Document MGvwyk9YdjVxRxbB3ak4Ledq7
R26 3280
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.
AR226 _ 3280
i ORUNOACK-LABGRATORILH t FOR ANGEWANDTE SI0LOSGIoEl
Terrestrial Plants ToxAicity, Seedling Emergence ECO idaJn 50-- 8 (ra by 2000
sponsor (--unr
DreDupeonts LTD
Author Ske Foy
Test Faciity DoRRKANaootEACnWKeA-LpTAaEBuOSBRsiiAroTLO10R0UM
B31 ter Sarstedt
Laboratory project 1D Synio. Lincasn
`Study No. of the st panics.)
Page 10151 2003b.a0t5e.02
Company Saniized. Does not contain TSCACBN
A re ~
jeport
Page 2 of 51
+
; StatemofeGnLtP Compliance
y
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Test Facility
C i t oto Ts 'DR.U.NOACK-LABORATORIFUOHRANGEWANDTE BIOLOGIE
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company 54
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Statement of the Quality AssuranceUnit
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RUNOAGKLABORATORIUM FOR ANGEWANGTE 810L0GIE
--~
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Page 40151
Ci 226.10 OECD-- Guideline 2m-- 08pOeragllyEme2r3g0e0n)ce
PrSojeec:to.
Personnel Involved
Study Divctor:
S(EinkgeinFeierl,aBictechncogt)
:
ty
Techical Stat:
PKiertsatenMaekvsan SBiamrobnarea WPiioecnnkor
Guay Assurance Unit oop:
(GsuidorougnisM)ahrmann-Kalaboids pSursaonmneiBecker
TDeisstcitnogroPfactie:
(OrB.iUldoiosN)ose
teeon
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conany5ania0.00%
_ voscsmowowmrenmenaness
~~
Reg
Page 5 of 51
Table of Content
rm
43
Fresh Weight (Biomass)
23
~--
1"
GLP Certificate of DR.U.NOACK-LABORATORIUM
`company.
51
2
~ ooo S0s. NOAGKCLABORATORIUM FORANGEWANDTE SIOLOGIEPage sors
ace. 1o OECD Guideline 208 Draft uly 2000)
Studyto
List of Tables
Page
Table 1: Tablo2:
SFhroosoht WHeeiigghhtt:s NNOOEECC,,EECCzzssaannddEECCsssVVaalluueesswwiithhCCoonnffiiddeenncceeRRaannggee((55))
Table3: vNithuComnofifbdEemneecergrReadngSeeed(l5)ings: NOEC, ECzs and ECs Values
5
Table 4: Tables:
Oats: Rape:
Pytatoic Phytotoic
Effects Efecs
and and
Rateof Emergence Rate of Emergence
aftr afer
21 21
Days Days
20 2
Table: Soybean: Phycloic Efecs and Rate of Emergence afer 21 Days Table7: Inibtion of Shoot Height
2 =
Table: Table:
IInnhhiibbiittiioonn ooff EFrmeesrhgWeediSgehetdlings
22
abl 10: abl 11:
Oats: EmergedSeoclings on Day7 Rape: Emerged Seedlings on Day7
= 2
~
Tablo 12: Table13:
SOaotysb:eaEnm:oErmgeerdgSeedsdSleiendglsinognsDoany D14ey
=
Table 14; Table 15:
RSaopyeb:eanE:meErmgeerdgeSdeeSdinegseodnoDinaDyna1gy4 1s4
aas
Tabl 16: Tablo 17:
ORaatpse::EEmmregrgeeddSSoedeidlnigngssoonn DDaayy2211
3 3
abl 16: Tabl 16:
SOaotysb:eaVni:suEamleOrbgseerdvSaeteidolnisngasnodnNuDmabye2r1of Dead Plants on Day 7
5
Table 20: Table 21:
RSaopyeb:eaVni:suVailsuOablseOrbvsaetrivoantsioannsdaNnudmNbuemrboefrDoefaDdePaldanPtlsanoins DoanyO7ay7
a 7
Table 22: Table 25:
Oats: Rape:
Visual Visual
Observations Observations
and and
Number of Number of
Dead Dead
PloanDnay1s4 Plants on Oay doy
14
s 38
|
Tablet: abl 25:
SOaotyebsooVni:suaVlisOubasleOrbvsaetrivoantsioannsd aNnudmbNeurmboefrDoefadDePaldaPntlsanotns oDanyD21a1y4
39 w
Table 26: Table 27:
