Pliovie M-50 Marvlnol 7H-53
Factory Drear A?5a, .uftMjy
SAMPliC AT 2nd Coating Head
UTS Udlr
Windup
lUtS
1500 gal Bulk Storage
Mixing platform Mixing platfom Mixing platform
1500
1505 1510 1015
P*d* 2 ai' 2
pra a VDilL 0HL3*rtII.i M^aOlaA J*P ^ 0J2 ppa
'i .
3.1 * 0.2 ppa
55 2.0 Psm IS * l.o ' ' J.3 * 0.1 ppa
o
m1
z o
1
.
1
smD
1 1
!
i
I'
1
I1i
WOt 0N30
SilPLi KO. PC?2-016-
133 13C
ISA
lod 3U-1
IiIa
US
?-HKT
SSOtS-I-SlOU Celennered Auto Seating
590D-T-3U2 Calendered Auto Tria
CATin iatijk
sou uialt
Holl #10760
PiUi-ucTiat batk LA 4 y5/71
ya 4 y?/7U
HSAEISG
HiSM
do/2o
Vygm 120,/Vygen 110
Vygeo 120
SA4FUE AT heading
Heeding
LcTi
yi0/71i
L/10/7L
Page 1 aT 2 | ppm JL.IL ( CHLMIES ::JH1L2
bona
hot Tasted
HJTSi Above eemplee teken In nerron mouth battles with neturel rubber U>ppere.
590d-T-J01I Calandarad Auto
Seating
j RoU I'LJLU* j
j
j
yti 4U/S/Tle
ao/20
i Vygen 120Aygen 110
1
Aicron
li/lb/7it
6 ppa*
SOTSi The above ample was taken In 1* os wlae nouth bottle# with feflon/biutyl rubber lined caps.
This ie a repeat of Staple 13B taken 0 days later.
The accuracy of Staples 13a-15C is considered to be at leaat * 20%t but tbs calibration curves m not guaranteed accurate at A10 ppn. At this point.
the calibration curve# uere radon to giva occurata anevarea<.l ppa,
i
---------------------------- :--------------------------------------------------- 1------------------------------------------------------------------------------1------------------------------------ !--------------
7331-301*2
P0 *1*1*51*3*-!
li/lO - h/lV/lk
Vygan 120
Akron
1*/3V 71*
0.6 ppn
9530 Starcraft
Calandered Canpar
Catling_____________
5966-T-10(Jl2 Calanuereu xpandad Auto Seating
jioil *ho99$
Produced lat week January, 1971*
?
Aicron
5/20/71*
HeAt ajad 2U hoi-re at 15Q?F Heat ajoc 1*0 hours at 150 F
Akron kron
5/21/71* 22/71*
The i`d 1 lowing cocnpriaijs an amilt oi the yl,, ca*iMnr 11 n* oroduclng Goi t-Touch appareL, Green 7LoO on 5/2o/7(+.
Liquid Ploatlaol
iV:l6l7
Skin Coat (gelled only)
50 Marvtnol 5051 25 .larvlnol 53 25. flipvie A-90
50 `tarvinol 5051 25 larvlnol 53 25 Pliovlc .1-50
i lat Coating Elead
Gera pen' iron release pa E'er *t exit oi oven jl
11*25
U32
5-0 Z 0*2 ppn
J 3.1 * J.3 , pm
GENC 20881
35-6 35-7 35-3 35-?
Coapaund
Hot IrlA
Finisnea ooltaron 201d-1055 Finished Boltaron 201ti-1055
NSWCJ.S HSTJrfN
-iisi:*
Vygen 220 Asntaoula
Vygen 220
Ashtabula
S.vli'Lil -t
FeadroiLL Conveyor*'
Calanaer*'
Vygen 220 Ashtabula
Guillotine
Vygen 220 Ashtabula
Guillotine
^ Samples taken in wlae ao^th U os bottles with Te lon/butyl rubber cap 1:
o
Samples taken in narrow +outh bottles with butyl stopper^ and crisps a .tuit tal retainers.
100? 1010 1015
101 d
Piga li of I, .II.iL
3<i.%
2.9 J.5 ?:a
2.9 *
h*0 ^0.5 ppm
2.5 ^ 0.5 ppa
GENC 20862
GENC 20863
SO.
