Document M4x2Lp2NjvO9dLXjzyx2j1aNx
CG 1 < DATE )
CODE YE-698-31 I /V
( LOT )
552?* l b s . < EST WT )
PROCESSES < ) YE-698-D <T>
APPROVE! FWP 10/15/82
'ft COMTYP JOB NAME: 1YE698DMT
BLENDED BACK: 0&--TT~Fr?K98,
S55S|T1
EQUIP |
MENT i I
NAME; MOLYBDATE ORANGE
------------ j -------- ---------------------------- ------------
USE 1
iI ACCT
LBS | N-CODE | LBS
----------- 1
1
PREP 1
l^V'OBTAIN SODIUM SULFATE FOR S-13
i jr \ CALCULATE 6 SET ON BADGER METER FOR. S-16
(NITRIC ACID WEAK)
Ito'ft %
84 I 108-A |
_1?J 11 33-D |
84 60
OBTAIN SODIUM CHLORIDE FOR S-33 OBTAIN. SODA ASH FOR S-37
734 | 146 1
4-A 1I 734 3-A |i 146
OBTAIN SODIUM SILICATE FOR S-39 OBTAIN SODA ASH FOR S-43
237 | 32-D |1 237 35 | 3-A J1 350
OBTAIN ANTIMONY TRIOXIDE FOR S-46
70 1 711-B 1 7
351 WEIGH SODIUM CHROMATE INTO V-351 ., _ ,, ^
10-D 1 1885
o
o p t r mk ^1l ,32.27_%i
OPTR_____, MK____,_______7. |
-------------- ---------------------------------------------- --------------- 1
1i
1ii1 1--------
359 WEIGH IN SODIUM MOLYBDATE SOLUTION
| 423-D 1 303
3 OPTR_____, MK IpL, T-li_<?, hJLZiZ]
OPTR
MK T-
____% i
35S IN 10" (500 G) WATER INTO V-358 |
4
IN V-359 INTO V-351 6 PUMP IN V-351
I
I. LS TO 55* <260.0 G)
I
H^V^IFT IN N-108-A FROM J
,
I
I VrUSFPIR 5 MIN 6 RECORD: PH^.4l(9.'-1 0.0)
|
|1#*T ADJ TO PH 9.8-9>9 & RECORD: PHjpJ?_.
I
(CAUSTIC SODA SOLUTION)
ASSUME 5%I______
ASSUME 66%|_jfei:
ADD N-33-D FROM S 2 USING BADGER METER
|
AD*i TO 66" <3121 G) AT 67-69*F
I
''RECORD: VOL&,," 6 __feX.*F
|
STIR 5 MIN 6 RECORD: PH_____ <7.4-7.6) 6
|
G/ML
.080-1 .083 )
I
NOTE IF G/ML. OUT OF LIMITS FILL OUT CHECK
LIST 6 ATTACH. TAKE 1 QT SAMPLE
7-D 33-D
SV i-rT"RUN 20" <996 G) WATER INTO V-JJklL?
I
5 RECORD N-41-D STORAGE TANK TO PUMP FROM.
CIRCLE ONE: 402 41 411 42 424 425
CHECK WITH CU SUPV:
^STORAGE TANK MUST CONTAIN AT LEAST 2376
GAL: 402-49", 41=25', 411=48", 420=25",
424-25", 425s:31 ' k STORAGe 't ANK MUST HAVE STIRRED AT LEAST
I
|
\yr\
2 MIN SINCE LAST ADDITION OR ADJUSTMENT ^STORAGE TANK MUST BE ISOLATED UNTIL ALL
PUMPING FOR THIS BATCH IS COMPLJTE, SET METER FOR 300 G 6 PUMP TO SV
0(jT 29198?
N40871
LOT: "EQUIP MENT'I _____t __ SV 122
5| CONT i
I I 123
124
11 11 I[ 1I 11 11 11 11 !1 fi (1 11 11 I1 11 1i 11 I1 11 Ii 1I I1 11
CGMTYP JOB NAME: 01YE69SDMT
PAGE 02 '
DATE PRINTED: 1 0M 5/82 I USE | N- iACCT
LBS | CODE | LBS
AT APPROX 100 G WHILE CONTINUING TO PUMP,
CHECK PH 6 DENSITY. RECORD BELOW. IF NOT IN RANGE, STOP PUMPING 6 SEE SUPV. * PH :_______<2.2-3.7)
* DENSITY:__.______G/ML (1 .270-1 .328) IF S-22 OK 6 WHEN S-21 COMPLETE, RECORD
DENSITY _______ G/ML ON TRAPPED SAMPLE FROM END OF S-21 PUMPING.
