Document M4JKNO7JbYyLgY4KMpG2evJ5M

(conoco) Interoffice Communication To From K. C. Hunt, Refining, Ponca City j, j. Mangelinkx, Refining, Lake Charles Dale July 15, 1977 Subject Sample Analyses We are sending via the company shuttle three charcoal tubes for Benzene Content, data sheets are attached. DATA SHEET AMBIENT AIR SAMPLES (CHARCOAL TUBE ABSORPTION) 1. Plant: Lake.Charles Refinery 2. Sample ID: LC-SZ- H I _________ Lot No. of Tube /o 3. Sampling Date*~> /* s'/1Time Started C^A^Time Ended -3. Elapsed Time 4. Atm. Press.n It. H ________________ mmHg, Temp.X <. .*7c. 5. -Area the Sample Represents /oujA_______ o P ____________ p ai 6. Name of Person V.'ho Took the 5ample________ Q J llj JAt ___________________ 7. Pump Calibration Data: Atmos. Press. mmHg, Temp. 3 1. C. Pump Flow RateV ?cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM SAL 000009111 DATA SHEET AMS TENT AIR SAMPLES (CHARCOAL TUBE ABSORPTION) 1. Plant: Lake.Charles Refinery 2. Sample ID: LC-3Z- V ^Lot No. of Tube/ O 3. Sampling Date _______ Time Started *-*ir**Time Ended 3.J * s>m Elapsed Time__nevus 4. Atm. Press . in i.HmmHg, Temp.* 6. 5. -Area the Sample Represents Pc>iv A_______ f* t- aa/T" , _____________ c. ______ 6. Name of Person Who Took the Sample wn-faeo QOlu 7. Pun? Calibration Data: Atncs. Press. mmHg, Temp. X 7. op. Pump Flow RateS /cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM SAL 000009H2 DATA SHEET AMS I ENT AIR SAMPLES (CHARCOAL TUBE ABSORPTION) 1. Plant: Lake,Charles Refinery 2. Sample I 0 : LC-3Z- H Jt _______ Lot No. of Tube______ / & (+ 3. Sampling DateQ /17 Time Started C ^Ai^Time Ended Elapsed Timem#vas A. Atm. Press.">">/ V mmHg, Temp.____________________________ 5. -Area the Sample Represents ______ p 3 /. Ic. tv ________ T ft T0A_____________________________________________________________________________ 6 . Name of Person Who Took the Sample R o <-A vq____________/< o o 7. Pump Calibration Data: Atmos. Press. *> H.o mmHg, Temp. l"7-f c. Pump Flow RateS' 3cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. Sampling and analytical method-' Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM 00009113 SAL 0 (conoco) Interoffice Communication to k. C. Hunt, Refining, Ponca City F rom J . J Mangelinkx, Refining, Lake Charles d3:<? July 11, 1977 Subject Sample Analyses We are sending via the company shuttle three charcoal tubes for Benzene Content, data sheets are attached. We request an additional supply of charcoal tubes. SAL 00000911* OATA SHEET AV,f: :e::t AIR SAMPLES (CHARCOAL T'jBE ABSORPTION 1. Plant: Lake .Carles Refinery 2. Sample I v: LC-3Z- 3 S'Lot Ho. of Tube / O ________ _ 3. Sampling Daten/*>/'?'? Time Started r} 4 m fine Ended X 3 Elapsed Time_0 .S' 4. Atm. Press.1 Ol.Q _______________mmHg, T ep.X 9 . f'__C. 5. Area the Sample Represents c~ q a* q tv ArT* *aj v *t , #-+** a/ 6. Mams of Person Who Took the Sample A M 0 /J Gr &MTA y 7. Pump Cali brati cr. Data: Atmos. Press . n c?.<h mmHg, Temp. Z C./ Pump Flow Rate V^ cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. Sampling and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide 11. TSL Analysis Data: PPM SAL 000009115 DATA SHEET ambient air samples (charcoal tube absorption) 1. Plant: Lake.Charles Refinery 2. Sample lu: LC-BZ- 3 ? Ssr.pl inq Date 3. 1 /" in y Elapsed Time 4. Atm. Press. rl *7 /. 0 5. Area the Sample Represents Lot No. of lube /00 Time Started C HS A* Ti me Ended ^ H. ? Routl* mmH c , Tero. 81 P p'T itJ u At t T & Z69 *7181 C. 6. Name of Person Who Took the Sample f) w______ J*\o ft R tty 7. Pump Calibration Data: Atmos. Press. mmHg, Temp. 3. - ? c. Pump Flow Rate._____________ ^ ^________ cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .10. 11. Sampling and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide TSL Analysis Data: PPM SAL 000009116 3.---US (CHARCOAL ABSORPTION) 1 Plant: Lake.Ch-rlrS --rir.zry 2 Sample I D: LC-BX- H Q Lot No. of Tube____________________/___O___C____________ 3 Sampling Da te.*~7 /'* / Tire Started 6 ^^A^Tiire Ended -* 3 * Elapsed Tire_______ H. 9 m*oas 4 Atm. Press. 1 n i. o* 9 10 11 11 ^ i era. * 7.f C. 5 6 Name of Person Wh r T : c > the Sample A L- f& D______ A ^ J A ft.__________ __ 7 Pump Calibration Lata: Atmos. Press. "7cf.5 nrHc, Temp. 3. c. / op. Pump -low Pate^ ? cc * s/min - 8 Remarks: Include ary psrti ner.t information such as spills, leaks, sampling *:r lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in Job performance 10. Sampling and analytical method: Absorption or charcoal Desorption 'with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM SAL 000009117 Interoffice Communication to K. C. Hunt, Refining, Ponca City rrom ate J. J. Mangelinkx,Refining, July 7, 1977 Lake Charles Subject Sample Analyses We are sending via the company shuttle three charcoal tubes for Benzene Content, data sheets are attached. CC: ME0-THM-FIlE(2) SAL 000009118 Q DATA SK ::t AK31EKT AIR SABLES (CrA TUBE ABSORPTION! 1. Plant: Lake.Charles ?ef'ir.ery 2. Sample ID: LC-3Z- 3 5 3. Sarolinc Date 7 / 0 // nn Elapsed Tir. 4. Atm. Press. HL c 5. -Area the Sample Repress r. ts Let No. of Tube / oc Tire Started r) ^Mlime Ended Z Hcva 5 mmHp, Temp. Xc.O oc P o M P H oo-i e> A 0 M A V 6. Mane of Person Who 7c:< the Sample K /K> 7. Pump Cali braticn Data: ,h 'J s. Press. *7 c S' mrr'q, TemD. 2. .f, v C. Pure rtow Rate> H$ cc's/min. 8. Remarks: Include ar.y z e r 11 r: ert ir.forrnation such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. S-amp ling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph11 11. TSL Analysis Data: PPM SAL 000009119 DATA SHEET AM5!E:;T air samples (charcoal tube ABSORPTION) 1. Plant: Lake.Charles Refinery 2. Sample I 5 : LC-3Z- 3 ** 3. Sampling Cate_______ O Jn )n~> Elapsed Time____ 4. Atm. Press. cf. C 5. Area the Sample Represents^ Lot No. of Tube/ o <* _Time Started "7 00 A*Time Ended Z. ***" Pfi* _______ ~7 WQV* s _mmHg, Temp._________ Z C. ^c. 6. Name of Person Who Took the Sample________ S ft L- &-/ BA RT&L- 5 7. Pump Calibration Data: Atmos. Press. mmHg, Temp. 2. , c* op. Pump Flow RateH 3cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. S-ampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM SAL 000009120 3 DATA SHEET AMBIENT AIR SAMPLES (CHARCOAL TUBE ABSORPTION) 1 . Plant: Lake.Charles refinery .2 Sample I D: LC-3Z- 3 *7Lot No. of TubeJ 0 L* 3. Sampling Date________ J 7 Time Started 4MTime Ended Z HS~ P^\ Elapsed Time. 9t4_oun.s 4. Atm. Press.__________ __________________ mmHg, Temp . X .0__C. 5. Area the Sample Represents P u ** t* H oo$ E. 8 oR. ________ 6. Name of Pers on Who Took the Sample \A/ tL L. /AM J 7. Pump Calibration Data: Atncs. Press. *7 c 9 . S~ mmKq , Temp. 2 c. Pump Flow Rate S& cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance ,10. 11. Sampling and analytical method* Absorption or charcoal Desorption with carbon Gas chromatograph11 disulfide TSL Analysis Data: PPM SAL 000009121 (conoco) Interoffice Communication to K. C. Hunt, Refining, Ponca City From J. J. Mangelinkx,Refining, Lake Charles Date June 21, 1977 subject Sample Analyses He are sending via the company shuttle three charcoal tubes for Benzene Content, data sheets are attached. lb CC: MEO-THM-FI SAL 000009X22 DATA SHEET A,M3I'NT AIR SAMPLES (CtAP.CCAL TUBE A5S0PA' PI2nt: /> fj. / c- Savoie ID: C-" (f "* *3 Samol ing Cate ^ ~ Z o * i 7 Lot No. of Tube /^6 Ti-rre Started _lA7i-9 Ended * // Elapsed Time________ H C 3 AUA'wrfJ Atn. Press.*"7 C t. f Area the Sample Represents rrnKg , Tenp. P Ro O vc-'T' 2 ?. o =c. & AJ i 'T , ** Z c; Mt V o T S i tt At AA/ Name of Person Who Took the Sanole & A At-D Gr Pumo Calibration Data: Atros. Press. rr.nc. Taro, z r. c Pump Flov; Rate :c* $J~ir. Remarks: Induce any pertinent information such as 5"*'".`sf 'ea^.s, sanding for lab, etc, if any, v/rich may be cause for escape cf hydrccertcns into the air. 9. TSL Analysis Data: ooooo^ sM- DATA SHEET A.