2SA-1
a-2 A-J 256-1
o-i
25C-1
C-2 251-1
L-2
D-3
252-1
i-2
i-3 2! :-X
a-2 2o.-v
CJliASTuiA
PRODUCT
Ooltarai 1JS0-20T9 Calendared Corrosion assistant Type I tor Tanas, etc.
Acryllvin 3360
T hvr.no tormable
IlcT.TIUCATIC'l Pisco *213521
wjii>cti:-i CATS
deceived 5/11/76
Aged 16 hours at ISO0? Aged 1 weak st anhiant
Received
S/13/76
Holtaron LCWtJ-1332 i.ieraoTomable Pips Covering
doltaron ooOO-52>6 Calaadarua z Press
|
i
Leninated TbarBoforubla
rcraft
Chalrmat 6551-V axtruaed
1 t/lt.'if Jfi -iJj-i-luJO ,Jri nt. *'i uuun i on 7i*si.Ul laps
uuik FVC Resin
i[oatod to 370F in Agsstat vscuua Tomer
------------------------- h
Received 5/13/7 i*
Heated to 370F la igaatat vacuum lornar Received 5/13/76
Heated to 370F in A^astat vacuus 1`onwr Aged 1 wean at ambient
Received 5/13/7U A^ad 1 weak at ambient A^ed 2 weeks at ambient djcelvod
5nun
Heatea to 370 F in Agestat vacuum former
tliSUi
Vyjan 1J5 +9W)
Vygen 302 (67.3*)
M226
(26.2*)
Acrylic
Vy^en 65
Vygen d5 (e>7.d5t)
Vy^en 310
Pa/itasote Yygen 220
AT
Akron akron
Axron
AKron Aaron kxron .ucron a* ran
5/11/76
5/15/76 5/21/76 S/lU/lli
S/H/l h
5/Ui/Ti,
S/lU/71
sni/iu
5/16/76 5/16/76 5/16/76
5/21/76 5/2 J/7 6 5/15/76
5/17/76 5/16/76
Pag. 2 of 6
Jpn IZiTi. Tno.aTi ;i^;isa
u.2,2.9 * 1 ,'psi
3.6 * 0.5 pp Q.6,3.4 0.1 ppm 53.2,55.3 2 pp
* 3 ppa 1<I?.9,121.0 * 5 pp*
97.5,109.1 5 59.cJ,o9.3 ' 5 ppn
Ole 1,05*0 * 3 p? 1.0,0.o 0.5 ppa j.2,02 * j.1 ppra 117 * 5 ppm
lUi+O 10 pos
GENC 20864
iVL?Li ..a. .JS7 2-013-
2QA 200 200
zol
20a 201 --
21/-1 r-2 r-3 f-i*
r'-CCUCT
lEiNnncuTicn
PSOCUCTTCH EATS
.iesin
SJiPLEL AT
CATS
Page 1 of ^
ppn Vil\iL CrfLOHirS H'iOMZci
oaltaroa 1055-237? Calsacered Typ t iligia far Tanks, ate.
Lot #?di*500-A
1/2/71*
Fantajote Jygen 105
rucron
L/la/71*
15 ppm
HOTSi The above sample was taken in 1* os wide mouth bottles with Teflon/butyl rubber lined caps*
The accuracy of samples 13A-15C is considered to w at laaat * 2OS, but t na calibration curves arc not guaranteed accurate at <10 ppm. At this point, the calloration curves were redone to give accural-a anwara al<l Pfn.
Acrylivin 3360-1016 &xtrudea iVC/Acrylic Vacuum tamable
5/1/71*
Vyjan joe
Akron
5/3/71*
31 * 2 ppn
aoltaron 1009-2206 Extruded ?VC Profile
Lot 42621*d-2
5/1/1U
Vygen ti5 Precompounded
-r_r
5/i/71*
60.6 ^ 5 ppa
Clear Chairast 6551-9000 dxtruced
5/1/7L
Vygan 310
Akron
5/3/71*
1*1 * 1 ppm
Baltarjn 2003-1195 Calendered Print Stuck
V22/71.