USING DENSITY FROM S-23, FIND METER SETTING FOR
SECOND PUMPING IN TABLE BELOW. NOTE: TABLE ACCOUNTS FOR 300 G ALREADY PUMPED IN S-21 . CIRCLE DENSITY & SETTING IN TABLE BELOW.
t a b l e *
G/ML 1 .270 1 .271 1 .272
1 .273 1 .274 1 .275
1 .276 1.277 1 .278 1 .279 1 .280 1 .281
1 .282 1.233 1 .284 1 .235 1 .286 1 .286 1 ,287 1 .288 1 .289
1 .290
SETTING | G/ML SETTING 1 G/ML
1673 | 1 .291 1534 1 1.312
1670 | 1.292 1527 1 1.313
1663 | 1 .293 1521
1 1.314
1656 | 1 .294 1515 1 1.315
1649 | 1 .295 1509 I 1.316
1641 | 1 .296 1503 1 1.317
1634 | 1 .297 1497 1 1.318
1627 | 1 ,298 1490 1 1.319
1620 f 1.299 . 1484 1 1.320
1614 | 1 .300 1478 1 1.321
1607 | 1.301 1473 1 1.322
1600 | 1 .302 1467 1 1 .323
1593 | 1 .303 1461
[ 1.324
1536 | 1 .304 1455 1 1.325
1580 | 1.305 1449 1 1.326
1573 | 1 .306 1444 1 1.327
1566 | 1 .307 1 438 ! 1.328
1566 | 1.307 1438 1 1.328
155? | 1.308 1432 [ 1.329
1553 | 1 .309 1427 1 1.330
1546 | 1 .31 O 1421
1 1.331
1540 | 1 .311 1415 1 1.332
SETTING! 1410 | 1404 | 1379 |
1374 I 1388 | 1383 1 1378 | 1372 | 1367 1
1362 [ 1357 | 1351 I 1346 | 1341 | 1336 | 1331 | 1326 | 1326 [ 1543 | 1537 | 1532 |
1526 |
I 1 i I
fI iI I I
i
l1
1[
11 ii 1 '! 11 1| 1I
11 1( 1i
if 1[
1! 1 -! iI ii 1j 1f ii
II I |1{
i1
[25
I I 126
I [27 128
I I 12? I
1301
SET METER 6 PUMP _______ ,G (RECORD FROM TABLE)
FLUSH LINE WITH WATER INTO SV FOR APPROXIMATELY 30 SECONDS
ADJ LEAD NITRATE TO 76' (3625 G) AT 67-69*F.
RECORD: ______ ___ F
STIR 5 MIN 6 RECORD PH: __ (2.2-3.7)
IF NECESSARY ADJ TO PH 3.0-3.1
ASSUME 66%
& RECORD PH: ______
ASSUME 50%
NOTE: DILUTE N-?-D 10:1 WITH WATER BEFORE ADDING
RECORD: _______ G/ML (1.143-1.144) IF OUT OF SPEC FILL OUT CHECK LIST 6 ATTACH.
STIR AT 67-69*F FOR S~3l . TAKE 1 G)T SAMPLE.
I1 I 41-0 | 5110
I 57-A [___
II I 33-D I____ I 7-D |______
II II II II
\ DUP050059635
-> ....
i ......... '
lllSIlilHI
llllllllllpllllil;
COHTYP JOB NAME: 01YE698DMT PAGE 02
LBS
AT APPROX. ;100.. G WHILE CONTINUING TO PUMp 7~*
CHECK PH i, DENSITY. RECORD BELOW. IF NOT
IN RANGE* STOP PUMPING , SEE SUPV.
* PH?Jfc3|fe ,<2.2-3.7)
DENSITY- bjkl^L G/ML< f. 270-1 .328)
, .|
\ J^JS-rTTS-22 qK^WHEN S-21 COMPLETE, RECORD
|
.. J 1 DENSITY/-2Zt L G/ML ON TRAPPED SAMPLE ' I L^-FROM END OF "S-21 PUMPING.
| |
USING DENSITY FROM S-23, FIND METER SETTING FOR |
T - I SECOND PUMPING IN TABLE BELOW. NOTE'. TABLE
j
| I ACCOUNTS FOR 300 G ALREADY PUMPED IN S-21 .
|
1 I CIRCLE DENSITY & SETTING IN TABLE BELOW.
|
II
#.**# TABLE #***
i
1 I G/ML
i i 1 .270 1 I 1.271 ? i 1 .272
i I 1 .273 L ) 1.274
1 1 1.275 J 1 1 .276 1 1 1 .277
I I 1.278 11 I i 1 .280 1 J 1 .281 1 i 1 .282 1 i 1 .283 1 J 1 .284 ! I 1 .285
1 1 1 .286
1 ! 1 .287 I I 1.288 i I 1 .289
t I >K290
SETTING !1 G/ML
1644 |1 1.291
1637 i1 1.292
1630 iI 1.293
1623 1i 1.294
1616 1I 1.295
1609 1 1.296
1602 |1 1.297
1595 1 1.298
1588 1 5R7
11 1.299 | 1.300
1575 11 1.301
1568 1 1.302
1562 11 1.303
1555 11 1.304
1549 |] 1.305
1542 || 1.306
1535 1i 1.307
1528 |1 1.308
1522 Ii 1.309
1515 11 1.310
1510 1! 1 .31 1
SETTING 1 1504 1 1487 1 1491 I
1485 1 1479 1
1473 1 1467 1 1461 1
1455 i 1443 1 1 444 1 1438 .1 1432 1 1426 1
1420 1
1416 1
1410 1
1404 1 1399 i 1393 i 1387 1
G/ML 1.312 1 .313 1 .314 1 .315 1.316
1.317 1 .318
1 .319 1.320 1 .321 1.322 1 .323 1.324 1..325
1.326 1-.327
1 .328 1.329 1.330 1.331 1.332
SETTING 1382 1376 1371
1367 1361
1 356 1351 1 345
1340
1335
1330 1324 1319 1 315. 1310
1 305 1300
1295 1290 1285 1280
.SET METER & PUMP
<RECORD FROM TABLE)
FLUSH LINE WITH WATER INTO SV FOR APPROXIMATELY
'`^-''SECONDS
i
ADJ LEAD NITRATE TO 3625 G <76"-242/245 &. 74.5"
i i 247) AT 67--69F
j
RECORD:
