Document M4Ow0vY4DdwKmemkywjGgyBLk

ANALYZER CARRIER GAS BANK SYSTEM The carrier gas bank system will automatically switch the carrier gas banks to the analyzers. MON-ARC SPECIALTY GASES is responsible for changing out empty banks and resetting regulators. This system is set up so that the banks will automatically switch at 120* PS1. This is done with check valves and regulator pressure settings. EXAMPLE: When BANK A" is on line the bank pressure is approximately 2500* PSI. The output pressure of regulator "A" is 140* PS1. This regulator feeds regulator X". Regulator "C has an ouput of approximately 100* PSI. Check valve B" keeps regulator A from back-pressuring regulator B . When BANK "A drops below 120* PSI BANK "B will come on line because of the check valve arrangement. After BANK "A'is replaced, but before* it is put on line. BANK "B is set at 140* PSI and regulator A" is set at 120* PSI. This will keep BANK "B" on line and BANK 'A" ready when BANK B is empty. ALARMS: There are four different bank systems for the analyzers, (hydrogen, nitrogen, helium, zero air >. Each system has an alarm for low pressure. EXAMPLE If BANK A drops below 120* PSI. the pressure switch on A will actuate; also. BANK "B will come on line. In this situation there will be no alarm. With BANK A empty and BANK `B drops to less than 500* PSI. pressure switch B will actuate causing an alarm. This is a warning that both banks are near empty. ACTION NEEDS TO BE TAKEN. CORRECTIVE ACTION: CONDITION *1: A) Verify both banks are low by looking at inlet pressure gauge on both regulators A and B . DO 0146.4R OONFTDFNTTAI c B) Check to insure both banks are in service; valves open. O Call MON-ARC SPECIALTY GASES and tell them you need a bank of carrier gas. Di If unable to reach MON-ARC. there is a spare bank of each gas kept at the main instrument shop. A cherry-picker is required for transportation of the bank ' CONDITION 2: A) If alarm sounds and both banks have sufficient pressure check the outlet pressure of regulators A and B (should be 120 - MO* PSD. B) Check valves 1 and 2 to insure they are open. C) If valves 1 and 2 are open check output pressure of regulator C\ This should be approximately 100 PSI DI If you cannot restore pressure block valve *3 and openvalve *5 ai valve *6. Also, open valve on single cylinder. This puts the single cylinder on line which will give you approximately 24 hours of rui time. E) Notify analyzer person of situation as soon as possible. 47? 0 PSL 1 1& y7>'* PSL 2 !___ __________ ___ I * PSL 3 NOTE: ML SWITCHES WILL OPEN ON DECEASING PRESSURE. t: A PSL 4 ii - AC TO ANNUCIAT AN OPEN CIRCUIT 1 SOUND THE ALARM 14649 r-ONFTOFNT TAt r C r> N. ( .TO *- > - '( AukLyzeK . jao Bauk A /%* &a*IK O S/M4^E CVL/NOfK DO 014650 CONFTDFNTTAl, DO 014651 OONFTDFNTTA CARRIER CAS BANK SYSTEM 100* .......o wJo RIG. *C* V3 TO ANALV7IHS VS VI V? CHECK VAIVE 'A- z CHECK VAIVE*# 100* REG. 'A 120* MO* 81EEO VALVE O oiil.' REG. *8 170* 140* BLEED VAIVE BANK "A BANK "B V_____ / SIN6L E CYLINDER TYFiS F PE3AWI1(N] PIPING AND INSTRUMENT DIAGRAM (P&ID) INDEX FLOW SHEET. INDEX & INSTRUCTION. (LEGEND & REFERENCE SHEET), PLOT PLAN. ETC. CIVIL, CONCRETE (FOUNDATION), ETC. STRUCTURAL & ARCHITECTURAL PIPING MECHANICAL INSTRUMENTS ELECTRICAL NON-PROCESS EQUIPMENT (A.C.), ` . MOD V GRAPHICS & ALARM PANELS ' COMMUNICATION * HEAT & MATERIAL BALANCE (HMB) ALTERNATE SOURCE TEMPORARY DRAWING id: IF & 8 1/2* x ir 22" X 34' P 11* X 17* TVF1S F F& RHPID3 10/89 H ORIGINAL ORAWING (RECORD DOCUMENT / AS EXISTS / AS BUILT) 2 PROJECT DRAWING (PROPOSED ADDITIONS, TIEPOINT, PROPOSED MODIFICATIONS, DEMOLITIONS, ETC.) 3 DEMO DRAWINGS A) XB1-100-N50-001 (MANUAL)' ;> V ^ :~ * kB) B1-X100-N50-001 (ELECTRONIC^FOR: ARCHIVE). CVOQN/RHPID3JX3N Sap. 13,190116*3:02 - :;V'" ' - ;' y-`' no 014466?5? "7',. rONFTDDFNNTl T Al DRAWING NUMBERS 1) DRAWING NUMBERS ARE ISSUED BY ENGINEERING RECORDS A) CONSUELLA ELLIS EXT. 6806 2) CHECK WITH PLANT FOR NUMBERING SYSTEM A) SOME PLANTS SECTION OFF BY AREAS B) SOME PLANTS NUMBER BY TRAINS C)SOME PLANTS USE NEXT NUMBER AVAILABLE NOTE: TRY TO AVOID USING A,B*C, ETC. 3) DO NOT REUSE VOIDED OR SUPERSEDED DRAWING NUMBERS A)VOID DRAWINGS BY PERSON AND DATE B)SUPERSEDE BY NEW DRAWING NUMBER OR NUMBERS 4) PROJECT OR 'P* DRAWINGS A) AN ORIGINAL P&ID SHOULD BE ISSUED BEFORE *P* DRAWINGS ARE CREATED B) ONE (1) 'P" DRAWING IS MADE FOR ALL ON-GOING PROJECTS C) RECONCILE ALL COMPLETED PROJECTS ON ORIGINAL DRAWING 5) DEMO OR *X* DRAWINGS A)USED FOR ONE PROJECT B)SHOULD BE MANUAL CJMAKE ELECTRONIC DEMO DRAWINGS UNDER SPECIAL CONDITIONS NOTE: SEE B.J. JOHNSON EXT. 6S76 FOR STORING DEMO DRAWINGS C^DGN/DWGNUM.DQN Oct 28,180118:17:00 RJH 10/28/81 00 014650 CONFTDFNTTAl f ENGINEERING RECORDS DRAWING NUMBER CONVENTION 10-1 -<51 STANDARO DRAWING NUMBER B 1 1000-N50-001 THIS LETTER OICTATES T*C SIZE OF TIC ORAVING. EXAMPLES* A - 81/** X II* B 22* X 34* B 24* X 36* C - 18* X 24* C * 28* X 24* 0 - 11* X 17* THIS LETTER AM) NLUCER COeiNATION OICTATES THE PLANT COOE. THIS NUMBER OICTATES TIC . -- DISCIPLINE OF TIC ORAVING. EXAMPLES* 81 - UCEXES. FLOW SHEETS 1 -PS 10'S 2 - CIVIL 3 - STRUCTURAL 4 - PIPING 5 - VESSEL 6 - INSTRUMENTATION 7 - ELECTRICAL 8 - MOO V GRAPHICS *) COMMUNICATION 18 - ICAT 6 MATERIAL BALANCE THIS IS TIC ACTUAL ORAWIM) NUMER. SHEET 1 OF 2 * - .. . .. ' ' i DO 014654 OONFTDFNTTAt ENGINEERING RECORDS DRAWING NUMBER CONVENTION 10-1-SI ADDITIONAL LETTERS ACCEPTED TO THE STANOARO FB4-1000-N50-001 THIS LETTER IS USED TO IMDICATE FIRE PROTECTION DRAWINGS. J XB1-1000-N50-001 THIS LETTER IS USED J TO INDICATE A DEMOLITION DRAWING. B1 1000-N50-001P THIS LETTER IS USEO TO IMDI CATE TRACING OF A PIPE SPOOL. TB4 J THIS LETTER IS USED TO INOICATE A PROJECT. PROPOSED. OR PRELIMINARY 1000 - N50 - 00 r HISC ADDITIONS TO THE STANOARO T*S LETTERS ARE USED TO INOICATE A TEMPORARY ORAWING. zrBL A pi 1000-N50-001 1000-N50-001 THIS LETTER 1$ USED TO UOICATE A DRAWING IN OUR DIVISION PLOT PLAN SYSTEH. g^ SUCLE OR DOUBLE I> LETTERS ARE ALLOKO TO KEEP: 'A CERTAIN SEQUENCE OP,;- ; : \ . oraminos tooether. " ' \T ' 1000AA-N50-001 VL - A . -" eifCT 7 OF 7 ` I;,-.1*.*' *' V- r' T 'is' V."--DO 014655 ` W-Hfe conftdfnttai f LINE BUBBLE LINE NUMBER PIPING SPECIFICATION SERVICE DESIGNATION PIPING SIZE (WAT-100 -6" -A ~) T=E I TRACING SPECIFICATION C=F4 t INSULATION TYPE A CLASS ' ' .* ^ '* ^* . 1 ; V* - -> ' ' - > ` k SKv,' * f . ;* T^. r .v - ' v*V- , >jW *-*', ? --fc'* -''/ L r-,',>*' *'* - S*,, ;-T` ' /& o,- r0>0n 014656 . CONFIDENT!Al OONF T OTNT T Al n 00 1* i8 i _i_____________1-___________*_______________ HI----f 1--TIPIUTIM * him -- . -B= ________,____________________ OAAVtHC DOCK _____u 1 llSSL IfSr. k BUsr1 im? ii J ft I! LINE SERVICE DESIGNATION PRO PW STM CL2 CTS CON HO MOH N2 CTR OM VNT REF IA INH FW OW DRN SA PROCESS PROCESS WATER STEAM CHLORINE COOLING TOWER WATER SUPPLY CONDENSATE HOT OIL METHANOL NITROGEN _______ COOLING TOWER WATER RETURN OIL MIST VENT REFRIGERANT INSTRUMENT AIR INHIBITOR FIREWATER POTABLE WATER DRAIN SULFURIC ACID V* : 014659 . V"-* j . - .. ,, . PIPING SPECIFICATIONS PEC SERVICE 'cRRr-2p; feAf5$buCT CRU&ASoUCT CELL EFFLUENT Ft PN.IA.CT< ON:.. M2 ` "Hf ^CRyOEPROOUCT VAPOR " (CORROSIVE) liOS7a^! ^5S3T?"EN iW -kj' nRAI--N rR PRESSURE/TEMP PSIC/ F 408/100 - 384/400 408/100 - 384/400 285/100 - 200/400 285/100 - 200/400 285/100 - 265/180 f75/100 - 225/212 75/100 - 225/212 275/100 -175/350 285/100 - 170/500 20* VAC 20* VAC - 25/2. 446/100 - 404/550 445/100 - 445/400 446/100 - 379/650 285/100 - 200/400 212/100 285/100 - 70/150 285/100 - 200/400 230/100 - 160/400 600/100 - 415/400 600/100 - 480/400 600/100 - 475/650 285/100 - 170/500 446/100 - 404/550 200/1025 285/100 - 185/400 285/100 - 230/400 230/100 - 185/400 285/100 - 200/400 673/100 - 501/725 446/100 - 446/400 446/100 * 404/550 200/AMO. 100/150 ANSI FLANGE RATING PSIG 300 150 150 150 150 150 150 150 N/A N/A 300 150 150 150 150 150 3O0 300 150 150 150 150 150 300 150 150 150 150 ro> o Z3 -on o-1 T1 * z O' >, H-T<> Oo' V.j>: 1 ' ' 'if- PIPE MATERIAL A-333 A-333 A-333 A-333 PPL LINED KYNAR LINED TFE LltCD CS FRP FRP CS CS CS CS CS gal. CS CS SS 304L SS 304L MONEL MONEL cs/ss cs/ss INCONEL 600 A-20 CS MONEL CS CS CS GAL. CS CS/SS CS PVC GAL. CS C O N FID E N T TAI. AAHL ANALYSIS ALARM' HIGH OR LOW ACV ANALYZER CONTROL VALVE AE ANALYZER ELEMENT AI ANALOG INPUT AO AOV AR AT BMS CGA , CGM ANALOG OUTPUT AIR OPERATED VALVE ANALYSIS RECORDER ANALYSIS TRANSMITTER BURNER MANAGEMENT SYSTEM COMBUSTIBLE GAS ALARM COMBUSTIBLE GAS MONITOR n : CT CONDUCTIVITY TRANSMITTER ? CV FLOW CONTROL VALVE : oi> DIGITAL INPUT DO DIGITAL OUTPUT EBV EMERGENCY BLOCK VALVE EV ELECTRIC VALVE (SOLENOID) EW EMERGENCY VENT VALVE - FAH FLOW ALARM HIGH f FAHL FLOW ALARM HIGH OR LOW f ' FAL FLOW ALARM LOW FE FLOW ELEMENT FFA FLAME FAILURE ALARM / / FFIC RATIO FLOW* INDICATING CONTROLLER >. FFS FLAME FAILURE SWITCH r FI FLOW INDICATOR(LOCAL) : FIC FLOW INDICATING CONTROLLER FR FLOW RECORDER FRC FLOW RECORDING CONTROLLER FSH FLOW SWITCH HIGH FSHL FLOW SWITCH HIGH OR LOW FSL FLOW SWITCH LOW , Si-FTiV. FLOW TRANSMITTER ii- GFO , GROUND FAULT DETECTOR ' * GL -:: GREEN LIGHT .W: B8BB HICi; HAND INDICATING CONTROLLER HOA _ : HAND-OFF-AUTO SWITCH HAND SWITCH HSA ,, HAND SWITCH ALARM V. I/Pi5{; transducer o>vI/S- CURRENT/SPEEO TRANSDUCER a /II3* CURRENT INDICATOR (AMPS) o t IR ,C CURRENT RECORDER -* >,IT.'i^; CURRENT TRANSMITTER LAH y LEVEL ALARM HIGH ff'/'LAHH LEVEL ALARM HIGH-HIGH ~ LAHL LEVEL ALARM HIGH-LOW `, LAL\' LEVEL ALARM LOW LC LEVEL CONTROLLER LCV LEVEL CONTROL VALVE utr WEIGHT INDICATOR CON. Jt WEIGHT TRANSMITTER CON LE LEVEL ELEMENT ZSC LIMIT SWITCH CLOSED LI LEVEL INDICATOR ZSO LIMIT SWITCH OPEN LIC LEVEL INDICATING CONTROLLER LIT LEVEL INDICATOR TRANSMITTER LR LEVEL RECORDER LRC LEVER RECORDING CONTROLLER LSHH LEVEL SWITCH HIGH-HIGH LSHL LEVEL SWITCH HIGH-LOW LSL LEVEL SWITCH LOW LT LEVEL TRANSMITTER PAH PRESSURE ALARM HIGH PAHL PRESSURE ALARM HIGH OR LOW PAL PRESSURE ALARM LOW * PB PUSH BUTTON PCV PRESSURE CONTROLLER (SELF-CONTAINED) PDAH PRESSURE DIFFERENTIAL ALARM HIGH PDAHL PRESSURE DIFFERENTIAL ALARM HIGH OR LOW PDI 1PRESSURE DIFFERENTIAL INDICATOR PDIC PRESSURE DIFFERENTIAL INDICATING CONTROLLER PDR PRESSURE DIFFERENTIAL RECORDER PDRC PRESSURE DIFFERENTIAL RECORDING CONTROLLER OPT PRESSURE DIFFERENTIAL TRANSMITTER PI PRESSURE INDICATOR PIC PRESSURE INDICATING CONTROLLER PR PRESSURE RECORDER PRC PRESSURE RECORDING CONTROLLER ,PSH PRESSURE SWITCH HIGH PSL PRESSURE SWITCH LOW RL RED LIGHT RO RESTRICTING ORIFICE SC SPEEO CONTROLLER SDA SHUTDOWN ALARM SG SIGHT GLASS SSH SPEEO SWITCH HIGH SSL SPEED SWITCH LOW ST SPEED TRANSMITTER TAH TEMPERATURE ALARM HIGH TAHL TEMPERATURE ALARM HIGH OR LOW TCV TEMPERATURE CONTROL VALVE TE TEMPERATURE ELEMENT TP PRESSURE TRANSMITTER TR TEMPERATURE RECORDER TSH TEMPERATURE SWITCH HIGH TT TEMPERATURE TRANSMITTER UA UNIT ALARM VAH VIBRATION ALARM HIGH VE VIBRATION ELEMENT VFD VARIABLE FREQUENCY DRIVE VI VIBRATION INDICATOR TWOGAL LOME EUIBELI LINE NUMBER 7 size7 V SPEC -----------j TRACING --^ 71 INSULATION (PRO-12604- 1 1/2* -X ) T^ST----- ----- FC7 TV IPO GAIL LONE (NlTOINiy^TO@lNli DESTINATION 1 DESTINATION 2 DRAWING NUMBER ON OR OFF PAGE LEFT OR RIGHT T-100 A/B B1-100-NS0-001 \ > / NON-DIRECTIONAL STM-40101-24*-X 235 STM HEADER B1-401-V51-001 BI-DIRECTIONAL WELL NO. 21 STORAGE WELL L B1-1021-B60-001 TO AND FROM ADJACENT PAGE LEFT OR RIGHT E-101 A/B/C 1b1-2505-P45-002 -(PRO-12604 - 11/2* - X ) P-101 A/8 B1-2505-P45-002 <reO-12604-ll/2* -X^) BHP1D4 10/69 OJDQN/RHP1D4IX3N 8p. 13,109116:1834 * DO 014662 - CONFTDFNTTAt ONiiaG@MMiTOINI@ LON I PROCESS (THIN) PROCESS (THICK) ELECTRICAL OR T.C. INSTR AIR OR PNEUMATIC CAPILLARY TUBING HYDRAULIC SIGNAL LINE DATA HIWAY SERIAL LINK FIBER OPTIC T? /' 0 ' X X X X X- X X X -X X X X X -X -t--t--t--fc--t--t--b--t--t--fc--t--t--t--- 00000000 -0 00000 typocal DNsirimuiMiENir tta PREFIX ROOT - SUFFIX FIELD O MOUNTED BEHIND CONTROL 0 ROOM PANEL MOUNTED CONTROL ROOM 0 PANEL MOUNTED LOCAL FIELD BEHIND PANEL MOUNTED LOCAL FIELD PANEL MOUNTED CONTROL ROOM MICRO DEVICE cpu-room ^ ~ MICRO DEVICE FIELD COMPUTER DEVICE CPU-ROOM COMPUTER DEVICE CONTROL ROOM COMPUTER DEVICE RHPID6 10/M CVDGN/RHP1D5.DGN S*p. 13,190116*433 ,* .V': 00 014663 W CONFTDFNTT A( TWO AIL I@(U)0(PMiMT TA PREFIX ROOT SUFFIX TRACING _J L INSULATION T-ST C-E7 TWDaL BQWY SVH1ILS RHPID6 10/80 IX GATE VALVE CX DIAPHRAGM VALVE tm PLUG VALVE IX NEEDLE VALVE Dea BALL VALVE CX GLOBE VALVE CX BUTTERFLY VALVE rear barstock valve CX slide valve Cg] 3-WAY VALVE C^3 4-WAY VALVE eg] 3-WAY PLUG VALVE 4-WAY PLUG VALVE DgCl 3-WAY BALL VALVE 4-WAY BALL VALVE DO 014664 OONFTDFNTTAI TmPOCAIL @IMTIF&ll V&ILVI MODULATING ON/OFF SOLENOID MOTOR v-- PRESSURE REGULATING ?mm 8VI TRP TRAP SYMBOL TP TIE POINT ECCENTRIC REDUCER CD CONCENTRIC REDUCER ANGLE VALVE r-**i CHECK VALVE Dga TRANSFLOW VALVE Y OR 45 DEG. VALVE r4i SPRING bOADEO CHECK VALVE D PIPE CAP PIPING NOZZLE. / ^PIPING NOZZLE W/FLANGE V- P=-------------------I-II FLANGE BREAK-OUT FLANGES TO PLANT DRAIN SYSTEM RHPID7 10/80 C^0GN/RHPI07JX3N S#p. 15,1091 0823:13 Y OPEN FLOOR . DRAIN U TRENCH ORAINv. : . ii'. Yi-4'' '* D0 014665 ' ' ; ,: ;L: CONF T DFNT T Al - - i' .'