`?:E\7 AIR SAMPLES CHARCOAL TUBE AESOP. ^Td*. 1. Plant: A- AK 2. Sa-role ID: i- - ' Qj- I *~f 3. Saroling Date - Z o - l "> Lot No. of Tubs* c Tire Started 9 ^ A*V l~e t>.c~d 4,'.^ ^ El 203et 7ire_V 6 6>t wt? j 4. A.tr. Press. >6f. T r~Hg Tenp.X ^. O*c. 5. Area the Sards represent; CvTSiO M. At A* & <Z, ________ 6* & t 7~ ________ 6. Ne~e of Perscr Vrp ~pc< the SarpTe_______ ^ >*-^a<?q y __________ 7. Puro Cali bra tier. Tata: Atr.os. Press.^irrHc, T =ro. X S. (+ Pump Flow Rate_____ VH pc'ddr. C Rerarks: Induce ary rsrtir.ert inferredon such as s; fLor lab, etc. if ary, which ray be cause fo: hydrccarcers *.ntc tr.e e;r. r;, sereling escape cf 9. TSL Analysis Data: ooooo9lZ^ SM- DATA SHEET AMBIENT AIR SAM?LES (CHARCOAL TUBE AESOP.-T;:N 1. Plent: ' NAME c-/*-**>-* 2. Savoie ID: ^ ~ ~ Lot No. of Tube 3. 5anol inq Date C - -L ^ O *7 1 toe Started y Elapsed lire__________ H ~7 J >1x> / 0 c. A**1 -? ^ /*A 4. Atn. Press. t 4T rrHg, Tenp. 1 *-t.H sc. 5. Area the Sample Reoresents ^ X P&-A.L# c Ls-TAA'Z- &ASGrJJve~ O P AfirT O ft 6. Nar.e of Person Who Took the Sanple AiuA&*c. & u 2. 2. i fis 0 7. Po~o Calibration Data: Atros. Press. rrr~.nc. 13--. 1 S*- L C Pu^p Flow Rate_____ Sf :c' c --:r 8. Rerarks: Include any cert inert irfcrration such as sc:*'st *e='.s, sanding for lab, etc. if ar.y, which ray be cause for ssc-ne cf hydrocarbons into the air. 9. TSL Analysis Data: SAL 000009125 (conoco) Interoffice Communication to K, C. Hunt, Refining, Ponca City J. J. Mangelinkx,Refining, Lake Charles Date June 16, 1977 Subject Sample Analyses We are sending via the company shuttle three charcoal tubes for Benzene Content, data sheets are attached. 009VZ6 SAC OOO r'livr DATA SHEET sables (charcoal tube asscea- 1. Plant: C. t4 A a bp s 2. Sample ID: i~-~ - to 3. Sanolinq Date c- - * S-11 Lot No. of Tube /o C Time Started $ A* 7i-e Ended / <Z* Pa Elao SrC 7i"2 Z 9 1 SiiAsUT&S r. < 4. Press. 7 Cf.c rmHc, leap. * --C. 5. Area the Sarde Ee:'-=sents -- P-- um-p -- S R 0 VJAR.O &4S-T TAMM paum 6. Ne-s of Person V r.z . oc< the Sa~ole .J.J. AAJ&u j as n* 7. PUT.D Calibrsti or. Seta: Atrcs. Press. 7c^,c rr:rzt Terr. U.i C Pmp Flow Pvate SS cc's'~ir. 8. Remarks: Ir.cluca c'.y rtirert ir.forration such as s d V s . *5c<s, sampling for Ub, etc if ary, vA.ich ray be cause -or scare cf hydrocarbons r.tc fre air. 9. TSL Analysis Data: SAL 000009127 Af'2!'1- DATA SHEET 7. ^ p 17 r 7 10 (CHARCOAL TUBE AESOP. 1. Plant: ^Ak c-* a at.?$ 2. 5a-.ol a ID: 3. Sampling Date 6 -1$- 77 Lot No. of Tube ;06 Time Started 3 T:~e Ended-2. * ^ ^4 Elapsed Tire 3 D? C* A\ //**T0s 4. Atr:. Press._______ PC^.C rrHc, Tenp.j. 9. ?= c. 5. Area the Sards ."saresents ^ t C ~r x* t-Zj'T e *l O ft pU-i ^ fi^LU'i ____ QOTStUZ 6. Here of Person Who ~o:< t're S=~.ple J.J. ____________________ 7. Put-.d Calibration Data: Atros. Press. 7cr,C rr.Hc, Taro. 3. c. 3 c Purp Flovf Rate O_____________________ cc's'"ir. 8. Rererks: Induce any pertinent 1 r.for. for lab, etc. if ary, vr.ich hydrecartens into ere air. ion such as sc y be cause for e cIfRS 9. TSL Analysis Data: SAL 000009128 AVcIENT AIR SAMPLES (C-ARCCAL TUBE ABSCr.-TIE'i 1. Plant: '"f c- * * Al.? S 2. Sarnie ID: l c - 3. Sardinq Date t> - f S - ~t Elao sec Tire Lot No. of Tube /0C Tine Started % ^ ^ AM 71-= Ended 3 3 pm 3^5^ a* 4. Atn. Press. ~> c Tercp. i ?. $ *C. 5. Area the SaT.pl e P.esresents -** > ctm. . A> A -- m*i, . o v-r.t, n * --*-- 6. Ns" of Person V he "oc< the $ = -.?'! e J,J. Ai A a/ a// * 7. Po-.o Calibratior. Data: At.ros. Press. rr.rr, Tern. A c. 3 C Punp Flow Rate CO cc's r 8. Rerarlcs: Induce any oertinert ir.forretion such as sc" ~s, 1 aa ' 3 , S .iCil inq for lab, etc. if ar.y, v,'-ich ray be cause for ^s* esc ace cf hydrocarbons into the air. 9. TSL Analysis Data: SAL 000009129 (conoco) Interoffice Communication to K. C. Hunt, Refining, Ponca City From J. 0. Mangelinkx,Refining, Lake Charles Date June 15, 1977 subject Sample Analyses We are sending via the conpany shuttle four charcoal tubes for Benzene Content, data sheets are attached. SAL 000009130 r* \ *5T- V s;V`LS {ChARCCAL TUBE A5$C?.-7rt** 1. Plant: * * * e 2. Ser.ole IP: *- ^ ^ c Let Ns. of Tube / * _______________ _________ 3. Se-pling Pets **">? Tf~e Started Elaose-: Tire3 0 2. Muuvres O 7f-* Ended -? *PM 4. At". Press.~7 C 7. C.rrre, 7&-np.3. 3. 3_____________________________________ _*c. 5. Area the ScT.pl e Pssresents______ ft gAac>pt^rAvg______ mot* A j o _____________________ o < a t_____________________________________ ___________ 6. Har.e of Person Wn: tre Sr:'-J.J. ______ 7. Put.d Cal-Ibraticn Lata: At"os. Press. ict.c rmrt, Ters. ?unp Flow Pete<f S sc1s ~ir. ^ y. y C 8. Rererks: Induce a*. i--crret1on such es s:d*s, leers, seeding for let, = ^voh rey be cause ~tr e:'c~"d escece cf hydrocaret::s ir.se tr.e a *, r. 9. TSL Analysis Data: ooo09 \3' CAT.-. SHEET AVBIEKT AIR SAMPLES (CHARCOAL TUBE ABSOPAtrCt 1. Plant: t***6 7 8 9e-**'** 2. S2-d1s ID: l c. - 0 2 - ">Lot .Vo. of Tube 1* 3. Se-olinq Pete <* - tH-m Tire Started 0 s<iA+< ?i~e Ended/3^ />/H Elapsed Ti.ca3 C ai;a/ >rg5 4. Atr. Press,________ T C7.C rr.Hg, 7enp.2 V. *fSC. 5. Ares the Semple Represents_______ OR a v* ty_______ t a ql .________ fi. A F A & U i- A ^ a _________________________________ 6. Ns~e of Person Wr: Tcc> the Sanp'e_____ J.J. A1 A a/ / a/M it 7. Pirno Cal ibrgticr. Sets: Atros. Press. 1 c c rrrj-*q, Tero. 3. H. */ C Pump Flov; Rate>T /cc's'-ir. 8. Remarks: Induce any pertinent ir.fcrretion such as sd'."s, leers, sarjoMnq for let, etc. if cry, which rsy be cause `or *zrz^i' escece cf hydrocarbons ir.tc the cir. 9. TSL Analysis Data: SAL 000009132 A!'5I EVf AI?. SAMPLES 'C'-AP.CCAL TUBE ASSC?.TM:*. 1. Plant: *-A* 2. Sa-.ole 10: ^ ^ - g g - g 3. Sarolir.q Data - / *i - 7 7 Let No. of Tube/ < Tire Started * l*An Ti-g Ended V /3/*m Elapsed TireS OS M t **'*'&* 4. At-. Press.?t7,crrrg, 7sop.z. H. H _____________________________________ =C. 5. Area the Sample Represents__________*>AJ caao^at g<^AAPtfy6 7 6. fJe-5 of Person Wro "o:> the Sample3 - 0. At a a/ __________________ _ 7. Pur.o Calibration Data: Atros. Press. rctHc, Taro. ^ f, y C Punp Flow RateV C______________________ :c1 s '~i r. 8. Rerarks Include any sertinert infer, for lat, etc. it cry, v<^* cn hydrccarrcns into the cir. :ion such as s: :y be cause rcr lsa<s, sa-cl ir.g -si sscace cf 9. TSL Analysis Data: ooooo^3 sM- * l hi?, samples tube as sc Plant: C~ /\ f2 u s 2. Serole 10: A. ~ 2. ? Let No. of Tubs/ o __________________ _ 3. Sc'olins Cate <* - t *i - T "? Tire Snarled J ^ ^ /^Ai Sneed *i * ^ p Elapsed Tire ^ s+h,tS 4. Atr. Press.^ C S'. Z. r~Hg, Tenp.Z S. &=C. 5. Area the Serple .".sorasents c.tfsnjf A-&.A4 . QUilst-4 M I O 0A 6. Ne~e of Person V.r.z 7oc< the S=r?'e WA'ffA. T J.J. At A- ** C-&L- / / A; C- 6 7 x 7. Pur.o Calibration Date: Atros, Press. 7 6^.2, nr-Hr^ Tero. 3- .S', o e Rerarks: Include for lab, hydrccar Pirip ? 1 ow RateifQ O____________________ sc's '-ir. ion such 25 s: v be cause ~cr <s, sending escece cf C-H0*4tST uJtvC, Qa*20m -TOTAL f> H O S f AT AS Q.PA&&MT 9. TSL Analysis Data: 000*13^ SAL 0 (conoco) -V Interoffice Communication to K. C. Hunt, Refining, Ponca City From 0 0 . Mangelinkx, Refining, Lake Charles Date June 14, 1977 subject Sample Analyses We are sending via the corpany shuttle five charcoal tubes for Benzene Content, data sheets are attached. We request an additional supply of charcoal tubes. lb / CC: ME0-THM-FILE(2) 000009135 SAL DAt~. -"li 1 Argil ST A IP. SAf-'PLES (C---.P.CQAL TUBE AESOr.~T::v 1. Plant: l~ A K c./f A 2. Sarole ID: L- O - B X -- tLot No. of Tube 7 & 3. Sampling Date 6-/307 Tire Started %zxAh Ti~e Ended f H~*A * Elapsed Tire Aw a*. 