Document MJ3B2GaK4bq8ded3MR0EvX9az

" E P AUnilodSIIIII 0 =-~~ ""'oetio Region 6 Compliance Assurance and Enforcement Division INSPECTION REPORT Inspection Date(s): Media: Regulatory Program(s) 08/27/2018 th rough 08/31/18 EPCRA Section 313- Toxic Release Inventory (TRI) Reporting Company Name: Facility Name: Facility Physical Location: Mailing address: County/Parish: Website: Facility Contact (for TRI): Rubicon LLC Rubicon LLC 9156 Highway 75 Geismar, Louisiana 70734 P.O. Box 517 Geismar, Louisiana 70734 Ascension Parish www.rubiconllc.us Philip Kerr (225) 242-5027 I Senior Environmental Engineer FRS Number: TRI Facility ID Number: NAICS: 110000597373 70734RBCNN9156H 325194- Cyclic Crude, Intermediate, & Gum & Wood Chemical Manufacturing 325211 - Plastics Material & Resin Manufacturing Personnel participating in the inspection: David Riley US EPA Region 6 John Penland US EPA Region 6 Chris Simms LDEQ Cory Lormand LDEQ Karen Price LDEQ Michelle Eaglin Rubicon LLC Philip Kerr Rubicon LLC Thesia Krajewski Rubicon LLC Ron Miller Rubicon LLC Christy Blanchar d Rubicon LLC EPCRA 313 Inspector RCRA Inspector RCRA Inspector RCRA Inspector RCRA Inspector Environmental Engineering Manager Senior Environmenta l Engineer Senior Environmenta l Engineer Environmental Engineer EHS Manager (214) 665-7298 (214) 665-9717 (225) 219-3318 --- (225) 219-3612 (225) 242-5590 (225) 242-5027 --- (225) 242-5573 (225) 242-5353 EPA Lead Inspector Signature/Date D~~ David Riley v II/5 ~~~ Da~e Supervisor Signature/Date ~SC)< Troy~uck~ i l 5'1'' Date 6ENFORM-019-R7 (2/15/ 2017) 1 Section I-INTRODUCTION Rubicon LLC Inspection Date: 08/27 -31/2018 PURPOSE OF THE INSPECTION The purpose of this inspection is to evaluate compliance with Section 313 of the Emergency Planning & Community Right-to-Know Act (EPCRA) for the Rubicon LLC facility located at 9156 Highway 75, Geismar, Louisiana, 70734. The EPCRA 313 program has not been delegated to any state, so compliance inspections are conducted by the EPA. It was conducted concurrently with a Resource Conservation and Recovery Act (RCRA) inspection led by John Penland of the EPA's Region 6 office, with several representatives of the Louisiana Department of Environmental Quality's (LDEQ) RCRA program in attendance. Whi le the LDEQ was notified of the EPCRA 313 portion of the inspection in advance, a representative for that program did not attend. The EPCRA 313 inspection covered the 2013 through 2017 calendar years and was initiated following a review of the facility's reporting history in the Toxic Release Inventory (TRI) database, which is the repository for reports submitted pursuant to EPCRA 313. There are three criteria that a facility must meet in a calendar year to be subject to reporting for that year: 1. The facility has 10 or more full -time employees, or the equivalent of 20,000 or more hours worked by all full-time, part-ti me, and contract employees. 2. The facility is in a covered primary North American Industry Classification System (NAICS) code. 3. The facility manufactures, processes, or otherwise uses any listed toxic chemical above a specified threshold amount. I arrived at the facility at 10:00 am on August 27, 2018, for an unannounced inspection, accompanied by John Penland of t he EPA's Region 6 office, as well as Chris Simms, Cory Lormand, and Karen Price of the LDEQ. I met with Michelle Eaglin, Philip Kerr, Thesia Krajewski, and Ron Miller of Rubicon LLC. I presented my EPA enforcement credentials to the Rubicon representatives and informed them that part of the inspection would involve a review of the facility's manufacturing process, its annual usage of reportable toxic chemica ls, and any releases, transfers, or other waste management of those chemicals. For TRI-related matters, I communicated primarily with Philip Kerr of Rubicon. Business cards are in Appendix 1. FACILITY DESCRIPTION Rubicon is a joint venture between Huntsman and Lanxess. The facility has been in operation since 1966 and currently has approximately 430 employees, with an additional 270 contractors. The facility produces polyurethane chemicals. Methylene diphenyl diisocyanate (MDI), diphenylamine (DPA), hydrochloric acid, ammonia, and polyether polyols are manufactured for sale. Diaminodiphenylmethane (DADPM), phosgene, aniline, and nitrobenzene are manufactured for internal use. Manufacturing facilities include two nitrobenzene plants, three aniline plants, two DPA plants, two DADPM plants, three MDI plants, three pure MDI plants, an MDI variants plant, a 2 Rubicon LLC Inspection Date: 08/27 -31/2018 specialty polyo ls plant, and a maleic anhydride plant. Other areas include a laboratory complex, two painting contractor yards, a maintenance building, and two closed impoundments. Wastes generated onsite are primarily directed to four Class 1 hazardous waste injection wells, or to six incinerators, five of which are coupled with industrial boilers. Wastes are also managed offsite. Two facility maps are contained in Appendix 2. The facility lists two NAICS Industry Codes on its TRI reports: 325194 (Cyclic Crude, Intermediate, & Gum & Wood Chemical Manufacturing) and 325211 (Plastics Material & Resin Manufacturing). Both Industry Codes are included in the Subsector Code 325 (Chemical Manufacturing), which is a covered code for TRI reporting. A general process description and flow diagrams are contained in Appendix 3. Section II- OBSERVATIONS CHEMICALS SUBMITTED TO THE TRI DATABASE For each of the years 2013- 2017, the facility submitted Form R reports for over 40 chemicals which are manufactured, processed, and/or otherwise used. These chemicals have a manufacturing or processing threshold of 25,000 pounds, and an otherwise use threshold of 10,000 pounds, except for the chemical category "dioxin and dioxin-like compounds", which has a threshold of 0.1 grams for manufacturing, processing, or otherwise use. Appendix 4 contains a table of chemicals submitted to the TRI database for 2013- 2017, as well as annual chemical usage tables for 2015- 2017 that were provided by the facility. Usage is calculated from purchase records, production reports, and other sources. The list of chemicals reported from year to year is consistent, with the following exceptions: Chemical 1,4-Dichlorobenzene Diaminotoluene (mixed isomers) Propylene Years not reported 2014 2016,2017 2013,2014 Reason Usage varies from year to year. Removed from process. Discovered during performance test in 2015, began reporting it that year. The facility's usage tables show all TRI chemicals that are manufactured, processed, or otherwise used, along with whether they are used at an amount> or< threshold . As indicated, the facility opted to report some chemicals with annual usage amounts that are just below threshold . Rubico n provided verbal clarification on how certain chemicals are used in their various processes and confirmed that usage of some chemicals exceeds 1,000,000 pounds annually. 