*? j. LME TOdlilOlN]' (mEZZD LINE SERVICE 01 THRU SB PAGE NUMBER (B1-105-XXX-001) OIMSTiyiMlINlT IN) y (Ml 1110 INI' PREFIX PAGE NUMBER (B1-243-XXX-001) 01 THRU SB PREFIX POINT NUMBER CAN NUMBER SYSTEM NUMBER OINlSTiyUllNlT iYM!lILS INSTRUMENT ELEMENT O THERMOWELL |>! RESTRICTING ORIFICE # CRITICAL INSTRUMENT HEX IVH SAMPLER (ANALYZER) E3 DIAPHRAGM SEAL ROTOMETER INLINE INSTRUMENT RHPID10 1O/B0 C^DON/RHPtDlO.DON Sap. 15,1091 09:1326 i.l. - DO 01466? ';J, i-r-- OONFJOFNTTA! ' -S. iAFETY KMOlPdEOT SPECTICLE BLIND HAMER BLINO FI TRACING T=SI!L T=NONE PS* PS* RHPID11 10/B9 C^DGN/RHPID11.DGN Sp. IS, 10911030622 <jT" V- INSULATION TRACING AND INSULATION PIPING C=F7 C*F4PP T*STM T=NONE C=F7 C=F4PP PS= PS= .* DO 014608 CONFIDENT T A1 iOTS B>EWE1LIPEB SYIIEOL: CO PITOT TUBE GEAR PUMP MONO PUMP RHPID17 9/91 C^DGN/RHPIDI7JDOH Sp. 16,169117:38:05 + .-I , *,-i \'s ' ; t-5"^mT. ,- * : -* .?<*** .v\j * - . .* -s. 'Fv^ DO 014670 nONFTOFNTTAI. - '' *-v >' 7 >'* ' Vv-y zj: MTO!. SST^TTOM L W M@ W RHPID12 10/80 ;' no oi4f>7i ` CVDGN/RHP1D12.DGNS*p. 15,199111:1432 ' ' r?f f ONFTDFNT T Al P>U1MIP STATOIM @ILE> V8 IMID W RHPIDU 10/00 C:/DGN/RHPID14.DGN Sop. IS, 19911123:18 no 01 46^0 tdfnttai conf TWOAIL (H1 RHPID13 10/80 C:/DGN/RHPID13.DGN8p.15,1991 11:3341 4-. ?; - DO 014670 C0NFTDFNTTA1. TI RAFIK ATM Eli Piwoa TEMP ELEMENT W/ THERMOWELL TEMP ELEMENT WO/ THERMOWELL DUAL TEMP ELEMENT W/ THERMOWELL TT W/ THERMOWELL AS A UNIT TT (FIELD MOUNTED) W/ SEPARATE THERMOCOUPLE * WELL TEMP INDICATOR W/ THERMOWELL SPECIFIED TOGETHER CAPILLARY TEMP INDICATOR W/ THERMOWELL & INDICATOR SPECIFIED TOGETHER THERMOWELL ONLY RHPID1S 10/89 C-/0GN/RHPID15.DGNS*p. 15,199111:3fc26 ^ v- DO 014674 OONFTDENTT Al MM-OME FL@W IIWOCI MAGNETIC FLOW METERS. TURBINE METERS. VORTEX SHEDDING METERS, SONIC METERS, TARGET METERS. AND OTHER SIMILAR IN-LINE FLOW DEVICES Ft FT 101 102 ORIFICE PLATES FLOW TRANSMITTER W/ REMOTE TRANSMITTER W/ BUILT-IN TRANSMITTER FLOW METERS ROTAMETER ORIFICE RHPID16 10/89 ,, C^DON/RHPIOI 0.OGN $p. 15,1961 1153:39 ORIFICE PLATES. DUAL-FLOW TRANSMITTER no 01 4fj7Fi rONFTDFNTTAI SCHEMATIC ON MATERIAL LIST (7) TBV Vi' NPT-????? (F) ROSEMOUNT MOUNTING AOAPTOR.???? HUBER MAGNUM SERIES S22 OBL.FLG. 3J WITH MOUNTING BRACKET NOTESt 01 4f>7F, r,nNFTOFNTTAl 1 ALL P1PE.F1TTINGS & VALVES SHALL CONFORM TO PIPE SPECS. 2. SUPPORT TUBING CONTINUOUSLY FROM PROCESS TO TRANSMITTER. < 3* FIBERGLASS CHANNEL EXTREN 500) 3. TU8ING SHALL SLOPE FROM PROCESS TO INSTR. A MINIMUM OF !4*PER FOOT. 00 NOT TRAP. SPEC. BY HPS THE DOW CHEMICAL COMPANY ** SA01-7G851 CHECKEO. ?? VINYL II - - . . . ;.V; -' APPD. - FLOW "TRANSMITTER DETAIL f' -h , ` > v- - .0 \ - , ' oatej 3/16/88 REVISION OATE A B | . -------------------------------------------- ------------------------------- --:--------1----------------- ; 1 BLOCK CC r;, INSTRUMENT ` ' `V- INSTALLATION DETAIL OCTAL N& ar 2 -"-*A6-1077 TAG ITEM -1 SCHEMATIC Or MATERIAL LIST (7) TBV J$*NPT-????7 (2) TBV Vz' NPT-????? @ J4*MALE PLUG **T *V4*npt male connector ALL TUBING TO BE %' MONEL ALL TUBE FITTINGS TO BE MONEL ALL TUBE VALVES TO BE SWAGELOK M44S6 BALL VALVE ,a HUBER MAGNUM SERIES S21 SNG. FLG. 7> WITH MOUNTING BRACKET NQTESi 1. ALL PIP&FITTlNGS & VALVES SHALL CONFORM TO PIPE SPECS. 2. SUPPORT TUBING CONTINUOUSLY FROM PROCESS TO TRANSMITTER. C y FIBERGLASS CHANNEL EXTREN 900) ^ __ 3. TUBING SHALL SLOPE FROM PROCESS TO INSTR.A MINIMUM Oi 00 01 4677 PER FOOT. 00 NOT TRAP. CONFTDFNTT Al SPEC. BY HPS THE DOW CHEMICAL COMPANY * SS01-76A2C OCCKEOi ?? VINYL II BLOCK K INSTRUMENT . APPth FLOW TRANSMITTER OETAIL INSTALLATION DETAIL OATEi 3/16/8*5 REVISION OATE A : | OCTAL ML -------------------------------------------------------------------------------------------------------- 1 WT l flf 2_____ A6-1071 TYPOOAIL OM8TAILILATOON V TRP 1 NOTIi STRAIN1R UiKD IP NOT INTIRNAL TO TRAP on oi467a CONFTDFNTTAI CW T-XXXXX 00 014679 OONFTOFNTT AL Y>M*Y SET o I50PSIC SET Q 10PSIG , TYP. A VHT- SET 150PS1G TYP# PflQ-XXXXX- X -X ) DO 014880 oo 014681 CONFTDFNTTAl I USE k CARE OF PORTABLE COMBUSTIBLE GAS k OXYGEN METERS I. REASONS FOR HAVING THESE METERS A. DIVISION HAS 22 PLANTS WITH PIPES. VESSELS, AND CONTAINERS WITH FLAMMABLE. EXPLOSIVE AND NON LIFE SUPPORTING ATMOSPHERES. B. EMPLOYEES MUST ENTER OR OTHERWISE BE EXPOSED TO THESE ATMOSPHERES FROM TIME TO TIME. C. METERS ARE USED TO ASCERTAIN THE CONDITION OF THE ENVIRONMENT TO WHICH WE ARE GOING TO EXPOSE OUR PEOPLE. D. LET'S US KNOW WHETHER IT'S SAFE TO OPERATE EQUIPMENT. f I on 014<Sfl3 CONFTOFNTTAl III. ABOUT THE METER (actually two meters in one) A. OXYGEN - ELECTROCHEMICAL FUEL CELL THAT DEVELOPS A VOLTAGE WHICH IS PROPORTIONAL TO THE OXYGEN CONCENTRATION OF THE GAS PASSING THROUGH THE CELL. THE CELL IS DEPLETED OR USED UP AS OXYGEN MEASUREMENTS ARE MADE. B. COMBUSTIBLE - CATALYTIC BEAD IN CELL WHOSE TEMPERATURE IS CHANGED BY THE AMOUNT OF COMBUSTIBLE GAS IN THE SAMPLE. AS THE TEMPERATURE IS CHANGED, ITS* RESISTANCE CHANGES. UNBALANCING ONE LEG OF A WHEATSTONE BRIDGE CIRCUIT COMPARED TO A SECOND BEAD WITHOUT CATALYST THAT WILL NOT REACT TO THE COMBUSTIBLE GAS. THIS TYPE OF CELL REQUIRES SOME OXYGEN (10%) FOR SUCCESSFUL OPERATION. I On f'rwr IV. TERMS A. LEL (LOWER EXPLOSIVE LIMIT - The least concentration of a combustible as m air that will lKnite B. VAPOR DENSITY - The weiRht of a sas as compared 10 air. C. OXYGEN DIFICIENT OR RICH ATMOSPHERE The combusubJe as sensor requires at ieast 10 * oiVRen anti a maximum of 25 oivgen to work accurately ii DO 0146R.S donftdfnttai lover EXPLOSIVE LIMIT (LEL) 00 014686, OONFTDFNTTAI. OXYGEN DEFICIENT ATMOSPHERES & YOU nXYRFN % IN AIR (APPROX. 21 X NORMAL) 12 - 18% 10 - 12% AT RFST SlfiNS & SYMPTOMS BREATHING & PULSE RATE INCREASED; COORDINATION POOR. DEEP, FAST RESPIRATION; GIDDINESS; POOR JUDGEMENT; LIPS BLUE. 8 - 10% 6-8% 4% 0% NAUSEA; VOMITING; INABILITY TO MOVE FREELY; UNCONSCIOUSNESS; ASHEN FACE. 8 MINUTES - 100% FATAL 6 MINUTES - 50% FATAL 4 MINUTES - ALL RECOVER WITH TREATMENT \ 1 COMA IN 40 SECONDS; CONVULSIONS; RESPIRATION CEASES. INDIVIDUAL IMMEDIATELY BECOMES UNCONSCIOUS; WILL RECOVER ONLY IF GOOD AIR IS IMMEDIATELY AVAILABLE WARNING: THE WARNING SYMPTOMS OF AN ATMOSPHERE DEFICIENT IN OXYGEN ARE COMPLETELY INADEQUATE AND, ALTHOUGH. A TRAINED OBSERVER MAY, WHEN ALERT, RECOGNIZE THE INCREASE IN PULSE AND RATE OF BREATHING IN TIME TO RETURN TO GOOD AIR, THE AVERAGE INDIVIDUAL FAILS TO RECONIZE THE DANGER UNTIL HE IS TOO WEAK TO SAVE HIMSELF, ESPECIALLY WHERE THE RETURN TO GOOD AIR INVOLVES CLIMBING STAIRS OR A LADDER. DO 014687 CONF TDFNT T At. EXPLOSIMETER LIMITATIONS-IT CAN'T DO IT ALL Instruments by design and application, have specific limitations. The Explosimeter is no exception. The following information indicates these areas, and it's imperative that anyone operating an explosimeter know and understand them before using them in the field. 1. The explosimeter is a tool to assist in the planning and preparation of some jobs (hot work, vessel entry, etc.). It does not replace pre paration,planning, and common sense, and should not be regarded as a guarantee that a job is safe. The explosimeter cannot measure or detea chemical irritation and/ or toxicity. The explosimeter is designed to process certain gasious or "dry" vapor samples only. It should not be used on liquids, solids, dusts, mists, or wet" vapors. A. The explosimeter is designed for use over a temperature range of 10 - 110 F. If a unit is to be used in a area where the ambient temperature is 110 F or above, the explosimeter should be first checked and calibrated under similar conditions. Make sure-the area used to check the meter is known to be free of combustibles. Sample temperatures should be the same as the explosimeter, otherwise, condensation of the sample vapors may occur causing false readings. 5. The explosimeter is designed to detea the presence of flammable gas or vapors in air; it will not work on such gases in inert at mospheres. 6. The explosimeter should not be used to check for flammable mix tures which contain less than 10% or more than 25% oxygen. DO O14688 OONFTDFNTTAl 7. There are some gases which affect the accuracy of, or damage, the oxygen sensor. Strong acid gases (HQ, sulfuric, etc.) may damage the oxygen sensor by permanently changing the pH in the electro chemical cell R. Some gases or vapors, even though non-flammable, may result in explosive readings if sampled. Helium, because it is lighter than air, has a cooling effect on the sensor causes a negative response. Argon tends to insulate the sensor and cause an increase in the meter s response. Many Freons decompose upon contact with the sensor and cause an explosive reading. 9. Tetraethyl lead, silicones, and many sulfur compounds will poison the catalytic activity of the combustible sensor causing incomplete combustion and lower explosive readings or no response at all. 10. Keying portable radios within 10 feet of the explosimeter can cause false readings on the explosimeter. r>0 014689 ( t'ONFTOFNTTAI PRE-USE CALIBRATION CHECK OF BIO MARINE 902 & GASTECH GX-3 COMBUSTIBLE GAS/02 MONITORS 1. CHECK UNITS WITH HOSE & PROBE CONNECTED.. 2. CHECK FILTER & WATER TRAP. SHOULD BE CLEAN AND DRY. 3. CHECK BATTERY VOLTAGE. NEVER CALIBRATE ANY METER WHILE PLUGGED INTO THE CHARGERl 4. CHECK PUMP FLOW AND ALARM. 5. CHECK OXYGEN READING IN AIR. SHOULD BE 21%. IF NOT, ADJUST TO READ 21%. 6. CHECK COMBUSTIBLE GAS ZERO. IF NOT ZERO, ADJUST TO READ ZERO. 7. INTRODUCE CALIBRATION GAS (2.3% METHANE IN AIR). COMBUSTIBLE GAS METER SHOULD GO UPSCALE TO 2.51 ON BIO MARINE UNITS OR TO 55% LEL ON GASTECH UNITS. IF READING IS INCORRECT, ADJUST WITH GAS SPAN POT TO OBTAIN PROPER READING. THE SPAN POT FOR 310 MARINE UNITS IS LOCATED ON TOP CONTROL PANEL. THE SPAN POT FOR THE GASTECH GX-3 UNIT IS LOCATED IN THE FRONT CHAMBER, FSPAN POT #3. \ 8. IF UNITS CANNOT BE ADJUSTED PROPERLY, OR IF YOU FEEL THE UNIT IS NOT OPERATING CORRECTLY, DO NOT USE IT. TAG THE UNIT AND SEND IT TO THE CENTRAL INSTRUMENT SHOP FOR A THOROUGH CHECKOUT AND REPAIR.