4. Atn. Press. c S.L rrHc, Temp.X S. U=C. 5. Area the Sample represents ^A^ry T~ A g * , ft A f A 0 U_______ U A v A A/____________________________________________________ 6. Name of Person Vr.o Took the Sample A1 _______________ 7. Porno Calibration Data: Atmos. Press. L rtr.Kc Tors. >-c C. Pump Flow PateC X o _________________cc,s'"1r. S. Remarks: Induce any pertinent information such as sod's. 'a<s, sending for lab, etc. if ary, which ray be cause for strok'd escape cf hydrocarbons into the air. 9. TSL Analysis Data: SAL 000009136 DATA SHEET Aral ekt A ip. samples (charcoal tube aesof>t::n 1. Plant: t-A .2 Sar.ole ID: L C- - U 2. * 2______ Lot No. of Tube 3. Serving Date 6 - /3Q") Time Started JOG Ti-s Ended ? rJAM Elapsed Time 3 ^ A<ivurts 4. Atn. Press. C f. C-rtrrc, Temp,1 H. 5______________________________ `C. 5. Area the Sample Represents C-AS c- M 8. P ** A-*r ^ o A A AW v WiU./a#m Ai LAfl ^ 6. Name of Person Who Took the SampleJ. J. Ai A */c St-1 a*ai * 7. Pirr.o Calibration Data: Atmos. Press. tS. L, psriic. Taro. Pump Flow RateG *7 O sc1 s '~ir. 2^ c C 8. Remarks: Include any pertinent information such as sz-'.'s, Tea<s, striding for lab, etc. if ar.y, which may be cause for acre--escape cf hydrocarbons into the air. 9. TSL Analysis Data: S4L 00OO9i 37 t T T* r S-fPLES (CHARCOAL TUBE AESCE-7::*. 1. Plant: ^A>i 2. Serole ID: C. ~ ~ oc3_______Lot So. of Tube/ 3. Sampling Pets 6 - / J Tire Started Eleosec T:~e_____ 3 C- / Ti-e Eoced -2 Ph\ 4. Atr. Press. co r-'rz, ^ 3~. C;C. 5. Area the Sar.pIs r.aorsssots frftAUlT^ T A fl^E, &}+?* L. Z-AUAA/ 6. Nc~e of Parser v M <V V > vu* 7. Puro Calibrcf'c 8. Remarks: Ir.clu for 1 hydro p--os. Prass. 7tT;fe____ "*"= ------------------- ------------------- C ?*-p Flow --------- cc'sMr. ; = r:-r.err ir.forrat:on such as s:**. * s, laa<s, se-noling , - ary, verier. r*y be cause ~:r a: :' escace cf *r.rr ora air. 9. TSL Analysis Data: SAL 000009138 AP3IEN7 AIR SAMPLES (CHARCOAL TUBE ABSO~~::\ 1. Plant: ***** 2. Samole ID: L C - g H Lot No. of Tube / & L_________ ___ 3. Sampling Date & - 13- 77 Time Started % STi~e Ended Z Elapsed Time3 S3 A> ivur# j 4. Atm. Press.CvT* O mr.rlg, Temp.^ 5"^ C________________________________'C. 5. Area the Sample Represents________ RBSgtofiLH oc~'rt></ k>Grti*f -) o *0 / _____________ _____________ _________________ _________ 6. Name of Person Who Took the Sample J. J- Af A k> c. ) K*U 1*______ __________ 7. Pumo Calibration Data: Atmos. Press. C rrriic, Trro. l, c Pump Flow Ratef 3cc's'-ir. 8. Remarks: Include any pertinent information such as sc;'.`s, 7se<s, samcling for lab, etc. if any, 'which ray be cause for a:rc~"s` escape cf hydrocarbons into the air. 9. TSL Analysis Data: SAL 000009X39 DATA SHEET ANRIENT AIR SABLES (CHAP-COAL TUBE AESOFAT:!' 1. Plant: ^A*e 2. Sar.ole ID: J- C- ~ U 2; ~ S~ lot No. of Tubs /PC 3. Senolinq Oats 4 * < 3 - 7 *7 Elapssc 7i t e *i Tire Started*7 PA' 4. At.n. Press.________7QT-Cnr:Vs, Tenp. 2 H- S~ ~C. 5. Area the SaT.pl a Represents C-AS c. H H t> m a t O G-fl p*ph y _______U/i ____________________________________________ _____________ 6. Nst* of Person Vrc Tocfc the Sarple J .J. M krtJGrLtwu a ________ _ 7. Purd Calibration Data: Atrcos. Press. ~>^S* c, nrHc, Taro. 3. S'. L C Pump Flow Pate*7 o______________________ :c's''"ir. 8. Rerarks: Include any oertir.ert irfcrration such as soil's, l=a<s, seroMng for lab, etc. if ary, which ray be cause for a:-": -#* escape cf hydrocarbons into the air. 2. /lours CcUef 7 phtfi'th 9. TSL Analysis Data: SAL 000009140 (conoco) Interoffice Communication to K. C. Hunt, Refining, Ponca City From J. J. Mangelinkx,Refining, Lake Charles Date July 5, 1977 Subject Sample Analyses We are sending via the company shuttle three charcoal tubes for Benzene Content, data sheets are attached. . J/ Mangeliijkx 'S /lCbC: ME0-THM-FllE(2) SAL 0009141 DATA SHEET AMBIENT AIR SAMPLES (CHARCOAL TUBE ABSORPTION) .1 Plant: Lake Charles Refinery .2 Sample ID: LC-BZ- 3 _______ Sampling Date _ JPjJLb. ? 3. Elapsed Time____ Lot No. of lube/ O _________________________ Time Started *1 00 A^Tiroe Ended 3" /m t'.O 4. Atm. Press.Oil.*)mmHg, Temp.^ ?C. 5. Area the Sample Represents______R. Q *+./l t v k>\t a/ 6. Name of Person Who Took the Sample K aj _ 7. Pump Calibration Data: Atmos. Press. 0 6 9. ^ mmHg, Temp. 10.0 op. Pump Flow RateH *7cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, ' sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. Sampling and analytical method: ( Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data*. PPM 0000091^ SM- DATA SHEET AMBIENT AIR SAMPLES (C- ARCOAL 7-JBE ABSORPTION 1. Plant: Lake.Charles Refinery 2. Sample ID: LC-3Z- 3 3 3. Samolinq Date Elapsed Time 4. Atm. Press. 5. Area the Sample Represents Lot No. of Tube / 0 t? Tire Starts d C ***** A* Tire Ended i Hr S'. o He**. % mmHq, Temp. oc- o pzaatoA 6. name of Person Who 160k the Samp le -5 c. n A o QA 1. Pump Calibration Data: Atncs. Press. 9 C?. C nm'fc, Ter-o. X"7.o Oq% 8. Remarks: Pump Flow Rate_<3" R.cc's/min. Include any pertinent information such as spills, leaks* sampling for lab, etc. if any, 'which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .10. Sampling and analytical method* Absorption or charcoal Desorption with carbon Gas chromatograph disulfide 11. TSL Analysis Data: 0000091 SAL i; DATA SHEET AMS IEHT AIR Sr.v?LES (CHARCOAL TUBE ABSORPTION') 1 . Plant: Lake.Charles Refinery 2. Sample I D: LC-3Z- 3 *j _________ Lot No. of Tube/ O t* Sampling Date______ n )S/1 ______ Tire Started ChS 4*iTime Ended X. ***" f*M 3. Elapsed Time_________ S'. &______ 4, Atm. Press.*1 Q t. mmHg, Temp.3. Jp. ?C. 5. Area the Sample Represents R A , ^ /ZAP 6. Name of Person Who Took the Sample R o 8AT________At i $ 7. Pump Calibration Data: Atmos. Press. ")C*7- ^ mmHq, Temp. 2 "7. C. Pur.p Flov: Rate&cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, ' sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM ____ u (conoco) Interoffice Communication to From K. C. Hunt, Refining, Ponca City J. J. Mangelinkx, Refining, Lake Charles Da:= July 1, 1977 Subject Sample Analyses Me are sending via the company shuttle seven charcoal tubes for Benzene Content, data sheets are attached. 00091A5 SM 00 DATA SHEET AMBIENT AIR SAMPLES (CHARCOAL TUBE ABSORPTION) 1. Plant: Lake.Charles Refinery 2. Sample I D : LC-5Z- Z ZLot No. of Tube/ o C 3. Sampling Datec / 3 t> J1 Time Started C v^^MTime Ended Z ** /*a> Elapsed Time_J .S' W 0u& s 4. Atm. Press."7 0*7. ___________ mmHg, Temp.Z <. *7c. 5. -Area the Sample Represents'T' c. 0 f*//fT& 6. Name of Person Who Took the Sample_______ W i A- L / A ** sS ^ 'T'T&AJ 7. Pump Calibration Data: Atnos. Press. *176.1 mmHg , Temp. 27.1 c. Pump Flow RateV$cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .10. 11. Sampling and analytical method: Absorption on charcoal Desorption with carbon Gas chromatograph disulfide TSL Analysis Data: PPM SAL 000009146 DATA SHEET AMBIENT AIR SAMPLES (CHARCOAL TUBE ABSORPTION) 1. Plant: Lake.Charles Refinery 2. Sample ID: LC-3Z- Z 3Lot Mo. of TubeJ 6 C 3. Sampling Date^/jo/77 Time Started C __________ Time Ended Z. ^ /*At Elapsed Time____________ 7 ,8 H s 4. Atm. Press.________ 7 6^.3mmHg, Temp. 5. -Area the Sample Represents 7~ C c. ,J _________3 0 - S'Oc. .C o js-rfrvj. m A A/ 6. Name of Person Who Took the Sample*T S C)______________ S /|lT TO/^______ 7. Pump Calibration Data: Atnos. Pr e s s . *7 7 s./ mmHg , Temp. -39./ 0 p, Pump Flow RateV *7cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. Sampling and analytical method: Absorption on charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM ^0000 VT DATA SHEET aksiekt air samples (charcoal tube absorption) 1. Plant: Lake.Charles Refinery 2. Sample ID: LC-3Z- Z *4_________ 3. Sampling Date_______C /2 Lot No. of Tube/ 0 O T i me Started CH Am Time Ended 3. J P/* Elapsed Time*1.2' H o* s 4. Atm. Press._________ 9 6 9 3mmHg, Temp. 5. Area the Sample Represents~7~ C C. ___________ <2 . V * a c o AJ'T pi QL Ma6 7 8 9 10 11 6. Name of Person Who Took the Sample U/ oAs P As 7. Pump Calibration Data: Atmos. Press . 