3 Rubicon LLC Inspection Dates: 08/27-31/2018 Appendix 1 Business Cards Rubicon LLC Inspection Dates: 08/27-31/2018 Appendix 2 Facility Maps Rubicon LLC Inspection Dates: 08/27-31/2018 Appendix 3 Process Description & Flow Diagrams Rubicon LLC Inspection Dates: 08/27-31/2018 Appendix 4 Chemical Usage TRI Reporting: 5-year History Chemical Name 1,4-DICHLOROBENZENE 2,4-DINITROPHENOL 2-METHYLPYRIDINE 2-NITROPHENOL 4,4'-METHYLENEDIANILINE 4-NITROPHENOL ACRYLIC ACID AMMONIA ANILINE BENZENE BORON TRIFLUORIDE CARBON TETRACHLORIDE CHLORINE CHLOROBENZENE DIAMINOTOLUENE (MIXED ISOMERS) DIBUTYL PHTHALATE DICHLOROMETHANE DIETHANOLAMINE DIISOCYANATES DIOXIN & DIOXIN-LIKE COMPOUNDS DIPHENYLAMINE ETHYLENE GLYCOL ETHYLENE OXIDE FORMALDEHYDE HYDROCHLORIC ACID HYDROGEN FLUORIDE MALEIC ANHYDRIDE M-DINITROBENZENE METHANOL N-BUTYL ALCOHOL NICKEL COMPOUNDS NITRATE COMPOUNDS NITRIC ACID NITROBENZENE O-TOLUIDINE PHENOL PHOSGENE PICRIC ACID PROPYLENE PROPYLENE OXIDE QUINOLINE SODIUM NITRITE SULFURIC ACID TOLUENE 2013 yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes no yes yes yes yes yes 2014 no yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes no yes yes yes yes yes 2015 yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes 2016 yes yes yes yes yes yes yes yes yes yes yes yes yes yes no yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes 2017 yes yes yes yes yes yes yes yes yes yes yes yes yes yes no yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes yes Rubicon LLC TRI Usage Summary - 2015 Description 1,1,1-Trichloroethane 1,2 Dichlorobenzene 1,2,4-Trimethylbenzene 1,4 Dichlorobenzene m-Dinitrobenzene 2,4-Dinitrophenol 2-Methylpyridine 2-Nitrophenol 4,4'-Methylenedianiline 4-Aminobiphenyl 4-Nitrophenol Acetonitrile Acrylic Acid Aluminum Oxide Ammonia Aniline Antimony Arsenic Barium Benzene Beryllium Bifenthrin Boron Trifluoride n-Butyl Alcohol Cadmium Carbon Tetrachloride Chlorine Chlorobenzene Chlorodifluoromethane Chloroform Chromium Cyclohexane Diaminotoluene (mixed isomers) Dibutyl Phthalate Dichloromethane Diethanolamine Diisocyanates Dioxins and Dioxin-Like Compounds Diphenylamine Ethylbenzene Ethylene Glycol Ethylene Oxide Formaldehyde n-Hexane Hydrochloric Acid Hydrogen Fluoride Isopropyl alcohol Lead Maleic Anhydride Mercury Methanol Methyl Isobutyl Ketone Usage (pounds) <10,000 <25,000 <10,000 >25,000 >25,000 >25,000 >25,000 >25,000 >25,000 <25,000 <25,000 <25,000 >25,000 <10,000 >10,000 >25,000 <25,000 <25,000 <25,000 >25,000 <25,000 <10,000 <10,000 >25,000 <25,000 >25,000 >10,000 >10,000 <10,000 <25,000 <25,000 <25,000 >25,000 >10,000 <25,000 >25,000 >25,000 >0.00022 >25,000 <10,000 >10,000 >25,000 >10,000 <10,000 >10,000 <10,000 <10,000 <100 >25,000 <10 >25,000 <10,000 Reported? No No No Yes Yes Yes Yes Yes Yes No Yes No Yes No Yes Yes No No No Yes No No Yes Yes No Yes Yes Yes No No No No Yes Yes Yes Yes Yes Yes Yes No Yes Yes Yes No Yes Yes No No Yes No Yes No Comments Form R Form R Form R Form R Form R Form R Below threshold, reported Form R Form R Form R Form R Form R Below threshold, reported Form A Form R Form R Form R Form R Form R Form R Below threshold, reported Form R Form R Form R Form R Form R Form R Form R Form R Form R Below threshold, reported Form R Form R Form R Description Methyl Tert Butyl Ether Nickel Compounds Nitrate Compounds Nitric Acid Nitrobenzene N-Nitroso-diphenylamine o-Toluidine Phenol Phosgene Phosphine Phthalic Anhydride Picric Acid Polychlorinated biphenyls Propylene Propylene Oxide Quinoline Silver Sodium Nitrite Sulfuric Acid Thallium Toluene Xylenes Usage (pounds) <10,000 >10,000 >25,000 >25,000 >25,000 <25,000 >25,000 >25,000 >25,000 <10,000 <25,000 >25,000 <10 >25,000 >25,000 >25,000 <25,000 >10,000 >10,000 <25,000 <10,000 <10,000 Reported? No Yes Yes Yes Yes No Yes Yes Yes No No Yes No Yes Yes Yes No Yes Yes No Yes No Comments Form R Form R Form R Form R Form R Form R Form R Form R Form R Form R Form R Form R Form R Below threshold, reported Form R Rubicon LLC TRI Usage Summary - 2016 Description 1,1,1-Trichloroethane 1,2 Dichlorobenzene 1,2,4-Trimethylbenzene 1,4 Dichlorobenzene m-Dinitrobenzene 2,4-Dinitrophenol 2-Methylpyridine 2-Nitrophenol 4,4'-Methylenedianiline 4-Aminobiphenyl 4-Nitrophenol Acetonitrile Acrylic Acid Aluminum Oxide Ammonia Aniline Antimony Arsenic Barium Benzene Beryllium Bifenthrin Boron Trifluoride n-Butyl Alcohol Cadmium Carbon Tetrachloride Chlorine Chlorobenzene Chlorodifluoromethane Chloroform Chromium Cyclohexane Dibutyl Phthalate Dichloromethane Diethanolamine Diisocyanates Dioxins and Dioxin-Like Compounds Diphenylamine Ethylbenzene Ethylene Glycol Ethylene Oxide Formaldehyde n-Hexane Hydrochloric Acid Hydrogen Fluoride Isopropyl alcohol Lead Maleic Anhydride Mercury Methanol Methyl Isobutyl Ketone Methyl Tert Butyl Ether Usage (pounds) <10,000 <25,000 <10,000 >25,000 >25,000 >25,000 >25,000 >25,000 >25,000 <25,000 <25,000 <25,000 >25,000 <10,000 >10,000 >25,000 <25,000 <25,000 <25,000 >25,000 <25,000 <10,000 >10,000, <1,000,000 >25,000 <25,000 >25,000 >10,000 >10,000 <10,000 <25,000 <25,000 <25,000 >10,000 <25,000 >25,000 >25,000 >0.00022 >25,000 <10,000 >10,000 >25,000 >10,000 <10,000 >10,000 >10,000 <10,000 <100 >25,000 <10 >25,000 <10,000 <10,000 Reported? No No No Yes Yes Yes Yes Yes Yes No Yes No Yes No Yes Yes No No No Yes No No Yes Yes No Yes Yes Yes No No No No Yes Yes Yes Yes Yes Yes No Yes Yes Yes No Yes Yes No No Yes No Yes No No Comments Form R Form R Form R Form R Form R Form R Below threshold, reported Form R Form R Form R Form R Form R Form A Form R Form R Form R Form R Form R Below threshold, reported Form R Form R Form R Form R Form R Form R Form R Form R Form R Form R Form R Form R Description Nickel Compounds Nitrate Compounds Nitric Acid Nitrobenzene N-Nitroso-diphenylamine o-Toluidine Phenol Phosgene Phosphine Phthalic Anhydride Picric Acid Polychlorinated biphenyls Propylene Propylene Oxide Quinoline Silver Sodium Nitrite Sulfuric Acid Thallium Toluene Xylenes Usage (pounds) >10,000 >25,000 >25,000 >25,000 <25,000 >25,000 >25,000 >25,000 <10,000 <25,000 >25,000 <10 >25,000 >25,000 >25,000 <25,000 >10,000 >10,000 <25,000 <10,000 <10,000 Reported? Yes Yes Yes Yes No Yes Yes Yes No No Yes No Yes Yes Yes No Yes Yes No Yes No Comments Form R Form R Form R Form R Form R Form R Form R Form R Form R Form R Form R Form R Form R Below threshold, reported Form R Rubicon LLC TRI Usage Summary - 2017 Description 1,1,1-Trichloroethane 1,2 Dichlorobenzene 1,2,4-Trimethylbenzene 1,4 Dichlorobenzene m-Dinitrobenzene 2,4-Dinitrophenol 2-Methylpyridine 2-Nitrophenol 4,4'-Methylenedianiline 4-Aminobiphenyl 4-Nitrophenol Acetonitrile Acrylic Acid Aluminum Oxide Ammonia Aniline Antimony Arsenic Barium Benzene Beryllium Bifenthrin Boron Trifluoride n-Butyl Alcohol Cadmium Carbon Tetrachloride Chlorine Chlorobenzene Chlorodifluoromethane Chloroform Chromium Cyclohexane Dibutyl Phthalate Dichloromethane Diethanolamine Diisocyanates Dioxins and Dioxin-Like Compounds Diphenylamine Ethylbenzene Ethylene Glycol Ethylene Oxide Formaldehyde n-Hexane Hydrochloric Acid Hydrogen Fluoride Isopropyl alcohol Lead Maleic Anhydride Mercury Methanol Methyl Isobutyl Ketone Methyl Tert Butyl Ether Usage (pounds) <10,000 <25,000 <10,000 >25,000 >25,000 >25,000 >25,000 >25,000 >25,000 <25,000 <25,000 <25,000 >25,000 <10,000 >10,000 >25,000 <25,000 <25,000 <25,000 >25,000 <25,000 <10,000 >10,000, <1,000,000 >25,000 <25,000 >25,000 >10,000 >10,000 <10,000 <25,000 <25,000 <25,000 >10,000 <25,000 >25,000 >25,000 >0.00022 >25,000 <10,000 >10,000 >25,000 >10,000 <10,000 >10,000 >10,000 <10,000 <100 >25,000 <10 >25,000 <10,000 <10,000 Reported? No No No Yes Yes Yes Yes Yes Yes No Yes No Yes No Yes Yes No No No Yes No No Yes Yes No Yes Yes Yes No No No No Yes Yes Yes Yes Yes Yes No Yes Yes Yes No Yes Yes No No Yes No Yes No No Comments Form R Form R Form R Form R Form R Form R Below threshold, reported Form R Form R Form R Form R Form R Form A Form R Form R Form R Form R Form R Below threshold, reported Form R Form R Form R Form R Form R Form R Form R Form R Form R Form R Form R Form R Description Nickel Compounds Nitrate Compounds Nitric Acid Nitrobenzene N-Nitroso-diphenylamine o-Toluidine Phenol Phosgene Phosphine Phthalic Anhydride Picric Acid Polychlorinated biphenyls Propylene Propylene Oxide Quinoline Silver Sodium Nitrite Sulfuric Acid Thallium Toluene Xylenes Usage (pounds) >10,000 >25,000 >25,000 >25,000 <25,000 >25,000 >25,000 >25,000 <10,000 <25,000 >25,000 <10 >25,000 >25,000 >25,000 <25,000 >10,000 >10,000 <25,000 <10,000 <10,000 Reported? Yes Yes Yes Yes No Yes Yes Yes No No Yes No Yes Yes Yes No Yes Yes No Yes No Comments Form R Form R Form R Form R Form R Form R Form R Form R Form R Form R Form R Form R Form R Below threshold, reported Form R Rubicon LLC Inspection Dates: 08/27-31/2018 Appendix 5 Certification Dates of Forms Page 1 of 7 TRI EZ Query Results TRI Facility Id Equal to 70734RBCNN9156H Reporting Year Greater than/Equal to 2013 Results are based on data extracted on 12-SEP-18 Page No. 1 Generated SQL Select distinct V_TRI_SUBMISSIONS_EZ.TRI_FACILITY_ID, V_TRI_SUBMISSIONS_EZ.FACILITY_NAME, V_TRI_SUBMISSIONS_EZ.REPORTING_YEAR, V_TRI_SUBMISSIONS_EZ.CHEM_NAME, to_char(V_TRI_SUBMISSIONS_EZ.RECEIVED_DATE, 'YYYY-MM-DD'), to_char(V_TRI_SUBMISSIONS_EZ.ORIG_RECEIVED, 'YYYY-MM-DD'), V_TRI_SUBMISSIONS_EZ.REVISION_CODE_1 from V_TRI_SUBMISSIONS_EZ where (V_TRI_SUBMISSIONS_EZ.TRI_FACILITY_ID = '70734RBCNN9156H') and (V_TRI_SUBMISSIONS_EZ.REPORTING_YEAR >= '2013') order by V_TRI_SUBMISSIONS_EZ.REPORTING_YEAR asc , V_TRI_SUBMISSIONS_EZ.CHEM_NAME asc TRI Facility Id Facility Name Reporting Year 70734RBCNN9156H RUBICON 2013 LLC 70734RBCNN9156H RUBICON 2013 LLC 70734RBCNN9156H RUBICON 2013 LLC 70734RBCNN9156H RUBICON 2013 LLC 70734RBCNN9156H RUBICON 2013 LLC 70734RBCNN9156H RUBICON 2013 LLC 70734RBCNN9156H RUBICON 2013 LLC 70734RBCNN9156H RUBICON 2013 LLC 70734RBCNN9156H RUBICON 2013 LLC 70734RBCNN9156H RUBICON 2013 LLC 70734RBCNN9156H RUBICON 2013 LLC 70734RBCNN9156H RUBICON 2013 LLC 70734RBCNN9156H RUBICON 2013 LLC 70734RBCNN9156H RUBICON 2013 LLC 70734RBCNN9156H RUBICON 2013 LLC 70734RBCNN9156H RUBICON 2013 LLC 70734RBCNN9156H RUBICON 2013 LLC 70734RBCNN9156H RUBICON 2013 LLC 70734RBCNN9156H RUBICON 2013 LLC 70734RBCNN9156H RUBICON 2013 LLC 70734RBCNN9156H RUBICON 2013 LLC Chemical Name 1,4-DICHLOROBENZENE 2,4-DINITROPHENOL 2-METHYLPYRIDINE 2-NITROPHENOL 4,4'-METHYLENEDIANILINE 4-NITROPHENOL ACRYLIC ACID AMMONIA ANILINE BENZENE BORON TRIFLUORIDE CARBON TETRACHLORIDE CHLORINE CHLOROBENZENE DIAMINOTOLUENE (MIXED ISOMERS) DIBUTYL PHTHALATE DICHLOROMETHANE DIETHANOLAMINE DIISOCYANATES DIOXIN AND DIOXIN-LIKE COMPOUNDS DIPHENYLAMINE Orig Received Received Revision Code Date 1 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 https://ofmint.rtpnc.epa.gov/enviro/ez_build_sql2.get_table 9/19/2018 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 2013 2013 2013 2013 2013 2013 2013 2013 2013 2013 2013 2013 2013 2013 2013 2013 2013 2013 2013 2013 2013 2013 2014 2014 2014 2014 2014 2014 2014 2014 2014 2014 2014 2014 2014 Page 2 of 7 ETHYLENE GLYCOL ETHYLENE OXIDE FORMALDEHYDE HYDROCHLORIC ACID (1995 AND AFTER "ACID AEROSOLS" ONLY) HYDROGEN FLUORIDE M-DINITROBENZENE MALEIC ANHYDRIDE METHANOL N-BUTYL ALCOHOL NICKEL COMPOUNDS NITRATE COMPOUNDS NITRIC ACID NITROBENZENE O-TOLUIDINE PHENOL PHOSGENE PICRIC ACID PROPYLENE OXIDE QUINOLINE SODIUM NITRITE SULFURIC ACID (1994 AND AFTER "ACID AEROSOLS" ONLY) TOLUENE 2,4-DINITROPHENOL 2-METHYLPYRIDINE 2-NITROPHENOL 4,4'-METHYLENEDIANILINE 4-NITROPHENOL ACRYLIC ACID AMMONIA ANILINE BENZENE BORON TRIFLUORIDE CARBON TETRACHLORIDE CHLORINE CHLOROBENZENE JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUL-01-2015 RR4 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-27-2014 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 https://ofmint.rtpnc.epa.gov/enviro/ez_build_sql2.get_table 9/19/2018 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 2014 2014 2014 2014 2014 2014 2014 2014 2014 2014 2014 2014 2014 2014 2014 2014 2014 2014 2014 2014 2014 2014 2014 2014 2014 2014 2014 2014 2014 2015 2015 2015 2015 2015 2015 Page 3 of 7 DIAMINOTOLUENE (MIXED ISOMERS) DIBUTYL PHTHALATE DICHLOROMETHANE DIETHANOLAMINE DIISOCYANATES DIOXIN AND DIOXIN-LIKE COMPOUNDS DIPHENYLAMINE ETHYLENE GLYCOL ETHYLENE OXIDE FORMALDEHYDE HYDROCHLORIC ACID (1995 AND AFTER "ACID AEROSOLS" ONLY) HYDROGEN FLUORIDE M-DINITROBENZENE MALEIC ANHYDRIDE METHANOL N-BUTYL ALCOHOL NICKEL COMPOUNDS NITRATE COMPOUNDS NITRIC ACID NITROBENZENE O-TOLUIDINE PHENOL PHOSGENE PICRIC ACID PROPYLENE OXIDE QUINOLINE SODIUM NITRITE SULFURIC ACID (1994 AND AFTER "ACID AEROSOLS" ONLY) TOLUENE 1,4-DICHLOROBENZENE 2,4-DINITROPHENOL 2-METHYLPYRIDINE 2-NITROPHENOL 4,4'-METHYLENEDIANILINE 4-NITROPHENOL JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-30-2015 JUN-28-2016 JUN-28-2016 JUN-28-2016 JUN-28-2016 JUN-28-2016 JUN-28-2016 JUN-28-2016 JUN-28-2016 JUN-28-2016 JUN-28-2016 JUN-28-2016 JUN-28-2016 https://ofmint.rtpnc.epa.gov/enviro/ez_build_sql2.get_table 9/19/2018 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 2015 2015 2015 2015 2015 2015 2015 2015 2015 2015 2015 2015 2015 2015 2015 2015 2015 2015 2015 2015 2015 2015 2015 2015 2015 2015 2015 2015 2015 2015 2015 2015 2015 2015 2015 ACRYLIC ACID AMMONIA ANILINE BENZENE BORON TRIFLUORIDE CARBON TETRACHLORIDE CHLORINE CHLOROBENZENE DIAMINOTOLUENE (MIXED ISOMERS) DIBUTYL PHTHALATE DICHLOROMETHANE DIETHANOLAMINE DIISOCYANATES DIOXIN AND DIOXIN-LIKE COMPOUNDS DIPHENYLAMINE ETHYLENE GLYCOL ETHYLENE OXIDE FORMALDEHYDE HYDROCHLORIC ACID (1995 AND AFTER "ACID AEROSOLS" ONLY) HYDROGEN FLUORIDE M-DINITROBENZENE MALEIC ANHYDRIDE METHANOL N-BUTYL ALCOHOL NICKEL COMPOUNDS NITRATE COMPOUNDS NITRIC ACID NITROBENZENE O-TOLUIDINE PHENOL PHOSGENE PICRIC ACID PROPYLENE PROPYLENE OXIDE QUINOLINE https://ofmint.rtpnc.epa.gov/enviro/ez_build_sql2.get_table Page 4 of 7 JUN-28-2016 JUN-28-2016 JUN-28-2016 JUN-28-2016 JUN-28-2016 JUN-28-2016 JUN-28-2016 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LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 2015 2015 2015 2016 2016 2016 2016 2016 2016 2016 2016 2016 2016 2016 2016 2016 2016 2016 2016 2016 2016 2016 2016 2016 2016 2016 2016 2016 2016 2016 2016 2016 2016 2016 2016 Page 5 of 7 SODIUM NITRITE SULFURIC ACID (1994 AND AFTER "ACID AEROSOLS" ONLY) TOLUENE 1,4-DICHLOROBENZENE 2,4-DINITROPHENOL 2-METHYLPYRIDINE 2-NITROPHENOL 4,4'-METHYLENEDIANILINE 4-NITROPHENOL ACRYLIC ACID AMMONIA ANILINE BENZENE BORON TRIFLUORIDE CARBON TETRACHLORIDE CHLORINE CHLOROBENZENE DIBUTYL PHTHALATE DICHLOROMETHANE DIETHANOLAMINE DIISOCYANATES DIOXIN AND DIOXIN-LIKE COMPOUNDS DIPHENYLAMINE ETHYLENE GLYCOL ETHYLENE OXIDE FORMALDEHYDE HYDROCHLORIC ACID (1995 AND AFTER "ACID AEROSOLS" ONLY) HYDROGEN FLUORIDE M-DINITROBENZENE MALEIC ANHYDRIDE METHANOL N-BUTYL ALCOHOL NICKEL COMPOUNDS NITRATE COMPOUNDS NITRIC ACID JUN-28-2016 JUN-28-2016 JUN-28-2016 JUN-28-2016 JUN-28-2016 JUN-28-2016 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 https://ofmint.rtpnc.epa.gov/enviro/ez_build_sql2.get_table 9/19/2018 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 70734RBCNN9156H RUBICON LLC 2016 2016 2016 2016 2016 2016 2016 2016 2016 2016 2016 2017 2017 2017 2017 2017 2017 2017 2017 2017 2017 2017 2017 2017 2017 2017 2017 2017 2017 2017 2017 2017 2017 2017 2017 Page 6 of 7 NITROBENZENE O-TOLUIDINE PHENOL PHOSGENE PICRIC ACID PROPYLENE PROPYLENE OXIDE QUINOLINE SODIUM NITRITE SULFURIC ACID (1994 AND AFTER "ACID AEROSOLS" ONLY) TOLUENE 1,4-DICHLOROBENZENE 2,4-DINITROPHENOL 2-METHYLPYRIDINE 2-NITROPHENOL 4,4'-METHYLENEDIANILINE 4-NITROPHENOL ACRYLIC ACID AMMONIA ANILINE BENZENE BORON TRIFLUORIDE CARBON TETRACHLORIDE CHLORINE CHLOROBENZENE DIBUTYL PHTHALATE DICHLOROMETHANE DIETHANOLAMINE DIISOCYANATES DIOXIN AND DIOXIN-LIKE COMPOUNDS DIPHENYLAMINE ETHYLENE GLYCOL ETHYLENE OXIDE FORMALDEHYDE HYDROCHLORIC ACID (1995 AND AFTER "ACID AEROSOLS" ONLY) JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-29-2017 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 https://ofmint.rtpnc.epa.gov/enviro/ez_build_sql2.get_table 9/19/2018 Page 7 of 7 70734RBCNN9156H RUBICON 2017 LLC 70734RBCNN9156H RUBICON 2017 LLC 70734RBCNN9156H RUBICON 2017 LLC 70734RBCNN9156H RUBICON 2017 LLC 70734RBCNN9156H RUBICON 2017 LLC 70734RBCNN9156H RUBICON 2017 LLC 70734RBCNN9156H RUBICON 2017 LLC 70734RBCNN9156H RUBICON 2017 LLC 70734RBCNN9156H RUBICON 2017 LLC 70734RBCNN9156H RUBICON 2017 LLC 70734RBCNN9156H RUBICON 2017 LLC 70734RBCNN9156H RUBICON 2017 LLC 70734RBCNN9156H RUBICON 2017 LLC 70734RBCNN9156H RUBICON 2017 LLC 70734RBCNN9156H RUBICON 2017 LLC 70734RBCNN9156H RUBICON 2017 LLC 70734RBCNN9156H RUBICON 2017 LLC 70734RBCNN9156H RUBICON 2017 LLC 70734RBCNN9156H RUBICON 2017 LLC HYDROGEN FLUORIDE M-DINITROBENZENE MALEIC ANHYDRIDE METHANOL N-BUTYL ALCOHOL NICKEL COMPOUNDS NITRATE COMPOUNDS NITRIC ACID NITROBENZENE O-TOLUIDINE PHENOL PHOSGENE PICRIC ACID PROPYLENE PROPYLENE OXIDE QUINOLINE SODIUM NITRITE SULFURIC ACID (1994 AND AFTER "ACID AEROSOLS" ONLY) TOLUENE JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 JUN-27-2018 Total number of records returned from your query: 215 Number of Records shown on this page: 215 *** Output to CSV File ***The result set above presents a list of unique data in the output. 