Document MG6yMnDMN1Bxv0358KmVJeNOa
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RESIDUAL VCM ANALYSIS TEXAS CITY VINYL RESINS PRODUCTION
Hay, 1976
Author:
R. M. Arnold L. D. Morgan
KudVtii JON 14 1976
R. N. WHEELER, JR.
Supervisor:
G. F. Tacquard
Date:
June 9, 1976
Attached In Table I Is a sumnary of the residual VCH levels In suspension vinyl resin products produced during the month of May. Essentially all of the QSAN-7 production shown in this data Is resin having the QSAL-7 molecular weight. Thus, a slight increase in residual VCM levels of QSAN-7/QSAL-7 pro duction was observed when compared with actual QSAN-7 produc tion during April. A slight decrease in residual VCM in QSAH-7 production during the month was also observed. Individual bin and blend data for suspension resin produced during the month are shown In Tables II-VIII.
Also shown in Tables IX and X are residual VCM levels in non solvent and solvent production during May. One VMCH bin and one VYHD bin were blended to achieve 1 ppm VCM.
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Attachments
RESINS LABORATORIES UNION CARBIDE CORPORATION CHEMICALS AND PLASTICS DIVISION
TEXAS CITY PLANT
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TABLE I
SUMMARY OF VCM ANALYSIS OF SUSPENSION VINYL RESINS May, 1976
Resin Type
QSAN-7 QSAL-7 QSAH-7 QSAP-7
VCM. ppm Blend
-- 13 16 10 42 29 14 20
Pet Blends <10 DDm VCM
64 59 16 62
<1 ppm VCM
12 9
46
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Blend No.
6800 6806 6809 6810 6811 6812 6813 6814 6815 6816 6817 6818 6819 6820 6821 6822 6823 6824 6825 6826 6827 6828 6829 6830 6831 6832 6833 6834 6835 6836 6837 6838 6839 6840 6841 4842 6843
TABLE II
ftESIOUAL VCM CONTENT OF QSAN-7 BLEND SAMPLES
May, 1976
VCM, ppm
Blend No.
VCM. ppm
6844
7 6845
17 6846
29 6847 13 6848
7 6849 4 6850
4 6851 24 6852
5 6853 10 6854 3 6855 13 6856 7 6857
17 6858
1 6859 32 6860 30 6861
3 6862
9 6863 13 6864 8 6665 14 6866 7 6867 103 6869 8 6870 22 6871
1 6872 17 6873 148 6874 10 6875 25 6876 3 6877 12 6880 11 6881 35 6882 24 6883 10 6884
11 8 20 4 9
3 10 15
3 5 1 2 <1 9 <1 4 31 34
2 <1
1 3 12 5 ' * 3<1
10 10 73
5 12 19 <1
2
13
13 4
7
Blend No.
6885 6886 6888 6889 6890 6892 6895 6896 6897 6898
VCM. ppm 1 3
22 <1
4 4 2 1 2 1
TABLE III RESIDUAL VCM CONTENT OF QSAH-7 BLEND SAMPLES
May, 1976
Blend No. 1820 1821 1822 1823 1824 1825 1826 1827 1828
VCM, ppm 10 22 67
270 111 93 22 72 24
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TABLE IV .
RESIDUAL VCM CONTENT OF QSAP-7 BLEND SAMPLES M*y, 1976
Blend No.
714 715 740 741 742 743 744 746 747 748 749 750 751 752 753 754 755 756 757 758 759 760 761 762 763 764 765 766 767 768 768 770 771 772 773 774
VCM. pan
15 <1
2 16
<1
10 <1
6 1 25 <1 <1 <1 31 <1 14 20 <1 2 <1 34 3 21 <1 190
1 2 <1 173 15 <1 <1
65 <1 65 <1
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TABLE V
RESIDUAL VCH CONTENT OF QSAL-7 BLEND SAMPLES
May, 1976
Blend No. 969 970 971 972 973 976 977 979 981 982 983
VCH. ppm 18 11 11 <1 48 <1 5 6 <1 3 2
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Bin No.
704 702 703 708 706 709 705 701 702 703 704 702 705 701 703 701 704 701 704 706 702 709 708 703 701 705 706 704 708 702 705 701 704 709 709
708 701 708 704
Date
5II -1 II II II
5II -2 II
I5I -3 II II II
454 -4 II II
5-5 I5I -6 II II II
I5I -7 II II
I5I -8 II
I5I -9 II II II
5-10 5-11
VCM, ppm
13 8 5 8 26 27 7 1 <1 37 139 <1
71 <1 <1 <1
6 7 7 7 24 229 10 24 22 43 71 6 8 26 8 12 8 13 26
12 13
4 13
TABLE VI
RESIDUAL VCM CONTENT OF QSAL-7 BIN SAMPLES
bin No.