* 1 PRE-USE CALIBRATION CHECK OF GASTECH 1214SMP COMBUSTIBLE GAS/02 MONITOR 1. CHECK UNITS WITH HOSE & PROBE CONNECTED. 2. CHECK FILTER & WATER TRAP. SHOULD BE CLEAN AND DRY. 3. PRESS RED "POWER" SWITCH TO TURN UNIT ON. THE STATEMENT "GASTECHTOR ON - TAKE TO GAS FREE AREA" WILL SOUND AND DISPLAY WILL BLINK. THE UNIT DISPLAY WILL CONTINUE TO BLINK FOR A TWO MINUTE WARM-UP PERIOD. 4. AFTER THE TWO MINUTE WARM-UP PERIOD HAS ELAPSED, THE STATEMENT "PRESS ADJUST BUTTON" WILL SOUND. PRESS THE BLACK ADJUST BUTTON. UNIT SHOULD THEN READ 20.9% 0, and 0 COMBUSTIBLES. ANYTIME THE ADJUST BUTTON IS PRESSED THEREAFTER, THE UNIT WILL DISPLAY THE NUMBER OF BATTERY HOURS REMAINING. on 014690 5. CHECK PUMP FLOW. ft rONFTDFNTTAl 6. INTRODUCE CALIBRATION GAS (2.5% METHANE IN AIR). METER SHOULD READ 551 LEL. IF NOT, ADJUST SPAN POT LOCATED ON SIDE OF UNIT AND MAKE METER READ 55%. 7. IF UNIT CANNOT BE ADJUSTED PROPERLY, OR IF YOU FEEL THE UNIT IS NOT OPERATING CORRECTLY, DO NOT USE IT. TAG THE UNIT AND CHECKING FOR COMBUSTIBLE GAS IN INERT BACKGROUND USING SPECIAL FITTING ON STANDARD EXPLOSION METER 1. Calibrate unit without special fitting using 2.5% Methane in air cal. gas. Combustibles should read 55% LEL. If not, adjust span so that meter does read 55% LEL. Oxygen should read 21%. 2. Put special fitting on unit and introduce cal. gas again (2.5% Methane in air). Combustibles should read approximately 27.5% LEL. Oxygen should read 2IS. 3. Put 2.5% Methane In Nitrogen in unit. Combustibles should read about 27.5% LEL. Oxygen should read approximately 10.5%. 4. THE UNIT IS NOW READY TO BE USED. 5. After a line has been checked with a standard (without fitting) meter and the line has less than 10% oxygen, you would then use the special meter (with fitting) and check the line for combustibles. f i 6. Always be aware of your oxygen reading when using the meter with the fitting on it. Your oxygen reading can tell you many things. For example, the oxygen reading taken without the fitting must differ from oxygen reading taken with the fitting in place. NOTE: ANY COMBUSTIBLE GA5 READING OBSERVED WHILE USING THE UNIT MUST BE MULTIPLIED BY TWO TO OBTAIN THE ACTUAL %LEL. rONFTDFNTTAl METERS ARE NOT DESIGNED TO TAKE LIQUID SAMPLES ' DO 01469? rONFTDFNTTAt CAUTiON 1 NITROGEN PAD IN use1 ON FLAREPACK. ME7ERS SHOULD NOT BE USED TO IEA SURF COMBUSTIBLE GAS IN ATMOSPHERES THAT ARE OXYGEN DEFICIENT 00 014690 COIMFTDFNTTAI. V r ^ GAS TCT~ORR CXKLLEE TAKF TO BLASSS AttFA `TEfRA ETHVL LEAD OR SILICON COMPOUNDS POISON COMBUSTIBLE GAS SENSORS DO 0 1 4 6 9 4 OONFTDFNTTAL BE" ALERT! O1 4 ^ CONFTOFNTTA! DO 0 1 4 6 9 6 C O N F ID F N T T A l ------------------------------- ---------------- - w * .---------- Ul L / WHEN ACTING AG SAFETY OBSERVER Always look for potentme hazards FROM SURROUNDING AREAS BE ALERT! 00 O ? 4697 CCiNF 7 OF NT IAL ACIDSAFE. CMP MINIMUM SAFETY EQUIPMENT REQUIRED IN C!. M. P . ACID AREAS WALK - THRU OPEN LINES BLEED DOWN C--202 BTMS. E-212 H2S04 T/C RACK (CAR CONNECTED) T--900 C--650 C--202 DECKS H2S04 T/C RACK (CAR NOT CONNECTED) C-210 C-200 / C-201 BTMS. P-30) 'S C-610 / R-600 SLICKER SUIT / GOGGLES / RUBBER BOOTS, GLOVES SAME AS ABOVE SAME AS ABOVE SAME AS ABOVE SAME AS ABOVE GOGGLES GOGGLES GOGGLES GOGGLES GOGGLES GOGGLES FULL ACID SUIT SAME AS ABOVE SAME AS ABOVE SAME AS ABOVE SAME AS ABOVE FULL ACID SUIT GOGGLES (EXCEPT H2S04) SLICKER SUIT / GOGGLES / RUBBER BOOTS, GLOVES SAME AS ABOVE SAME AS ABOVE SAME AS ABOVE SAMPLES. C-200 / C-201 C-610 C-650 H2S04 T/C C-202 BTMS. SLICKER SUIT / GOGGLES / RUBBER BOOTS, GLOVES SAME AS ABOVE FULL ACID SUIT FULL ACID SUIT FULL ACID SUIT * CONTRACTORS IN AC I*) AREAS FOLLOW A DIFFERENT SET OF PROCEDURES. (SEE PROCEDURE FOR CONTRACTORS WORKING IN ACID AREAS.) revised: 2/91 JRC/DRD Ol 46923 oonftdfntta, *- + - ** iS&L pBKkiij !l > / \ CHLORINATED METHANES SAFE JOE PROCEDURE .apartment:, CMP ob Title: R--250 PROBLEM SOLVING -cope: GENERAL INFORMATION ON POSSIBLE PROBLEMS AND CORRECTIVE MEASURES 1. POSSIBLE CAUSES OF HIGH INLET PRESSURE ON R-250A A. The reactor is carbaning up causing a large pressure drop making it more di-f-ficult to run the same loads. (May need to cut the reactor rates and run in this condition until the reactor can be recharged) t k w.''c Lwivc 1 ^z "3 cp. ^ rcC'c'^or ^ 0 u ii F`" in^5 ) - > t i .... w c r.c c-iz-.-r ] ca ; c ,-er -from E-256 into E-245, causing : r, \j 1 r, E-245 which results ir. pressure swings. (Check tr:''"".:" + r ; _ -a Lure pro-fils, carrying over liquid can - . t'"c c .7 c c c ' and oil tempers ture ' s tc decrease. Also - k i. s "-i-u',:: -flow r.eters, a- they are swing badly that ' : -..........-_:.ccic fracing af-csc the -flow meters. - r -- 1 rr r t r -- - -- k >'t * a f r r; =r c: t? ir-ir fiM p,,ne;<-*A high, inlet pressure Ur-./ THE ME011 LOU PRESSURE SWITCH ACTIVATED. pump trapped o-ff lore. When activated it 4- 4-- c- j1 i> i l tr1 y pur. p * . Have someone check pumps and reset switchgear, cr repair. R Recirculation valve on pumps is opened to much -for the load you are attempting to run. a. Cut the recirculation valve back C. Excessive rates or, both R-250's. (cut rates) ' -T-- * j li DO 014699 CONFTOFNTTAl Vi, HE adt V!v R-250 PROBLEM SOLVING PAGE 2 ' I ON r-ROM 3 L' . ;witch Ma 1 f unc tioned . .. I f the au:; i 1 lary pump activated, did the switch clear. i. Check TDC group 77, meoh -flow transmitter and see it the incoming flow is still stable. . Check E-256 level and valve output. Has the valve output started increasing trying to maintain level, if not the switch is probably bad . Contact instrument personnel to repair has to be shutdown/h.-2l 3 i-- I I --' 1 *.*_ "W _ *-- A- . ^11^ t I/-1,--rl-11 >--i --. _ i i i- i ..... . C W 1. i I g uc. - tr.e column recycle temporctare to cecrea.se the overhead :.. r H _ i u c quc,,;. r; relemns. r: r: the overheat temp :cr tre 1 is C Cr ,Ti Jj tz f >c. u. l_Cl O'*" the quench erheaca. i pi \ J ^ W1 V1! *_ I *- > tc tlit. tnre, from Eh-Z59 should be about 1. i , O; *. w C_ ! o tLi lee if it's running ^ v tc cA 1" . . ehac,: L" Lvf ref la,: flow. May be to low (increase) Cheer. C-203 R-12 level may be to low (increase) 7 Blow down the level transmitter it may be full of oil causinq a misce11aneous reading. e. Check E-259 level transmitter. If this trans is indicating a level and E-259 is actually empty, we will be blowing baiK to C-350 (this is just as if the system wasn't on line! Z. Increase in Ml from C-840. a. Check. C-S4C overhead temperature, Make sure it is running normal. If not qoto "b" L. Cneci. D-E340 R-12 level. Should be running appro:-; 357.. DO 014700 CONFTOFNTT Al -'.m&t " %T j# ^ 3t-j. , * aw. ***'--+* -<- ' - * R-250 PROBLEM SOLVING OOKTI NJATION- PROM "#5 " -- PAGE 3 C. Sor, acne may have increased the N2 seal purges on K~350. Check arid make sure its C?i t 3. normal rate. L. A piece of equipment which contain N2 due to padding or purging has jsut been placed in service. E. N2 ESW ' s on the R-250's are leaking by. Manually block them in. L. PEE SI EMI REASONS WHY THE INDEPENDANT HIGH LEVEL ALARM ACTIVATED ON E-E5E. A. It is aetua11y true. .ediatly cut back you level in E-256 monitoring the don't want to take a chance of pumping liquid into fT* - - - 1 --If w J. w. U I CA + i_ --,, T _ t_ r_ ^ 1 U > L . w i i Lc C i Ci ! ill L 1 fb I =r > pressu the icck both level transmitters see if they agree. Should be m.r.1,,0 ucoro,. ELMO'... If are both running within their range arlw a..!' e_ ills Si-, i to i. may1 to bac. However; if ... io.,L:c) tr a, c,,,. vlc : -s :c<-.oir.q within tL normal range ii 1.111--. ri^^iiiw^.i.i xCiC^ ir.diuQ 11.1 a u c 113) is rCu^inC -* *-- --^ v."wt. i * *i- i,'r UfLciLi v' r *l * !\l>Tt_ i yww c =.n ij i _ ic- ; W 1 . _ \ Ic u c w wi ,, I, J. gc q, u . i -c -. O, bJ l t v dvet w i loll i _j tr.ey are swinging then across the flow oriface. failing. ti' a.'.s.i.itiers checked by instrument personnel. . c.'c c.'.cci.s o,.. . ha. a instrument personnel check Will THE AD I BAT I L MOREL SLOWLY INCREASING. When the isothermic section of the reactor starts to carbon up it degreases the amount of reaction that takes place in the sop section therefore; the reaction increase in the bottoms i-------cion. With more reaction there is more heat. (INCREASE THE OIL TEMPERATURE A PEW DEGREES HOTTER THAN NORMAL. THIS WILL HELP BRING THE REACTION BACK UP INTO THE ISOTHERMIC SECTION). If the Inlet OIL TEMPERATURE is too low it will cause the icotncrmic section of the reactor, to run at a cooler rate which will not be suffecient to react the HCL and MEQH. As in item (A; the r..a_jc: itv of the reaction will take place ir the bottom of the reactor. (INCREASE THE OIL TEMPERATURE D IT E NORMAL OPERATING LEVEL) Excessive rates can cause the bottoms temperature to increase iLOWER THE RATES UN THE REACTOR TO REDUCE TEMPERATURE) 00 014701 r.ONFTOFNTTAl y-- s ' ( 'n i i *1. h I R--250 PROBLEM SOLVING PAGE 4 e. POSE I EuE causes of low inlet and reactor temperatures.. ft. Licuid in the inlet line a. Check E-25E level, it may be carring over liquid (see item.it 11 ) . h. Lest heat transfer in superheaters. V, * a. Check oil temperature to superheaters and also check control temperature. (IF THE OIL TEMPERATURE IS OPERATING ELcQW NORMAL CONDITION INCREASE) , ,,> - - .. f. c. Lew til flow to the reactor due to low setpoint settir.q, control valve problems,transmitter problems and pump problem. < II sne nr c re nctucr were cc orift nigh at would ct.w.se one .'w.lvc- cucpw.t to decrease, thus ceore-esane the actual oil . - ow tlrcc.gr. t,L reactor. Check the total oil flow transmits t_ the i1 occ tore and do some calculation to see af the number: jcl tweer, '0 pounc de psr.d ir.q JFE' E ~-^Lufi.(TL2 rL^nW^n. Tplt* c Ta HLsh1 *1 t or c 1 j t w KI" 1-- " :r ittci' is malfunctioning blew tr.c hagr. ant low level legs of the transmitter down arid sec if after blowing dawn it quits swinging. If not nave instrument personnel check. ;i:_E REASONS THE LOW LEVEu ALARM ACTIVATES ON E-256. E-25E level is actually low. a. Check- the pressure control valve. If the level is actually lower than normal the valve output on the steam valve will be higher than normal, for any given feed rate. The pressure me, br falling. If the exchanger goes empty the steam valve will go wide open trying to control pressure and the pressure wil! or.tinup tc fall. IP " Oo COh/p? T0b1ptNyt0xp01 m*L. _ ar? i ****<- -ILO-aiLf R-250 PROBLEM SOLVING PAGE CJNT INL AT I ON OF ITEM #10 b. Check the redundant transmitter on E~256 which is located in group 118 on the TDC. See if the level indication agree's with the control transmitter. If so than the transmitter is I probably ok. If not have instrument personnel check the i> transmitter. \ ' r ., * . / ' V- } s j >t 4 c. The level setpoint may be set to low. (increase) i s'. d. The P-255 tripped off line or the recirculation valve on the pump is open to much for the feed rate you are trying to run (there is a MEOH header low pressure switch which will activated if the pressure gets low and it will enegize the auxiliary P-255). e E-25i `PF.; .'RE SLOWLY-DECREASING AND STEAM VALVE RE-'ESKS THE '.CD ICON KEEPS YLL FROM GOING ON HEAT UF. rzbiccr. porn., ssi vc a ha./n't been met -. H flow ..as g"ester cr.ar 3O'O'O+f hr or the HCL control vr . 