RSaopyebseanV:isuVailsuOablseOrbvsaetrivoantsioannsdaNnudmNbuemrbeofroDfeaDdePaldanPtlsanotnsDoany2Da1y 21
40
Table 26: Table 20
Oats: Oats:
Shoot Shoot
Height Hoignt
[em] em]
P1o00s,ie3d20Coantnrdol1,00100
and 32 molkg moka OW
OW
" 2
Table 30: Tale 31:
Rape: Rape:
Shoot Shoat
Height Height
em] cm]
Posled 25, 50
Control, and 100
6.25 and 12.5 mg/kg OW
mak
OW
" "
~~
Table 52: Table 33
Soybean: Soybean:
Shoot Shoot
Height Height
[om] [cm]
1P0o0o,le3d20Conatnrdol,100100amnadk3a2
malky OW
OW
riee
sanitast4- posse
compe
DRUNGACK-LABORATORIUM FOR ANGEWANDTE BIOLOGIE
--_
- Roper : Page 7of51
ace. to OECDJG-- eueidelinToee 20-- 8 (DraSfet0ngJulE-- yme2r0g0e0nce -- PrSotjuecdtyN.ol
Table 34: Oats: Fresh WeiognDhay2t1 Table 35: Rape: Fresh Weight on Day 21
a @
Table 36: Soybean:Fresh WeiongDhayt21
a
List of Figures
Page
Figure 1: atsRe:laSthiaoonttoHetihgahTteasttela2m1 CDoanycsen(tMreatainon= nSDS)oil
2
Figure 2: RfnagReelsatSihoonotoHtehieghTtesattelrla2m1CDoancyesnt(rMaetainon+iSnOS)oi
2
Figur3e: SReolatiyoSnhbtoottehHeTiegashttalnfetmer:C2o1nDceanytsrat(ioMn ien=SaoSiDln)
Fl
Figure 4: atRse:laFtrieonshtoWetiheghTtesatfteHre2m1CDoancyesnt(rMaetainon+iSnDS)oil
2
~.
Figure 5: RianpRaei:aFiroenshtoWtehiegThetsatfltiea2m1CoDnacyesnt(rMaetaionn+inSOSo)il
2
Figure 6: SoyRbeelaatni:onFrteosthheWeTiesgthtllaefmtrC2on1ceDnaiyrsai(onMno<SaoSilOn)
2
Figur7e: O{a2tRsel;aEtmioonrgtoedtSheooTdesitngHseamfeCorn2c1entDraaytsio(nMienaSnai+ SD)
2
Figure 8: RBaplea:iEmner1gehdeSeTeedsltiengms aCtotnec2e1ntDraatyison(MianaSnoi+ SD)
2
Figure 9: Soyebleaatni:onE1merthgeedTeSseeHdleimngCsonacfeenrtr2a1tiDoanysn(SMoielan + SD)
2
Figure 10: Rape: Shoot Hoightafter 21 d Figure 11: Rae: Fresh Weight after 21 &
2 2
`compen ganiDoezs1 ed.inTSCACE!
~
TH.
1 Summary
TS CompanySanitized.onetcmn rac
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e port DRUNOACKLABORAeTORRUA T FOR ANGEWANDTE BIOLOGIE TT
Csce. o to OECD-- Gulaai-- n 208 orf uy20_0--0
Sonice:J
Tab 1. Shoo Hag: NOEC, ECsand EG Volos with Gonfdencs Range 5) wore| Fon | seem| Eom | pepe
C Cf E A E D| ews [w owoonTT |eow0m|[ [mg/kg OW]| [mg/kg DW)| [mg/kg DWI [mg/kg OW) | [mg/kg DW]
Tab Fresh Weight NOEG, EnG dEiVee with Cofidarc Rargs (5)
=
wren| fon | seen
nor oW
nhoav ingha ov | mats OW)
~
ff oe [oo[|oeor| [m o-meT]onwr|[w-er|]
[omen | mo[vow | - [ew | - |
Tae: Numbaof mareSeelings: NOEG, EG ndEG Vals wlth Cdn Range 0)
or moo ov
msarooo|w ntEoonow|| mstow0n1
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--
compenany Sentizespossnotcont in TSCA CB}
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OR UeNOeACeKLABORATORIM FOR ANGEWANDTE SI0LOGIE Page 10151
CV see to OECi D Guo 5i '08 ora ly-- 2000) ) issncetLD
2 Characterisation Data of the Test Item
rest imen
)
sath Number
cas
Cramice! characterization
d
Pury
Aepoarance Water sabi
stbilty in water
iCo-pparourafrooaryolaeithhaannoct!8886..98%% ((8aa)). Votowish sold vax 112347 ayri aatt 1225 odeggrreees, $5114 2593 llLL,, 8n=17(OOuUPORnO,,2026020)2
[--
Density eee Expy date Rocommonded storage. Storage testing faity Retention +
Ca. 1.7 glom esses mimeeee
Unlimited stood under te recommended conditions.