___ #F & ICE CONSUMED (3300/BLOCK) ! 330X.
STIR 5 MIN 6 RECORD PH: O-iQ <2.2-3.7)
j
USE TI TRIMETER TO ADJUST N-41-D PH #*#
IF NECESSARY ADJ TOPH 3.0-3.1
h RECORD PH:
ASSUME 66% j ASSUME 50%
3T.E: DILUTE N-7-D 10:1 WITH WATER BEFORE ADDING]
RECORD : ^$4 G/ML <1.143-1.144) IF OUT OF SPEC)
ILL OUT CHECK LIST 6 ATTACH.
STIR AT 67-69F FOR S-31. TAKE 1 QT SAMPLE.
CODE I LBS
41 D 57' A
5110
337-
DUP050059636
1,0 T : EQUIP MENT
COMTYP JOB NAME; 01YE69SDMT PAGE 03
DATE PRINTED;10415/82 USE I N- IACCT LBS | CODE I LBS
OBTAIN 1 QT SAMPLES OF S-18 6 S-30 SOLUTIONS
& TITRATE TWICE NOTIFY SUPV IF ML N-10-D IS NOT IN RANGE
7*1-7-4 OR IF THE TWO TITRATIONS DIFFER BY
MORE THAN 0.10 ML N-10-D (IF YES, FLUSH ALL EQUIPMENT & REPEAT TITRATIONS). DO NOT
PROCEED IF N-10-D TITRATION IS OUT OF RANGE
ADJUST V-358 FOR A TITRATION PH OF 2d U'TCT2.2U|
FROM FINAL IN-LINE TITRATION, RECORD L.OWEST J
PH ___ &__ML_N_-_iO_-_D_. ________A____
WHEN S-31 ~TITRATION~OK~ STRIKE~V-358-THRU
BOTH UNDERSURFACE DISTRIBUTORS INTO SV IN
16-18 MIN RECORD: START
, TOTAL MIN,__Ij O-__--
NOTE: STRIKE TIME UP WHEN 1/2 VAT BOTTOM SHOWS
UBBLES APPEAR IN SIGHT GLASSES
IMMEDIATELY DUMP IN N-4-A FROM S 3 6 SET TIMER
< 15 MINUTES
TING S 33, WASH IN V-35S *
STIR 2 MIN & RECORD PH_Azs_( 1 .8-2.5)
BXS,
__( MUST BE + )
STIR TOm OF 15 MIN FROM S-33 6
RECORD: TEMP_fe&__*F (67-73*F)
P N-3-A FROM S-4
R 3 MIN R IN N-32-D FROM S-5
IR 2 MIN IN LIQUID ALUM USING BADGER METER
TIR 3 MIN & FLUSH ALUM LINE WITH WATER
^Jx DOMP IN N-3 FROM S-6
$t>r\ STIR 4 MIN FOR S-48
jf
734
i
33-D 7-D
u
115-D1 367 I
7390 7
SV
RUN IN HYDROCHLORIC ACID USING WEIGHT & FLOW
| CONTROL PANEL
MK___
/ MK_______ ___________%
6"TDURING S-44 SIFT N-711-B FROM S-7 INTO V-390
ITH AGITATOR ON IN 1-2 MIN
STIR 1-2 MIN TO MILKY SOLUTION
WHEN S-44 COMPLETE, IMMEDIATELY RUN IN N-711-B
SOLUTION GRADUALLY OVER 5.MIN PERIOD INTO SV
| WATCH FOAM!!! IF FOAMING IS EXCESSIVE, STOP
L^T3NTIL FOAM SUBSIDES.
>?^HDCfMP IN BLANC FIXE N
&T\ WHEN SCHEDULED, DUMP IN BLEND BACK LISTED ON
TOP OF PAGE 1 -
RECORD: CODE _______ LOT__________
R 20 MIN
ECORD : PH_\2iX__ (5.8-6 - 0)
ST I IF NECESSARY, ADJ TO PH 5.8-6.0
JlT 6 RECORD: PH-_______ _____
ASSUME 50% ASSUME 66%
ypT I FLOOD TO 153" (7298 G) 6 STOP AGITATOR
3J3-- I 28-D | 105
,,___J 28-D i __,,
, j --------
330,/1
i 128-AI
I I
330
7-D I. 33-DI,
J
S/ffiML S&ai-
DUP050059637