'c tp'j-1- sn ' t it "ZE^C when the ''HCL AOV" switch sc. * to tra ig-'r pc-s_tic" ;;,d the reset button was hit. It;:, w:: ci:, newever; er.ee the modicor. opened the . ;L. AO. ' the oper:tor fazlcs tc reS'Sh the minimum i-iiL. c1- Mi flew requires in the time frame <120 sec) allowed i -- 3 ` < M -- Cl mm i c. . when using the HCL heatup or Ml and the flow falls below tht m^r.iT.tiT. setpoints. Tr.s "AOV" has mal f un ticned. Cneck the air to the AOV, If ok, have instrument personnel check transmitter. Lr . Faulty HCL ADV SWITCH on tne board. Have instrument personnel checl . D Fault in the program. If items "Aa,B & C" are ok contact modico; personnel. .V - D0 014703 CONFTDFNTTAL wmpumim :E' -4.. Q'J'C ^j-A PURPOSE: BASIC PUMP MODULE This module is to familiarize you with the Basic Operation and maintenance of a pump. On completion of this module, you have a basic understanding of how a pump operates and the necessary maintence required for. proper pump operation. r RESOURCE: (Pump Pilot Course,Human Resource,Pump manual) REQUIRED LEVEL OF PERFORMANCE: 100% OBJECTIVES: 1. Explain the operation,function, maintenance and instrumentation on the following. A.'Seal D. Seal Flush G. Lubrication B. Coupling E. Motor + Starter H. Impeller C. Coupling Guard F. Recirc. Flows 2. Physically locate and explain the function and operation of a start/stop station and the corresponding switchgear,including auto or remote start/stop and variable speed on any given pump. 3. Explain and special safety hazards associated with the equipment. 4. Explain what the major causes of bearing failure are,and how these conditions can be eliminated. 5. Explain what the major causes of seal failure are, and how these conditions can be eliminated. 6. Demonstrate checking and adding oil to any given pump. 7. Demonstrate how to properly locate all pump parts at the cellulose warehouse using the pump parts book. 8. Demonstrate the proper procedure for taking a pump out of service and checking it for maintenance. 9. Complete a simplified drawing of the oil miBt system. 10. Explain the function of the oil mist system and how it operates. 11. Explain how you would determine what type oil is used for the oil mist system. 12. Explain why rotation is checked on a pump after the motor has been changed out or the electrical system has been worked on. 13. Explain the following. A. Mag Drive Pump C. Centrifical Pump B. Can Pump D. In Lin Pump D0 014704 OONFTDFNTTAl 14. Explain the difference between a Mag Drive Pump and a Canned Pump. DIFFERENCES BETWEEN CAN AND MAG DRIVE PUMPS Both canned pumps and magnetic drive pumps have moving parts and sleeve bearings, which are lubricated by pumping fluid through them. They both lose efficiency because of the can. Magnetic drive pumps use conventional,exterior mounted motors,were as canned pump motors are an integral part of the pump. The canned pump motor is subject to the heat of the pumped fluid and the motor also adds heat to the pump. In a mag drive pump the only barrier between the fluid and the moving parts is a non-magnetic can . In a can pump the motor shell provides containment since there are no moving parts outside of the can. This allows the can pump to be used with a higher pressure application. The can motor is considered safer for critical application. Although the mag drive pump can be made thicker to retain high pressure,it further reduces electrical efficiency. _____ HO 014705 OONFTDFNTTAl MAGNETIC DRIVE PUMPS Magnetic drive pump looks like a regular conventional pump, but their operating principles and design are quitedifferent. The main and most distinct difference is that magnetic drive pumps are sealless - no mechanical seals as in conventional pumps. In magnetic drive pumps, a conventional motor drives a magnet which in turn drives another magnet that is attached to the back end of the pump shaft. The two magnets are separted by a non-magnetic can (shroud). This shroud,which is usually .020-.080" thick, is the only protection you have of maintaining the liquid within the pump or preventing an environmental incident. For this reason, the shroud should be monitored at all times. Nearly all malfunctions can be detected by monitoring the liquid temperature in the shroud area. Approximatly 3-5X of the pumped fluid is required to lubricate the shaft sleeve bearings and remove heat in the magnet area. The main reasons for magnetic drive pump failures are: 1. running dry/cavitation 2. dead heading 3. solids in the fluid 4. permanently greesed anti-friction bearings The magnetic drive pumps are equipped with two thermocouples to show signs of these problems. The front thermocouple measures the temperature of the recirculated fluid used to lubricate the bearings and remove heat from the magnet area. This thermocouple will protect us in the event we dead head the pump,start the pump with the suction blocked or anything else that will cause this fluid to heat up. The back thermo couple monitors the temperature of the bearings or misalign ment problems. These temperature points should normally run about 10-15 deg c above the inlet fluid temperature with the alarm set at 20 c above the inlet temperature; therefore as the ambient temperature changes or during seasonal changes we may have to adjust the alarm setpoint. The most important thing is that if you get the alarm 20 c above the inlet temperature, you must react quickly. The recirculated fluid serves a very vital function to the operation of the pump. As indicated above, its purpose is to lubricate the shaft sleeve bearings and remove, heat in the magnet area. There is a minimum flow required to remove the necessary heat from the pump. This is the reason for the automatic recirculation valve on P-259B. If someone blocks in the discharge, the automatic recirculation valve automatically bypasses a designed amount of fluid to remove the heat. If this is also blocked in, you will wreck the pump. MAG DRIVE PUMPS PAGE 2 TROUBLE SHOOTING If you get an alarm 20 deg c above the inlet temperature, immediatly investigat to try to determine the problem. 1. Look at the discharge pressure guage to make sure the pump is not cavitating. If it is, immediatly shut the pump down and correct the problem. 2. Listen closely for any noise. This is also an indication of cavitation or the pump may be running dry. 3. Check to make sure that everything is lined up properly. Check the pump recirculation first. 4. Feel the pump by hand to see if it is truly running hotter than normal; however,if both temperature points increased, the instruments are probably correct. 5. If all else fails, call maintenance tech to check for vibration or excessive rubbing problems. The main point to remember is that you need to take action as soon as you get an alarm. GR 9/89 DO 014707 OONFTDFNTTAI CANNED MOTOR PUMPS A canned motor pump is a sealless centrifugal pump. In the pump the motor rotor is connected to the pump shaft and enclosed in a non-magnetic "can". This assembly is then inserted into the motor stator. The magnetic stator drives the rotor,just as with a conventional motor. Since the can is imposed within the magnetic field, the motor efficiency is reduced; The rotor and all the bearings and moving parts of a canned motor pump are inside the can and exposed to the pumping fluid. This requires a sleeve-type bearing that must be lubricated by the fluid. Canned motor bearing especially the rear bearings can get quite hot. Heat is generated by bearing friction as well as by the totally enclosed motor. To prevent flashing or decompositon of the lubricant and premature bearing failure, canned pumps must provides a positive flow of pumping fluid through the bearings. In some applications the fluid may have to be cooled or filtered before entering the bearings. GR 9/89 DO 01470ft rONFTDFNTTAI ITEM BASIC PUMP MODULE RESOURCES DEFINITION ADAPTER - A mechanical piece used to permit assembly of two other parts or for a spacer. ADAPTER,BEARING - A cylindrical piece used to mount a beraing on a shaft. ADAPTER,TUBING - A cylindrical piece used to connect discharge case to encloseing tube. BASE - A metal pedestal to support a pump. BASE PLATE - A metal plate on which the pump and motor are mounted. BEARING,INBOARD - The bearing farthest from the coupling of a pump. BEARING,OUTBOARD - The bearing nearest the coupling of a pump. BEARING,JOURNAL THRUST - A removable cylindrical piece mounted on the shaft and which turns in the bearing. BOWL - The enclosure within which the impeller rotates. CAN,ROTOR - A thin cylindrical part that separates the motor rotor from the pumped fluid.(can pumps) CAN,STATOR - A thin cylinedrical, non-magnetic part that separates a stator core assebly from the pumped fluid.(can pumps) CASING - The portions of the pump which includes the impeller chamber and volute. CAVATION - When the pressure at the inlet drop too low then bubbles form and absorb heat. As these bubbles move out to the higher pressure the bubbles collapse. This collapse can be quite violent and can cause severe damage. COUPLING- A device which is used to connect the motor to the pump. COUPLING GUARD - A protective shield which is placed around/over a coupling. COUPLING KEY - A rectangular piece of metal used to prevent the shaft from rotating inside a coupling half. DO 014709 ----------------------------------------------------------------------------------------------------------- ---------------- CONFTDFNTTAI DEFLECTOR - A flange or collar around a shaft, rotating with it to prevent passage of liquid,grease,oil or heat along the shaft. DISCHARGE CASE - A guide for liquid flow from the bowl to th pump column. PAGE 2 FRAME - The part of the pump which the bowl and bearing housing are assembled to and houses the rotating unit. GASKET - material such as garlock or teflon of proper shape and characteristics for the use in Joints and between flanges to prevent leackage. GASKET,BOWL - A gasket (garlock,teflon) that is used to seal the joint between the main pump body and the bowl. GASKET,IMPELLER - A material used (teflon) to seal the joint (space) between the end of the pump shaft sleeve and the impeller. GLAND - A follower which compresses packing in a stuffing box or retains the stationary element of a mechanical seal. HOUSING,BEARING - A body in which the pump bearings are mounted. HOUSING,STATOR - A body in which the stator is mounted.(elec ) IMPELLER - The bladed member of the rotating assembly of the pump which imparts the principal force to -the liquid pumped. IMPELLER KEY - a rectangular piece of metal used to prevent the impeller from rotating relative to the shaft. LOCKWASHER - A device used to prevent loosening of a nut. OILERS - A device/sightglass which is used on the bearing housing of a pump to maintain a level of oil in the bearing housing. OIL SEALS - A device used in the bearing housing of a pump to seal the oil in and keep it from escaping to atmosphere. OIL MIST SYSTEM - A system which supplies a fine oil mist through tubing into the bearing housing of a pump. This type system eliminates the use of oilers on a pump. 00 014710 OONFTDFNTTAI PAGE 3 RELIEF VALVE - A mechanism to control the maximum pressure that the pump can put out. ROTOR ASSEMBLY - A rotating assembly of an electrical machine containing laminations and conductors,interaction with a stator core assembly produces torque. SEAL - A device used to prevent the flow of a liquid from the pump suction/stuffing box to the atmosphere. SEAL,MECHANICAL - A device flexibly mounted on the shaft in or on the stuffing box and having a smooth face held against the stationary sealing face. SEAL,MECHANICAL COMPONENTS - A compresson unit,hard face (rotating units) and a carbon (stationary unit) STATOR CORE ASSEMBLY - The fixed assembly of an electrical machine containing lamination and windings which creates magnetic fields. STRAINER - A device used to prevent large objects from entering a pump.