Document M4mV2OKzGVMrM2x8RyXJg3z7
C.V. 260
CODE RT-531-D
>/) MMl 1982 J({ d a t e * y
F2J32
( LOT >
9P ,V0EST. WT- 643 LBS*
PKG __
D * V. 303/ 315/ 317 , (32|, .(323
PROCESSES
APPROVED??* ^
< )RT-531~D <N> EWK 11-24-81 COMTYP JOB NAME: 40RT531DHN TYPED BY: JMH
STANDARD HRS. ___________ TIME 'T
PREPARATION NOTES: SUPVVR NOTE: DO NOT USE V-303 FOR NAPHTHANILS WHEN CAMPAIGNING DALAMARS YC-39-A, YC-40-A, YT-839-P, YT-840-P/ YT-858-D, AND
YT--968-D.
SEMI-BLEEDING
NAME: NAPHTHANIL RED LIGHT
OBTAIN 4-NITR0-2-AMIN0T0LUENE FOR S6 OBTAIN 3-HYDR0XY-2-NAPTHYLAMIDE FOR SIB CLEAN, DRESS, CLOSE 34* CLARIF PRESS 15 FRAMES
I USE LBS
| N-CODE | ACCT 1 LBS
--------- ------ 1----------
504-C I 150-C |
RUN |l X_" <486 G> WATER INTO V-__t
RUN IN HYDROCHLORIC ACID FROM V-324
M_______ l_______
DUMP IN FROM SI
LOT *
4-NITR0-2-AMIN0T0LUENE
i
28-D I 126 504-C
gj'HTffALE 3 ^:.IT:rrOJ~^i'iiil4.iilXJ.AIlf7'Um I
1 ADd- TO _>V* (1020 G) AT 40-45 DEG F
1X33
57-A |JLfQ
'SIPHON IN SODIUM NITRITE IN 7-10 MIN
I
M______7--|
725-A i 95
St ir s min & r e c o r d : c r __:_<+>, Ki_.ir__(+> i
NOTE : < 1 > IF CR-, KI- ADD 20* *AS IS*
1
INCREMENTS HYDROCHLORIC ACID ASSUME 32% |
28-D
RECORD: CR<+> KI< + >
I
I (2) IF CR+, KI- ADD 10* "AS IS* INCREMENTS I
SODIUM NITRITE
ASSUME 33% I
725-A |____
RECORD: CR ,,.__< + > KIL______< + >
I
I STIR 10 MIN AT 40-45*F MAINTAIN | FOR SI 3 RECORD : TIME START,
CR, +KI | JUNili 1882
SLURRY DICALITE FILTER AID IN 40 GAL WATER I
I IN DRUM & PRECOAT CLARIF PRESS
!
5 1 777-A tt
5
WHEN S11 STIR COMPLETE DUMP IN ACTIVATED I
BON I
IMP IN DICALITE^FILTER AID
1 STIR 30 MIN AT fofB DEG F
ASSUME 33% i
MAINTAINING +KI/fe4R/<l23.
/
RECORD: START.JLLJt L___ + )
RUN 13* < 177G) WATER INTO V-^T
SLURRY TRISULPHOIL SOAP D IN 25G WATER &
OUR IN
DUMP IN 3-HYDR0XY-2-NARTHYLAMIDE FROM S2 L
STIR 30 MIN OR LpNGER^O WET.
LOT
RECORD: START.
rl4fJr
sIFfS
! I I
15 |
10 1 1____________ 1____________
1
l'
. i1 16 |
>JTi
113-B ' 15
777-A 725-A
57-A
10
--m.m,
....WWW
3 9-A
16
150-C 370
N38126
Ui wi i ) ir JU1? rmi'IC.
I 2 <3 1 vnr<
rnun.'
u h 11 f k i n mu: nn/ vu/ r i
EQUIP KENT
302 11
' OF 3 CG 40 CODE RT-531-D <N>
I USE i N-CODE i ACCT
I LBS I
I LBS
WATER INTO V-3:0r *
I.. I
IN SODIUM HYDROXIDE
ASSUME 50%
f^g.I 7-D
'PHON IN ACETIC ACID 0 STIR 3 MIN ,
I- ^ I
> <T
nM_,,_,,____xL________,1
1*^^
RECORD PH_lvV>6.7-7.5) IF NECESSARY ADJ TO|
I 6*7-7.5, y
ACETIC ACID ASSUME 70%i__
I RECORD PH__VL SODIUM HYDROXIDE ASSUME 50%I
I ,y> i //&
!