Fantasota Vygan 220 42 Calender
Akron
L/2L/71*
275 * 5 ppm
doltaron 1055-2029 Calendered iligld Type I
lor Tanks, etc*
L/22/71*
Pantasote Vygen 105 */l Calender
Akron
1*/21*/71*
5.9 + 1 para
3oltaron 200U-S012
CalenOarun Paoia^tng
Him
______________
1*/22/71* '
Pantasote Vygen 220 03 Calender
Akron
L/2L/71*
ho * 5 ppm i
mi aging stud/ is underway to cetermlna both the level of VC In roll goods ana the loss of VC with exposure, n sample piece was renewed from tine middle of a tightly wrapped roll* Samples 2Lu-2lb were aged at anbiont on my office uallj Samples 21f-2lr' were a geo In a 15dr oven vltn low ,d.r circjliuon.
Jtoltaron 2JOu-L-2d?2 .. jpju Print
-** ><>
ryi/?ii
V j,i iii 220
1/6/71*
* 5 ppm
r/7/7U
5/d/7u 6/13/?b
ai.oru^ 2 ^ pp 75.7,t-o.o *, ^ ppw
i*i* * 1 pom
GENC 20865
r:-oio~nr-
J5.0JHET7S
Pag 1 oT 1
r--Slj0 nolle \uboy Calling
Tile dalencored
niSiTiriaria: Soil #23705
paouictrar Hats
rlSJTV Vygan SO
sm?ij: at Akron
cats
unsm
CHL2ATD2 MOSOH2R 9 ppn
NOTE: Above ample taken In narrow mouth bottles with natural rubber stoppers 7ha accuracy of Samples 13k-ISC la conaldared to ia at least * 20J, but tia calibration curves are not guarantaad accurate at <10 ppn. at tbla point,
tna callcratlon curves wara radona to give accurate answera at <1 ppm. j
|
j|
Ar. aging stuuy la underway to determine both the level of V1 til roll gooua a no the Iojj j! VC
exposure, a sample pleca waa removed Iroes
the middle of a tightly wrapped roll, Sonpiea 211-211] ware aged a t ambient on ay office well j Samples 21 d-2 li were %ed In a 15aF oven ultn low air circulation.
----
-------. ------------------- ........... - -- 7172-^14-
---
jjod Jrade Uo3
r-i*r?r. io.;ri x.
------- ---------------------------------- 1 l.*zs j_
'-r--
5/23/Tij. r
Vygen 310
-I
..T Akron
___L..T;______ 5A3/7U
rz-i .IttV~
-
omzO 10
vo I
l
ij
I i
i t
!
i i i
j
1
s.--:?:.: .0.
2272-Jld2U-1
-.-3 216-1
.--2 3-3
6U
?.iXf_T
I23iri-XCUnQK
CJUM30S
PrfXUCTIJl EATS
.133 N
3AMF_c3 AT
DATS
Page L of 1
ppm V IN XL f 31J -tlC3 .1A.at.-t
UJ iL-in, avii/ is underway to detaraina doth tha laval of VC In roll ;aada and the loss of VC Kith exposure. A sample placews renewed from the middle of a tightly wrapped roll. Samples 21A-21D were aged at and lent on ay office wail; Samples 213-211' ware a0-ed in a 15oF ovan ultn low air clrculaU.cn.
Contract Wallcovering F-OT-dS
P0 W7752t,
5/6/7 i.
C.5 * 0.5 ppm
lixhtudight Aallcoverini; .-"<-*115 Calendared
20 #00331
.010* joalaola film for toilet seat dotteex for Baneke
.311" Fa ranhi o ,iln for toil Jt coot tii for &sne2e
2J ifdlli37
>0 #00799
5/7/71, 5/3/71,
5/o/71,
5/7/71. 5/1/ Ik
/'ll/ 7li '
0.5.J.3 * 0.2 ppm hone * OTl ppm 0.5 * 0,5 pp
J.6,0.2 * 0.2 ppm Hon* 0.1 ppn 0,1 * 0*1 ppra
0.1 * 0*1 ppfl
GENC 20867
If
n u';TT!-ie,,Tio:;
bjiia
P3jr:cTn:ijj.Ti
diSIS
S^'.rLlX ~T
Page 3 of J
r.o-5 vi:rr-
Cr.LOsILa /d, J.-C.l
The following compris' a an audit of #2 Jat Zone.