(usually wire mesh screen type) STUFFING BOX - A portion of the casing through which the shaft extends and the packing and a gland or a mechanical seal is placed to prevent leakage. TEST VALVE - A device to control the flow through the test pipe. Do 747l1 c'ONF Tt)FNTTAl BASIC PUMP MODULE RESOURES MECHANICAL SEALS Pumps handling hazardous or expensive liquids, or liquids where the necessary leakage from the stuffing box is objectionable, are often furnished with a mechanical seal. A mechanical seal consists of a rotating element and a stationary element. The sealing faces are highly lapped surfaces (extreamly flat) on materials selected for there low coefficient of friction and their resistance to corrosion by the liquid being pumped. The faces have a minute running clearance and normally run with a very thin film of liquid. In addition, there must be means of loading the seal and providing flexibility. This is accomplished by the use of springs and shaft packing or with a flexible member of some organic material. Mechanical seals are more widly used than shaft packing because they require less maintenance and hold leakage to a minimum. The stationary seal ring is usually made of carbon. The rotating seal ring unit is comprized of a compression ring (springs) and a seal ring (hard face) and the seal ring is faced with a special metal where it comes into contact with the stationary unit (carbon). The compression unit is held in place on the shaft by alien screws. This allows the compression unit and the seal ring to move freely on the shaft. The entire sealing unit operates by the springs pushing against the compression ring and compress the flexible (0) ring against the shaft and seal ring against the carbon to prevent leakage at this point. There are some applications which require a seal flush to cool down the seal. Excessive heat will cause the seal to lose its load carrying capacity. Also if the liquid contains solid corrosive material a seal flush will keep the seal faces clean. Seal typically fail because the carbon weares out. How ver there are other causes of seal failure such as EXCESSIVE HEAT,SHAFT MISALIGNMENT,PUMP MISALIGNMENT,BAD PUMP BEARINGS, PUMP CAVITATION AND DIRTY SERVICE. 00 01471? CONFTDFNTTAL MECHANICAL SEALS PAGE 2 HEAT causes a varity of problems that are not always obvious. When a teflon chevron ring (a ring inside the rotating seal ring used for sealing against the shaft) gets hot it will get soft and extrude into parts of the seal and cause the seal ring to lock on the shaft, then the seal is no longer able to move on the shaft and compensate for wear. Excessive heat will cause some acids to become very corrosive. Loss of a seal flush will cause the seal to overheat. Running a pump dry will cause the sealing faces to lose its film of liquid between them and overheat and cause excess friction and damage to the seal. DIRTY SERVICE will cause the small springs to become clogged and will lose its ability to move on the shaft and compensate for wear. The abrasive particles may cause a grinding action on the shaft. If the stuffing box is small the solids will build up and prevent the fluid from reaching them. BAD BEARINGS,SHAFT MISALIGNMENT AND PUMP MISALINMENT cause the seal to separate slightly allowing for uneven wear of the carbon and rotating seal ring thus resulting in leakage. DO 014710 C0NFTDFNTTA1 BASIC PUMP MODULE TANDEM SEALS Tandem seals are a specially designed seal for use in pumps where fluid problems exist. In our case they are mostly installed on equipment which contains METHYL CHLORIDE which has a one hundred pound reportable. Tandem seals consist of two bellows seals with one gland. The inside seal has an oil flush which cools and lubricates the seal. The oil (cp 6000) which lubricates the seal comes from and external oil pot located next to the pump. The oil enters the seal where it comes in contact with pumping paddles which are built into the seal itself. The pumping paddles help move the oil through the seal and back to the oil pot. If the inside seal should start to leak the product will enter the oil and then the oil pot. It will cause the pressure on the pot to increase. This is one good indic ation that the inside seal has blown. If this should occur, depressure the oil pot to the throx and block it back in.Monitor the time in which it takes for the pot to repressure back up. If it pressures back up fairly fast,the pump needs to be taken down and the seal repaired. Seal failure will result if the oil flow to the seal is lost. If the oil pot goes empty, the seal will run dry and overheat. If the oil level is to high it will become harder for the oil to circulate through the pump because of the extra head pressure (the oil returns to the pot about midway). Therefore it is very important that we maintain the proper oil level in the oil pot. If oil needs to be added to the oil pot, it is best to swap pumps and shut the pump down before adding oil. This will keep from running the seal without an oil flush. Use only CP-6000 in the oil pots for these seals. Do not use any type of regal oil. Standard regal oils are hydrocarbon based and will react with the HCL to form carbon. This carbon can get between the seal faces and cause the seal to fail. The following pumps have tandem seal installed on them. P-252 A&B P-256 A&B P-511 P-513 P-803 A&B P-804 A&B T-851 T-850 BLOCK 43 BLOCK 43 T-104 * S C-850 REFLUX GR 9/89 D 014714 r-0NFTDFNTTA, BASIC PUMP MODULE RESOURCES IMPELLER Centrifugal force is the force of spinning. When an object is spun in a circle.it pushes (outward from/inward towards) the center of the circle. One way to increase the energy of a liquid is to whirl the liquid around in a circle. When it is spun around it pushes (inward to the center/outward from the center) of the circle. This outward force is called centrifugal force. This is how a centrifugal pump operates. The liquid enter through the suction piping into the eye of the spinning impeller, the impeller wirls the liquid around in a circle. The liquid is forced from the center to the outside of the impeller. As the liquid starts to move to the outside of the impeller it picks up velocity as the liquid moves from the tips of the impeller into the case, its velocity is decreased and that sudden decrease in velocity causes an increases the pressure. GR 89 DO 014715 rONFTDFNTTAI COOLING TOWER 1020 SAFETY A ------------------------------------------------------------------------------------------------------------------------------------- PURPOSE: TO FAMILIARIZE YOU WITH THE BASIC SAFETY KNOWLEDGE REQUIRED WHILE OPERATING A COOLING TOWER AND RECIRCULATING COOLING WATER SYSTEM. RESOURCES: P&ID'S, EXPERIENCED PERSONNEL, PRESSURE VESSEL DATA SHEETS REQUIRED LEVEL OF PERFORMANCE: 100% CORRECT OBJECTIVES: 1. State the hazards of the following chemicals A. HCL 'B. Chlorine C. Treatment Chemicals 2. State the procedure to be followed in the case of inhalation of the following gases. A. Chorine B. HCL 3. State the reasons the following areas are restricted. Also explain the restrictions. A. Tower Internal Walkway B. Fan Shroud Area C. Chemical Addition Area D. Acid Injection Area E. Chlorine Injector 4. State the hazards to plant personel in the cooling tower area created by the following. A. Wet Surface B. I ce C. Rotating Equipment frO 01471^ rONFTDFNTTAI ( COOLING TOWER 1020 PROCESS FAMILIARIZATION TANKS AND VESSELS PURPOSE: TO FAMILIARIZE YOU WITH THE PURPOSE, DESIGN, AND OPERATION OF MAJOR TANKS AND VESSELS IN YOUR AREA. UPON COMPLETION, YOU WILL BE ABLE TO POINT OUT (ON A BLANK DRAWING) THE INTERNAL AND EXTERNAL COMPONENTS (FLANGES, TAPS, BAFFLES, ETC) AND EXPLAIN THEIR FUNCTIONS. RESOURCES: P&ID'S, EXPERIENCED PERSONNEL, PRESSURE VESSEL DATA SHEETS REQUIRED LEVEL OF PERFORMANCE: 100% CORRECT* 1 OBJECTIVES: 1. Locate the following tanks and vessels in your area and explain their purpose. Include inlet and outlet service flows, destinations and product content (shell & tube). A. T-1020 (HCL SUPPLY TANK) B. T-1021 (TREATMENT CHEMICALS TANK) C. CL-1020 (CHLORINATOR) D. V-1020 (FILTER) E. CT-1020 (COOLING TOWER) 2. Draw a simplified diagram of the equipment listed above and label the parts in their appropriate location. 3. List all the places we will supply cooling tower water to. 4. What is the purpose of the 8" line that ties into the cooling water return header. 5. What is the purpose of the 3" line that comes off of the return header and ties into the permitted outfall line. 6. State the purpose of the vent line on T-1020. 7. State where T-1020 gets its feed from. 8. State the purpose of the 3" line off the top of T-1020 to the permitted outfall. DO 014717 CONFTDFNTTAI COOLING TOWER 1020 COOLING SYSTEM FUNCTIONS -( ----------------------------------------------------------------------------------------------------------------------------------------------------------PURPOSE: To Familiarize you with how a cooling tower functions as a thermal management system to reject heat RESOURCES: Experienced Personnel, Operating Manuals REQUIRED LEVEL OF PERFORMANCE: 100% CORRECT OBJECTIVES: 1. State how a cooling tower rejects heat. 2. State the definitions of the following terms A. Blowdown B. Evaporative losses C. Induced Draft D. Fouling E. Scale F. PH 3. State the reason for blowdown of a cooling water system. 4. Describe the effect of CL2 as a biocide with respect to the PH of the system. Oo CO/VP Tr^NTTAl COOLING TOWER 1020 PROCESS FAMILIARIZATION ( VALVE OPERATION PURPOSE: TO FAMILIARIZE YOU WITH THE LOCATION, TYPE, OPERATION AND PURPOSE OF ALL VALVES USED IN YOUR AREA. CONTROL VALVE OPERATION WILL BE COVERED IN "CONTROL AND SENSING SCHEMES" SECTION. RESOURCES: PLANT FLOW SHEETS, EXPERIENCED PERSONNEL, PICS DISPLAY REQUIRED LEVEL OF PERFORMANCE: 100% CORRECT OBJECTIVES: 1. PHYSICALLY LOCATE, OPERATE (AS APPLICABLE), AND STATE THE FUNCTION OF ALL VALVES IN THE COOLING TOWER AREA. A. AO(512) T-1020 LEVEL CONTROL VALVEB. AO(511) VALVE TO OUTFALL OR TO T-510 C. AO(502) PROCESS H20 MAKE UP D. DO(513) HCL SUPPLY TO T-1020 E. DO(504 ) 3 WAY VALVE TO OUTFALL OR T-510 2. GIVEN ANY VALVE, STATE IF OPENED OR CLOSED. 