Roam tomperaur (20), protected from lsu.
Room amperature,prolctd rom male and ght
Atioas 1g has boon rtainad
.
daoensttiicnagtfonopcarameter Name, bch umberand colour, Ne
he tot Hom and ho information concamin to et fom ware provided by (no Sponsor Company Sani" zed. 0ous not contain TSCAC)
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NOAGKLABORATORIUN FOReAeNGEWANDeTeE BIoOLOGmIE nes Pago T0151
L sce. ta o OECD Guii daine 508(Dn raft Jy 2e 000) ) sSeiso SE
3 Method
`GUIDELINE
FOFaCDe2p0l8a(nDsraTfetsdtioncgu,me(nPta,r JAu)ly.S2e0e0d0i)n,gTeErmreesrtgreianlc(eNon-
TOYFPTEHeANSDTUPDUYRPOSE
Deteinrsmianmaetriogneonfcefoofiefofdeicntgssofansdohnecosraproyrsatedagcehaorfigcraolwsth fos eros plan species.
principle of the test faohremtesastoriuteemDwuacisonunittnecnodrepveoterarpteyr7d idinatyois.hthTenhusemoibseeirendowifhnisgceshciltihsenogswseredes
olanaewatfeonvanosuostopdyoantdanshcoostymhpelofmts.anAdfseha21t deaeyns th
lant wore measured
--_
Test systems Three plant species of diferent fami wore tested
Wonocotyidonas:
Avena sativa (oats), Fiamingsster
Gramineae
Oicatledonae: Glycine max (soybean)', Jutro
Brassica napus (rape)', Poten
Leguminosae Brassicaceae
oRftonsonesftorytshteesmoslacton Tauhiodesipneec.ies are recommended species accoring fo the tet
Origin
Storage
* SLOoOcWHEoSwTSPAEATTKUGSbrG.M,BIHm,RPhoasitnffaoclhd 11-11937,, DD--T269423976RBaesrtagtetn
3 G25R,O0T.Z2N2E8R87PFHLAaNZmENaZUCHT GMBH & Co. KG, Margaretenhof T2h2o5s-ee0d)s waanrdepsettoorcediaodthfomosfitghatcainidymastsotoorme eumnptovr5a.ure
~ Gompany Sanizad. Doss not contain TSCA CBA
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Project-No}
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i H oe OME morasY ot oye,0)
von
MN
(tert.-methyl-butyl-ether) (see table below) "Soil test con-| Amount|Amounotf| Conc. of| Stock.[ rectweighing | Stock | Solvent
fr [ok Tos[osa| eso tos[rosa|
- ||
[wesailwoszia]- |3 | lsowrlosenn] | =|
3 ooT[eisseJ]wsoesrae ||2zs [|weeset | |2-s [|s- eme1 | w-o| |= - 1|
to [wes [rosz | 10 [110 |os [oss] 0 | -|
scacel sod. Dosspetoonia
company 58%
~
pre
ES Sadling emergence
soe ND
below). The test concentrations 320 and 1000 mglkg DW were
~~
Soil test con-| Amount|Amounotf| Cenc. of| Stock
Stock| Solvent
soil sand | Stock | volume" NN volume.
s Nen FeTse[ere | sso |sz J ste |
- |- lswsfomes]- |o | - | --- Twessluessi| | as|
oeooT |sszJ |eeteo T|s0o[[osx a[[2-s1 Jow-sos1| s- o [1--|1
ThTosLesIsTheo [-T-1 -1-1
pes
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| [as|
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wo
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e[3s 80e|
repens ne
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REFERENCE ITEM eNorrse--ron--e f--om is recommended fr is est acsong 0
contol
s eplcats applied wih cua san.