13A
Vicuna Footuaar
Factory Order 10592
_3pac. 13-132-006
133
Vicuna footuaar
Factory Oruer 10592
Spac. 13-132-006
5/20/71 5/20/71
Vygen 110 Vygen 110
Jat done Unwind
altar iBcueslng Bel ore Finishing
13C
Vicuna footuaar
Factory Oraer 10592
Spac. 13-132-006
5/20/71
Vygen 110
(ind-Cp
53A 5900X5012 Calendered PC 0122133
Automotive Saatlng
Pallet 01-A
Tag #9dl9jO
Heoeived 1/15/71
Vygen 120
533 5900X9012 Calendered PC 0122133 Automotive Seating* Pallet 01-A Tag #981910
Received 1/15/71
Vygen 120
Akron
530 5900T9012 Celenoared PC Ou22133
Automotive Seating
Pallet 01-A
Tag #901910
deceived 1/15/71
Vygen 120
53D 59OOT9012 Celenoared PC 0122133 Automotive Seating Pallet 01-A Tag #961910
Received 1/15/71
Vygen 12Q
53S 5900X9012 Calendered PC OUZ2133
Automotive Seating
r Hat 01-A
Tag #901910
Received 1/15/71
Vygen 120
Akron
53F 5900X9012 Calendered PC 0122133
Automotive Seating
Pallet 01--n
Tag #901910
Received 1^15/71
Vygen 120
Akron
O Sterci'-l't
Seating
Catalogue #15-35-0215 Color 1(032 done White
P.O. #19179
0/73
Saco Sh-et - Vv ; .r. lit Topskin - Vygen 110
U10 1150 1152 V13/71 i>/13/71 0/13/71 6/13/71 6/13/71 o/U/74
^ V74
HiD 3.2 * 0.1 ppm lUcC 0.1 * 0,1 pun Ashtabula 2,L p?m Ksntabulu l*d ppm Siam Shan. Diam. Sham. K .Da,
QENC 20660
3*tt?L NO. 37 H 371
37J
P.IXE'CT Bar.ouryed Coxpoujd .lillaa Canpour.a Strip
ViU Strip
111 ---1 i K2. TlilCATIOH
paacDcnoN eats
aam
itiSIH Vygan ISO Vygen 120
Vygan 120
--- ----
U
37 E.
-3--7-.1 37M 370
- ----- -- 37 P
Hot Trim
Uni inia had Procuct T-9J12
?0 585 doll rflO
Print Ink (Solution) - -- -------*
Tint Ink (Solution J.
....... -
'"
tini3ft (Solution)
...........
-- -...............
Unfinished T-P012
7.-185
| I-----------------------
Vygen 120 Vygen 120
Vyfton 123 Vygen 123 Vygen 3020 or Vygen 123
37*
rinlahea T->012
,
The rollowliu comprises on audit or jrl Jot Zona expending Vlnollo upholstery 5/20/7J*.
1*2A Unexpanded Calenaered
--- _ ----------- , .. ta--+erlal
-- --
Q 1,-7 3
mz **
J: finiahec, .^xnanii**ri J-hoaaad
o -----
io 1,2':
Vtnolle executive
'
Jpholafsry
o i
j
U3026 UB030
"
larton"' Oroar ymu
.
VyKen 110 Vygen 110 Vygen 110
S.J1PAT
EATS'
Lrop Dill
1038
Conveyor between drop ana feed oilHe
101i3
Conveyor between feed mill and calendar
101*9 u__________
#2 calendar - Windup
1051* 1103
Page 2 of 3 ppn Visit, CH 1*3=1 Hi ICUOtt^t 15 * 2 ppa 10+2 ppn
o>2 * 2 ppn
2 .t 0*5 ppn 6.0 ^ 1 ppa
#1 Printer Unwind
_____
tfl Printer iindup
i
_______
Jot 2one Lat-Oif
Setwoen omoosaor a;3C top: inlaid, it/
Jinouo
1100 1112 1115
1.1 * 0.3 pa.it J.7 + 0.1 ppn 0,7 T 0*1
1
GENC 20870
sx:?i \o* 15 a
21C-1 0*2
211-1
O-Il
37> 37 J 3/0 3U 37. 37 -
?i0 L'CT
irJ1* TTFI CATION
Pdxocnca Bars
am.**
rests
"* T?%' '
.....----
S^PLiB AT
Dili
Page 1 of 3 j ppn vua
' CHLORIDE HOtiOMER
?02o-T-13dl2 Calendered Expanded
Automotive
Po /00395
3A1/H*
----------------------- _J
.*
3aso 50/50 Vygen HO/Vygen 120
Skin Vygen 120
rutran
1/16/71
|
i
----------------- i
3 ppra
_____________
5/Tc: Tr.e a or.'* :a .pla was t:;-. in 1 ot wide south bottles with Teflsn/butyl rubber lined ceps
l The accuracy of st-iulas 13f.-15C is considered to ce et least * 20%, out tr.a callaration curves era not guaranteed accurate at <10 pp.i.