3. MANUAL VALVES ASSOCIATED WITH CT-1020 ARE AS FOLLOWING: CL-1020 (CHLORINATOR) A. DOUBLE BLOCK AND BLEED ON CTW TO CL-1020. B. CHLORINE TO CL-1020. T-1020 (HCL) A. B/V UPSTREAM OF AOV ON INLET LINE TO T-1020. B. DOUBLE BLOCK AND BLEED UPSTREAM OF LCV OR FCV TO CT-1020. C. MANUAL BYPASS AROUND LCV. T- 1 02 1 (TREATMENT CHEMICAL) A. 2" DRAIN UNDER TANK. B. (2) B/V UPSTREAM OF P-1021. C. (1) BLEED VALVE AT P-1021. COOLING TOWER (CT-1020) A. (3) SUCTION B/V TO P-1020 A,B,& C. B. (3) DISCHARGE B/V ON P-1020 A,B, & C. C. B/V ON RECIRCULATION. D. B/V ON RETURN COOLING WATER HIGH & LOW POINT TIE-IN TO CT-1020. E. B/V OFF COOLING TOWER WATER RETURN TO CL-1020. F. 3" B/V UPSTREAM FCV TO THE OUTFALL. DO 014719 CONFTOFNTTAl COOLING TOWER 1020 PROCESS FAMILIARIZATION ( MECHANICAL EQUIPMENT PURPOSE: TO FAMILIARIZE YOU WITH THE FUNCTION, LOCATION, AND MAINTENANCE OF THE MECHANICAL EQUIPMENT IN YOUR AREA. UPON COMPLETION, YOU WILL BE ABLE TO PHYSICALLY LOCATE AND STATE THE FUNCTION AND MAINTENANCE REQUIREMENTS OF ALL MECHANICAL EQUIPMENT IN YOUR AREA. RESOURCES: EXPERIENCED PERSONNEL, EQUIPMENT MANUALS, DATA SHEETS REQUIRED LEVEL OF PERFORMANCE: 100% CORRECT* 1 OBJECTIVES: 1. PHYSICALLY LOCATE AND EXPLAIN THE OPERATION AND FUNCTION OF THE FOLLOWING: A. P-1022 B. P-1020 A/B/C C. FA-1020 A/B (DO(502 ) , DO(512) & DO(522)) (DO(501) & DO(511)) 2. EXPLAIN HOW THE FANS ARE CONTROLLED. (AO(501) & AO(521)) 3. PHYSICALLY LOCATE THE FOLLOWING ON THE ABOVE LISTED PUMPS. A. FIELD SWITCH B. MAIN SWITCH GEAR C. SUCTION AND DISCHARGE BLOCK VALVES D. BLEED E. SEAL PURGE (IF APPLICABLE) F. TEMPERATURE TRANS (IF APPLICABLE) 4. PHYSICALLY LOCATE THE FOLLOWING ON THE ABOVE LISTED FANS ITEM-1 A. FIELD SWITCH B. MAIN SWITCH GEAR C. VIBRATION TRANSMITTER/PROBE 5. STATE HOW THE FANS ARE CONTROLLED. DO 0147P0 CONFTDFNTT Al COOLING TOWER 1020 PROCESS FAMILIARIZATION ( CONTROL AND SENSING SCHEMES PURPOSE: TO GIVE YOU A GOOD UNDERSTANDING OF THE CONTROL AND SENSING SCHEMES THE CT-1020 AREA, INCLUDING LOCATION AND PURPOSE OF KEY INSTRUMENTATION. RESOURCES: P&ID'S, EXPERIENCED PERSONNEL REQUIRED LEVEL OF PERFORMANCE: 100% CORRECTI. OBJECTIVES: 1. EXPLAIN THE FUNCTION OF THE FOLLOWING CONTROLLERS AND HOW THEY OPERATE. A. AO(512) T-1020 LEVEL CONTROL VALVE ' B. AO(511) VALVE TO OUTFALL OR TO T-510 C. AO(502 ) PROCESS H20 MAKE UP D. DO(513) HCL SUPPLY TO T-1020 E. DO(504 ) 3 WAY VALVE TO OUTFALL OR T-510 2. PHYSICALLY LOCATE THE FOLLOWING INSTRUMENTATION AND EXPLAIN THEIR FUNCTION. ALSO, STATE THE CONTROL VALVE THEY ARE ASSOCIATED WITH . A. AI(506) T-1020 LEVEL B. AI(516) T-1021 LEVEL C. All 504,514) CT-1020 SUMP LEVEL D. AI(581 ) AIR INLET TEMP. FOR FAN CT-1020 A E. AI(591 ) AIR INLET TEMP. FOR FAN CT-1020 B F. AI(583) PROCESS H20 RETURN TEMP. G. AI(592 ) CT-1020 SUMP TEMP. H. AI(505 ) CT-1020 RETURN HEADER ORGANIC ANALYZER I. AI(526) FLOW TO OUTFALL J. AI(512) PROCESS H20 MAKE UP FLOW TO CT-1020 K. AI(503,513,523 ) P-1020 A/B/C AMPS L. AI(515 ) CT-1020 PH ANALYZER M. AI(525) CT-1020 PUMP DISCHARGE PRESSURE ?* N. AI ( 521 ) T-102(? LEVEL 3. DRAW A DETAILED DIAGRAM OF THE SYSTEM,INCLUDING ALL CONTROLLERS AND INSTRUMENTATION IN ITEMS *1 AND *2 DO 014771 OONFTDFNTTAt COOLING TOWER 1020 CONTROL AND SENSING SCHEMES (MOD V OPERATIONS) PURPOSE: TO GIVE YOU A GOOD UNDERSTANDING OF THE MOD CONTROL AND SENSING SCHEMES THE CT-1020 AREA. UPON COMPLETION'YOU SHOULD BE ABLE TO START UP THE SYSTEM USING THE MOD AND EXPLAIN WHAT TAKES PLACE IN EACH STEP. RESOURCES: P&ID'S, EXPERIENCED PERSONNEL REQUIRED LEVEL OF PERFORMANCE: 100% CORRECT OBJECTIVES: 1..WITHOUT USING THE ENGLISH LANGUAGE, BE ABLE TO SUMMARIZE WHAT OCCURS IN EACH STEP, USING THE STEPPING DIAGRAM. 2. START UP CT-1020 ON THE MOD AND EXPLAIN WHAT IS TAKING PLACE. 3. EXPLAIN ANY GIVEN ALARM. 4. USING THE MOD DEMONSTRATE ENERGIZING A FAN 5. DEMONSTRATE HOW TO SHUT THE SYSTEM DOWN USING THE MOD 6. CHANGE ANY GIVEN SETPOINT. 7. USING THE MOD DEMONSTRATE HOW TO SWAP MP-1020'S. 8. BE ABLE TO ANSWER ALL THE QUESTIONS ON THE COOLING TOWER SIMULATION SCRIPT DO 0147?? CONFTDFNTTAl COOLING TOWER 1020 PROCESS FAMILIARIZATION ( AREA HAZARDS & PROTECTIVE MEASURES PURPOSE: TO FAMILIARIZE YOU WITH THE HAZARDS AND PROTECTIVE MEASURES TO REDUCE THOSE HAZARDS IN YOUR AREA. RESOURCES: S&LP, EXPERIENCED PERSONNEL, SAFETY PROCEDURES REQUIRED LEVEL OF PERFORMANCE: 100% CORRECT OBJECTIVES: 1. STATE THE CHEMICAL HAZARDS ASSOCIATED WITH CT-1020,CL-1020, T-1020 & T-1021 2. STATE THE HAZARDS OF ROTATING EQUIPMENT 3. STATE THE ELECTRICAL HAZARDS ASSOCIATED WITH CT-1020. 4. STATE ENVIRONMENTAL PROBLEMS AND ACTIONS TO BE TAKEN IN EVENT OF THE FOLLOWING SPILLS: A. HCL B. CHLORINE C. TREATMENT CHEMICALS 5. STATE THE PROTECTIVE EQUIPMENT REQUIREMENTS FOR MAINTENANCE ON THE FOLLOWING. A. HCL TANK AND LINES B. CL2 LINES C. CHEMICAL ADDITION LINES 00 014773 OONFTDFNTTAI COOLING TOWER 1020 PROCESS FAMILIARIZATION OPERATING DISCIPLINE ( PURPOSE: TO GIVE YOU A GOOD UNDERSTANDING OF OPERATING PARAMETERS OF THE MAJOR EQUIPMENT IN YOUR AREA. THE PROBLEMS ASSOCIATED WITH THE PROCESS BEING OUT OF OPERATING . PARAMETERS. RESOURCES: EXPERIENCED PERSONNEL, OPERATING MANUALS,MOD 5 PROGRAM REQUIRED LEVEL OF PERFORMANCE: 100% CORRECT OBJECTIVES: 1. STATE THE NORMAL OPERATING PARAMETERS OF THE FOLLOWING. A. AI(506) T-1020 LEVEL B. AI(516 ) T-1021 LEVEL C. AI(504,514 ) CT-1020 SUMP LEVEL D. AI(581 ) AIR INLET TEMP. FOR FAN CT-1020 A E. AI(591 ) AIR INLET TEMP. FOR FAN CT-1020 B F. AI(592 ) CT-1020 SUMP TEMP. G. AI(505 ) CT-1020 RETURN HEADER ORGANIC ANALYZER H. AI(526) FLOW TO OUTFALL I. AI(515 ) CT-1020 PH ANALYZER J. CONDUCTIVITY K. HCL CONCENTRATION L. CALCIUM 2. STATE THE RESULTS OF HIGH OR LOW PARAMETERS AND THE RESULTS IF IT REMAINS HIGH OR LOW. STATE WHAT ACTION YOU WOULD TAKE TO BRING THESE BACK TO WITHIN NORMAL OPERATING PARAMETERS. 3. EXPLAIN HOW HIGH COOLING TOWER TEMPERATURE AFFECTS PLANT OPERATIONS AND EFFICIENCY. 4. EXPLAIN WHAT THE FOLLOWING IS USED FOR AND THEIR PARAMETERS. A. HCL B. PHOSPHATE C. CL2 (38K) 5. LIST THE TRIPS FOR THE FOLLOWING EQUIPMENT: SEE MOD 5 CODE A. FA-1020 A/B/C B. CT-1020 00 014774 OONFTDFNTTAI COOLING TOWER 1020 SPECIAL SKILLS 4 ------------------------------------------------------------------------------------------------------------------------------ PURPOSE: TO ALLOW YOU TO DEMONSTRATE YOUR ABILITY TO PERFORM TASKS IN A LOGICAL AND SAFE SEQUENCE, USING ESTABLISHED JOB PROCEDURES. RESOURCES: PROCEDURES, EXPERIENCED PERSONNEL,LAB SAMPLE PROCEDURE REQUIRED LEVEL OF PERFORMANCE: 100% CORRECT OBJECTIVES: 1. GIVEN ANY OF THE FOLLOWING JOB PROCEDURES/CHECKLIST DEMONSTRATE/SIMULATE IN THE FIELD COMPLETING EACH TASK IN A LOGICAL SAFE MANNER. ' A. B. C. D. E. F. G. H. I. ADDING BETZ CHEMICAL (38K) TO CT-1020 UNLOADING BETZ TRUCKS CONTAINING COOLING TOWER CHEMICALS MAKING A COOLING TOWER ENTRY DEMONSTRATE LINING UP SYSTEM FOR START UP DEMONSTRATE SWAPPING PUMPS (FIELD) LINE UP T-1021 DEMONSTRATE STARTING AND STOPPING A FAN ADJUST CL2 FLOW TO CL-1020 ADJUST 38K TO COOLING TOWER WATER SMALL METERING PUMP 2. DEMONSTRATE RUNNING THE FOLLOWING SAMPLES FOR THE COOLING TOWER SYSTEM. A. PHOSPHATE B. CL2 C. PH D. CONDUCTIVITY E. CALCIUM 3. LIST THE STEPS (IN SEQUENCE) NECESSARY TO MAKE THE FOLLOWING EQUIPMENT READY FOR MAINTENANCE: A. COOLING TOWER 1020 B. FA-1020 A/B/C C. P-1022 D. P-1020 A/B/C 4. DEMONSTRATE THE PROPER PROCEDURE FOR CLEARING THE PROCESS LINES FOR MAINTENANCE. A. HCL LINES B. CL2 LINES D Ol4?pt- COOLING TOWER 1020 ( OPERATIONS ROUTINE CHECKLISTS PURPOSE: TO FAMILIARIZE AND ALLOW YOU TO DEMONSTRATE COMPLETING ROUTINE CHECKLISTS IN YOUR AREA. RESOURCES: EXPERIENCED PERSONNEL, ROUND SHEETS, OPERATING MANUALS REQUIRED LEVEL OF PERFORMANCE: 100% CORRECT OBJECTIVES: 1. DEMONSTRATE MAKING A ROUND USING CT-1020 ROUND SHEET, EXPLAINING EACH ITEM AND ITS IMPORTANCE. Do D'O/vo rDr/v COOLING TOWER 1020 ( OPERATIONS CAPACITY & EFFICIENCY PURPOSE: TO FAMILIARIZE YOU WITH THE CAPACITY AND EFFICIENCY IN THE COOLING TOWER AREA. REQUIRED LEVEL OF PERFORMANCE: 100% CORRECT* 1 OBJECTIVES: 1. STATE HOW EACH OF THE FOLLOWING AFFECT EFFIECIENCY. A. HEADER LEAK B. SLUDGE BUILD UP IN THE SUMP C. PITCH ON THE FAN BLADE D. 30 DEGREE OUTSIDE TEMPERATURE DROP OR RISE E. EXCESS COOLING TOWER BLOWDOWN DO 014707 rONFTDFNTTAI COOLING TOWER 1020 OPERATIONS ( EMERGENCY PROCEDURES PURPOSE: TO FAMILIARIZE YOU WITH EMERGENCY CONDITIONS AND PROCEDURES IN THIS AREA. RESOURCES: EMERGENCY STARTUP & SHUTDOWN PROCEDURES, PLANT PERSONNEL, REQUIRED LEVEL OF PERFORMANCE: 100% CORRECT1 OBJECTIVES: 1. GIVEN AN EMERGENCY SITUATION AND SHUTDOWN PROCEDURE IN THIS AREA, SIMULATE (IN SEQUENCE) SHUTTING THE AREA DOWN. EXPLAIN WHAT IS OCCURRING IN EACH STEP. INCLUDE PRECAUTIONARY MEASURES SUCH AS WASHING OUT AND PURGING EQUIPMENT. YOU WILL BE TESTED ON THE FOLLOWING: A. LOSE FA-1020 A B. LOSE P-1020 C. FIRE D. LOW WATER LEVEL IN SUMP 2. YOUR AREA HAS JUST EXPERIENCED A POWER FAILURE. EXPLAIN YOUR ACTIONS. (POWER IS STILL OFF). YOUR ANSWER SHOULD BE STEP-BY-STEP. DO 014708 OONFTDFNTT Al COOLING TOWER 1020 PROBLEM ANALYSIS PURPOSE: TO ALLOW YOU TO DEMONSTRATE YOUR ABILITY TO HANDLE ABNORMAL SITUATIONS (UPSETS) WHEN THEY OCCUR IN YOUR AREA. RESOURCES: PROCEDURES, EXPERIENCED PERSONNEL, OPERATING MANUALS REQUIRED LEVEL OF PERFORMANCE: 100% CORRECT OBJECTIVES: 1. LIST THE SEQUENCE OF STEPS YOU WOULD TAKE IF THE FOLLOWING CONDITION WERE TO OCCUR. A. ORGANICS APPEAR IN SAMPLE B. PH LOW OR HIGH C. CHLORINE IS TOO HIGH OR LOW D. CONDUCTIVITY IS TOO HIGH E. PHOSHATE IS TOO HIGH OR TOO LOW F. PLUGGED CHLORINATOR 12/91 GR/CB CT1020MD.IPT oo 0147C9 OONFTDFNTTAI AREA ACIDSAFE.CMP ___ CONTRACTOR _____________ MINIMUM SAFETY EQUIPMENT REQUIRED IN C.M.P. ACID AREAS MEASUREMENTS WALK - THRU WORKING ON C-202 BTMS. E-212 H2S04 T/C RACK T--900 C-650 C-210 C-200 / C-201 BTMS. C-202 DECKS P-301 S C-S10 / R--ECO SLICKER SUIT / GOGGLES / RUBBER BOOTS, GLOVES SAME AS ABOVE SAME AS ABOVE SAME AS ABOVE SAME AS ABOVE SAME AS ABOVE GOGGLES GOGGLES GOGGLES GOGGLES FULL ACID SUIT SAME AS ABOVE SAME AS ABOVE SAME AS ABOVE SAME AS ABOVE SLICKER SUIT / GOGGLES RUBBER BOOTS, GLOVES SAME AS ABOVE FULL ACID SUIT SLICKER SUIT / GOGGLES RUBBER BOOTS. GLOVES SAME AS ABOVE * A r'JLL ACID SUIT IS REQUIRED TO DO ANY TYPE OF WORK ON GROUND LEVEL AROUND H2S0*i ACID RUMPS. ANY DEVIATION FROM THIS REQUIRES PLANT SUF'T. APPROVAL. Irlrc^r' tv ) * TO DO WORK ON INSTRUMENTAT101)/ IN AREAS REQUIRING A FULL ACID SUIT TO BE WORN, THE THIN RUBBER GLOVES/ARE PERMITTED. revised: 10/90 L. London /t-A_S 00 014730 OONETDENTIAI II. OBJECTIVES A. TO HAVE YOU BECOME VERY FAMILIAR WITH THE OPERATION OF THE COMBUSTIBLE GAS/ OXYGEN METERS. ALSO, TO MAKE YOU AWARE OF THE METERS' LIMITATIONS. B. TO BECOME PROFICIENT AT TEACHING OTHERS WHAT THEY NEED TO KNOW TO OPERATE THE METERS CORRECTLY. I DO 014731 f ONFTDFNTTAl III. ABOUT THE METER (actually two meters in one) A. OXYGEN - ELECTROCHEMICAL FUEL CELL THAT DEVELOPS A VOLTAGE WHICH IS PROPORTIONAL TO THE OXYGEN CONCENTRATION OF THE GAS PASSING THROUGH THE CELL. THE CELL IS DEPLETED OR USED UP AS OXYGEN MEASUREMENTS ARE MADE. B. COMBUSTIBLE - CATALYTIC BEAD IN CELL WHOSE TEMPERATURE IS CHANGED BY THE AMOUNT OF COMBUSTIBLESAS IN THE SAMPLE. AS THE TEMPERATURE IS CHANGED. ITS' RESISTANCE CHANGES. UNBALANCING ONE LEO OF A WHEATSTONE BRIDGE CIRCUIT COMPARED TO A SECOND BEAD WITHOUT CATALYST THAT WILL NOT REACT TO THE COMBUSTIBLE GAS. THIS TYPE OF CELL REQUIRES SOME OXYGEN (1 OX) FOR SUCCESSFUL OPERATION. j DO 014730 rONFTDFNTTAI I ; 00 0TA733 conft^nttA IV. TERMS A. LEL (LOWER EXPLOSIVE LIMIT - The least concentration of a combustible gas in air that will ignite B* VAPOR DENSITY - The weight of a Ras as compared to air. C. OXYGEN DIFICIENT OR RICH ATMOSPHERE The combustible gas sensor requires at least 10* oivRen and a maximum of 2V* oxygen to work accurately i i OO 014734 CONFIDFNTTAl OXYGEN DEFICIENT ATMOSPHERES & YOU OKY6FM IN AIR UPPROX. 21Z NORMAL) 12 - 18% AT RFST SIGNS K SYMPTOMS BREATHING & PULSE RATE INCREASED; COORDINATION POOR. 10 - 12% DEEP, FAST RESPIRATION; GIDDINESS; POOR JUDGEMENT; LIPS BLUE. 8 - 10% NAUSEA; VOMITING; INABILITY TO MOVE FREELY; UNCONSCIOUSNESS; ASHEN FACE. 6-8% 8 MINUTES - 100% FATAL 6 MINUTES - 50% FATAL 4 MINUTES - ALL RECOVER WITH TREATMENT 4% COMA IN 40 SECONDS; CONVULSIONS; RESPIRATION CEASES. 