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EPA Home | Contact Us Last updated on Wednesday, September 19th, 2018 https://ofmint.rtpnc.epa.gov/enviro/ez_build_sql2.get_table 9/19/2018 Rubicon LLC Inspection Dates: 08/27-31/2018 Appendix 6 Form R Data 2013 - 2017 1,4-Dichlorobenzene Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 2014 M not reported 2015 M 2016 M 2017 M 0 2 0 NA NA 0 14,000 liquid waste NA NA 0 88 0 NA NA 0 13,000 liquid waste NA NA 0 88 0 NA NA 0 8,600; 6,500 liquid waste NA NA 0 89 0 NA NA 0 15,000; 5 liquid waste NA NA driley: produce, byproduct, impurity driley: incin., incin. driley: incineration NA NA NA NA 2 88 88 89 NA NA NA NA NA NA NA 14,000 14,002 NA NA NA NA NA NA NA 13,000 13,088 NA NA NA NA NA NA NA 15,000 15,088 NA NA NA NA NA NA NA 15,000 15,089 2,4-Dinitrophenol Reporting year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 M 2014 M 2015 M 2016 M 2017 M 0 0 0 NA NA 0 6 wastewater NA NA 0 0 0 0 0 0 0 0 0 NA NA NA NA NA NA 0 0 0 2 1 3 wastewater wastewater wastewater NA NA NA NA NA NA 0 0 0 NA NA 0 5 wastewater NA NA NA NA NA NA NA 0 0 0 0 0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 6 2 1 3 5 6 2 1 3 5 driley: produce, byproduct, impurity driley: incineration driley: neutralization, air/steam stripping, settling, other 2-Methylpyridine Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 M 2014 M 2015 M 2016 M 2017 M 0 910 NA NA NA 0 NA liquid waste boiler NA 0 0 0 980 1,050 950 NA NA NA NA NA NA NA NA NA 0 0 0 NA NA NA liquid waste liquid waste liquid waste boiler boiler boiler NA NA NA 0 860 NA NA NA 0 NA liquid waste boiler NA driley: produce, byproduct, impurity driley: incineration 910 NA NA 130,000 NA NA NA NA NA 130,910 NA 980 NA NA 130,000 NA NA NA NA NA 130,980 NA 1,050 NA NA 140,000 NA NA NA NA NA 141,050 NA 950 NA NA 130,000 NA NA NA NA NA 130,950 NA 860 NA NA 140,000 NA NA NA NA NA 140,860 2-Nitrophenol Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 M 2014 M 2015 M 2016 M 2017 M 0 0 NA NA NA 0 NA wastewater NA NA 0 0 0 0 0 0 NA NA NA NA NA NA NA NA NA 0 0 0 NA NA NA wastewater wastewater wastewater NA NA NA NA NA NA 0 0 NA NA NA 0 NA wastewater NA NA NA NA NA NA NA 0 0 0 0 0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 0 0 0 0 0 driley: produce, byproduct, impurity driley: neutralization, air/steam stripping, settling, other 4,4'-Methylenedianiline Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 M, P 2014 M, P 2015 M, P 2016 M, P 2017 M, P 22 31 0 140,000 NA 0 100; 23,000 gaseous; wastewater NA NA 0 30 0 190,000 NA 0 130; 25,000 gaseous; wastewater NA NA 0 30 0 310,000 NA 0 240; 19,000; 1,400 gaseous; wastewater NA NA 0 30 0 140,000 NA 0 130; 270,000 gaseous; wastewater NA NA 0 30 0 160,000 NA 0 170; 1,500; 24,000 gaseous; wastewater NA NA 140,000 53 100 NA NA NA NA NA NA 23,000 163,153 190,000 30 130 NA NA NA NA NA NA 25,000 215,160 310,000 30 240 NA NA NA NA NA NA 20,400 330,670 140,000 30 130 NA NA NA NA NA NA 270,000 410,160 160,000 30 170 NA NA NA NA NA NA 26,000 186,200 driley: produce, onsite use/processing, sale/distribution; reactant driley: landfill; incineration; incineration driley: scrubber; neut., stripping, settling, other 4-Nitrophenol Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 M 2014 M 2015 M 2016 M 2017 M 0 0 NA NA NA 0 NA wastewater NA NA 0 0 NA NA NA 0 NA wastewater NA NA 0 0 NA NA NA 0 NA wastewater NA NA 0 0 NA NA NA 0 NA wastewater NA NA 0 0 NA NA NA 0 NA wastewater NA NA NA NA NA NA NA 0 0 0 0 0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 0 0 0 0 0 driley: produce, byproduct, impurity driley: neutralization, air/steam stripping, settling, other Acrylic acid Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 M 380 1,700 0 NA NA 0 NA gaseous NA NA 2014 M 390 1,600 0 NA NA 0 NA gaseous NA NA 2015 M 390 1,800 0 NA NA 0 NA gaseous NA NA 2016 2017 M M 380 1,700 0 NA NA 0 NA gaseous NA NA 710 1,900 0 NA NA 0 NA gaseous NA NA driley: produce, byproduct driley: incineration NA 2,100 NA NA NA NA NA NA NA NA 2,100 NA 2,000 NA NA NA NA NA NA NA NA 2,000 NA 2,190 NA NA NA NA NA NA NA NA 2,190 NA 2,080 NA NA NA NA NA NA NA NA 2,080 NA 2,600 NA NA NA NA NA NA NA NA 2,600 Ammonia Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 M, P, OU 2014 M, P, OU 2015 M, P, OU 2016 M, P, OU 2017 M, P, OU 7,100 7,800 0 350,000 2,100 19,000 0 700,000 NA 0 2,100 14,000 0 550,000 NA 0 2,100 13,000 0 740,000 NA 0 480 gaseous; wastewater; gaseous NA NA 47 gaseous; wastewater; gaseous NA NA 29 gaseous; wastewater; gaseous NA NA 51 gaseous; wastewater; gaseous NA NA 2,100 14,000 0 720,000 NA 0 320 gaseous; wastewater; gaseous NA NA 350,000 15,000 NA NA NA NA NA NA NA 480 365,480 700,000 21,000 NA NA NA NA NA NA NA 47 721,047 550,000 16,100 NA NA NA NA NA NA NA 29 566,129 740,000 15,000 NA NA NA NA NA NA NA 51 755,051 720,000 16,000 NA NA NA NA NA NA NA 320 736,320 driley: produce, onsite use/processing, sale/dist., byproduct; reactant; chem. proc. aid driley: incineration driley: absorber; neut., settling, other; scrubber Aniline Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 M, P 2014 M, P 6,600 20,000 0 1,700,000 NA 0 4,900 22,000 0 1,500,000 NA 0 100; 12,000 wastewater; liquid waste; gaseous; gaseous boiler NA 150; 6,900 wastewater; liquid waste; gaseous; gaseous boiler NA 1,700,000 27,000 1,500,000 27,000 2015 M, P 5,000 17,000 0 2,200,000 NA 0 240; 7,200; 4,000 wastewater; liquid waste; gaseous; gaseous boiler NA 2,200,000 22,000 2016 M, P 2017 M, P 4,800 4,800 15,000 13,000 0 0 1,900,000 2,100,000 NA NA 0 0 170; 4,100; 130; 50,000 8,200 wastewater; wastewater; liquid waste; liquid waste; gaseous; gaseous; gaseous gaseous boiler boiler NA NA 1,900,000 20,000 2,100,000 18,000 driley: produce, on-site use/processing, sale/dist.; reactant driley: landfill; incineration; incineration driley: neutralization, settling, other; incineration; scrubber; condenser 100 NA 1,900,000 NA NA NA NA 12,000 3,639,100 150 NA 1,700,000 NA NA NA NA 6,900 3,234,050 240 NA 1,700,000 NA NA NA NA 11,200 3,933,440 130 NA 1,400,000 NA NA NA NA 50,000 3,370,130 170 NA 1,700,000 NA NA NA NA 12,000 3,830,170 Benzene Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 P 2014 P 2015 P 2016 P 2017 P 1,400 1,400 1,500 25,000 21,500 17,000 0 0 0 5,900 1,700 3,400 NA NA NA 0 0 0 100; 320; 7 130; 200; 6 240; 59; 7 wastewater; wastewater; wastewater; wastewater; wastewater; wastewater; liquid waste; liquid waste; liquid waste; gaseous; gaseous; gaseous; gaseous gaseous gaseous boiler boiler boiler NA NA NA 1,200 1,500 14,000 13,000 0 0 2,900 3,000 NA NA 0 0 130; 17; 5 170; 79; 1 wastewater; wastewater; wastewater; wastewater; liquid waste; liquid