*t ttils point, tr.e calibration curves were redone to give accurate answers at <1 ppn.
1
I
i
[
.i
nit aging stuuy is unccrway to determine both Ua level of 70 in roll goous anu the loss of VC with exposure, a sample piece was rarevac iron the
middle of a tightly wrapped roll. Samples 21A-21B were aged at ambient on ay olfice wall} Samplee 210-211:' were aged in a 156F oven with low air circulation.
il j^aao Vinelie Calendared Expanded Uatuletery
PO *6911
Shipped h/ZS/7k ,
Base LOA
Vygen 110/Vygen 50 Skin Vygen 110
Akron
S/o/71
0*5 ^ 0.5 pp
f *
5/7/71 5/0/71
02 ,0*3 * 0*2 ppn .None + 07l ppm
VJ0-r-?012 Culexmaruti Auto Seating
Piece Jr012213-3 Pallet 01-A Tag *961910
deceived W15/7 n
Vygen 120
A* ran
5/0/71
5.6 * 0.5 pp
5/7/71 i/o/71 i/13/71
1.3,1.0 ^ 0.2 ppa none + 0.1 pan
The following co: .crisis an audit of the 2 calar.esr line producing T-9012 on 9/25/71.
.(as in
Lianln tie sin .(coin
;tlt Car /.CiXiolOb
ltd Car fn A auOICo ict Car it irXlcl/o idt Car y.-i-rlie 13'
Vygen 120
Vygen 120 Vvk*ll 120 7/gen 120
j
Railroad car Hatch yl
t 0323
1 2? + ii jjpn
1........ -
| Hatch f2
! UJJ5
o pui
Hatch *3
| 3312
\ Js;2, 11 ;J
j Hatch ,v5
j 0350
' 7, 1 ; 1 p/fl
1 :ui1
Vy^m\ 120
Chute frjiu bin
1 lul>
! l;5 * 2 ,:j:i
.u,-jc.- tj trolley
-U
_ |__ _ ccnve/or
-t
-4 / 120 V' ygen 120
Upper alent-er
j dhuto fr. lower olencur l Into -til rtan bury
1027
iJo J 1 a no : 2 |-J.a
QENC 20871
afi-oid-~
uS-i-oa Li-UJ) tiS-100li 1.5-1005 iiS-1006 U5-10QT
i*5-100d U5-1W 05-1010
ub-ioa
15-1012 15-1013 US-1010 15-1015 05-lOlo 1.5-1017
1.5-i ,113
i*5-10l6
ri-\?r.i :.:r^
Tha following eomprisl a (touad Habin Tasting Yygen 120C Vygen 1200 Vygan 120C Vygen 12QC Vygen 120C '/ygan 120C Vy*:a 1200
Vygan 120C Vygan 1200
Vyuen 12GC
Vy,'tm 1200 Vygwi 310 Vr^en 310 Vygwi 310 Vygen 310 ; Vyj:en 310 | Myj;en 310 | V/gan 310
i Vygen 310
' ASHTABULA
^Ashtabula Iryar samples taken o?o/ tJT* #3 Dryer1 <r3 Iryar 41 Iryar1
41 Dryer^
41 Dryar1 nl Eryer1 *3 iryar1
41 Eryer ifl Dryer1 #3 Eryer1 ^3 Dryer1 jf2 Dryer #2 Er/er
Dryer rf2 Lr/ar #2 Er/er j/2 Dryer 42 Dryer
f- -
42 Lryer I
Page 1 of 2
-^m - I-'.-L
10:50 am 10:50 an
D2D (Ashtabula o/7/7it) 371* (Ashtabula 6/7/7it)
10:50 am
oQU 5 (o/7/TJ*)
10t50 am
ol5 * 5 (SStE o/7/7U
10:50 am
567 (Warn. Sham. o/7/7U
10i30 am
tJO (Elam. Sham. O/7/Tu)
10*50 am
7_
L30 (ridtL 0/7/7U)
19.5 *.2 (.-&D o/li/71)
" (xiiL j/21'71)
10t50 am
10(50 an
10:50 am
10i50 am
11:30 am
11(30 am
LI 130 am
Hi30 ant
11:30 am
11:30 am
11:30 am i
r
J LI: ^0 rkit
320 (nsataDula)
1<J (ushtabula o/l/7U)
23 (Ashtabula o/7/?Li)
* 3 (rt*D o/7/IL)
10 * Z {nuL o/ iV7u)
56 <Eia i.
