Document M6vgQ4nJ1vx5mm3ep7LLjryz
s.v.
C.V. 260
DATE PRINTED^. 4y^K'82
D.V. 303, 315, 317,(32?, .fett/
CC 4
CODE RT-531-D
JUN i 0 1982
( DATE >
FZKze
< L0T >
EST. WT. 643# LBS.
PKG
JUN15198Z
PROCESSES
< >RT-531-D <N> COHTYP JOB NAME: TYPED BY: JMH
APPROVED BY
EWK 11-24-81 40RT531DMN
STANDARD HRS.
TIME________ M
PREPARATION NOTES: SUPVR NOTE: DO NOT USE V-303 FOR NAPHTHANILS WHEN CAMPAIGNING DALAMARS YC-39-A, YC-40-A, YT-839-P, YT-840-P, YT-858-D, AND YT-868-D.
EQUIP MENT
NAME: NAPHTHANIL RED LIGHT
OBTAIN 4-NITR0-2-AMINOTOLUENE FOR S6 OBTAIN 3-HYDR0XY-2-NAPTHYLAMIDE FOR SI8 CLEAN, DRESS, CLOSE 24' CLARIF PRESS -
15 FRAMES
RUN 40 (486 G) WATER INTO
RUN in iH- YDROCHLORIC ACID FROM V-324
ML
! DUMP IN FROM SI
LOT
^^NITR0-2-AMIN0T0LUENE
USE LBS
N-CODE
504-C 150-C
ACCT LBS
.23CP.
28-D 504-C
126
J^MP^-STIR 15 MIN TO WET
LOT
TO J?___* <1020 G> AT 40-45 DEG F SIPHON IN SODIUM NITRATE IN
3X330
4-eH^STIR 5 MIN , REC0RDT-CRl$fl< + >, KlI^J_< + )
SC Hist:
*2
I NOTE: (1) IF CFC-, KI- ADD 20* *AS IS*
I INCREMENTS HYDROCHLORIC ACID ASSUME 32% I RECORD: CR< + > KI( + > | (2> IF CR+, KI- ADD 10* *AS IS* INCREMENTS
1 SODIUM NITRITE
ASSUME 33%
l^KTCORD : CR< + ) KI_< + )
1<n STIR 10 MIN AT 40-45*F MAINTAINING +CR, +KI
FOR SI3 RECORD: TIME START_j>_?^
^\2^\
12 I SLURRY DICALITE FILTER AID IN 40 GAL WATER
IN DRUM & PRECOAT CLARIF PRESS
DV 1113/fotHEN S11 STIR COMPLETE DUMP IN ACTIVATED
15
4 Of CARBON
|i< | DUMP IN DICALITE FILTER AID
10
\\S | STIR 30 MIN AT 40-45 DEG F
ASSUME 33%
! j MAINTAINING +KI-FOR- S23.
,
I RECORD: STARTJjClJ______ KI__ _TT,,_-< + >
330 5
RIJN 13" (177G) WATER INTO V-330
5Y TRISULPHOIL SOAP D IN 25G WATER 6
JUR IN
DUMP IN 3-HYDR0XY-2-NAPTHYLAMIDE FROM S2 6
I STIR 30 MIN OR LONGER TO WET. -LOT ^
I RECORD: START_________
! *+ >*.* -
-k-tel..
tV
16
95 28-D 725-A
777-A
113-B
777-A 725-A
57-A
15 10
39-A 150-C
DUP050047484
EQUIP I WENT !
I PACE 2 OF 3 CG 4 CODE RT-531-D <N>
USE IBS
302 )/(& >'Hmm* *-WG> WATER INTO V-302
I ^32,
6 ^21^0UR IN' SODIUM HYDROXIDE
ASSUME 50%
I
|2*>TsiPH0N IN ACETIC ACID & STIR 3 MIN _
I
.
f?^T
~ ps
M___ L______ ldliLl 30-D f
422 | RECORD PH_/l C_ < 6.7-7.5) IF NECESSARY ADJ TO I
I I 4*7-7.5. ~~
ACETIC ACID ASSUME 70%I
I I RECORD PH__/_r SODIUM HYDROXIDE ASSUME 5%|
i
N-CODE
7 HD
30-D 7-D
I ACCT j LBS I --,
L //C>
( am:
/Z*~
.