1 o- t mmHq , Temp. -3 1 -/ op. Pump Flow RateS' 7cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. S-ampling and analytical method: Absorption orv charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM 0000091^ SAL DATA SHEET AMDIENT AIR SAMPLES (CHARCOAL TuS ABSORPTION) 1. Plant: Lake.Charles Refinery 2. Sample lu: LC-3Z- fLot No. of Tube / & C 3. Sampling Date______/ \7/7 T i me Started t Time Ended 3 /*/j Elapsed Ti me) 'S'- O At * a/ r fc S 4. Atm. Press._______^ fmmHc, Temp.Z. S'^_____________________________________________ C. 5. -Area the Sample Represents_ P flo QO cTT pfi. A^TJ QArfrTt o*s ________ 6 ATC/f/^6 & _____________________________________ 6. Name of Person Who Took the Sample Q ^4________Gr ft /\ : p______ ___ 7. Pump Calibration Data: Atmos. Press. 7 7^. t mmHg, Temp. Z 9./ 0c. Pump Flow RateH 7 U cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .10. 11. Sampling and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide TSL Analysis Data: PPM ooooo^9 sM- AOJ)T r\. ii DATA SHEET S (C--PC0A.L T`J3E ABSORPTION) 1. Plant: Lake.Charles ry 2. Sample ID: LC-3Z- Z S_________ Lot No. of Tube______ / O (+_______________ 3. Sampling Dat=_ c As A ? _ir:e Started 3** /p/iTime Endedi"* /^i El a p s e h Tire______________ f S* &______ ai > a/ v t 4. Atm. Press._______0 . ! 5. -Area the Sample Pepreser. "'Hg, Temp ^ ^ C- T in c. Cm- Pc S O tm t AS 6. Name of Person Wrc . cck the 5a-ple__ kjfLL^/ u QB'T 7. Pump C a 1 i b r a t i c r. Data: A'~;s. Press. mnHq, Temp. ZO ~ / c. ?-mp r'i Ov. Rate__________ H Occ's/min. 8. Remarks: Include ar.y percir.er.t information such as spills, leaks, sampling r lab, etc. if any, which may be cause for abnormal escape cf hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump v/orn in job performance 10. S-air.plinc and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11.. TSL Analysis Data: PPM SAL 000009X50 DATA SHEET AMBIENT AIR SAMPLES (CHARCOAL TUBE ABSORPTI ON) 1. Plant: Lake.Charles Refinery 2. Sample ID : LC-3Z- 3 0Lot No. of Tube/ O C_______________________________ 3. Sampling Date^ /3 e/~) 7 Time Started/ 3 p^T 1 me Ended / HSm Elapsed Time.* f. o At * re s 4. Atm. Press.7 C *?, JrnmHg, Tenp._j T.VC. 5. Area the Sample Represents L. A a o ^ A-r o 8.-4 . sf a, c. h/*\sT 6. Name of Person Who Took the Samp! e <= t- * frea o______ aiu>s 7. Pump Calibration Data: Atmos. Press. 0 C1.3 mnKg , Temp. 1 0. o Op. Pump Flow Rate,H *i 5____________________ cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM SAL 000009151 DATA SHEET AMBIENT AIR SAMPLES (CHARCOAL TUBE ABSORPTION) 1. Plant: Lake.Charles Refinery 2. Sample I D : LC-3Z- 3 /Lot No. of TubeJ O 3. Sampling Datec/fe/-}'? Tir.e Started _____________________________________ Time Ended nHSA*^ Elapsed Time___J S. o__________________ 4. Atm. Press.^ <* 3mrcHg, Temp.-2, *7. V__c. 5. -Area the Sample Represents ua g if t Q / S Tl l L- A'T/O*'7- A 8L _____________________________________________________________ 6. Name of Person V.'ho lock the Sample ^vjj -l- c. q q /< ________ 7. Pump Calibration Data: Atrcs. Press. T c 9.3 mr.Kq, Temp. 3 1-Q C. Pump Flo,.' RateH H S cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. S-ampling and analytical method: Absorption or charcoal Desorption vn th carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM 000009152 SAU Interoffice Communication To FrO'"' Da:? SuS;?c; K. C. Hunt, Refining, Ponca City J. J. Mangelinkx, Refining, Lake Charles June 29, 1977 Sample Analyses We are sending via the company shuttle three charcoal tubes for Benzene Content, data sheets are attached. We request an additional supply of charcoal tubes. CC: MEO-THH-FILE(2) 000009^53 SM- DATA SHEET ' akbiest air samples (charcoal tush absorption) 1. Plant: Lake.Carles Refinery 2. Sample 15: LC-3Z- Z S________ 3. Sampling Date__ */**> 77 7 Lot No. of i ube Tine Started / ^ C_ Ti me Ended lA Elapsed Time____ i S- O A^tAJ f T0 j 4. Atm. Press.________ & - /____________ 5. -Area the Sample Represents^ jrmKo, Temp.3. O /C. F- i & v Ct\m e j Z-j-rtv c- ft ZPaPL m at_______________ 6. Name of Person l-.'ho Took the Sample lASooOfjot** y & o Af C- 7. Pump Calibration Data: Atmos. Press. H 1 o. 1 mmHq , Temp. Z *). t C. Purp F1 ov; PateHI C . cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling -or lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM. SAL 00000915* DATA $HEE~ amd:e.:t air samples (charcoal tube absorption 1. Plant: Lake.Charles Refinery 2. Sample ID: LC-3Z- 3, c.Lot `<`3. of Tube/ O 3. Sampling Date< J i.zj /? 7 Tine Started n\oo AMTime Ended ___________ Elapsed Tire* 4. Atm. Press.t. inmHg, Temp.2. O At** t e s , 3c. 5. -Area the Sample Represents ^ <- A-rg-zf/vU c- a3*9^/a/^ am Pi* 3 6. Name of 0arson Who Took the Sample__ ~T M l,LlS> 7. Pump Calibration Date: Atmos. Press. mnrlg, Temp. 3 *>. / c. Punp -1 ow RateH~> Lcc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. Sampling and analytical method-' Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM SAL 000009155 I Mi u SH ( CHARC ABSORPTI u.< j_ 1. Plant: Lake.Charles '.a-irary 2. Sample I D : LC-3Z- Z 9Lot No. of Tube/ 0 3. Sampling Date0 / * *? /7 7 Tire Started u iasaw Time Ended H' 3# A *+ Elapsed f-'-e ____________ / S'. O_______ m*a*vtS 4. Atn. Press.n *) fi . f-"Ho, Tenp.X S'- 3C. 5. Area the Sample Represents ** X. Af/gAMg/f & ________ q A Jot i _______ 5 A *>s*c&*___________________________________________________ 6. Name of Person V.'hc 7 c: > ore 5arc? 1 e A? Al 7. Pun? Cal i brati cr. 7sca : Atmos . res s . *1 ~7 o . t rr-Mg , Temp. 20./ Qq. :vo: " cw PateV 7 Occ's/min. 8. Remarks: Include any certir.ert information such as spills, leaks, sampling -*:r lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air.9 10 11 9. Sample Procedure: Personal Sampling pump worn in job performance 10. Sampling and analytical method: Absorption c-r charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM 9\*b 00 000 sM- (conoco) Interoffice Communication tc K. C. Hunt, Refining, Ponca City from 0 0 'langelinkx, Refining, Lake Charles Da:- June 28, 1977 subject Sample Analyses We are sending via the company shuttle three charcoal tubes for Benzene Content, data sheets are attached* SAL 000009157 *f7 * T v- tus* asscp":;*. 1 =1>r+; 2. Ser.oie IS; L-a~ G 3. SaroHr.q Cate * *? Let No. of Tubs / <^ <______________ Ti~e Started C ** r a* ~*-g Enceo Vnzizi lira O.f J 4. Atr. Press.*7 __________rrrg, T&-p.J o -C. 5. Area the Serple represents F ** m ^ c. R. o Q A r3 6. Ne-e of Parser. **: fre Ss~?:eJ /HcftArAQ 7. Pert Cal fDrcf :'c` Cate; At-os. Press. *7 7 A ^ rr>'r ? 7=ro. -3. 9. ^ Ptzrp f 1 ov/ PeteC O te's'-ir. til Ml 8. Rerarks r.c'.:.oe *-y ror ;ee. ett h* Ion such 2 v be cause > 9. TSL Analysis Cate: SAL 000009155 DATA SHiiT AN3IHNT AIR SAMPLES (C-.ARCCAL TUBE ASSORT: 1. PI ant: ^"A***X 2. Sard 2 ID: i~ ^ " G 3 \ O 3. Sanding Pete Elapsed Time Let No. of Tube / & t* Tire Started C ** S d -- Ended *~} .$T3 J4oufr-5 jo 4. Atm. Press.C rr.Kg, Temp.3 o_______________________________________________ =c, 5. Area the Semple Represents -7~amx ^ -<rT" ^ AA*i_______________ _____________________________________________ *T A >W< . 6. Name of Perssr. Who Took the Sample ; A >t # L ________ 7. Piece* Calibration Date*. Atmos. Press. ~?7Kf` rooHc, Taro. XO.2. Pump Flow Rate___________SV_________ __~c` s '"ir. ( 8. Remarks: Induce any pertinent infer ration such as soil's, I ears, seating for lab, etc. if ar.y, which ray be cause for errc''~a* escace cf hydrocarbons into the air. 9. TSL Analysis Data: 000009159 SAL 1. Plant l_ A * C- H-A #. S 2 8 10: A. c_ B ~ ~ f _-- - 'Id. of Tube 3. Ssr.olir.? nt. cA-)/r7_T<re Sorted c v / 6C ?1- inced 3 J5 A>* 4. At-. Press.