0% INDIVIDUAL IMMEDIATELY BECOMES UNCONSCIOUS; WILL RECOVER ONLY IF GOOD AIR IS IMMEDIATELY AVAILABLE WARNING: THE WARNING SYMPTOMS OF AN ATMOSPHERE DEFICIENT IN OXYGEN ARE COMPLETELY INADEQUATE AND, ALTHOUGH, A TRAINED OBSERVER MAY, WHEN ALERT, RECOGNIZE THE INCREASE IN PULSE AND RATE OF BREATHING IN TIME TO RETURN TO GOOD AIR, THE AVERAGE INDIVIDUAL FAILS TO RECONIZE THE DANGER UNTIL HE IS TOO WEAK TO SAVE HIMSELF. ESPECIALLY WHERE THE RETURN TO GOOD AIR INVOLVES CLIMBING STAIRS OR A LADDER. LEAN MIXTURE - aeter hind rises to i reading EXPLOSIVE MIXTURE - meter hand rises to reading in alarm zone (201 and above) in 10. in <0 y Ww -------- no 1LEL 100 RICH MIXTURE - meter hand goes full scale and then falls to zero or belov D0 01473ft 0ONFT0FNTTAI PRE-USE CALIBRATION CHECK OF BIO MARINE 902 t GASTECH GX-3 COMBUSTIBLE GAS/02 MONITORS 1 l' CHECK UNITS WITH HOSE & PROBE CONNECTED. 1 2. CHECK FILTER 6 WATER TRAP. SHOULD BE CLEAN AND DRY. 1 3` CHECK BATTERY VOLTAGE. NEVER CALIBRATE ANY METER WHILE PLUGGED INTO THE CHARGER. 1 4* CHECK PUMP FLOW AND ALARM. 1 5. CHECK OXYGEN READING IN AIR. SHOULD BE 21%. IF NOT, ADJUST TO READ 21%. 1 6. CHECK COMBUSTIBLE GAS ZERO. IF NOT ZERO, ADJUST TO READ ZERO. 1 7. INTRODUCE CALIBRATION GAS (2.5% METHANE IN AIR). COMBUSTIBLE GAS METER SHOULD GO UPSCALE TO 2.5% ON BIO MARINE UNITS OR TO 55% LEL ON GASTECH UNITS. IF READING IS INCORRECT, ADJUST WITH GAS SPAN POT TO OBTAIN PROPER READING. THE SPAN POT FOR BIO MARINE UNITS IS LOCATED ON TOP CONTROL PANEL. THE SPAN POT FOR THE GASTECH GX-3 UNIT IS LOCATED IN THE FRONT CHAMBER, SPAN POT #3. | 1 8* IF UNITS CANNOT BE ADJUSTED PROPERLY, OR IF YOU FEEL THE UNIT IS NOT OPERATING CORRECTLY, DO NOT USE IT. TAG THE UNIT AND SEND IT TO THE CENTRAL INSTRUMENT $HOP FOR A THOROUGH CHECKOUT AND REPAIR. PRE-USE CALIBRATION CHECK OF GASTECH 1214SMP COMBUSTIBLE GAS/02 MONITOR 1 1` CHECK UNITS WITH HOSE & PROBE CONNECTED. 2. CHECK FILTER & WATER TRAP. SHOULD BE CLEAN AND DRY. 3. PRESS RED "POWER" SWITCH TO TURN UNIT ON. THE'STATEMENT "GASTECHTOR ON - TAKE TO GAS FREE AREA" WILL SOUND AND DISPLAY WILL BLINK. THE UNIT DISPLAY WILL CONTINUE TO BLINK FOR A TWO MINUTE WARM-UP PERIOD. 4. AFTER THE TWO MINUTE WARM-UP PERIOD HAS ELAPSED, THE STATEMENT "PRESS ADJUST BUTTON" WILL SOUND. PRESS THE BLACK ADJUST BUTTON. UNIT SHOULD THEN READ 20.9% 0, and 0 COMBUSTIBLES. ANYTIME THE ADJUST BUTTON IS PRESSED THEREAFTER, THE UNIT WILL DISPLAY THE NUMBER OF BATTERY HOURS REMAINING. 00 014737 5. CHECK PUMP FLOW. OONFTDFNTTAI 6. INTRODUCE CALIBRATION GAS (2.5% METHANE IN AIR). METER SHOULD READ 55% LEL. IF NOT, ADJUST SPAN POT LOCATED ON SIDE OF UNIT AND MAKE METER READ 55%. 7. IF UNIT CANNOT BE ADJUSTED PROPERLY, OR IF YOU FEEL THE UNIT IS NOT OPERATING CORRECTLY, DO NOT USE IT. TAG THE UNIT AND cpwn TT TO THE CENTRAL INSTROMEUT SHOP F0R A THOROUGH CHECKOUT CHECKING FOR COMBUSTIBLE GAS IN INERT BACKGROUND USING SPECIAL FITTING ON STANDARD EXPLOSION METER 1. Calibrate unit without special fitting using 2.5X Methane In air cal. gas. Combustibles should read 55X LEL. If not, adjust span so that meter does read 55X LEL. Oxygen should read 2IX. 2. Put special fitting on unit and Introduce cal. gas again (2.5X Methane In air). Combustibles should read approximately 27.5X LEL. Oxygen should read 2IX. 3. Put 2.5X Methane In Nitrogen In unit. Combustibles should read about 27.5X LEL. Oxygen should read approximately I0.5X. 4. THE UNIT IS NOW READY TO BE USED. 5. After a line has been checked with a standard (without fitting) meter and the line has less than IOX oxygen, you would then use the special meter (with fitting) and check the line for combustibles. f 6. Always be aware of your oxygen reading when using the meter with the fitting on it. Your oxygen reading can tell you many things. For example, the oxygen reading taken without the fitting must differ from oxygen reading taken with the fitting in place. NOTE: ANY COMBUSTIBLE GAS READING OBSERVED WHILE USING THE UNIT MUST BE MULTIPLIED BY TWO TO OBTAIN THE ACTUAL XLEL. 2.5X Methane In Air DO 014738 OONFTDFNTTAI ONLY TRAINED AND CERTIFIED PERSONNEL ARE ALLOWEDT( USE DO 014739 CONFIDENT! Al, THE ONLY WAY TO TELL IF AN LXPLOSIfAETER IS GOOD IS T( PASS A CALIBRATED GASTHRU 11 .. DO 014740 OONFTDFNTTAI MAN! WHAT IS THAT STUFF? HE-X> t PERSONNEL CHOSEN AS SAFETY OBSERVERS SHOULD BE FAMILIAR VJITH COMPOUNDS FOUND IN "WE PLANT AND PLANT PRODUCTS ... ARE THEY FLAMMABLE ? HEAVIER OR LIGHTER THAN AIR? TOXIC? CORROSIVE T>0 01474-] OONFTDFNTTA! METERS ARE NOT MSI&NED TO TAKE LIQUID SAMPLES VIIK'D "DIRECTION r~rn r> WHEN ACTING AG SAFETY OBSERVER o Z) 2o n^ 2 NJ Always look for potential hazards H -Ei --< U> FROM SURROUNDING AREAS CAUflON MITAO&EN "PAD iNUSff Ion FLAM HEM* METERS SHOULD NOT BE USED TO MEASURE COMBUSTIBLE GAS IN ATMOSPHERES THAT ARE OXYGEN DEFICIENT ' ^roV?4'' F*TTA, '--GAS TECT-ORR CRAZEEE TAKE TO BLASSS AREA TETRA ETHYL LEAD OR SILICON COMPOUnDS POISON COKBUSTIBLE r.a* QCMQfYRR ^ONFTDFNTT BE" ALERT! 2*10 PM THU. , 26 APR., 1990 PAGE 1 SPECIFICATIONS CATALOG PROFILES 10 - 2000 PROFILE #* DETERMINANT #* DESCRIPTION* LOU SPEC* HIGH SPEC* 102 1 DIMETHYL ETHER 2 METHYL CHLORIDE 3 METHANOL 103 I DIMETHYL ETHER 2 METHYL CHLORIDE 3 METHANOL 4 UT* HCL 109 i METHYLENE CHLORIDE 2 UINYLIDENE CHLORIDE 3 TRANS 4 M4 CAREON TET 5 CHLOROFORM . a AMYLENE 7 CIS 8 BRCLME 9 A-DI H1 PPM HCL 10.00 2 0.00 : - rr5 m PPM HCL 10.00 l FF'M WATER 80 . j0 METHANE 10.00 4 EThYLENE 2 00 ETHANE 2.0 0 6 ACETYLENE 2 00 7 DIMETHYL ETHER 1o 3 0 8 METHYL CHLORIDE 9 8 0 C 0 0.0 1 020UoC . 9 UINYL CHLORIDE 2 5.0 0 i 0 METHANOL 10 0 0 i 1 METHYLENE CHLORIDE 50,00 12 ETHYL CHLORIDE 50.0 0 i 3 FREON 12 1.00 14 PROPANE/BUTANE /w\ ,, J"n' -I /. f r I 1;/1y/ 1 METHYLENE CHLORIDE 930000,0 1020000. 2 ETHYL CHLORIDE 5.00 3 METHYL BROMIDE 4 UINYLIDENE CHLORIDE 5 ALLYL CHLORIDE 6 TRANS 5.00 5 0.00 5.00 60 , 'J 0 D 014747 ^ONFTDrNTTA! 112 113 114 1i 1 i/ 112 118 2io pm ' ihu , 26 "Hpk . , ~iyyu SPECIFICATIONS CATALOG DETERMINANT #* 7 8 9 10 1 2 3 4 5 DESCRIPTION* : > /. y Tel------------------- ------- CHLOROFORM Ml/01 A-DI/M4 <?* c. METHYLENE CHLORIDE A-DI CHLOROFORM CIS M4 |-HbL 4 PROFILES 10 - 2000 LOW SPEC* HIGH SPEC* 1 , 00 50.00 5.00 5.00 *0,0 K.< 2.0000 . 0050 . 0025 .0100 ,ro 10.0000 1 2 3 `4 " 5 6 1 2 3 4 6 PPM CHLORINE METHYLENE CHLORIDE A-Di CHLOROFORM CIb 114 T~ 'T~ METHYLENE CHLORIDE a-d: L ;i L 0 K' oi` u hi t1 CIS M4 PPM CHLORINE 600.00 1500.00 . 0200 .6)5^ . 0005 600.00 . 0200 .0150 . 0005 1500.00 1 PPM Uh^ER 2 PPM HCL 20.00 5.00 1 methylene CHLORIDE 0.00 50.00 UINYLIDEnE CHLORIDE 0 . 00 10.00 3 TRANS 6.00 10.00 4 M4 CARBON TET 0.00 200.00 3 CHLOROFORM 980000.0 1020000. 6 AMYLENE 7 CIS 0.00 30 00 8 BRCLME ISO . 00 250.00 9 A-DI 0.00 2 5.00 10 PPM WATER 0.00 2 5.00 11 PPM HCL 10.00 S.c 12 PPM CHLORINE 1 . METHYLENE CHLORIDE. On 74748 CONF T0FNTJAI 2*10 PM THU . , '26 ' HVK . , ivyu SPECIFICATIONS CATALOG PROFILE #* 113 DETERMINANT # 2 3 4 5 6 7 8 9 10 11 12 13 DESCRIPTION* C - `pi /tr/n ; TRANS A-DI CHLOROFORM TCE METHYL CHLORIDE UINYL CHLORIDE CIS EDC M4 B-TRI UNSYM-TET SYM-TET 1 19 1 PPM UATER 2 PPM HCL 1 WT-2 HCL 2 DIMETHYL ETHER 3 METHYL CHLORIDE 4 METHANOL r noc PROFILES 10 - 2000 LOU SPEC* HIGH SPEC* 1.8000 M' 80.00 7.00 )# +3 123 124 1 WTH HCL 2 DIMETHYL ETHER 3 METHYL CHLORIDE 4 METHANOL _ * ^; * * 1 METHYL CHLORIDE 2 METHANOL 3 METHYLENE CHLORIDE 4 M4 CARBON TET 3 CHLOROFORM 6 UTY HCL 1 DIMETHYL ETHER 2 METHYL CHLORIDE 3 METHANOL ' 1 WTX H2S04 2 DIMETHYL ETHER 3 METHYL CHLORIDE 4 METHANOL \% 4* 3s3 1 ff'*' S ft*' 0&L *7^ f^rrv vo'/0 -- ys /C DO 014749 OONFTDFNTTAI SMPLP01 UNIT 1 2:14 PM THU., 26 APR., 1990 SAMPLE POINTS 2 C202 BTMS 3 C610 REFLUX 10 C 840 BTMS 11 C 850 OVH 12 C 802 REFLUX 13 C 802 BTMS 14 T 803 A 15 T 803 B 16 C 803 BTMS 17 C 806 OVH 18 C 806 BTMS 19 Ml FORWARD 20 C 200 21 C 201 22 C 610 BTMS 23 C 650 BTMS 24 D 650 25 C 210 BTMS 26 T 104 A 27 T 104 B 28 T 814 29 T 511 30 T 514 31 T 804 A 32 T 804 B 33 T 100 34 T 101 35 T 103 36 T 1050 37 T 810 38 T 808 39 T 805 40 T 806 A 41 T 806 B 42 T 102 43 T 303 44 T 1010 45 T 251 46 D 455 47 Ml TRUCKS 49 M2 TRUCKS 50 R 750 CONDENSATE 51 M3 TRUCKS 53 M2 BARGES 54 M3 BARGES 55 METHANOL BARGES 56 CHO STANDARD 57 CHI STANDARD 58 CH2 STANDARD 59 CH3 STANDARD PAGE 1 DISPLAY UNIT CODE PROFILE 12 13 1 10 1 11 1 12 1 13 1 14 1 15 1 16 1 17 1 18 1 19 1 20 1 21 1 22 1 23 1 24 1 25 1 26 1 27 1 28 1 29 1 30 1 31 1 32 1 33 1 34 1 35 1 36 1 37 1 38 1 39 1 " 40 1 41 1 42 1 43 1 44 1 45 1 46 1 47 1 49 1 50 1 51 1 53 1 54 1 55 1 56 1 57 1 58 1 59 102 103 110 111 112 113 114 115 116 117 118 119 120 121 122 123 124 125 126 127 128 129 130 131 132 133 134 135 136 137 138 139 140 141 142 143 144 145 146 147 149 150 151 153 154 155 156 157 158 159 DO 014750 OONFTDFNTTA! SMPLP01 UNIT 1 CMP 1 CMP THU ., 26 APR., 1990 SAMPLE POINTS 60 CH4 STANDARD 61 Ml R/C HEEL SAMPLE 1 62 Ml R/C HEEL SAMPLE 2 63 Ml R/C HEEL SAMPLE 3 64 Ml R/C HEEL SAMPLE 4 65 Ml R/C HEEL SAMPLE 5 66 Ml R/C HEEL SAMPLE 6 67 CH5 STANDARD 68 CH6 STANDARD 69 CH7 STANDARD 70 CH8 & 9 STANDARD 71 Ml R/C FNL SAMPLE 1 72 Ml R/C FNL SAMPLE 2 73 Ml R/C FNL SAMPLE 3 74 Ml R/C FNL SAMPLE 4 75 Ml R/C FNL SAMPLE 5 76 Ml R/C FNL SAMPLE 6 78 CH10 STANDARD 79 CH11 STANDARD 80 CH11 STANDARD B 81 M2 R/C FNL SAMPLE 1 82 M2 R/C FNL SAMPLE 2 83 M2 R/C FNL SAMPLE 3 84 M2 R/C FNL SAMPLE 4 91 M3 R/C FNL SAMPLE 1 92 M3 R/C FNL SAMPLE 2 93 M3 R/C FNL SAMPLE 3 94 M3 R/C FNL SAMPLE 4 95 M3 R/C FNL SAMPLE 5 96 M3 R/C FNL SAMPLE 6 99 RECHARGE H20 MACHINE PAGE 2 DISPLAY UNIT CODE prof; 1 60 1 61 1 62 1 63 1 64 1 65 1 66 1 67 1 68 1 69 1 70 1 71 1 72 1 73 1 74 1 75 1 76 1 78 1 79 1 80 1 81 1 82 1 83 1 84 1 91 1 92 1 93 1 94 1 95 1 96 1 99 160 161 162 163 164 165 166 167 168 169 170 171 172 173 174 175 176 178 179 0 181 182 183 184 191 192 193 194 195 196 200 DO 0147M CONFTDFNTT Al P Mb F L,L 0 1 ' i K C i' i l_ Yt : I 02 10Y 10 9 .1 .. . 2:10 F'M THU , 2 <5 APR., 1990 SPECIFICATIONS CATALOG DETERMINANT # = DESCRIPTION: PAGE 1 PROFILES 10 - 2000 LOU SPEC' HIGH SPEC: 3 DIMETHYL ETHER 2 METHYL CHLORIDE 3 METHANOL 1 DIMETHYL ETHER 2 METHYL CHLORIDE 3 METHANOL 4 WT'K HCL 1 METHYLENE CHLORIDE 2 UINYLIDENE CHLORIDE 3 TRANS 4 M4 CARBON TET [/ CHLGROFCRM c AMY LINE C1S fj BRCLME A - DI /' X > F'M `HCL 10.00 20.00 Ai> 30. *> - FTTi HCL 10.00 F PM WATER SO . 00 METHANE <4 ETHYLENE 10.00 2 00 El H A i\ E 2 . OU 0 ACETYLENE 2 00 / DIMETHYL ETHER 10,00 b METHYL CHLORIDE 9 8 0 0 0 0.0 1 0 2 0 0 0 C. 9 UINYL CHLORIDE 2 5.0 0 1 'J METHANOL 10.00 , 1 METHYLENE CHLORIDE b 0.0 0 1 4 ETHYL CHL.OF IDE 5 0.0 0 i 3 FREON 12 1,03 PROPANE/BUTANE 1 METHYLENE CHLORIDE 980000.0 1020000. ETHYl chloride 5 . 00 */ METHYL BROMIDE 5.00 4 UINYLIDENE CHLORIDE 50.00 b ALLYL CHLORIDE 5.00 6 TRANS 60.00 00 014750 C.ONFIOFNTTW rib.'U-o: 2=10 PM THU, 26 APR , , 1990 SPECIFICATIONS CATALOG DETERMINANT #: DESCRIPTION: PAGE 2 PROFILES 10 - 2000 LOU SPEC: HIGH SPEC 7 fCE b CHLOROFORM 9 Ml/Ul 10 A-DI/M4 1 . 00 50.00 5,00 5.00 SO, 1C 1 METHYLENE CHLORIDE .0050 2 A-DI .0025 3 CHLOROFORM 4 CIS .0100 ,V?ro 5 M4 2,0000 10.0000 1 PPM CHLORINE 600.00 1500.00 2 METHYLENE CHLORIDE .0200 . ClS 3 A L) 1 ' 4 CHLOROFORM 5 CIS .0005 6 M4 1 M 11 H Y L E N E CHLORIDE, . 0200 ,OiFo / A-0I t> L:1 l 0 A i,! DRM 4 CIS M4 .0005 6 fPM CHLORINE 600 , 00 1500.00 L PPM WrlTER 2 PPM HCL 2 0.00 5 . 0C 1 MLiHYlENE CHLORIDE 0 , 00 50 . 00 * UINYLIDENE CHLORIDE 0 , 00 10.00 3 TRANS 6.00 10.00 - M4 CARLDN TET 0.00 200 . 