waste; gaseous; gaseous; gaseous gaseous boiler boiler NA NA 5,900 26,000 1,700 23,000 3,400 18,500 2,900 15,000 3,000 15,000 driley: reactant driley: Subt C landfill; incineration; solvents/organics recovery driley: neutralization, stripping, settling, other; neut., settling, other; incineration; scrubber; condenser, scrubber, incineration 100 NA 730,000 NA NA 7 NA 320 762,327 130 NA 510,000 NA NA 6 NA 200 535,036 240 NA 450,000 NA NA 7 NA 59 472,206 130 NA 260,000 NA NA 5 NA 17 278,052 170 NA 290,000 NA NA 1 NA 79 308,250 Boron trifluoride Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite 2013 2014 2015 2016 2017 FORM A FORM A FORM A FORM A FORM A Carbon tetrachloride Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 M 2014 M 2015 M 2016 M 2017 M 950 27,000 0 NA NA 0 4,800 wastewater; wastewater; gaseous; gaseous NA NA 950 27,000 0 NA NA 0 4,300 wastewater; wastewater; gaseous; gaseous NA NA 950 26,000 0 NA NA 0 4,300 wastewater; wastewater; gaseous; gaseous NA NA 950 24,000 0 NA NA 0 2,900; 2,200 wastewater; wastewater; gaseous; gaseous NA NA 950 30,000 0 NA NA 0 2; 10,000 wastewater; wastewater; gaseous; gaseous NA NA NA 28,000 NA NA NA NA NA NA NA 4,800 32,800 NA 28,000 NA NA NA NA NA NA NA 4,300 32,300 NA 26,950 NA NA NA NA NA NA NA 4,300 31,250 NA 25,000 NA NA NA NA NA NA NA 5,100 30,100 NA 31,000 NA NA NA NA NA NA NA 10,000 41,000 driley: produce, byproduct driley: incineration; incineration driley: neut., settling, other; neut., settling, other; scrubber; absorber, scrubber, incin. Chlorine Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 P, OU 2014 P, OU 2015 P, OU 2016 P, OU 2017 P, OU 7 0 0 7 2 140 460 480 500 490 110 120 100 120 130 NA NA NA NA NA NA NA NA NA NA 0 0 0 0 0 NA gaseous; gaseous; wastewater; gaseous NA gaseous; gaseous; wastewater; gaseous NA gaseous; gaseous; wastewater; gaseous NA gaseous; gaseous; wastewater; gaseous NA gaseous; gaseous; wastewater; gaseous NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 260 580 580 630 620 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 260 580 580 630 620 driley: Reactant; manf aid, ancillary/other driley: absorber, scrubber; scrubber; neutralization settling, other; absorber, scrubber Chlorobenzene Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 OU 2014 OU 2015 OU 2016 OU 2017 OU 12,000 150,000 0 140,000 NA 0 12,000 160,000 0 110,000 NA 0 13,000 150,000 0 150,000 NA 0 100; 250,000 gaseous; wastewater; gaseous; wastewater NA NA 140; 150,000 gaseous; wastewater; gaseous; wastewater NA NA 240; 18,000; 170,000 gaseous; wastewater; gaseous; wastewater NA NA 11,000 140,000 0 120,000 NA 0 130; 71,000; 110,000 gaseous; wastewater; gaseous; wastewater NA NA 13,000 180,000 0 190,000 NA 0 170; 180,000; 40,000 gaseous; wastewater; gaseous; wastewater NA NA 140,000 160,000 100 NA NA NA NA NA NA 250,000 550,100 110,000 170,000 140 NA NA NA NA NA NA 150,000 430,140 150,000 163,000 240 NA NA NA NA NA NA 188,000 501,240 120,000 150,000 130 NA NA NA NA NA NA 180,000 450,130 190,000 193,000 170 NA NA NA NA NA NA 220,000 603,170 driley: chemical processing aid driley: Subt C landfill; incineration; incineration driley: scrubber, incineration; neut, settling, other; scrubber; neut., settling, other Diaminotoluene (mixed isomers) Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 P 2014 P 2015 2016 2017 P not reported not reported 0 0 0 14 14 18 0 0 0 200 210 0 NA NA NA 0 0 0 100; 8,600 130; 1,700 240; 654 liquid waste; liquid waste NA NA liquid waste; wastewater NA NA liquid waste; wastewater NA NA 200 210 0 14 14 18 100 130 240 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 8,600 1,700 654 8,914 2,054 912 driley: reactant driley: Subt. C landfill; incineration driley: incineration; other, settling, neutralization, other Dibutyl phthalate Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 P, OU 2014 P, OU 2015 P, OU 2016 P, OU 2017 P, OU 13 430 0 27,000 NA 0 100; 7 gaseous; wastewater; liquid waste NA NA 16 420 0 6,800 NA 0 150; 750 gaseous; wastewater; liquid waste NA NA 8 430 0 12,000 NA 0 240; 8,900; 9,700 gaseous; wastewater; gaseous NA NA 8 410 0 4,500 NA 0 130; 720 gaseous; wastewater; gaseous NA NA 250 490 0 22,000 NA 0 170; 10,000; 7,100 gaseous; wastewater; gaseous NA NA 27,000 440 100 NA NA NA NA NA NA 7 27,547 6,800 440 150 NA NA NA NA NA NA 750 8,140 12,000 438 240 NA NA NA NA NA NA 18,600 31,278 4,500 418 130 NA NA NA NA NA NA 720 5,768 22,000 740 170 NA NA NA NA NA NA 17,000 39,910 driley: reactant, ancillary/other driley: landfill; incin.; incin. driley: incineration; neut., other; incin., consdenser Dichloromethane Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 M 2014 M 2015 M 2016 M 2017 M 220 430 0 NA NA 0 100 gaseous; gaseous; wastewater NA NA 220 220 820 520 0 0 NA NA NA NA 0 0 130 gaseous; gaseous; wastewater NA NA 240 gaseous; gaseous; wastewater NA NA 220 520 0 NA NA 0 130 gaseous; gaseous; wastewater NA NA 220 560 0 NA NA 0 170 gaseous; gaseous; wastewater NA NA NA NA NA NA NA 650 1,040 740 740 780 100 130 240 130 170 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 0 NA NA NA NA 750 1,170 980 870 950 driley: produce, byproduct driley: landfill driley: scrubber, incin.; scrubber; neut., settling, other Diethanolamine Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 P 2014 P 2015 P 2016 2017 P P 0 0 0 0 0 2 2 0 0 0 0 0 0 0 0 NA NA NA NA NA NA NA NA NA NA 0 0 0 0 0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2 2 0 0 0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2 2 0 0 0 driley: reactant Diisocyanates Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 M, P 2014 M, P 2015 M, P 2016 2017 M, P M, P 140 200 51 20 0 0 NA NA NA NA 0 0 3,700; 24,000 NA NA NA 10,000; 22,000 NA NA NA 260 19 0 NA NA 0 9,000; 23,000 NA NA NA 160 18 0 NA NA 0 7,000; 11,000; 15,000 NA NA NA 100 19 0 NA NA 0 5,100; 25,000; 550 NA NA NA NA 190 3,700 NA NA NA NA NA NA 24,000 27,890 NA 220 10,000 NA NA NA NA NA NA 22,000 32,220 NA 279 9,000 NA NA NA NA NA NA 23,000 32,279 NA NA 180 120 7,000 NA NA NA NA NA NA 26,000 33,180 5,100 NA NA NA NA NA NA 26,000 31,220 driley: produce, onsite use/processing, sale/distribution; formulation component driley: Subt C landfill; incineration; incineration Dioxin & dioxin-like compounds Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 M 2014 M 2015 M 2016 M 2017 M NA 0.66 0 0.093 NA 0 NA gaseous; wastewater; liquid waste NA NA NA 0.64 0 0.09 NA 0 NA gaseous; wastewater; liquid waste NA NA NA 0.6738089 0 0.0952751 NA 0 NA gaseous; wastewater; liquid waste NA NA NA 0.67 0 0.1 NA 0 NA gaseous; wastewater; liquid waste NA NA NA 0.67 0 0.095 NA 0 NA gaseous; wastewater; liquid waste NA NA 0.093 0.66 NA NA NA NA NA NA NA NA 1 0.09 0.0952751 0.64 0.6738089 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 1 1 0.1 0.095 0.67 0.67 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 1 1 driley: produce, byproduct driley: scrubber; neutralization, settling, other; incineration Diphenylamine Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 M 2014 M 2015 M 2016 M 2017 M 180 19,000 0 3,600 NA 0 110; 5,900 liquid waste; wastewater; gaseous boiler NA 130 20,000 0 2,700 NA 0 130; 4,900 liquid waste; wastewater; gaseous boiler NA 130 20,000 0 1,400 NA 0 240; 240; 1,900 liquid waste; wastewater boiler NA 120 19,000 0 1,200 NA 0 130; 1,400 130 18,000 0 2,400 NA 0 170; 250; 4,600 liquid waste; liquid waste; wastewater wastewater boiler boiler NA NA 3,600 19,000 2,700 20,000 1,400 20,130 1,200 19,000 2,400 18,000 driley: produce, sale/ distribution driley: Subt. C landfill; incineration; incineration driley: incineration; neutralization, air/steam stripping, other 110 NA 530,000 NA NA NA NA 5,900 558,610 130 NA 530,000 NA NA NA NA 4,900 557,730 240 NA 570,000 NA NA NA NA 2,140 