______ 5. Area the S-rsle Pe:-esen's. -rA/Jfi PAfLH 3 3o c. RVV QQUJV AA-BA 6, fir? of Per 7 Ptr.o Calibr eR ks C. A C- Pur? :T s 1 Or.' p't 7 7/-P rri ^5^ rtinert *;r~crretion such 25 if er./, vr:ch rev be cause i-- A 7=r-. 10.7, C tc*sr-:r. ss, sc^oling escece cf 9. TSL Analysis Cafe: q\t> 0000 (conoco) Interoffice Communication ~o K. C. Hunt, Refining, Ponca City J. J. Mangelinkx, Refining, Lake Charles Da:s June 24, 1977 Sample Analyses We are sending via the company shuttle three charcoal tubes for 8enzene Content, data sheets are attached. SAL 000009161 Q DATA SHEET AVEISVT AIR SAMPLES (CHARCOAL TUBE A5SC~T::% 1. Plant: C-$ 2. Serole ID: LC- &2 - J C Lot No. of Tube ) O0 3. Sanoling Pete C /z 3J17 Tire Started ***A\ Ti~s Ended Z ^ /*A Elapsed Tire________ 0 . ^ Z. A g < 4. Atn. Press. T 9 /. 3_________rrHg, Temp.3 &. 5. Area the Sar.pl a Represents ** / 8.f0/lA J________ _=C. 6. fiere of Person Wr.c Toc< the Sample C,h#.UTt# J bA)$ 7. Puro Calibration Data: Atmos. Press. *7 mHc, Terr. J/. 7 Pump Flow Rate___________ ^C>cc's'-ir. qq 8. Remarks: Include any partinert information such as sciVs, lee's, sending for lab, etc. if ar.y, which ray be cause "or circle* escape cf hydrocarbons into the air. 9. TSL Analysis Data: ooooo^62 s&- DATA SHEET A.VHIEVT A IP. SAMPLES (CHARCOAL TUBE ABSOFA~::\ 1. Plant: <~*A*L0S 2. Savoie ID: 3. Sampling Date ^ /? 3 - ~7 7 t_Qt *;0b 0f Tube ^^ 6 Time Started **** A* Ti-s En-'ed 2,io yoyv Elapsed Time__________ 4. Atm. Press._________7 *? / J______ rrHg, Temp.3^-35c. 5. Area the Sample Peo-resents <^QKBA_______________ 6. Name of Person t 7. Putoo Calibration OC< tre Sir,gig C-&A*LfrS________ p a: Atros. Press. *3f"?0. 7 innHc, Tsro. 3/ 7 Pump Flow Rate_____________ ^^ cc's'dr. 8. Remarks: Induce any osrtinert information such as sc* for lab, etc. if ar.y, vTr.ich ray be cause for hydrocarbons into the air. <s, 5 2-nding escice cf 9. TSL Analysis Data: 0000'' r*.-I AIR SAMPLES > CHARCOAL TUBE AS SOFAT: I'* 1. Plant: J- A 2. Sar.ole ID: t- - 8 2 $ Lot No. of Tube / O Ce> 3. Sampling Pete ^ '3.3 -*7^ Tire Started C ^ ^ Am Ti-g t>,ced 3 ^ ^ Elapsed Tire________ *? 1. A 4. Atn. Press. 7 ^ / 3 rrrHg, Temp.3 o . 3 5. Area the Serde represents ^ <2./? & f 0 A A1 ;c. 6. Nere of Perse" Who 7oc< the Sample ""T"^ ^ L. t % 7. Purp Calibration Data: Atros. Press. 7* 7g- 7 nr.Kc, Taro. 3 A 7 "c Pimp Flow Rate 2,cc's '_ir. 8. Remarks Induce ary r-ert inert ir.forration such as sc* for lab, etc. if ary, which ray be cause for hydrocarbons into the air. , sanding sc= oe **f 9. TSL Analysis Data: SAL 000009164 CONTINENTAL OIL COMPANY PONCA CITY, OKLAHOMA REFINING TECHNICAL SERVICES LABORATORY Pit. : File: Date: LC 662.1 924 6-8-77 LABORATORY NO.: CHARGE: SUBJECT: F-24-77 LC 49 Summary of Benzene Concentration in Gasoline and Blending Streams - Lake Charles Refinery ANALYTICAL DATA: Sample Number PC 1520 PC 1521 PC 1522 PC 1839 PC 1840 PC 1841 LC 232-77 LC 344-77 LC 345-77 LC 640-77 LC 641-77 LC 642-77 Sample Unleaded Regular Premium Regular Premium Unleaded Vol.: Benzene in Finished Gasoline Samp!e Date Benzene, Vol . March.T977 March 1977 May 1977 May 1977 May 1977 May 1977 1 .5 1.0 1. 1 1.1 1.0 1.1 Sample Number PC 1342 PC 1843 PC 1844 PC 1819 PC 1846 PC 1847 PC 1848 PC 1849 PC 1850 LC 643-77 LC 644-77 LC 645-77 LC 646-77 LC 647 -77 LC 648-77 LC 649-77 LC 650-77 LC 651-77 Vol .S Benzene of Refinery Streams Sample Sample Date Benzene, Vol.\ Coker Gasoline Thermal Gasoline TCC Gasoline #1 L.S.R. n L.S.R. Denuded Casinqhead #1 Reformate #2 Reformate Primary Tower OH May 1977 May 1977 May 1977 May 1977 May 1977 May 1977 May 1977 May 1977 May 1977 0.2 0.3 0.5 1.8 1.6 3.7 0.9 1.0 2.8 REFERENCE: Refining Technical Services Laboratory Report E-74-77 dated 5-19-77. Approved: '2L Associate Chemist L ;, Senior Technologist / cc: GAO-DRU-JRU-MEO-KCH-F SAL 000009165 (conoco) INTEROFFICE COMHUNICATION TO: FROM: DATE: SUBJECT: v M. E. Oliver, Refining, Lake Charles H. C. Anderson, Refining, Billings B. W. Marks, Refining, Paramount D. A. Lindberg, Refining, Wrenshall M. Lider, Refining, Ponca City E. W. Carpenter, Refining, Denver T. . Courtney, Refining, Ponca City May 27, 1977 Charcoal Tubes for Ambient Air Sampling We are shipping to you on May 27, 1977, 25 each charcoal tubes and 3 clip-on-guard tubes for use in sampling air for the subsequent analysis of the benzene content. We will supply you with all the necessary charcoal tubes for the duration of this project. Inform us when your supply gets short. If you already have clip-on-guard tubes please return those we have sent. Attached is an example data sheet which we will need for each sample. This data sheet must be complete to avoid foul ups in record keeping. Additionally it contains the necessary information for us to make analysis calculations. Attached also are recommendations for proper sampling and charcoal tube sample transmittal. Use your own system for identifying the charcoal tube samples, however insure the same identification is usedon the data sheet. Attached also is a copy of the method we will use for the analysis. We suggest you become acquainted with this method. We realize that you may not be responsible for the sampling program at your respective refineries, however we will be looking to you for assistance in monitoring the technical aspects of the sampling program. Your assistance with this project will be greatly appreciated. (Jr . Courtney Senior Technologist Technical Services Laboratory lm CC: GAO-RBB-DBS-JWD-IFW-RGA-KCH-F S*L 0009I66 DATA SHEET A?*31ENT AIR SAMPLES (CHARCOAL TUBE ABSOR? 1. PIent: 2. Samole ID: 3. Samolinq Date Lot No. of Tube Time Started Elapsed Time 4. Atn. Press.rnrr.Hg, Tenp.:C. 5. Area the Sample Represents______________________________________________________ 6. Name of Person Who Took the Sample________________________________________ ___ 7. Pur-o Calibration Data: Atmos, Press.Tero. ____________ Pump Flow Rate _______________ cc's'-ir. to II) 8. Remarks: Include any pertinent information such as st'',*s, la< for lab etc. if any, which ray be cause for hydrocarbons into the air. C 9. TSL Analysis Data: SAL 000009167 Interoffice Communication TO K. C. Hunt, Refining, Ponca City From J. 0. Mangelinkx, Refining, Lake Charles Date September 19, 1977 Subject Sample Analyses We are sending via the company shuttle three charcoal tubes for Benzene Content, data sheets are attached. SAL 000009053 DATA SHEET anbieiiT air samples (charcoal tube absorption) 1. Plant: Lake,Charles Refinery 2, Senpie ID LC-3Z- f 2. = 3. Sampling Da //s/n -} Elapsed Time____ Lot No. of lube______ / ^ ^ Time Started f.e //ca AS T i me Ended 3 70 />A> 4. Atm. Press.0 C C. OmmHg, Temp.2. *7. Z.C. 5. -Area the Sample Represents^______ PA*CSJ A A M A, ptwfiA fit*A vf ^ 6. Name of Person "no Took the Sample J TU O, 7. Pump Calibration Data: Atmos. Press. 0 6 jl mmHg, Temp. 2 J. 3 op. Pump Flow Rate___ S! ____ cc1s/min . 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in Job performance 10. S-ampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM 00000905^ SAL DA i n SHEET ANCIENT AIR SAMPLES (CH A'COAL TUBE ABSORPTION) 1. Plant : Lake,Charles Refinery 2. Sample ID: 3. Samolinq Date 9O 77 Elapsed Time Lot Mo. of lube /oU Time Started 7^*A*Time Ended fr.o tfouAS pi* oo 4. Atm. Press . "7 C C. o 5. Area the Sample Represents r.mHq, Temp. Pn oc.fJt -2 7.2. e6rtUftA. . T e <- . * z c-r u, < pdl. V 6. Marne of Person Who Took the S 5-pls ft 1 C S. UlOQAtlH 7. Pump Calibration Data: Atnos . Press. 7 mmHq , Temp . A J. 3 C. Pump Flow Rate cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .10. Sampling and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph11 disulfide 11. TSL Analysis Data: PPM SAL 000009055 DATA SHEET AMBIENT AIR SAMPLES (CHARCOAL TUBE ABSORPTION) 1 . Plant: Lake.Charles Refinery 2. Sample ID: LC-3Z- YHLot No. of Tube/ O ________________________________________ 3. Sampling Date Time Started "^^AMTime Ended 3 ^ f*M. Elapsed Time________________f~* & 4. At". P r e s s. _______?.feC..g________ mmHg, Temp.2 7, Z.C. 5. -Area the Sample Represents A/ X/iAoa/ a+&a"Tau 6. Name of Person Who Took the Sample________ A. J. MASH____________ 7. Pump Calibration Data: Atmos. Press. "? C? mmHg, Temp. 13-3 C. Pump Flow Rate_________ S'/cc's/min. S. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .10. S-ampling and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide 11. TSL Analysis Data: PPM S4L oo90S6 (conoco) Interoffice Communication to Frm Date subject k. C. Hunt, Refining, Ponca City J. J. Uangelinkx, Refining, Lake Charles September 13, 1977 Sample Analyses We are sending via the company shuttle three charcoal tubes for Benzene Content, data sheets are attached. We request an additional supply of charcoal tubes. 0000090^ sM- DATA SHEET amd:e:;t air samples (charcoal tube absorption) 1. Plant: Lake.Carlas Refinery .2 5 arple I D LC-SZ- O ? 3. Sampling Da ? 'i/7 7 Elapsed *ime_ Lot No. of iube_/ o C ____________________ Time Started 9 ^AhTips Ended 3 /Vh r //>oAs - 4. Atm. Press. *7 mmKg, Temp .3 ^ ^___________________________C. 5. Area the Sample Represents______________________________________ _________ Sf l F*r P* 6. *;are of Person V'ho Took the Sample WAQj _________ 7. Pump C a 1 i b r a t i c n Data: Atncs . Press. 7 C-7. / r.nHq, T e m p. 3. Si Pump F1 ow Pate . S 3cc's/min. 8. Remarks; Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .10- n. Sampling and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide TSL Analysis Data: SAL 000009058 AKBIEmT DATA SHEET samples (charcoal tuse ABSORPTION) 1. Plant: Lake,Carles Refinery 2. Sample ID: LC-iI- pPLot No. of Tube J & C_ 3. Sampling Date ^ Tire Started O^A^iTirne Ended Elapsed Time__ft*' & tfOU A. J 4. At". Press._ _mmKg, Temp.__ 31.2.c. t __ 5. -Area the Sample Represents_________ __ .___________________________________________ __ / /J 4 P&c*r./*> V________________________________ D /7T_____ 6. Name of Person Who Took the Sample JiM ____________ 7. Pump Calibration Data: Atncs. Press. 7C7. / mmKg, Temp. 2-S. <r C. Purp F1 c-` Pate_________ ________________ cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .10. Sampling and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide 11. TSL Analysis Data: PPM SAL 000009059 DATA SHEET AMS I E N 7 a: a samples (c- APCC-.L TUBE ABSORPTION 1 1. Plant : Lake.Charles Pa finery 2. bar pi e ID: LC-5i- Ft Lot No. of lube / t> c 3. Sampling Date // cl2ps edV"i-e Time Started *7 AAtTime Ended J f'* 0 //60A5 4. Atm. Press. 7 <-C. r 5. Are 2 the Sample Per resents r.mHq, Temp. 3 Z. -3. c. S AS $ P g C.~r*4Ar Of flT\ 6. Name of Person aho 7 c c !< the 5 enpl s O Ai0 C^AA C/tL*>9 fi* 7. Puiro Cal i brati cr. "ate: Atmos . Press. "><,7. f mrr.Kg, Temp. 2 f. C C. Purr F1 c v.' Rate ** ccrs/min. 8. Remarks: Induce ary pertinent i -formation such as spills, leaks, sampling for lab, etc. if any, which may he cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .1011. Sampling and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph11 disulfide TSL Analysis Data: PPM SAL 000009060 Interoffice Communication to K. C. Hunt, Refining, Ponca City From j. o. Mangelinkx,Refining, Lake Charles Date subject September 9, 1977 Sample Analyses We are sending via the company shuttle three charcoal tubes for Benzene Content, data sheets are attached. lb / CC: MEO, THM, FILE(2) SAL 000009061 DATA SHEET AMBIENT AIR SAMPLES (CHARCOAL TUBE ABSORPTION) 1. Plan t: Lake.Charles Refinery 2. Sample ID: LC-3Z- *7 C- 3. S- r.Dline Dats ^ &/"7 7 f7 Elapsed Time 4. Atm. Press. "7C-6.Y 5. -Area the Sample Represents Lot No. of lube /H Time Started '7'^^iTime Ended 3^ Pa-i * X.o //aoAS mmHg, Temp. & V A AO 1-"? c. 6. Name of Person Who Took the Sampl e A LUlp Grit t 0 Q.0~t 7. Pump Calibration Data: Atmos. Press. "7 <-7. f mmHqs Temo. Ac./ Op. Pump Flow Rate %5~& cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks. sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .10. 11. Sampling and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph11 disulfide TSL Analysis Data: PPM SAL 000009062 AMD I M DATA SHEET S A w = LES (CHARCOAL TD5E ABS03PTI OH ) 1 . Pian t: lZr a 5 '-nr.srv 2. SampIs ID: LC 3. Sen?ling Dat=_ 5 /f/n / 7^ El p5C i r.5___ Lot No. of lube/ O C___ Time Started 8^** Time Ended Vd* /*>t _1T*otfo u AS 4. Atm. Press.~7 *+ t+.H_______________ mmKg, lemp.____________ ____________________C. 5. -Area the Sample Pep res sr. ts A / A M **U#AU 6. Mens of Person V.'hc T: e ; the Sample Q fL U_____ tv/L-J6 7 8 9 _*_1_1________ 7. Pump Calibration Oats: Atmos . Press. remHq, Temp. 3.4,/ Qq Purz How RateH H________________________ cc's/mln. 8. Remarks: Include ary pertinent infornatlon such as spills, leaks, samplin' fcr lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .10. 11. Sampling and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide TSL Analysis Data: PPM 000009063 SAL DATA SHEET AMS I ENT AIR SAMPLES (CHARCOAL TUBE ABSORPTION) 1. ?\cr,z: Lake,Charles Refinery 2. Sample ID: LC-3Z- P*________ 3. Sampling Date Elapsed Time____ 4. At". Press.________ ^ 5. Area the Semple Represents__ Lot fio. of lubes v Tine Started 8^^*tTime Ended V TrO //OUAS mmHg, Temp.___________ 3. C-* ?C. S>JiA# T A/ v ~ 6. Name of Person Who Took the SampleJ ^_______________ ~T & B Q 7. p-jmp Calibration Data: Atmos. Press. O mmHga Temp. X Cr ( Qc. Pump Flov/ Rate__ ___cc`s/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if*any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn In Job performance . 10. 11. Sampling and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide TSL Analysis Data: SAL 000009064 (conoco) Interoffice Communication to K. C. Hunt, Refining, Ponca City From J. j. Mangelinkx,Refining, Lake Charles Date September 7, 1977 subject Sample Analyses We are sending via the company shuttle three charcoal tubes for Benzene Content, data sheets are attached. SAL 000009065 DATA SHEET a?-:s;e;;t ai3 s.-vples (c-arcoai tuse absorption) 1 Plant: Lake.Chari55 Rafinery 2 3 4 5 Area the Sample Represents PO P-'TA'T/dPj LtCUT T&t>cu + 'TflArCtefK *PSLKT6fl 6 r.'ame of Person Vr.c Took the Sample G-u AUM ffARV&Y _______ _ 7, Pump Calibration Tata: Atmos. Press. C 0 . k rmHg, Tenp. 2Ct 7 C. Pur.p Flow Rate __ cc's/min. 8. Remarks: Induce any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in Job performance 0- Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatcgraph 1. T5L Analysis Data: PPM SAL 000009066 DATA SHEET AHBIEiiT A': R SAMPLES (CHARCOAL TUBE ABSORPTION) 1. Plant: Lake,Charles Refinery r 2. Sample ID: LC-SZ- "7 V_________ Lot No. of Tube_______ J > 1+_____ 3. Sampling Da L Tims Started 7 ^^ArTime Ended 3 3 P* Elapsed Time_____ Fi t> /fQVAS ` ~- 4. Atm. Press.________ O _______ mmHg, Temp.3 3* 3__C. 5. -Area the Sample Represents,'T' flPtVlPO A'rACT**# *____________________ ___6 7 6. Name of Person V.'hc Took the Sample A fUi_______ $ *Tg _________ 7. Pump Calibration Data: Atmos. Press. Co. mmHg, Temp. X C,,7 op. Pump Flow Rate__ V9 __ cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10- Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11- TSL Analysis Data: PPM SAL 000009067 DATA SHEET AMSItwT AIR SAMPLES (CHARCOAL TUSE ABSORPTION) 1. Plant: Lake.Charles Refinery 2. 5anple I D : IC-3Z- 3Lot No. of Tube_________________ / & _________ 3. Semolina Date *7 Tins Started 7 *Ti me Ended 3^pa- // -------------------- --=--------- Elapsed TineFT O rfQO A S -- 4. Atm- Press._________ 7 C X,S~mmHg, Temp.