00 5 CHLOROFORM 980000.0 1020000, 6 AMYLENE 7 CIS 0.00 30.00 b BRCLME 150.00 250.00 9 A-DI 0.00 2 5.00 10 PPM WATER 0,00 25.00 1 1 PPM HCL 10.00 S.t 1 2 PPM CHLORINE 1 METHYLENE CHLORIDE 014750 rNFTOFNTTA| --------- ........... - --- --------------------------------------- _ ----------- mspecoi 2=10 PM THU , 26 APR., 1990 SPECIFICATIONS CATALOG PAGE 3 PROFILES 10 - 2000 F'Kui-'ILE ft* 1 13 DETERMINANT # 2 3 4 3 6 7 8 9 10 11 12 13 DESCRIPTION' r" TRAMS fl-Dl CHLOROFORM TL'E METHYL CHLORIDE UINYL CHLORIDE CIS EDC M4 B-TR] UNSYM-TET SYM-TET LOU SPEC' HIGH SPEC' 1.8000 /, 0*>l J 1? 1 PPM WATER 2 ' PPM HCL 80.00 7.00 120 1 WTfT HCL V DIMETHYL ETHER 3 METHYL CHLORIDE 4 METHANOL )g t* A3 i. 1 1 UT* HCL / DIMETHYL. ETHER 7 methyl chloride <4 MET i i h i i u i. +* 3v3 /2 14 METHYL CHLOKjUF. V METHANOL METHYLENE CHLORIDE 4 M4 CARBON TET V, CHLOROFORM 6 WT* HCL ) f>fy^ Sff** 12 124 1 DIMETHYL ETHER 2 METHYL CHLORIDE 3 METHANOL i 1 UT'/, H2S04 2 DIMETHYL ETHER 3 METHYL CHLORIDE 4 METHANOL OrtL *7 fprr\ D0 014754 OONFTDFNTT Al Ltd 2=10 PH THU. 26 APR., 1990 SPECIFICATIONS CATALOG KUHLt #i 125 DETERMINANT # DESCRIPTION: ; -' _/ UTS HCL PAGE 4 PROFILES 10 - 2000 LOU SPEC: HIGH SPEC ? MS**-*- j1 6 2 B 9 / 10 / 11 11 `.1 3 J4 IF METHANE ETHYLENE ETHANE ACETYLENE DIMETHYL ETHER METHYL CHLORIDE UINYL CHLORIDE METHANOL METHYLENE CHLORIDE ETHYL CHLORIDE FREON 12 PROPANE/BUTANE PPM UA7ER PPM HCL UISUAL APPERANCE 980000.0 U/U 10.00 5 00 5.00 10.00 10.00 1020000. 50.00 50.00 50.0 0 50.00 1 . 00 80.00 7 . 00 U/U MCI HAN[ 10.00 ETHYLENE 5 . 00 ETHANE 5.00 4 ACETYLENE 10,00 i., DIMETHYL El HER 10.00 t h E T H Y L CHLORIDE 980 0 00.0 10 2 0 U 0 0 . OINYL CHLORIDE 5 0.00 M E T H AIIJ L 50 . 00 ML I H YL L N [ CHIP P J. DL 5 0.00 ETHYL CHLORIDE 50 . 00 F KL0N 1 2 1.00 PROPANE/BUTAND 1. PPM UATER 80,00 .1 i PPM HCL 7 . OC 1 F UISUAL APPERANCE U/U U/U 1 METHANE 10.00 2 ETHYLENE 5*. CO 3 ETHANE 5 . 00 4 ACETYLENE 10.00 3 DIMETHYL ETHER 10.00 6 METHYL CHLORIDE 980000.0 1020000. 7 UINYL CHLORIDE 5 0.00 B METHANOL 50 , 00 9 METHYLENE CHLORIDE 5 0.00 i 0 ETHYL CHLORIDE 5 0.0 0 DO 014755 OONFTDFNTTAI 115 F' r L 0 1 2=10 PH THU. 26 APR., 1990 SPECIFICATIONS CATALOG PAGE 5 PROFILES 10 - 2000 PROFILE #= DETERMINANT #* DESCRIPTION* LOU SPEC* HIGH SPEC* 128 1 1 FREON 12 12 PROPANE/EUTANE 13 PPM WATER 14 PPM HCL 15 UISUAL APPERANCE U/U 1 . 00 80.00 7.00 U/U 129 1 METHANE 10.00 2 ETHYLENE 5,00 3 ETHANE 5.00 4 ACETYLENE 5 DIMETHYL ETHER 10.OC 10.00 6 METHYL CHLORIDE 960000.0 1020000. 2 UINYL CHLORIDE 50.00 B METHfiNOL .. 50,00 METHYLENE CHLORIDE ' 50.00 iu ETHYL CHLORIDE ' \ 1 FREON 12 50,00 1.00 i 2 PROPANE/EUTANE PPM WATER 80,00 PPM HCL 7,00 J 5 UISUAL APPERANCE U/W U 'U O O oo 1 METHANE 10,00 Jlo `-71 / ETHYLF NE ETHANE 5.00 z ACETYLENE n. DIMETHYL ETHER 1 0 , C0 10,00 6 METHYL CHLCPIDF 980000 , 0 1020000, i UINYL CHLORIDE A METHANOL Q METHYLENE CHLORIDE 5 0.00 50 . 00 L i' ETHYL CHLORIDE 5 0.00 1 1 FREON 12 1 . 00 1 2 PROPANE/EUTANE 1 PPM WATER 80 00 14 PPM HCL 7 . 00 1 5 UISUAL APPERANCE U/U U/U 17i 1 Ml/Ul .0005 2 METHYL BROMIDE . 0030 3 ETHYL CHLORIDE ,0100 4 PROPYLENE OXIDE . 0001 5 UINYLIDENE CHLORIDE .0100 6 METHYLENE CHLORIDE 98.0000 102.0000 0 01.4 756 ^onftdfnttai MCPLL01 Ph'Uh LE 131 17 2:10 PH THU. 26 APR., 1990 SPECIFICATIONS CATALOG DETERMINANT #: DESCRIPTION: PAGE 6 PROFILES 10 - 2000 LOU SPEC: HIGH SPEC 7 TRANS 0 A-DI 9 CHLOROFORM 10 CYCLOHEXANE 11 TCE 12 PPM WATER 15 PPM HCL 14 COLOR READING 15 UISUAL APPE.RANCE .0250 Clear . 0200 .0010 .0100 , 0350 .0001 75.00 5.00 5. C Tear 1 Ml /VI . 0005 2 METHYL BROMIDE .0030 ETHYL CHLORIDE .0100 4 PROPYLENE OXIDE . 0001 VINYL I DENE CHLORIDE` ' .01(0 ME r H Y l E(1E CHLORIDE- 90.0000 102.00/0 TRAN 0 .0/00 A-D1 ,0010 CHlORCFORM .0100 (} CYClOHEXANC .0250 . 0350 TCE . 000 1 PPM WATER 7 5,00 1 3 PPM HCL 5.00 C 01_ 0 R R E A DIN G 5, 1 VISUAL AfTfRfiMCE Clear Clear 1 '11/01 . 0003 - MLll.lL BkOMIDE .0030 El MIL CdlORIDE .0100 / ERCIPYLELL O^IDE .000 1 UINYLIDENE CHLORIDE , 01 u C t METHYLENE CFlGRIDE 9B , 00u C 102.00.0 / TRANS . 0200 A-DI .0010 y C H L 0 R L. F G R1 .0100 i 0 CYCLOHEXANE .0200 . C400 l: T LE .0001 i / PPM WATER 75.00 1 3 PPM HCL 5.00 14 COLOR READING 1 5 UISUAL APPERANCE Clear 5. Clear 1 Ml/Ul 2 METHYL BROMIDE .0005 . C 0: 5 0 DO 014757 OONFTDFNTIAl S P 11 0 I r R U! I L. L tl : i: '~i : 31 2 = 10 PM THU. , 26 APR., 1990 SPECIFICATIONS CATALOG DETERMINANT # = DESCRIPTION: 3 ETHYL CHLORIDE 4 PROPYLENE OXIDE 5 VINYLIDENE CHLORIDE 6 METHYLENE CHLORIDE 7 TRANS ti A-DI 9 CHLOROFORM 1 0 CYCLOHEXANE 1 1 TCE 12 PPM WATER 13 PPM HCL 14 COLOR READING 15 UI5UAL APPERANCE J Ml/VI 2 METHYL BROMIDE 3 ETHYL CHLORIDE i PROr-YLENE OXIDE VINYLIDENE CHLORIDE 4 METHYLENE CHLORIDE V TRANS !.i A - D 1 CHLOROFORM CYCLOHEXANE - j TCE i J. PPM Wf-TEF 1 4 PPM F'L_ i 4 C D L 0 R R E A D .1 N G j - VISUAL APPERANCE PAGE 7 PROFILES 10 - 2000 LOW SPEC* HIGH SPEC .4000 97.0000 . 0200 Clear .0100 . 6000 ' .0100 1015.000 . 0200 .0010 .0100 . 0400 . 0001 7 5.00 5.00 5. C 1 ea r 1 . 5000 96,5000 . 0200 Clear .0005 .0030 .0100 1 . G000 ,0100 10 0.00 0 0 . 0200 ,001 0 .0100 . 0400 , OOOl 75 . C 0 5 . 00 5 Clear 137 1 METHYLENE CHLORIDE / ETHYL CHLORIDE METHYL BR0M1DL /; U1NYLIDENE CHLORIDE 5 TRANS L CHLOROFORM 7 Ml/01 0 AMYLENE 9 PPM WATER 75.00 10 COLOR READING 1 1 VISUAL APPERANCE Clear 5. Clear 12 PPM HCL 5.00 1 Ml/Vl ,0005 r Oi N^r% mspl.coi 2=10 F'M THU. 26 APR,, 1990 SPECIFICATIONS CATALOG DETERMINANT #: DESCRIPTION: PAGE S PROFILES 10 - 2000 LOU SPEC: HIGH SPEC 2 METHYL BROMIDE . 0030 3 ETHYL CHLORIDE .0100 4 PROPYLENE OXIDE .4000 .6000 5 UINYLIDENE CHLORIDE .0100 6 METHYLENE CHLORIDE 98,0000 102.0000 2 TRANS . 0200 & A-D I .0010 9 CHLOROFORM .0100 10 CYCLOHEXANE . 0200 . 0400 1 1 TCE . 0001 12 PPM HATER 7 5.00 13 PPM HCL 5.00 14 COLOR READING 5, 15 UI5UAL APPERANCE C lear Clear 1 Ml/01 . 0003 'l METHYL BROMIDE . 0030 ETHYL CHLORIDE .0100 *\ PROPYLENE OXIDE 1.5000 1 . 8000 :> OINYLIDLNE CHLORIDE .0100 (, M E T11Y >,, E1! E CHLORIDE 96.5000 100.0000 / TRAN0 . 0200 j fl " J * .0010 y CEIL OF: OF URM .0100 j v C YCLOHEXANE . 0200 . 040 0 1 5 TIE . 000 1 11 F' F'M CATER 7 5.00 i ! P PM HLL i<, COLOR READING k X * 0 1OUAL APPERANCE Clear C lear Oo uT j M1 / 0 1 . 0003 . METHYL BROMIDE .0030 3 ETHYL CHLORIDE .0100 4 PROPYLENE OXIDE . 00C1 3 UINYLIDENE CHLORIDE .0100 6 METHYLENE CHLORIDE 98.0000 102.OOOU 7 TRANS . 0200 b A-DI .0010 9 CHLOROFORM .0100 10 CYCLOHEXANE . 0200 . 0400 11 TCE . 0001 12 PPM WATER 7 5,00 1 3 PPM HCL 5.00 14 COLOR READING 5, no 0 7 4 ~7 S <9 OOtyp Td^NT JAJ SPL.iLO 1 F'ROrlLE 2:10 PM THU. 26 APR., 1990 SPECIFICATIONS CATALOG DETERMINANT #: DESCRIPTION PAGE 9 PROFILES 10 - 2000 LOU SPEC: HIGH SPEC* 15 VISUAL APF'ERANCE Clear C1ea r METHYLENE CHLORIDE 200.00 0 INYLIDENE CHLORIDE 100.00 TRANS 20.00 4 M4 CARBON TET 250.00 5 CHLOROFORM 980000.0 1020000. 6 AMYLENE 10.00 20.00 7 CIS e BRCLME 8 0,00 300.00 9 A-D I 100.00 : o PPM WATER 50.00 4 1 PPM HCL 10.00 1 2 COLOR READING , 10 . J '? VISUAL APPERANCE Clear Clear 1 METHYLENE CHLORIDE 200.00 U INYL I DENE LhL0R I DE 100.00 TRANS 2 0,00 M4 CARBON TET 2 5 0.0 0 C H _ 0 R` 0 F 0 R M 980000 . 0 1020000. AMYLENE 10.00 2 0.00 r Is G0 . 00 EPC LME 500.00 A-DI 100.00 F PM * AT E F: 5 0.0 0 PPM HE! K . 0C i C 0 L n R P E f, D 1 N G 10 . j . 0 I 5 Li H L A i1 E R f: N C E C 1 ear C 1 cl r METHYLENE CHLORIDE l OINYlIDENE CHLORIDE ? TRANS 200 . 00 20 . 00 20 . 00 4 M4 CARBON TET 5 CHLOROFORM 980000,0 250 00 1020000. 6 AMYLENE 10.00 20,00 7 CIS 80.00 Li BRCLME 300.00 9 A-DI 100.00 1 0 PPM WATER 5 0.00 1 1 PPM HCL 10.00 1 2 COLOR READING 10 . 1 3 VISUAL APPERANCE Clear C 1 ea r METHYLENE CHLORIDE 200.00 mspe.cc 1 2*10 FM THU. 26 RPR., 1990 PAGE 10 SPECIFICATIONS CATALOG PROFILES 10 - 2000 !' R 0: IlE #* DETERMINANT #* DESCRIPTION LOU SPEC* HIGH SPEC 14 3 2 UINYLIDENE CHLORIDE 100.00 3 TRANS 20.00 4 M4 CARBON TET 250.00 5 CHLOROFORM 980000.0 1020000, 6 AMYLENE 10.00 20.00 / CIS 80.00 8 BRCLME 300.00 9 A-DI 100.00 10 PPM UATER 50.00 1 1 PPM HCL 10.00 12 COLOR READING 10 . 13 UISUAL APPERANCE Clear Clear 14 1 METHYLENE CHLORIDE -200.00 UIN Y LIDE N E CHLORIDE 100.00 T RANS 20.00 M4 CARBON TET 250.00 CHLOROTORM 980000.0 1020000. 'j AP1YLENE / CIS 10.00 20.00 eo, oo brclm: 300.00 A- DI 100.00 .1 0 PPM UATER 5 0.00 1 1 PPM HCL 10.00 J / COLOR READING 10 . U1SUAL AF'PE RANGE C Tear Clear 1 E "! H A N 0 L METHANOL 3 PPM WATER a PPM IICL .0100 200.00 15.00 i a/ 1 ETHANOL L. METHANOL 3 PPM UATER 4 PPM HCL 1 METHANE 2 ETHYLENE 3 ETHANE 4 ACETYLENE 5 DIMETHYL ETHER 6 . METHYL CHLORIDE .0100 200,00 15.00 980000,0 10.00 5.00 5.00 10.00 10.00 1020000 . 00 014761 C'ONF IDFNTT Al rir.F't col 2*10 PM THU. , 26 APR . , 1990 SPECIFICATIONS CATALOG PROFILE #s DETERMINANT #> DESCRIPTION: j47 7 OINYL CHLORIDE 8 METHANOL 9 METHYLENE CHLORIDE 10 ETHYL CHLORIDE J1 FREON 12 12 PROPANE/BUTANE 13 PPM WATER 14 PPM HCL 15 UOL, y. NITROGEN 16 OISUAL APPERANCE 17 SHIPPED ? 1 B SEAL NUMBER 1 9 SEAL NUMBER 2 0 SEAL NUMBER 21 SEAL NUMBE R PAGE 11 PROFILES 10 - 2000 LOU SPEC: HIGH SPEC: 50.00 50.00 50.00 50.00 1 .00 80.00 7.00 2.00 7. O oo 1 Ml/01 .000 5 ... METHYL BROMIDE .? ETHYL CHLORIDE .0100 I'-i PROPYLENE OXIDE i-., UINYLIDENE CHLORIDE , 0001 .010 0 d METHYLENE CHLORIDE 98 . 0000 102.0000 7 TRANS , 0200 8 A-DI 9 CHLOROFORM .0010 .0100 1 0 CYCLOHEXANE . 0200 . 0400 1 1 TOE . 0001 J PPM WATER 7 5.00 1 3 PPM FILL 5.00 C0L CR READING l r. OISUAL APPERANCE S 1 ear 5. Clear 1 d SHIPPED i 7 SEAL NUMBER 18 SEAL NUMBER 19 SEAL NUMBER 20 SEAL NUMBER 21 TRAILER tf i 30 1 PPM SULFITE 7 PPM PHOSPHATE 3 CONDUCTIUITY READING 13 1 METHYLENE CHLORIDE 200.00 UINYLIDENE CHLORIDE 100.00 DO 01 47,~> CONFTDFNTIAI mspl.co 1 2 = 10 F'M THU. 26 ftpR., 1990 SPEC IFI CAT IONS CATALOG PROFILE #= DETERfllNANT #s DESCRIPTION* 15L 3 TRANS 4 M4 CARBON TET b CHLOROFORM 6 AMYLENE 7 CIS b BRCLME 9 A-DI 10 PPM WATER 11 PPM HCL 12 COLOR READING 13 VISUAL APF'ERANCE 14 SHIPPED ? 15 SEAL NUMBER J, t> SEAL NUMBER 17 SEAL NUMBER i O J. u SEAL NUMBER PAGE 12 PROFILES 10 - 2000 LOU SPEC* HIGH SPEC 980000,0 10.00 Clear 20.00 250.00 1020000. 20.00 80,00 300.00 100,00 50.00 10.00 10 . Clear ] m / vi . 000 5 METHYL BROMIDE .0030 ETHYL CHLORIDE .0100 <4 P Fv 0 D Y L E N E OXIDE r VINYLIDFNE CHLORIDE . 0001 .0100 P METHYLENE CHLORIDE 96.0000 102.0000 TRANE .0200 ft - L I .0010 CHLUROrORM . 0 1 OU J U C Y l L 011E X ft Pi E . 0200 , 04 0 0 1 1 TEE . CC 0 1 PPM UftTER COMP 1 PPM WATER COMP 2 PRIM WATER COMP 3 3 5 PPM HCL COMP i J u PPM HCL LUni' / I > PPM HCL COMP 3 COlOR COM?' 1 COLOR COMP 2 2 0 COLOR COMP 3 2 J VISUAL APF'ERANCE 2/ S H I P P E D ? C 1 ee r C 1 eci r 2 3 BARGE ID # 1 METHYLENE CHLORIDE 2 VINYLIDENE CHLORIDE 3 TRANS 4 M4 CARBON TET 200.00 100.00 20.00 250,00 00 0147^3 ^ONFTDFNTTA! P Ei C 0 1 2=10 PM THU. 26 APR., 1990 SPECIFICATIONS CATALOG FF r 1 1-1 *1 = DETERMINANT #: DESCRIPTION: i S'i CHLOROFORM AMYLENE CIS BRCLME A-n t 10 PPM WATER COMF 1 11 PPM WATER COMP 2 iZ PPM WATER COMP 3 13 PPM HCL COMP 1 14 PPM HCL COMP 2 10 PPM HCL COMP 3 16 COLOR COMP 1 12 COLOR COMP 2 1C COLOR COMP 3 19 VISUAL. APPFRANCE , 1 SHIPPED ' 2 1 BADGE ID tl page; 13 PROFILES 10 - 2000 LOU SPEC* HIGH SPEC 980000.0 10.00 1020000. 20.00 80,00 300.00 100.00 Clear .Clear 1 ETHAN 0L 2 M n T Hi A N 0 L 3 PPM WATER COMP 1 P PM W A T E R COMP P P!'i W AT E R CO 1'. P P M n C L coi.p .; F1 ^ M H C 1, C CMP 2 P - M F C . COM! ' L Li L .J 1- L <M .' 1 C C 1- " R D vir COLO h C On:' E '. F; C i. ' li .0100 FT. T F, Y l t M E C rl L. A Di CHLOROr CRM Cl S r, M4 1 METHYLENE CHLORIDE 2 VINYLIDENE CHLORIDE 3 TRANS 4 M4 CARBON TET 5 CHLOROFORM 6 AMYLENE 7 CIS 014764 CNFTDFNT TAl