593,910 130 NA 520,000 NA NA NA NA 1,400 541,730 170 NA 580,000 NA NA NA NA 4,900 605,470 Ethylene glycol Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 OU 2014 OU 2015 OU 2016 OU 2017 OU 0 0 3,100 5 0 0 NA NA NA NA 0 0 NA NA NA NA NA NA NA NA 0 0 0 5 4 4 0 0 0 NA NA NA NA NA NA 0 0 0 NA NA NA NA NA NA NA NA NA NA NA NA driley: ancillary/other NA NA 3,100 5 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 3,100 5 NA NA NA 5 4 4 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 5 4 4 Ethylene oxide Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 P 2014 P 2015 P 2016 P 2017 P 57 3 0 NA NA 0 NA liquid waste NA NA 84 3 0 NA NA 0 NA liquid waste NA NA 20 3 0 NA NA 0 NA gaseous; wastewater NA NA 80 3 0 NA NA 0 NA gaseous; wastewater NA NA 39 3 0 NA NA 0 NA gaseous; wastewater NA NA NA NA NA NA NA 60 87 23 83 42 driley: reactant driley: incineration; incineration NA NA NA NA NA NA 33,000 NA 33,060 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 34,000 34,000 30,000 NA NA NA NA 87 34,023 34,083 30,042 Formaldehyde Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 P, OU 39 600 0 NA NA 0 100; 51 gaseous NA NA NA 640 100 NA NA NA NA NA NA 51 791 2014 P, OU 83 790 0 NA NA 0 130; 110 gaseous NA NA NA 870 130 NA NA NA NA NA NA 110 1,110 2015 P, OU 33 720 0 NA NA 0 240; 18 gaseous NA NA NA 753 240 NA NA NA NA NA NA 18 1,011 2016 P, OU 53 720 0 NA NA 0 130; 55 gaseous NA NA NA 770 130 NA NA NA NA NA NA 55 955 2017 P, OU 87 800 0 NA NA 0 170; 22 gaseous NA NA NA 890 driley: process, ancillary/other driley: Subt. C landfill; incineration driley: scrubber 170 NA NA NA NA NA NA 22 1,082 Hydrochloric acid (aerosol) Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 M, OU 780 5,900 0 NA NA 0 NA gaseous; gaseous NA NA NA 6,700 NA NA NA NA NA NA NA NA 6,700 2014 M, OU 62 10,500 0 NA NA 0 34 gaseous; gaseous NA NA NA 11,000 34 NA NA NA NA NA NA NA 11,034 2015 M, OU 3 10,000 0 NA NA 0 110 gaseous; gaseous NA NA NA 10,003 110 NA NA NA NA NA NA NA 10,113 2016 M, OU 16 10,000 0 NA NA 0 130 gaseous; gaseous NA NA NA 10,000 130 NA NA NA NA NA NA NA 10,130 2017 M, P, OU 430 11,000 0 NA NA 0 150 gaseous; gaseous NA NA NA 11,000 150 NA NA NA NA NA NA NA 11,150 driley: produce, onsite use/processing, sale/ distribution, byproduct; reactant; manf. aid, ancillary/other driley: Subt. C landfill driley: scrubber; scrubber, incineration Hydrogen fluoride Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 M, OU 2014 M, OU 2015 M, OU 2016 M, OU 2017 M, OU 0 3,600 0 NA NA 0 NA liquid waste NA NA 0 4,800 0 NA NA 0 NA liquid waste NA NA 0 7,700 NA NA NA 0 NA liquid waste NA NA 0 13,000 NA NA NA 0 NA liquid waste NA NA 0 18,000 NA NA NA 0 NA liquid waste NA NA NA 3,600 NA NA NA NA NA NA NA NA 3,600 NA 4,800 NA NA NA NA NA NA NA NA 4,800 NA 7,700 NA NA NA NA NA NA NA NA 7,700 NA 13,000 NA NA NA NA NA NA NA NA 13,000 NA 18,000 NA NA NA NA NA NA NA NA 18,000 driley: produce, byproduct; ancillary/other driley: incineration m-Dinitrobenzene Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 M 2014 M 2015 M 2016 M 2017 M 0 0 0 NA NA 0 NA liquid waste NA NA 0 0 0 NA NA 0 NA liquid waste NA NA 0 0 0 NA NA 0 NA liquid waste NA NA 0 0 0 NA NA 0 NA liquid waste NA NA 0 0 0 NA NA 0 NA liquid waste NA NA NA NA NA NA NA 0 0 0 0 0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 0 0 0 0 0 driley: produce, impurity driley: incineration Maleic anhydride Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 M 2014 M 2015 M 2016 M 2017 M 880 2,900 0 NA NA 0 100; 2,300 wastewater; gaseous; gaseous; gaseous; liquid waste boiler NA 870 850 2,600 3,100 0 0 NA NA NA NA 0 0 150; 3,400 240; 3,300 wastewater; wastewater; gaseous; gaseous; gaseous; gaseous; gaseous; gaseous; liquid liquid waste waste boiler boiler NA NA 2,600 2,800 0 NA NA 0 170; 3,700 wastewater; gaseous; gaseous; gaseous; liquid waste boiler NA 450 3,200 0 NA NA 0 170; 3,700 wastewater; gaseous; gaseous; gaseous; liquid waste boiler NA NA 3,800 100 NA 560,000 NA NA NA NA 2,300 566,200 NA 3,500 150 NA 580,000 NA NA NA NA 3,400 587,050 NA 3,950 240 NA 610,000 NA NA NA NA 3,300 617,490 NA 5,400 130 NA 280,000 NA NA NA NA 2,600 288,130 NA 3,700 170 NA 0 NA NA NA NA 3,700 7,570 driley: Produce, sale/distributio n driley: Subt. C landfill; incineration driley: neutralization, other; incineration,ab sorber; incineration, condenser; scrubber; incineration Methanol Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 P 2014 P 2015 P 2016 P 2017 P 1200 2,100 0 770,000 NA 0 NA wastewater; gaseous NA NA 840 2,600 0 1,100,000 NA 0 NA wastewater; gaseous NA NA 900 2,300 0 1,300,000 NA 0 10; 12 wastewater; gaseous NA NA 850 2,300 0 1,200,000 NA 0 NA wastewater; gaseous NA NA 940 2,500 0 1,300,000 NA 0 13; 8 wastewater; gaseous NA NA 770,000 3,300 1,100,000 3,400 1,300,000 3,200 NA NA NA NA NA NA NA NA 773,300 NA NA NA NA NA NA NA NA 1,103,400 NA NA NA NA NA NA NA 22 1,303,222 1,200,000 3,200 1,300,000 3,400 NA NA NA NA NA NA NA NA 1,203,200 NA NA NA NA NA NA NA 21 1,303,421 driley: impurity driley: incineration; incineration driley: neutralization, settling, other; scrubber n-Butyl alcohol Chemical name Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 P 2014 P 2015 M 2016 M 2017 M 10,000 360 0 22,000 NA 0 NA gaseous; wastewater NA NA 10,100 200 0 33,000 NA 0 NA gaseous; wastewater NA NA 10,300 470 0 30,000 NA 0 NA gaseous; wastewater NA NA 10,000 330 0 31,000 NA 0 NA gaseous; wastewater NA NA 9,000 110 0 32,000 NA 0 NA gaseous; wastewater NA NA 22,000 10,000 NA NA NA NA NA NA NA NA 32,000 33,000 10,000 NA NA NA NA NA NA NA NA 43,000 30,000 10,770 NA NA NA NA NA NA NA NA 40,770 31,000 10,000 NA NA NA NA NA NA NA NA 41,000 32,000 9,100 NA NA NA NA NA NA NA NA 41,100 driley: produce, byproduct driley: incineration; neut., other treatment Nickel compounds Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 OU 2014 OU 2015 OU 0 2,900 0 NA NA 0 220; 7; 430* gaseous NA NA 0 3,300 0 NA NA 0 240; 3 gaseous NA NA 0 3,000 0 NA NA 0 380; 4; 500* gaseous NA NA NA 2,900 NA 3,300 220 240 7 3 NA NA NA NA NA NA 430 NA NA NA NA NA 3,557 3,543 * = metals recovery NA 3,000 380 4 NA NA NA 500 NA NA 3,884 2016 OU 0 3,200 0 NA NA 0 390; 5 gaseous NA NA NA 3,200 390 5 NA NA NA NA NA NA 3,595 2017 OU driley: manufacturing 0 aid 3,400 0 NA NA 0 3,000; 7 driley: Subt. C landfill; solidification/stab. gaseous NA NA driley: other air emission NA treatment 3,400 3,000 7 NA NA NA NA NA NA 6,407 Nitrate compounds Chemical name Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 M 2014 M 2015 M 2016 M 2017 M NA NA 0 640,000 NA 0 NA wastewater NA NA NA NA 0 540,000 NA 0 NA wastewater NA NA NA NA 0 580,000 NA 0 3; 3 wastewater NA NA NA NA 0 350,000 NA 0 NA wastewater NA NA NA NA 0 850,000 NA 0 3; 2 wastewater NA NA 640,000 0 NA NA NA NA NA NA NA NA 640,000 540,000 0 NA NA NA NA NA NA NA NA 540,000 580,000 0 NA NA NA NA NA NA NA 6 580,006 350,000 0 NA NA NA NA NA NA NA NA 350,000 850,000 0 NA NA NA NA NA NA NA 5 850,005 driley: produce, byproduct driley: incineration; incineration driley: neutralization, settling, other Nitric acid Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 P 0 0 0 NA NA 0 NA NA NA NA 2014 P 0 0 0 NA NA 0 NA NA NA NA 2015 P 0 0 0 NA NA 0 NA NA NA NA 2016 P 0 0 0 NA NA 0 NA NA NA NA 2017 P 0 0 0 NA NA 0 NA NA NA NA driley: reactant NA NA 0 0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 0 0 NA NA NA 0 0 0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 0 0 0 Nitrobenzene Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 M, P 2014 M, P 2015 M, P 2016 M, P 3,300 3,600 0 310,000 NA 0 3,700 3,500 0 180,000 NA 0 100; 110,000 liquid waste; wastewater; gaseous; wastewater boiler NA 150; 16 liquid waste; wastewater; gaseous; wastewater boiler NA 3,700 2,600 0 340,000 NA 0 240; 