___________ 33.3 on. 5. -Area the Sample Reoresents__________ T*A AJi/f ^ ATAT /4 H~0 A U V_______ $ u\P H&MT& PA ArcA_____ 6. Name of Person l.'hc Took the Sample J/M SPA AV UPAAV 7. Pump Calibration Data: Atmos. Press. "7 60,1 mmKq, Temp. -It.7 op. Pump Flov/ Rate__ ______ sz ____ cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which, may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn In Job performance .10. Sampling and analytical method: Absorption or charcoal Desorption v;Ith carbon Gas chromatograph11 disulfide 11. TSL Analysis Data: SAL 000009068 Cconoco) Interoffice Communication to K. C. Hunt, Refining, Ponca City From J. J. Mangelinkx, Refining, Lake Charles oat* September 2, 1977 Subject Sample Analyses We are sending via the company shuttle three charcoal tubes for Benzene Content, data sheets are attached. SAL 000009069 oat;, sheet AM3I.7T AIR S A. " L S (CHtRCC-L T'JS ABSORPTION) 1. Plant: Lake .Charles "efinery 2. Samp7e i 0: LC-3Z- 9 OLot .h'o. cf Tube / & C_________________________ 3. Sampling Cats * A/77 Tirs Started 7J<Vl*iTir:a Ended 33 0 pfx Elapsed Time____________ ^ O______ Hqoa. $ 4. AtrPress._______ O Cf, ?rrrHg, lenp.Z. P- J_________________________________ C. 5. -Area the Sar.pl e Represents,______ u y-y______ ___________________________ 6 7 8 9 * 11 6. Name of Person Who seek the Sarpls Re>X>t\l.D e- AgjUA U AV 7. Pump Calibration Data: Atnos. Press. *7C4,V mmHq, Temp- 2.C.7 Qc. Pun? ~ 1 cv.' Pate___ S3 ___ c:* s/rr.in. 8. Renarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which nay be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .10. 11. Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph TSL Analysis Data: PPM 000009070 SAL TATA SHEET AMBIENT AIR SABLES ( C - A P C - L T 'JBEA 3SGPPTI0 \*i 1. Plant: Lake,Charles Tefir.ery 2. Sample I D : LC-SZ- 7 /_L c t No. of Tube__________________ / Q O______________ 3. Sampling Data*?/l/'77 Tire Started 0 7*AH Ti rra Ended 3 3 PA Elapsed TireS', 1+ooAS 4. Atm. Press.________ __________________r.r.Hg, Temp. ^ 9C. 5. -Area the Sample RepresentsJ A aj * t^ __________________6 7 8 9 * 1 6. Name of Person '.-'ho the Sample V A AY A1 o T G- a 7. Pump Calibration Data: Atmos. Press. 1 CC. H rr.m.r'c, Temp. 26,7 op P.rp -lev; Rate S 7____ ___c c's/fiiir,. 8. Remarks: Include ary pertinent information such as spills, leaks, sampling for lab, etc. if any, which ray be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .10. Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM SAL 000009071 DATA SHEET ambient air samples (charcoal tube ABSORPTION) 1. Plant: Lake.Charles Refinery 2. S amp 1e ID LC-3Z- n ^ 3. Ssr.pl ins Da Elapsed Time Lot No. of lube______________ Ti me S ta rted ~7 * i me Ended 3^ pf tfooAS 4. Atm. Press.________ 9 6 _________mmHg, Temp.__________ 2- ^9c. 5. -Area the Sample Represents y->oufZ g pA iAa* A AS 6 7 8 9 * 11 6. Nsre of Person Vino Took the Sample W. J OH/*S~raA/ 7. Pump Calibration Data: Atmos. Press. "7C&.V mmHg, Temp. 1C.7 c. Pump Flow Rate_______ _^LS ___ cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn In job performance .10. 11. Sampling and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide TSL Analysis Data: PPM SAL 000009072 Interoffice Communication to K. C. Hunt, Refining, Ponca City From j. J. Mangelinkx,Refining, Lake Charles Date Subject August 31 , 1977 Sample Analyses We are sending via the company shuttle three charcoal tubes for Benzene Content, data sheets are attached. SAL 000009073 DATA SHEET AMBIENT AIR SAMPLES (CHARCOAL TUBE ABSORPTION) 1. Plant: Lake.Charles Refinery 2. Sample ID: LC-BZ- C`7 Lot No. of lube J C 3. Sampling Date Time Started H** Am Time Ended 3 * 6 PM Elapsed Timeft 0 Houns 4. Atm. Press.CmmHg, Temp. 2. ?________ C. 5. Area the Sample Represents\aj / 40 0-A.______________ f QA.&M A a> 6 7 8 9 10 11 6. Name of Person Who Took the Sample H'AajU______ Gr- L au&A_____________ 7. Pump Calibration Data: Atmos. Press. ^ 7 o.f mmHg, Temp. 3 C.9 C. Pump Flow Rate____ SH __ c c's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM SAL 000009074 DATA SHE*' AMS AIR ? LES (CHARCOAL T;J5E ABSORPTION) 1. Plant: Lake, Chari as Refinery 2. Sample ID: LC-3Z- L-t__Lot No. of T ufce /ft _________ 3. Sampling Data______ ?/j J'7 Time Started 0*P>Winie Ended pt1 Elapsed Time!Pt V H 4. Atm. Press.*7 O 0mmHg, Temp._______________________ 2 5. -Area the Semple Represents______w f UOPA______ , 9 * 1 oc. 6. Name of Person Who Took the Semple C A ^ ft t At i & 7. Pump Calibration Date: Atmos. Press. **) ? <> mm.Hg, Temp. -2. 4. *7 C. Pump Flow Rate____ __ cc's/min. 8. Remarks: Include any pertinent information such ar spills, leaks, sampling for lab, etc. if any, 'which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump v/orn in job performance 10. Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM oooo9015 S M- DATA SHEET AMBIENT AIR SAMPLES (CHARCOAL TUSE ABSORPTION) 1. Plant : Lake.Charles Refinery 2. Sample ID: LC-3Z- 6 5 3. Samplino Date P,/7e'/*77 Elapsed Time 4. Atm. Press. 96 C 5. Area the Sample Represents Lot .Vo. of lube / & (* Time Started O 0JtfA**Time Ended 0UJl | mmHg , Temp. ? f". ? . i f,T~ c. 6. Name of Person Who Took the Sample LASAl>v. 7. Pump Calibration Data: Atnc s. Press. mmHq, Temp. xt.o oc Pump Flow Sate SY cc' s/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hy drc-ca rbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. S-ampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph11 11. TSL Analysis Data: PPM SAL 000009076 (conoco) Interoffice Communication To K. C. Hunt, Refining, Ponca City From J* J* Mangelinkx, Refining, Lake Charles ate August 26, 1977 subject Sample Analyses * v * We are sending via the company shuttle two charcoal tubes for Benzene Content, data sheets are attached. ooooo^1 DATA SHEET AMS1EUT -::R SAMPLES (CHARCOAL TUBE ABSORPTION1) 1. Plant: Lake.Charles Refinery 2. Sample 15: LC-5Z- (s CLot No. of lube______________ f/ _______________ 3. Sampling Date__ fAjf1 Time Started_2_^AM_Time Ended *j J' flAt Elapsed Ti me3. . & H ao A S 4. Atm. Press.T? C 6_ 9*mmHg, Temp._X 7 . -3.C. 5. -Area the Sample RepresentsQ oT St Q0_________________ A^A-ctf /MU?" 6. Name of Person V'f.o Took the Sample^ C~HAtLl>S K U. & ATtLitH 7. Pump Ca 1 i b r a t'< cr. Data: Atmos. Press. 0 C 3. o mmHg, Temp . 2.C. / Qq. Pump Flow Rate___ __ ccrs/min. 8. Remarks: Include any pertinent information such as spflls, leaks, sampling for Tab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the aTr. gArr 0A i vu0t*T D&aq / batt?*.-* 9. Sample Procedure: Personal Sampling pump worn in job performance 10. Sampling and analytical method-' Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM 000009073 SAV- DAiA SHEET AMBIE'ii AIRS ? LES (CHARCOAL TUBE ABSORPTION) l. Plant: Lake.Charles Refinery .2 Sample ID: LC-3Z- O S 3. Samp 1inc Elapsed iime__ 4. Atm. Press. 7 4^, ? 5. Area the Sample Represents Lot No. of lube___ /oC Time Started 7 30 Ai me Ended 3 1 PM 0.7 H & J mmKg, Temp._________ n. r________ c. o o-rstoe_____ Ai A C A4 / JUtS'T 6. Name of Person LTho Took the Sample_____ Ay____________ CA/A^__ 7. Pump Calibration Data: Atncs. Press . *7 t> J, o mrnh'g , Temp. X C. / C. Pump -low Rate___ So __ cc *s/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM SAL 000009079 (conoco) Interoffice Communication To K. C. Hunt, Refining, Ponca City From J. 0. Mangelinkx, Refining, lake Charles Oate August 23, 1977 Subject Sample Analyses We are sending via the company shuttle two charcoal tubes for Benzene Content, data sheets are attached. # 000009080 sM- DATA SHEET AMBIENT AIR SAMPLES (CHARCOAL TUBE ABSORPTION) 1. Plant: Lake.Charles Refinery 2. Sample- ID; LC-3Z- t 3 Sampling Date 3. J* y/i ? Elapsed Time 4. Atm. Press . Ot 5. Area the Sample Represents Lot No. of I ube / & lm Time Started 9 3 0 A* Time Ended 3 ^ * P*i r. 0 H 00 a i mrr.Hq, Temp. p* r*e 3 0. , / s*r C. 6. Name of Person Who Took the 5;role O HAAt^0S c. o o _______ 7. Pump Calibration Data: Atnos. Press. D O. Vmnrg, Temp. 3.C.V op. Purp Flov.' Rate%~ occ's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling Tor lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM SAL 000009081 DATA SHEET AMS TENT A: R SAMPLES (CHARCOAL TUBE ABSORPTION) 1. Plant: Lake.Charles Refinery 2. Sample I u: LC-3Z- C HLot No. of Tube_' & i- 3. Sampling Date_______ r/A>_Tirr.e Started 9 3 ^A^iTi me Ended 3 * * Elapsed Time 4. Atm. Press._______ 7 6 f, cmmHg, Temp.Z. 9. ^ C. 5. -Area the Sample Represents'f* / P f t 'nr0.fi,_______________________________________ .6 Name of Person 1- o Took the 5ample_ Unlrl-U VUrioAJ 7. Pump Calibratic: Data: Atmos. Press. 