SOLVENT CONTROL
8parmoepolnicasteseanppadadewdithpoqruaoratztmnrdt an fr methyl
osonme: ---
goalm Tomi
Tes conpimions Ouran
naostiis on of h quart sand ih sl: 20021121
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SCoomvptiaofnntghdaste:ats
fSrorsuiesd
--Sem--oif nosfehesquart sand ate
no he sll.
p0S0or2oi1z.ei2dz80
r
Company Sanitized. Does not contain TSCACBI
OFLU.NOACKLABORATORIUM FOR ANGEWANDTE BIOLOGIE
--~
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act. o OECD Guideline 2.08 Dra ly r2e0n00ce
aSoitoteo.KD
Number of ropicates Number of saads
GInrcaorppeoration of the quartz Souing of the seeds:
sand
nt
the
sil;
22000003.-0011.-1178
Compton date
2003.02.07
e8srtpeldiciantasrapenrdodmoiszeedlebvl,ocSkodleesnitgnc.oniol and control were
5 5004s were sown pr replicate
Test medium
O3v,ecrearltlifciaedrbLoUnFcAonstoelnlt;No. 2.2 131% and '; quartz sand (Non-GLP data)
S(Goeblrlattiytcpeehd:.LUSFpA2s2o3i0l0N2o. 22224802)lotaomny sandd(tOIN)
~
GCarrabonizc:ontent: PHvalue
<223m%m02% S604
cTohnedisoilonhssubnaeunses.ored at he test acy at groan house
FOroigRinS:GHLGANSOAWNISRTTASLGHTASFPTELYGEHRE (ULNUTFEAR)S,UOGbHeUrNoGSL-anUgNgDasse 40.
0-67346 Spoyer.
Test container
2Plasotmicvceornetauisneedr.s (standard flower pots) with a damotar of
Sowing .
STeesttonconatnadinseeresdiwnegrohoflielsewweirtoh m70a0gd wtriehataedsesaeidlienagciht(.see {oOengnelcisuzeetedadatwiannsecipehlsoasctaeersdyt.icnoenvteairnyehroslewearnedbcootvieormedwawtietrhesdoila.ndDur-
Application
hTheebceognitnri,ngslovfetnht sctoundtyr,ol and tt tam were applied once at
Applicaton technique nTotrtehaechsaais2o4rphtipornioerqutioltibersiutmarh.eTehsetcfoenmcewntarsatiinocnosrpoofrhateed
--
ester ars sxprossod in 101m of the ry weight f the sol.
Gompany Snitzed. Doss no contain TSCA CBI
_ _ emcdmowonmronwensnoe
__
ro
oy
= rlal --~
[mea |ms | eo | 6 |oo | [oms | t6-2 |eo-t0| 6 |wso0simoo|
[Rape | 7-26 |7-100 | 16 |os0xtion]
Cowecomens ]|
fa
2
=i
:5
~
Hs
2
Js not conta 1scACBI
--_
ORUNOACK-LABORATORFIOUMR ANGEWANDTE SIO-- LOGIE ----
sce 10 OECD Guideline 7,08 Draft ule2r000n)
Sc iotyir o: ee
TOYEPHEEAANSDURFERMEEQNUTESNCAYND. OBSERVATIONS
Tcohneimrsoooumsltyemtpeoruagtuhroeuatnhe treelsattiwveihhuarihceirlymowhoyeGrroegcroarsdhed Oavuetriyng dthaeyasbsoerrvmatiaon mpoerfbioedmeehregrerdapsecetdeisngwse,rneuombbseerrovfed Goad pants and vious pytoe afocts. OTSbeusoeernr.vvaastreiitaowtniesocninsntcwlehurdereadptahlelodvatrrioeapstliioscnyastm,epttahonemdrstnh(eoh.ip.soocsrhelydoorocsonislsr,tolinsom.STatas.r ing), formate affects and growth and evelopment Amndtohnroantadfohdfetaadhgpsaltanundtdsyshtahnoedtnpehcuhotmwoeofibeftmfeewerecgrrteedwmesereseesdduierntegedsr.mined
TESTDESCRIPTION
Day-t
Start 6a 0 Every working da Day, 14,20 Test onc:
cAfopatrmevclaaipmneitniarsoiynnsgNleO(1Nc0o-nGc1Le0nP0trtaats1ti0ow0na0sofpmea1rlmfooryDmWe)dO,wWiatnwhdea3ssdoeisdtoedns Booarsseipdenornaortmfhaecdtroworisohfa4f1avf0 t(chooentpceernaltnmrdiantsiaoorynybseLfaernto),mta1hno0dm1raao1nm00s60t.u2md5gy0/g 700 mak OW witha factorof 2 (ape). oTnheerstaevsptanmteduniautmvtwlasaothdhartaaauntd0ofm5it0nheeCdq,uwwairlethizgqhsueaardntdzau(sc,aan.id1.s)A,sfhoe ented quartz sand was mised with he sc. sTehnedsewsotroe sscownwas placed nth est containers and h: e Tost containers were botom watered and fnised as needed hVoeutplpanhtsowteirecoabfsoecrvsedanodrnnuummbbeerrooffdeemaedrpgleadntsseedings. Fiat shoot heights and resh weight measurements were
~
company Sa0tized. Does not contain TSCA cB!