12tfj`TUBN ON
AGITATOR t, ADD ICE. THEN 12X330
I J^tfHUT OFF AGITATOR
I-23A | PUMP DV THRU CLARIF PRESS INTO DV USED IN
I S 23. MAINTAINING TEMP AT 40-45*F.' RECORD:
START
TOTAL
I | |
}
I
| |
|
E: DO NOT USE V-303 - TOO SMALL
II
WHEN S23A CLARIF COMPLETE WASH DV <S4>
I LINES PUMP G PRESS FOR 2 MIN OR TO A -CR.
TEST ON A SAMPLE OF TOTAL PRESS EFFLUENT
I I I
i
|
\
I I WHICHEVER COMES FIRST. COLLECT WASHINGS IN |
L^TDV (S23) RECORD: START_7^__CRJL&i9&<-0R+> !
(25 ! WHEN S24 IS COMPLETE TEST DV/S23) ASSUME 33% I1
| I
RECORD: KIJ&&l< + > TEMPJZJ?.__<40-45* F) I________ I
WEIGH SULFAMIC ACID IN RUBBER BUCKET AND
I
I
NSE IN AND STIR 5 MIN.
|
QRD: KI_V_3.t.4 MUST BE - G IF NECESSARY I
1 | -- |
TO -KI WITH SULFAMIC ACID --*--
II
ADJ TO
(1925 G) AT 40-43 DEG F
11X33 I
57-A
725-A 57-A
395-D
395-D 57-A
I_____ I_____ 1
I 10-
1 <r~-
3?` (390 G) WATER INTO V-S*0/<&L
1
S /V^\Z4\ INSTALL TEMP CHART & SET AGITATOR AT 16 RPM!
33 9
13<T"wyEN SI8 STIR COMPLETE, POUR IN SODIUM
|
I J-'ffYDROXIDE IN 3-4 MIN.
ASSUME 50% i
132 I HEAT TO 128-132 DEG F AFAP G STIR 5 MIN TO I
DISSOLVE. STOP AGITATOR.
1
220
i 7-D I 110
IMMEDIATELY RUN V-330 AFAP INTO ,,CV*~.NO
AGITATION IN CV RECORD: STARTj
I .**-
TOTAL MIN __iJ2___
u*r POUR IN ACETIC ACID G STIR 5 MIN. '
RECORD: PHj?&#!.< 1075-1 TToT
ASSUME,'50%
I I If.F* NECESSARY ADJ TO PH 10.5-11.0
I ^rRECORD: PH_________
ASSUME 70%
|^6>^UN IN V-302 AFAP
I3STLJWIMP IN BARIUM SULFATE
HEATgJOf78-32 DEG F AND RE USD:
U.j SK1-DEG F AND REC,,_j KTL..DEG F
S28 COMPLETE, COUPLE DV UNDERSURFACE
65-70 MIN. MAINTAIN CV AT 78-82 DEG F
'RECORD: STARTSASrE^TOTAL MIN
____
STIR 5 MIN, DISCONNECT TRANSFER LINE AT CV
& RECORD: DIAZO__j-___ <+/-.)
BASE^*>_(MUST BE +> PH,,,,#*4.(4.2-4.6>
141 IF NECESSARY STIR TO - DIAZO RECORD:
STARTTOTAL MIN.
RECORD: DIAZO_________ MUST BE
BASE _________ MUST BE +
PH _______ _ <4.2-4.6)
I
35 I
jI
30-D 7-D
30-D
65-A
| 150 |______
I
|__v_,,
I | 35
DU P050047485
COMTY.P JOB NAME : 40RT531DMN
PAGE 03
DATE PRINTED:MM/DD/YY
USE I N-CODE OF 3 CG 40 CODE RT-531-D <N) | LBS
j ADD 30G WATER AT 130-140* TO jQRUM FROM HOT j 'ATER MIXER ADD BLAMCOL N 6STIR FOR S43 |
30 | 567-B
ACCT LBS
30
f)UR IN N-567--B SOLUTION FROM S42
I
T TO 194-196 DEG.F IN 55-60 MIN AND 7 |
ECORD: HT___y,,C^..DEG F AND REC_./_DEG F I
WHEN S44 HEATING COMPLETE, RUN IN ALUMINUM
LFATE SOLUTION THRU BADGER METER. NOTE: | 120 | 115-D
SE IN LINE AFTER N-115-D SOL'N.RUN IN.
STIR 30 MIN AT 194-196 DEG F
1 FLOOD TO 80* <792BG> AND STOP AGITATOR
I VAT I V-303|V-315|V-317|V--322|V-323 j S4 (486G) | 20'| 14* | 14* | 14* I 14' I S8 (10200)1 43*1 30' I 30" I 30* I 30*
I
FIN OPTR
I
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__ Z&3S. --.Jit.__ >.
60
I ___
DUP050047486
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