^
| >u (..t:
i li.o *.5 (
h
GENC 20873
LS-1UJ3 US-1021 1&-U22 US-1023 US-102 U US-1025 15-1026 US-1027 16-102$
Vygen 310 Vy~an 310 Vygan 310 Vyge: 110 Vygan 110 Vy^en 120 Vygen 120 Vygan 130 Vygen 130
ftSUTAoUl*
Vygen 110 Vygan 11C
f2 Cryer
*2 Liryer
f2 Uryer
Control
Bag
Control oKld Bag 2
if 3 Ir/er #3 Iryar2
#2 Dryer" ,(*2 Dryar^
Samples IDOL - 102U taken in wide mouth bottles >4ith Heoprene/Tei'lon cap liners. ^unpleo 10?5 - 103d toxen In serum oottles with r^aturul rubber stoppers
?a :* 2 i.f 2
LI:jj an
j
11:30 am
j
11:30 art
2J (Ashtabula t/T/7uJ
^ ; 5 (lit o ^,7^ ` /" 95 {shtabula c, T/77UU)
3Uf (*sht*oula o/7/7u) 23 (nshtabuLa o/7/7u) 25 (AShtaoula o/7/7LJ
QENC 20873
PLT3-020lJ&Al-SO
*2-50 136B1-50
32-50 U6CI-50
C2-50 13601-50
02-50
136E1-50
___E2-50 1360-6?
136*1-6? *2-69
136331-69
BB2-69 136B1-69 . =2-6?
____.'JsJj.'-'T____
National Vaoiaia Order He. 51332-2006oS30
#3 Calender Hus
national VacutK Onivr *> 51332-20066530
#3 Calender Bun
National Veeuua Order Ha. 51332-20066530
HI Calender Bun
National Vacuus Order No. 51332-20066530
HI Calendar Bun
National Vacuua Order No. 51332-20066530
H3 Calender Bun
B.F. Goodrich PVC daatn 103 OF
[Basin - Vygen 310 Lot 7615
For Acrylivin extrusion at Heuccnaratoun
acrylivin 3360-9000 Xryblena From Hanschel
33o0-9000 - Dryblend cycle 12 nin. Drop Teop. 220F - No v acuut Cool to 90 ana drop
Acrylivin extrusion 125 ail Sheet
Dryblend Iron Butler Tank 3360-32 9S
6/6/76
BfcO KXPEAIMSJtAL
iiSIN
Fantasota 220 Baein fraa SUo B
----. _ T
Henechel
1--T
6/6/76
6/6/76
6/6/76
Fantaaote 220 deala froa Silo B
Fantaaote 220 Reals Iron silo B
Hanschel Crop
120 aeconda - 20 nlnutai Non-agitating - Teap.<J0C
6/6/76
Farrel Continuous Mixer Stock 325F
6/6/76
6/6/76 6/6/76
Fantaaote 220 Resin tma Silo B
Fantaaote 220 Basin Iron Silo B
Stock fron Calender Feed Mill Stock lamp. 310F Thickness 230 ail*
6/6/76
Finished Calendered Sheet Calender Conditions in Book PE73-020-136
6/6/76
Fron bag - No history
6/6/76 6/6/76
Vygen 310 Lot 7615
Vygen 310 Lot 71(15
Iron bag at Hanschel Sixer
Hanschel .Fixer
6/6/76 6/6/76
6/6/76
Vygen 310 Lot 7615
Hanschel Mixer
6/6/T6
Fage 1 oT S
, n.-m.