6,800; 8,200 liquid waste; wastewater; gaseous; wastewater boiler NA 3,500 3,700 0 470,000 NA 0 130; 250 liquid waste; wastewater; gaseous; wastewater boiler NA 310,000 6,900 180,000 7,200 340,000 6,300 470,000 7,200 2017 M, P driley: 3,600produce, onsite 2,200 use/processing, 0 sale/distribution; reactant 440,000 NA driley: 0 landfill; 170; 8,500; 5,600 incineration; incineration liquid waste; wastewater; driley: gaseous; incineration; wastewater boiler NA other, settling, neut., other; condenser, scrubber, incin.; stripping, 440,000 5,800 other, neut., settling, other 100 NA 99,000 NA NA NA NA 110,000 526,000 150 NA 95,000 NA NA NA NA 16 282,366 240 NA 95,000 NA NA NA NA 15,000 456,540 130 NA 85,000 NA NA NA NA 250 562,580 170 NA 110,000 NA NA NA NA 14,000 569,970 o-Toluidine Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 M 2014 M 2015 M 2016 M 2017 M 0 38 0 230 NA 0 1 wastewater; liquid waste boiler NA 0 44 0 65 NA 0 1 wastewater; liquid waste boiler NA 0 43 0 270 NA 0 1 wastewater; liquid waste boiler NA 0 44 0 3 NA 0 1 wastewater; liquid waste boiler NA 0 43 0 0 NA 0 1 wastewater; liquid waste boiler NA 230 65 270 3 0 38 44 43 44 43 driley: produce, byproduct driley: incineration driley: other, settling, neut., other; incineration NA NA 160,000 NA NA NA NA 1 160,269 NA NA 150,000 NA NA NA NA 1 150,110 NA NA 150,000 NA NA NA NA 1 150,314 NA NA 140,000 NA NA NA NA 1 140,048 NA NA 180,000 NA NA NA NA 1 180,044 Phenol Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 M 2014 M 2015 M 2016 M 2017 M 93 220 0 450,000 NA 0 7 wastewater; wastewater; liquid waste; gaseous boiler NA 110 190 0 380,000 NA 0 3 wastewater; wastewater; liquid waste; gaseous boiler NA 110 150 0 370,000 NA 0 4 wastewater; wastewater; liquid waste boiler NA 110 140 0 360,000 NA 0 5 wastewater; wastewater; liquid waste boiler NA 110 130 0 180,000 NA 0 7 wastewater; wastewater; liquid waste boiler NA 450,000 310 NA NA 86,000 NA NA NA NA 7 536,317 380,000 300 NA NA 83,000 NA NA NA NA 3 463,303 370,000 260 NA NA 83,000 NA NA NA NA 4 453,264 360,000 250 NA NA 75,000 NA NA NA NA 5 435,255 180,000 240 NA NA 96,000 NA NA NA NA 7 276,247 driley: produce, byproduct, impurity driley: incineration driley: other, settling, neut., other; stripping, other, neut., settling, other; incineration Phosgene Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 M, P 200 5 0 NA NA 0 NA gaseous; gaseous NA NA 2014 M, P 360 5 0 NA NA 0 NA gaseous; gaseous NA NA NA NA 210 370 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 210 370 2015 M, P 240 5 0 NA NA 0 NA gaseous; gaseous NA NA 2016 M, P 280 5 0 NA NA 0 NA gaseous; gaseous NA NA 2017 M, P 240 3 0 NA NA 0 NA gaseous; gaseous NA NA NA NA NA 245 290 240 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 245 290 240 driley: produce, onsite use/processing; reactant driley: landfill; incineration; incineration driley: scrubber; scrubber, incineration Picric acid Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 M 2014 M 2015 M 2016 M 2017 M 0 0 0 NA NA 0 NA wastewater NA NA 0 0 0 NA NA 0 NA wastewater NA NA 0 0 0 NA NA 0 NA wastewater NA NA 0 0 0 NA NA 0 NA wastewater NA NA 0 0 0 NA NA 0 NA wastewater NA NA NA NA 0 0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 0 0 NA NA NA 0 0 0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 0 0 0 driley: produce, byproduct driley: stripping, other, neut., settling, other Propylene Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 2014 not reported not reported 2015 M 1 31,000 0 NA NA 0 NA gaseous NA NA NA 31,001 NA NA NA NA NA NA NA NA 31,001 2016 M 3 23,000 0 NA NA 0 NA gaseous NA NA NA 23,000 NA NA NA NA NA NA NA NA 23,000 2017 M 5 23,000 0 NA NA 0 NA gaseous NA NA NA 23,000 NA NA NA NA NA NA NA NA 23,000 driley: produce, impurity driley: scrubber Propylene oxide Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 P 2014 P 2015 P 2016 P 2017 P 150 140 32 30 0 0 NA NA NA NA 0 0 NA NA liquid waste liquid waste NA NA NA NA 55 30 0 NA NA 0 NA gaseous; wastewater NA NA 110 28 0 NA NA 0 NA gaseous; wastewater NA NA 93 28 0 NA NA 0 NA gaseous; wastewater NA NA NA 180 NA NA NA NA NA NA 320,000 NA 320,180 NA 170 NA NA NA NA NA NA 300,000 NA 300,170 NA 85 NA NA NA NA NA NA 300,000 NA 300,085 NA 140 NA NA NA NA NA NA 280,000 NA 280,140 NA 120 NA NA NA NA NA NA 280,000 NA 280,120 driley: reactant driley: incineration; incineration Quinoline Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 M 2014 M 2015 M 2016 M 2017 M 0 120 0 NA NA 0 3 gaseous; liquid waste boiler NA 0 170 0 NA NA 0 230 gaseous; liquid waste boiler NA 0 150 0 NA NA 0 68 liquid waste boiler NA 0 145 0 NA NA 0 4 liquid waste boiler NA 0 570 0 NA NA 0 62 liquid waste boiler NA NA 120 NA NA 160,000 NA NA NA NA 3 160,123 NA 170 NA NA 160,000 NA NA NA NA 230 160,400 NA 150 NA NA 170,000 NA NA NA NA 68 170,218 NA 150 NA NA 160,000 NA NA NA NA 4 160,154 NA 570 NA NA 170,000 NA NA NA NA 62 170,632 driley: produce, byproduct driley: incineration driley: incineration Sodium nitrite Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 M, OU 2014 M, OU 2015 M, OU 2016 M, OU 2017 M, OU NA NA 0 1,500,000 NA 0 14 wastewater NA NA NA NA 0 1,700,000 NA 0 NA wastewater NA NA NA NA 0 1,500,000 NA 0 7; 9 wastewater NA NA NA NA 0 1,700,000 NA 0 NA wastewater NA NA NA NA 0 1,600,000 NA 0 9; 6 wastewater NA NA 1,500,000 0 1,700,000 0 NA NA NA NA NA NA NA 14 1,500,014 NA NA NA NA NA NA NA NA 1,700,000 1,500,000 0 NA NA NA NA NA NA NA 16 1,500,016 1,700,000 0 NA NA NA NA NA NA NA NA 1,700,000 1,600,000 0 NA NA NA NA NA NA NA 15 1,600,015 driley: produce, byproduct; manf.aid, ancillary/other driley: incineration; incineration driley: other, settling, neut., other Sulfuric acid (aerosol) Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 OU 22 0 NA NA NA 0 NA NA NA NA 2014 OU 89 0 NA NA NA 0 NA NA NA NA 2015 OU 53 0 NA NA NA 0 NA NA NA NA 2016 OU 0 0 NA NA NA 0 NA NA NA NA 2017 OU 0 0 NA NA NA 0 NA NA NA NA driley: chemical processing aid, manufacturing aid NA NA NA NA NA 22 89 53 0 0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 22 89 53 0 0 Toluene Reporting Year Activities & Uses Form R element 5.1 Fugitive or non-point air 5.2 Stack or point air 5.3 Discharges to streams/water bodies 5.4.1 Underground injection onsite 5.5.4 Other disposal 6.1 POTW 6.2 Transfers to offsite locations 7.A On-site waste treatment methods 7.B On-site energy recovery processes 7.C On-site recycling processes Source Reduction & Recycling Activities 8.1.a Onsite disp - UI wells, RCRA landfills, etc. 8.1.b Onsite disp/releases 8.1.c Offsite disp - UI wells, RCRA landfills, etc. 8.1.d Other offsite disp 8.2 Energy recovery onsite 8.3 Energy recovery offsite 8.4 Recycled onsite 8.5 Recycled offsite 8.6 Treated onsite 8.7 Treated offsite Annual Reportable Amount ( 8.1-8.7) 2013 OU 300 18 NA 250 NA 0 100; 340 NA NA NA 2014 OU 300 19 NA 78 NA 0 140; 35 NA NA NA 2015 OU 2016 OU 0 890 NA 73 NA 0 240; 18 gaseous NA NA 21 410 NA 200 NA 0 130; 3,300 gaseous NA NA 2017 OU 21 400 NA 310 NA 0 170; 27 gaseous NA NA driley: ancillary/other driley: landfill; incineration driley: scrubber 250 78 73 200 310 320 320 890 430 420 100 140 240 130 170 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 340 35 18 3,300 27 1,010 573 1,221 4,060 927 Rubicon LLC Inspection Dates: 08/27-31/2018 Appendix 7 Air Emissions Data 2017 Rubicon LLC Inspection Dates: 08/27-31/2018 Appendix 8 Surface Water Data 2017 Rubicon LLC Inspection Dates: 08/27-31/2018 Appendix 9 Underground Injection Well Data 2017 Rubicon LLC Inspection Dates: 08/27-31/2018 Appendix 10 Basis of Calculations Rubicon LLC Inspection Dates: 08/27-31/2018 Appendix 11 Emails Riley, David From: Sent: To: Subject: Attachments: Phillip A Kerr <phillip_a_kerr@huntsman.com> Monday, October 01, 2018 1:39 PM Riley, David Re: [EXTERNAL] additional TRI questions TRI Questions Received from EPA September 25 2018 and Rubicon Responses.pdf David, Good afternoon, see the attached file with responses to your questions. Thanks. Regards, __________ Phil Kerr, PE Environmental Dept. Air Permits and Compliance Rubicon LLC 225-242-5027 Office 225-673-2470 Fax From: "Riley, David" <riley.david@epa.gov> To: "phillip_a_kerr@huntsman.com" <phillip_a_kerr@huntsman.com>, Date: 09/25/2018 10:51 AM Subject: [EXTERNAL] additional TRI questions Hello Phil - Here are some additional questions based on the information you provided: 1. Rubicon's annual list of reported chemicals is fairly consistent, with the exceptions listed below. Please explain why these chemicals were not reported for each of the specified years. 