705 706 702 703 707 702 701 705 703 701 704 708 702 706 707
703 605 706 702 601 703 607 705 606 603 708 702 704 703 701 609 601 403 412
414 402 406 604
Date
5II -11 II 11
N5-12 II
I5I -13
5II -14 II H II
5-15
II II II II II
5II -16 II II
51 -17 14 14 H 11 II II
5U -18 If
5M -19 II
May, 1976
VCM, ppm Bin No.
39 408 3 405 2 609
39 411 20 603 4 607 13 608 17 409 74 605 40 606 24 709 3 706 12 412 46 415 27 703
<1 406 8 702 3 414
21 409 7 705 4 708
33 702 1 402 6 709 5 703 4 702 4 411
<1 705 6 708 78 408
24 702 28 409
4 703 5 709 6 706 2 403 18 702 3 705
Date
I5I -19 N
51 -20 *1 II II II II
5H -21 II II II
5II -22 II II II U
5II -23 n H
5M -24 H It
I5I -25 II 1
5-26 N II
5II -27
VCM, ppm
11 4 1
33 12 <1 12 11 10
7 <1
2 22 15 12
Bin No.
412 406 414 409 411 415 405 403 406 606 412 603 409 411 609
5 601 3 606 12 608 4 607 2 414 <1 603 14 406 8
2 7
2 3
15 28
7
10 2
<1
4 <1
28 5 3
Date
5-27 5II -28 II I* II II
I5I -29 II
51 -30 II H II
II
5-31 II II II II II
VCM, ppm
15 31 15
5 46
2 2 <1 10 <1 40 2 18 4 3
<1 4 7 2 6 2
22
TABLE VII RESIDUAL VCM CONTENT OF QSAH- 7 BIN SAMPLES
May, 1976
Bln No.
409 403 412 405 408 411 412 414 405 402 408 406 403 415 412 414 402 406 408 405 415 409 406
Date
5-10
II
5-11 5-12
II
II
5-14
II
II
M
II
5-15
II
II
5-16
II
11
5-17
II
II
II
5-18
II
Milm.
257 12 2 6 52 12 15 31 33 28 32 27 10 <1 19 36
133 108
13 49 19 23 46
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TABLE VIII
RESIDUAL VCM CONTENT OF QSAP-7 BIN SAMPLES May, 1976
Bin No.
604 603 605 606 607 609 601 603 602 604 606 608 607 601 602 603 605 609 608 606 602 607 605 601 603 607 605 608 609 603 601 602 604 607
Date
5-1
II
II
5-2
II
II
II
5-3
II
ft
5-4
II
i
5-5
II
II
5-6
II
II
II
II
II
5-7
II
5-8
II
II
II
5-9
II
II
5-10
II
II
VCM
<1 12
2 1 2 2
9 23 <1 <1
1 <1 15
3 15 <1 22 <1 <1 17 <1 8 45 2 93 2 2 143 2 43 1 1
<1 1
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TABLE IX'
RESIDUAL VCM CONTENT OF NON-SOLVENT BLEND SAMPLES
May, 1976
VYNW
OYNJ
Blend No.
VCM, ppm
Blend No. VCM, DPn
3926 3927 3928 3929 3930
6 19 15 3 20 3 <1 21 <1
18 21 5
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TABLE X RESIDUAL VCM CONTENT OF SOLVENT VINYL RESIN BIN SAMPLE
May, 1976
VYHH
BIN NO.ppm, VCM
54 0.4 53 <.2 52 0.2 52 0.6 62 <0.2 63 0.2 54 0.2 51 <0.2 41 <0.2 61 <0.2 52 <0.2 62 <0.2 53 0.2 63 0.2
VMCH
BIN No.
82 71 73 82 84 72 81 73 74 84 72 83 71 82 72 81 74 84 71 73 74 83
ppm, VCM
<0.2 <0.2 <0.2
<0.2 <0.2 <0.2
<0.2
<0.2 <0.2 <0.2 <0.2 0.6 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2 <0.2
VYHD
BIN NO.
31 31 43 32 33 33 34
ppm, VCM
0.6 0.6 <.2 0.8 1.0 1.0 0.9
Resample
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DISTRIBUTION TEXAS CITY
Dr. C. E. Moyer/Dr. D. R. Montgomery Mr. M. E. Eisenhour Mr. R. L. Frantz Mr. J. L. Hockersmith/F. L. Johnson Mr. K. E. Ross Mr. F. S. Proven2ano
BOUND BROOK Dr. R. J. Anderson Mr. T. F. Archer Mr. E. Bell Mr. R, G. Davis
NEW YORK OFFICE Mr. A. E. Donaldson Mr. J. B. Hollingsworth Mr. S. A. Mortimer Mr. G. T. Scott Dr. T. T. Szabo
SOUTH CHARLESTON PLANT Mr. C. E. Fry Mr. R. N. Wheeler
TAFT Mr. A. S. Amatangelo
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