CHLJnKa MhJ.ta.s
136Q-69 ____ C2-69_
136D1-69
02-1*9 136E1-69
2-1*9 136F1-69
F2-69 13oal**-l*6
p.t;- -7 Acr/Ilrin Extrusion US aU Sheet
Acryllrla Extrusion 125 all SbMt
Icryllvln Extrusion 125 ail Shaat
AeryUvln Extrusion 125 all Shoot
2000-6072
121-1*5 136118-1*6
2006-6072
A2B-66 13 011C-1*6 "
2006-6072
via o t
_ A2C-66 13911-1*6
ft 5o *2-66
13UBU-66
82 *-66
136B1B-66
B2B-66 136B1C-66
B2C-I*6
Pantasote 220 ttealn 2006-6072 2006-6072 2006-6072
m?r: ication
Sxtrunad sbsat with vacuus at ala Up aaltaa
T h/6/T6
Bxtrudad abaat finlahad liS
X 6/6/76
fxtrudad ahaat at dia Up* , 6/6/76 aoltan without vacuoa
Extruded Aset finished without VACUUM
6/6/76
USD Lab trlala
6/5/71*
dSB Lab trlala KID Lab trlala BSD Lab trlala KiL Lab trlala SkD Lab trials Kill Lab trials
6/5/76 6/5/76 6/5/76 6/5/71* 6/5/76 6/5/76
am Eiraaniatm
disr:;
Tygan 310 Lot 7105
3a1! rtii. aT #1* - 6-1/2" Extrudar
6/6/76
Tyson 310 Lot 7105
#i* - b-X/2* iExtrudtr
6/6/76
Tygan 310 Lot 7105
#1* - 6-1/2" Extrudar
6/6/76
Tyson 310 Lot 7105
Jll* - 6-1/2" Extruder
Pantasote 220 In basa froa Silo B
Froa 7-1/2 lo. Farrel Banbury In lab - drop taap. 325F
6/6/76 0/5/71*
Pantasote 220 In baga froa Silo B
Panta aota 220 In basa froa Silo B
Froa 10"x20" Mill roll taap. 300F allied 10 nln. 310 to 320 F
Froa laboratory calendar 7 to 9 alia
6/5/71* 6/5/76
Pantasote 220 In bags froa Silo B
6/6/76
Tygan 220 Vygen 220 Vygsn 220
7-1/2 Lb. Banbury arop stock temperature J25F
-----------------------10'x20" mill roll tamp. 300F alock 310 to 320F
TE/fu 6/5/76
Froa laooratory calandar
7 to 9 alls thick
6/5/76
Psge 2 of $ ^isr
0-XJtIL dOh JCta
OENC 20*75
j. 13581-66 _ JS2-U6
13801-47 C2A-67
138a B-67
023-67
iMji.UCT Vygan 2ZO
iLaTT:icAn3:;
2006-6072 with Plntasota 220 raatn
and 6 phr 062
UD Lata trial
2006-6072 with Pantaaota 220 main and 062 apoxy
BU> Lab trial
13a CLC-67 C2C-67 .
136ttA-67 D2A-67
2006-6072 with Pantaaota 220 rasln
and 062 apoxy reala
no Lab trial
2006-6072 with Pantaaota 220 rasln
with 3 phr dlacrylata aonoaar
HbD Lab trial
138a B-67 020-67
138C10-67 L20-L7
2006-6072 with Pantaaota 22) rasln
with 3 phr dlacrylata
aonoaar
no Lab trial
2006-6072 with Pantaaota 220 raaln
with 3 phr dlacrylata aonoaar
no Lab trial
` MD StPcAMEiTAL
PHOELTCmtl IaTI
.-tisiti
Vygan 220
6/5/76
Pantaaota 220 froa bags
6/y?6 ` 6/5/76
Pantaaota 220 froa bage
Pantaaota 220 Iron bags
6/5/76
Pantasote 220
6/5/76
Pantaaota 220
6/5/76
Pantaaota 220
Sa'PLS T NOT In bags
LaTi 6/4/76
7-1/2 lb Tarrsl Banbury In lab - Crop tanp. 325*7 2 alnutas
10**20" 111 eurfaca roll 300 F.atodt 310 to 320 7
Calandarsd ahaat 7 to 9 alia
6/5/76 6/5/76 6/5/76
7-1/2 lb Banbury drop 320r 2 nin six
6/5/76
10"x20* lab nill surface roll 300F - stock tanp. 325F
6/5/76
Calendered ahaat 7 to 9 alls
6/5/71*
Fbga 3 of ;
?oa V1H1L CHLitTCE HCKHil
06NC 2*?