I TURN ON V-jgA*? AGITATOR , ADD ICE, THEN
'HUT OFF AGITATOR
PUMP DV THRU CLARIF PRESS INTO DV USED IN
i S 23. MAINTAINING TEMP AT 40-45*/ RECORD
S START :_?0<L_
TOTAL MIN^jGJt--
I NJ: DOIn OT USE V-303 - TOO SMALL
WEN S23A' CLARIF COMPLETE WASH DV <S4>
LINES^PUMP & PRESS FOR 20 MIN OR TO A -CR
ON A SAMPLE OF TOTAL PRESS EFFLUENT
IlCHEVER COMES FIRST. EflLBCT WASHINGS IN |
:S23) RECORD.: START/Jo ^-s ^CR.J2TT-<-OR+> I
S24 IS COMPLETE TEST DV(S23) ASSUME 33%1_
725-A l_
l CORD:
TEMP,,3SI__(40-45# F) |_
S7-A !
-SULFAMIC ACID IN RUBBER BUCKET AND I
IN AND STIR 5 MIN.
I 10 ( 395-D I 10
CORD: KI__-T__. MUST BE ~ 4, IF NECESSARY | rADJ TO -KL.WITH SULFAMIC ACID
I LI 395-D | _J<t_'
ADJ. TO
<1925 G) AT 40-45 DEG F
i x&sxrT' 57-A
8 130.
39* <3900 G) WATER INTO V-3
I
STALL TEMP CHART & SET AGITATOR AT 16 RPMI
EN Sf8 STIR COMPLETE, POUR IN SODIUM
I
I
HYDROXIDE IN 3-4 MIN.
ASSUME 50% I 220 1
HO 128-132 DEG F AFAP 6 STIR '5 MIN TO I
VE. STOP AGITATOR.
I
I I
7-D I 110
13
ATELY RUN V^ds^AFAP iNTp^cy/fNO' I I
ION IN CV. RECORD: STAm^&J\,VV
TOTAL MIN _S_______ N ACETIC ACID 0^STlR 5 HiN^^ ^
| I
I. I
h _\\JDl < i o3:i TT0T ' as s Dme~50% V.
ARY ADJ m PH 10.5-11.0
I
ASSUME 70% |.
-302 AFAP *
I
BARIUM SULFATE
!
78-82 DEG F -AND RECORD:
I
.._DEG F AND RFC___ jS>_,,_DEG F
|
COMPLETE, COUPLE DV UNDERSURFACE 1 i 65-70 MIN. .MAINTAIN CV AT 78-80 DEG F I
JT RECORD: START.fe|IfcM& TOTAL MIN
I
<T\ SnR 5 KIN, DISCONNECT TRANSFER LINE AT CV |
BASE PH
idJBETARfSEeCE:O_rRfMc<DlU_:4S<.TMD2UI-AB4SZET.6O)+_BJE$$+)cfcP. H<_i*f/c-J>o_<4 .2-4.61
l I
| I.
IF NECESSARY STIR TO s t a r t ^Mj a B*. t o t a l
- DIAZO min __
RE_C_O__RD:DUP050' 04|7i 477
I RECORD: DIAZO ___r~ __ MUST BE -
COHTYF
*
e q u ip '' WENT
MI SC ii
i@5 12
NAME - 40RT53iDMN
PAGE 03
DATE PRINTED:MM/DD/YY
USE PAGE 3 OF 3 CG 40 CODE RT-531-D <N) I IBS
N-CODE ACCT LBS
30G WATER AT 130-140* TO DRUM FROM HOT I MIXER ADD BLANCOL N ASTIR FOR S43 |
30
567-B
30
IN N-567-B SOLUTION FROM S42 TO 194-186 DEG F IN 55-60 MIN AND
e c o r d *. h t JISLv .--DEG F AND r e c .19X,,..d e g F 44 HEATING COMPLETE, RUN IN ALUMINUM
TE SOLUTION THRU BADGER METER* NOTE;
SE IN LINE AFTER N-11S-D SOL'NRUN IN. St ir 30 min a t 194-196 d e g f FLOOD TO 80* <79280 AND STOP AGITATOR
120 I 115-D
60
VAT I'V-303IV-315IV-317IV-322IV-323 S4 <486G> | 20*1 14* J 14* j 14* i 14* SB <10200 1 s 43'NO* 1^0" I 30" I 301
FIN OPT,
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f
DUP050047478
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