ORUNOACKLASORATORIUM FOR ANGEWANDTE SIOLOGIE
--~
re Ss
Page 18.0151
2ec.1-- SOEoCDaGuide-- line 2F08S(SrI-- aNtGulEyme2r0g0e0n)ce
Sstoatco,lgmmmnl
SCTAALTCIUSLTAITCSIOANNSD
NNeOeEmGeorfebdiosmoassdsi!ngs owaennreteWacfaaoyrreAendnacloeyussticfsooromftphVaoarrdeiedatnetcroempi(onAaltNeiOdoVncAoo)nftsartonaldtriDecUpacNlalNtyeEsST.iTgWTnheiestn
inPrnEqaguasl+VfOoarbnioatWnhcaeyNToAornsmataliywtseiyrseaondfdoVnEaerqiufaasnctVearaiNaonrcmealTietsyt Taerset0a.n05d
TrhoevaanivtyaofomrcoArNrOecVtAy acnondcDluUdMiNnEgTTt'hsa Ttohesr(sacacepftearbelence)
is a=005.
NcSohonrtsetotaltoirastsnidfcoatlleycassliocglunvlieafnitctiaoncntosnfttrroela.rnepcleicsatwesaorf tfhoeuncdobietrweaennd the
aent contol were summarized in a poled contol group
--
A"latGeoaaidopnlsantspowsesrielmeecaosurrdeidnagntdowheeigghueiddealnindeincluded in
InCtvoarlaulyesofagnrdowctohnfidence CrGaoalncttudlaevtnailcouenessiwtweaerrrveealctsaarwkeeernderocoultmciuWaaetppereodbriat(c1can9oa8rl6dy)isnisg.10a standard
procedure (BREITIG & TOMPLNG 1362)
Software
SESiiegomlmaaPosilt.oat6w(.viin(nd2d0oo0ww0ss))), rMrolIl..C6R2.O.00S3O(2F(0T1080C5)7O,)R,SPOSPRPSASSTSICOOINNRCPOORRPAORTAITOINON
- VALIDITY CRITERIA
Tchaetefso:llowing validity ciria m:ust be found in the conrl ropEO tnmeimnoiamnumsaoefd6i5ng%germowetrhgesnhcoeud not exh visive
Ephryomtooaxincsaufrfveicvtasl of th plants is at east 80% at the end of the test
DGUEIVDIEALTIINOENS FROM THE Nore --_
cschc oy oossneteo"
comps
--_
ee
pees Emergence
]
~~
`Sarstedt, D-31157 Sarstedt.
en poss ake in TSCACB
ORUNOACKLABORATORIUM FOR ANGEWANDTE BIOLOGIE
--_
a Report Ni Page 200151
Co act. 0mOECe D Guideline 208--dra-- pteepul-- EyTC2r0G0o0n)co
sSroc:vl
4 Results roNoelrsotattiosrticfaolrlycaslicgunlifaitciaonntsitfhrerenpcliecsatweesroef tohuencdonbteotlwaaennd tshoelvceonnttrcoolntarnodl wteheressourmmtarciozn-ed ina posed contro group.
44 Visual Phytotoxiity
nThetenplsan4ts wenmretergToeabdbsleserav2ae5ddi-na3gn7.d(asOyabys72e.r11v.4ataNinoudnmsb21earfroeogfivmviseeunralgepThdaybtsloeeleod1ii0cn-ga2fsf1eics(tdsga,eynn7u)r.mnTbaaTrbalboeflo2de12a0d
afer 21 dayas aroTegidvaenyi1n4Taaned 416-.5.1 (day 21). Ptotoic effects and rat of emergence
Told, ote Phyto Eats and atoof merge fer21 0a
~
Gone [teosss
to fs upca
nfiannets
mop ov) cals felslelrle] tm
==1 1
1-1-1 =]
control Co
= r r rr T-T-1Twl
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nd
tof Emergencestr 2 Foor os
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Vlafalorekls slolrleemwr]eats
F e=se E r E re er r e e
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betestee oe eeTol
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in
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Figuwe2: Rape: Shoot Heightafter 21 Days (Mean SD) in Relation to the Test item Concentration in
~ i II iss SN
emeatr Plants Jol, Seding Eero
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48Efect Love 46:1 InibtanofShaot Height, Fresh Wlght and Number of Emerged Seedlings he tabulated resus repress rounded ests clot an he exact ro dat
Tae: banof shot Hah omnton Sr on
a Fray
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