2C72-0H1&U-1
A-2 64B-1
3-2 66C-1
Pu. .7
Naveoaaratawa Plant 230o-6072 flaCd Stiollliar
2006-6072
PE73-020-146A-1
A-2 PDT3-020-1463-1
2006-o072
3-2 FC73-020-166C-1
C-2 66E-1
E-2 e>5--a
A-2 653-1
3-2
2006-6072
C-2 PE73-020-166E-1
-- -- ------------------------------
0-2 --- ------------------
Henschel Series
2006-1095 Compound Pantasote 220 Resin in ?S bags iron Silo 5 it Iron 6/10/7k Calender run
PL73-020-167A-1
A-Z
Henschel Series 2006-1095 Compound Pantoso ta 220 Resin
in ?2 bnri frpri Silo B u iron o/lV/Ii Calendar run
PD73-020-1473-1 3-2
1 6AO/7U
MtO tXPEKDtHTHL
iz^zr. -
Pantasote 220 from Silo B
3:.JL nT -
:,,ts
Henschel for #2 Calender 6AO/74
6/10/71. f'
Compound .or 20066072 Pantaaota 220 3*xLn
#2 Calendar Banbtuy Q 6/10/71. feed urop 3 minutes 325 F
6/ IQ/Vx
Compound lor 20066072 Panesso te 220 Resin
#2 Calendar faad alll. Roll twip. 2LQF Stock tamp. 310F Tina on mill Cl 16 min. L/li" thick
6/10/76
6/10/71.
Compound for 2GQo6072 Pantaeote 220 Basin
Finished Calendered Sheet 10 mils
1 ' --
Ub trials at
Compound for 2006-
Newcomers Uwn 6/10/71 1095 lob Studies
Pantasote 220
Henachel - 6-1/2 mm to 100F
6/10/74 6/10/74
Lab trials at
Compound for 2006-
Newcomers town 6/10/71 1095 lab Studies
Pantasote 220
Henechel to 160K in 13 minutes
6/10/74
PE !| af ;
pom .1JL Zr.L:.,ZlZ /AK-.1
OENC 20877
6501
02 65E-1
D-2 66A-1
A-2 52A 52 B 52 C 52D 521 sir
' p.o: :t
ni:TTcic-:io::
Hanachtl Sariaa
2006-1095 Conpound Pantaaota 220 Hasln In ? baga froa Silo 9 k froa 6/10/71* Calandar run
PD73-020-11?C-l '
BIT QC PitMENTAL f
?H0r;j0TI3tJ UTi
Ub trials at Mawcaaarstom 6AQ/7l>
Coppound for 2006*
1095 Ub Studiaa Pantaaota 220
SaiPli .-.T
Monachal to 160F wl th v acuua
C-2
Hanschal Sariaa
2006-1095 Coapound Pantaaota 220 UnIo In PE baga froa Silo B 6 froa 6/1077ti Calandar run
PD73-02O-U7S-1
- -2
PVC HeaLn uaad for 2006-6012 on 6AO/71
PD73-020-116E-1
E-2
Lab trials at HawcQrstotm b/10/71*
Compound for 2006* 109$ Lab Stualea Pantasats 220
Monachal nix to ldOF . with vacuum
-
Pantaaota 220
Sampled at Silo B on
froa Silo B
6/1Q/71* into a 3 layer
polyathylena bag and brought back to Akron
tUO. Bags opanao and 1' saiuplad 6/16/71.
The following ccnprlaai Hound Bobln Tasting of atx ting calendered at H&D 6/ C. Wssr on 6/1/71.
Pantaaota 220
ftofsr to PE73-020-1361 Bo Tin Stsblllssr
-
-
AtD
Pantaaota 220
Hafar to 2173-020-136*
-- __ ---------- ----------- ---- Mo Tin Sta&lllxar___ _ _
Pantaaota 220
Hafar to 2173-020-1361 Ho Tin SUblllaar__________
Pantaaota 220
Hafar to PE73-020-136A No Tin Stablliaor
Pantaaota 220 Fantaaoto 220
Hafar to PET3-020-136* Mo Tin Stabilizer
as'ftrttaa&s-13"
HID --------- _----------------------- ------------------------- _ _ ------
- - tiiii
! - Hull
i - tlkD
" itklJ J
-
6A0AI1
p*g 5 of 5
c
*
-------------pSVllM,------------ --
CrlLO:tILS 3QK0.<xt *
6/10/7U
.
__________
6/13/71
6/13/76
- - --
6/13/71
6/13/71
6/13/71 0/13/71
11 2.0 HID
16 2 itlD - . ---------
19.1 Aahtaoula
19.5 AahtaOula
Liam* Sham. Ham* Sham*