1,4-dichlorobenzene was not reported for 2014 Propylene was not reported for 2013, 2014 2. Regarding boron trifluoride: How is it otherwise used - as a chemical processing aid, a manufacturing aid, or ancillary or other use? 1  Is it directly reused in your process, or is some other activity performed on it? 3. Rainwater, cooling tower blowdown, and sanitary effluent are all directed into the Weak Effluent impoundment. After neutralization and mixing, the water is discharged to the Mississippi River. Chlorine is the only chemical that shows a corresponding release in Section 5.3 of the Form R. Is the chlorine in the surface water discharge coming from a process, or is it used to treat the water prior to discharge? 4. Please clarify the inclusion of the on-site waste treatment method "incineration - thermal destruction other than use as fuel" on the Form R reports. For example, Form Rs for 1,4-dichlorobenzene and acrylic acid show this method for the on-site treatment of liquid or gaseous waste streams containing these chemicals. Fairly high efficiencies for this treatment method are shown in regards to the destruction of the chemicals, yet no corresponding amounts of the chemicals are shown in Section 8.6 as treated on-site. Are the amounts represented elsewhere on the Form R? (In contrast, Form Rs for ethylene oxide and propylene oxide show the same method for the on-site treatment of gaseous/wastewater/liquid waste containing these chemicals. High efficiencies are shown, and corresponding amounts of the chemicals treated are shown in Section 8.6. [aside from ethylene oxide for 2014]) 5. The reports for 2-nitrophenol and 4-nitrophenol list stripping/other/neutralization/settling/other as a treatment sequence for wastewater containing these chemicals. The treatment efficiency is estimated to be 0 - 50%, and no releases or treated amounts are indicated on the reports. What happens to these chemicals during/after the treatment of this waste stream? 6. How many boilers are present at your facility, and what are their locations? Thanks for looking into these, and I may have some follow-up questions. David Riley EPCRA 313 Enforcement Officer US EPA Region 6 (EN-H3) 1445 Ross Avenue, Suite 1200 Dallas, TX 75202-2733 Phone: (214) 665-7298 Fax: (214) 665-6655 e-mail: riley.david@epa.gov 2 TRI Questions Received from EPA September 25, 2018 and Rubicon Response 1. Rubicon's annual list of reported chemicals is fairly consistent, with the exceptions listed below. Please explain why these chemicals were not reported for each of the specified years. 1,4-dichlorobenzene was not reported for 2014 Response: 1,4 Dichlorobenzene is variable from year to year. The amount in 2014 was well below reporting thresholds. Propylene was not reported for 2013, 2014 Response: Propylene was discovered in a performance test conducted in 2015. It was reported based on the results of the performance test for reporting year 2015 and subsequent years. 2. Regarding boron trifluoride: How is it otherwise used - as a chemical processing aid, a manufacturing aid, or ancillary or other use? Response: Boron trifluoride is used as a chemical processing aid. Is it directly reused in your process, or is some other activity performed on it? Response: Boron trifluoride is used in the process. 3. Rainwater, cooling tower blowdown, and sanitary effluent are all directed into the Weak Effluent impoundment. After neutralization and mixing, the water is discharged to the Mississippi River. Chlorine is the only chemical that shows a corresponding release in Section 5.3 of the Form R. Is the chlorine in the surface water discharge coming from a process, or is it used to treat the water prior to discharge? Response: The chlorine is residual chlorine from disinfection (treating) of water/wastewater. 4. Please clarify the inclusion of the on-site waste treatment method "incineration - thermal destruction other than use as fuel" on the Form R reports. For example, Form Rs for 1,4dichlorobenzene and acrylic acid show this method for the on-site treatment of liquid or gaseous waste streams containing these chemicals. Fairly high efficiencies for this treatment method are shown in regards to the destruction of the chemicals, yet no corresponding amounts of the chemicals are shown in Section 8.6 as treated on-site. Are the amounts represented elsewhere on the Form R? (In contrast, Form Rs for ethylene oxide and propylene oxide show the same method for the on-site treatment of gaseous/wastewater/liquid waste containing these chemicals. High efficiencies are shown, and corresponding amounts of the chemicals treated are shown in Section 8.6. [aside from ethylene oxide for 2014]) Response: The amounts are covered in Sections 5.2. and 8.1. 5. The reports for 2-nitrophenol and 4-nitrophenol list stripping/other/neutralization/settling/other as a treatment sequence for wastewater containing these chemicals. The treatment efficiency is estimated to be 0 - 50%, and no releases or treated amounts are indicated on the reports. What happens to these chemicals during/after the treatment of this waste stream? Response: These compounds undergo chemical conversion to organic salts within the process. Riley, David From: Sent: To: Subject: Attachments: Phillip A Kerr <phillip_a_kerr@huntsman.com> Thursday, October 11, 2018 7:20 AM Riley, David Question Responses Part 2 TRI Questions Received from EPA October 3 2018 and Rubicon Responses.pdf David, Attached are the responses to the questions you asked last week. Thanks. Regards, __________ Phil Kerr, PE Environmental Dept. Air Permits and Compliance Rubicon LLC 225-242-5027 Office 225-673-2470 Fax 1 TRI Questions Received from EPA October 3, 2018 and Rubicon Response 1. Specify quantities of acrylic acid, 2-nitrophenol, 4-nitrophenol, 2-4 nitrophenol and picric acid generated. Response: For 2017, the following quantities were estimated for the compounds requested: acrylic acid - ~1.4 million lb 2-nitrophenol - ~145,000 lb 4-nitrophenol - ~22,000 lb 2-4 nitrophenol - ~ 1.8 million lb picric acid - ~380,000 lb 2. Specify the salts that 2-nitrophenol, 4-nitrophenol, 2-4 nitrophenol and picric acid are converted to. Response: 2-nitrophenol and 4-nitrophenol form nitrophenolate C6H4(NO2)Na 2,4 dinitrophenol forms dinitrophenolate C6H3(NO2)2ONa Picric acid forms sodium picrate C6H2(NO2)3ONa Note: None of the salts noted above are TRI chemicals. 3. Verify 1,4 dichlorobenzene treatment values for the site boiler. Response: The treatment values of 1,4 dichlorobenzene for the site boilers/incinerators are estimated to be negligible. The chemical is removed from the process and shipped off site upstream of the boiler, as noted on the Form R. 6. How many boilers are present at your facility, and what are their locations? Response: There are five boilers on site at the following locations: Aniline-2 DPA-1 DPA-2 Maleic Anhydride (2)