9 C 0. I mmHq, Temp. 2 L.V Qq, Pump Flow RateS' occ's/min- 8. Remarks: Include any pertinent information such as spills* leaks* sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .10. 11. Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph TSL Analysis Data: PPM 000009082 SAL (conoco) Interoffice Communication to Frpm_ _ K. C. Hunt, Refining, Ponca City _J .MangellnkXj Refining, Lake Charles Date August 19, 1977 sublet Sample Analyses We are sending via the company shuttle two charcoal tubes for Benzene Content, data sheets are attached. lb / CC: MEO, THM, FILE(2) SAL 000009083 Da h S h c l T ambient air samples (charcoal tube absorption) 1. Plant; Lake.Charles Refinery 2. Sample ID: LC-5Z- Z, /___ , . . Lot Ko.. of Tube 7oC ~J 3. Sampling Dateth^/m Tine Started *> * Af-\ Time Ended 3 * Elapsed TimeT. 0 4. Atm. Press. X. mmHq, Temp.? C.*7*>c. 5. -Area the Sample Represents_______ fMjtag____ _____/^Ac.t4/A/)S7~ 6. Name of Person V.'r.o Took the Sample J OHM______ vT A JV Q&A J 7. Pump Calibration Data: Atncs. Press.9 cy, o mmHq, Temp. Z SI c op. Pump Flow Rate____ y 8 __cc's/min, 8. Remarks: Include ary pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure; Personal Sampling pump v/orn in job performance .10. 11. Sampling and analytical method Absorption or charcoal Desorption with carbon Gas chromatograph disulfide TSL Analysis Data: PPM 00908* SAL OOO DATA SHEET AHSIENT air samples (charcoal tuse absorption) 1. Plant: Lake.Charles, Refinery 2. Semple IQ: LC-Sl- L- 2^ ^ ^Lot No. of Tube ~ . ' c^- 3. Sampling Sate xfnA? _Time Started Ah Time Ended 3** /*M Elapsed Time____ _______ f. S tfwtis 4. Atm. Press.____________7C?. L _mmHg, Temp.3 f- t_________________________ c. 5. -Area the Sample Represents^ 'f* A / A/ T0 ft - / Vf** L at^A , 9 S'T" 6. Name of Person Who Took the Sample^ f/AMLO c.ofii-iAJ 7. Punp Calibration Data: .Atmos. Press. Ocy.o mmHq, Temp. 3. j*. C- Qc. Pump Flow Rate cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM sal 000090as (conoco) Interoffice Communication To K. C. Hunt, Refining, Ponca City 0. J. Mangelinkx,Refining, Lake Charles Da-.e August 16, 1977 s_Dject Sample Analyses We are sending via the company shuttle two charcoal tubes for Benzene Content, data sheets are attached. SAL 000009086 DATA SHEET AMDIEKT AIR SAMPLES (CHARCOAL TUBE ABSORPTION) 1. Plant: Lake . Charles. Refinery 2. Sample ID: LC-3Z- ~*i 3. Sarr.plinq Date 5"/y c/? 7 Elapsed Time 4. Atm. Press. 77/./ Lfrt Pvo. oT Tube 4, * " / O C* Time Started 7 Ti me Ended -3 PM f. 2- #>*> AS mmHq, Temp. 1 r..? c. 5. Area the Sample Represents OA.0 M AAJ , / A* S'T'Zl T CrAovt* 6. Name of Person V.'ho Took the Samp 1 e l~ - U . SRA ffMZfl. 7. Pump Calibration Data: Atmos. Press. 9 7^/ mmHq, Temp. Z 7. \ C> Pump Flow Rate_S *7cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump v/orn in job performance 10. S-ampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM SAL OOQOO9087 a?-;sie;;t DATA SHEET LES (CHARCOAL USE ABSORPTION') 1 . Plan*: Lake.Charles refirery 2. Sample ID: LC-C-- y O_______ 3. Sampling Date ?/*<*/'> 7 Elapsed Tire___ Lot No. c f Tub Tire Started O _____ Hot* A j / T> C* ________ Tire Ended 3 J ^ PAA 4. A. t rr,. Press.__________ O Q t / r.uiKg > Temp .___________ ?. VC. 5. Area the Sample Rerrsssr,t3_ _________________________ A/-1/A C. OAV 6. Name of Person Who Tc< the a mole_________ 7. Pump Calibration Data: A ores. Press . "7 f rnr.Hg . Terno. X7.^c. Pump r i o (' Rate____________VO_______ cc1 s/mi n . 8. Remarks; Induce a r.y parti nent information such as spills, leaks, sampling -:r lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. S-ampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM SAL 000009088 (conoco) Interoffice Communication To K. C. Hunt, Refining, Ponca City From J. J. Mangelinkx. Refining, Lake Charles Date Subject August 5, 1977 Sample Analyses * We are sending via the company shuttle two charcoal tubes for Benzene Content, data sheets are attached. We request an additional supply of charcoal tubes. SAL 000009089 DATA SHEET AMBIENT AIR SAMPLES (CHARCOAL TUBE ABSORPTION) 1. Plant: Lake.Charles Refinery 2. Sample ID: LC-5Z- S' ^ Lot No. of Tube_/ & C __________________________ 3. Sampling Data S'/s/7 -> _T i rri e' Started O'* *4^1Time Ended 3 ^^/Vi Elapsed TimeT- Z____________________ 4. Atm. Press._^ O * 7mmHg, Temp.__________________________ 3 0*0_C. 5. -Area the Sample Represents l* 7~ A jC/J^AJ *- VA/V S AVO*_ 6 . Name of P e r s o n Who Took the Sample _ 7. Pump Calibration Data: Atmos . Press. *7 C ft Q mmHg, Temp. X <51 C op. Pump Flow Rate^3____________________ cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling -or lab, etc. if any, which may because for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. Sampling and analytical method* Absorption or charcoal Desorption with carbon disulfide Gas chromatograph TT- TSL Analysis Data: PPM SAL 000009090 DATA SHEET AMBIENT AIR SAMPLES (CHARCOAL TUBE ABSORPTION) 1. Plant: Lake.Charles Refinery 2. Sample ID: LC-3Z- S ^ 3. Sampling Date_ S'Jsf/?? Lot No. 'of Tube} 0 Time Started 7^A^vTirne Ended 3 P* Elapsed Time^ Jt>*AS 4. Atm. Press . 7 7 >, 7 5. Area the Sample Represents mmHg, Temp. 327 C V A vs Of > LLA&O 6. Marne of Person V.'ho Took the Sample__ 7. Pump Calibration Data: Atmos. Press . 7 c t. C mmHg , Temp. ZS. C C. Pump Flow Rate__________H 7cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump v/orn in job performance 10. Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM >*** SAL 000009091 (conoco) Interoffice Communication to K. C. Hunt, Refining, Portca City From j. j. Mangelinkx,Refining, Lake Charles Date August 1 , 1977 subject Sample Analyses We are sending via the company shuttle tv/o charcoal tubes for Benzene Content, data sheets are attached. lb CC: MEO, THM, FIL/E(2) SAL 000009092 DATA SHEET AMBIENT AIR SAMPLES (CHARCOAL TUBE ABSORPTION*) 1. Plant: Lake.Charles Refinery 2. Sample IS: LC-3Z- S' CLot No. of Tube/ * C ______ 3. Sampling Date* TJ* ) 11 Time Started 0 tfA^Time Ended 3 ?/^\ Elapsed TimeT_________________H&</*.$ -- 4. Atm. Press. _________"> "> 3 - 2 5. -Area the Sample Represents mmHg , Temp.3^*3C. C- A A P mt~ & . / J ^ 6. Name of Person Who Took the Sample <J A M0J 0/l A */ 7. Pump Calibration Data: Atmos. Press . 1t. * Pump Flow Rate s3~ & mmHg , Temp. 16.7 C. cc1 s/min . 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. Sampling and analytical method: Absorption or charcoal Desorption v/ith carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM ^ SAL 000009093 DATA SH-ET AMBIENT AIR S.-.VPLES (CKARCCAL TUBE ABSORPTION) 1. Plant: Lake.Charles Refinery 2. Sample I D : LC-3Z- <5" S'Lot No. of Tube /O U J J3. Sampling Date______ * ~7 7 Tire Started ^^Time Ended 3 ***PM Elapsed Ti mef*- S'___________________ tfooA- J 4. Atm. Press.1 3. ZmmHg, Temp.3 Z. ____________________________________________ C. 5. -Area the Sample Represents c- a fl P&mt ^ &-+* to+s 6. Name of Person Who . cok the Samp 1 s & L-&$/z'T- 7. Pump Calibration Dene: Atmos. Press. *772-/ mmHg, Temp. 3.6.7 0 C. Pump Flew Rate____ rs __ cc1 s/min. 8. Remarks: Include ary pertinent information such as spills, leaks, sampling "tr lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9.. Sample Procedure: Personal Sampling pump worn in job performance 10. S-ampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM SAL 000009094 (conoco) Interoffice Communication To K. C* Hunt, Refining, Ponca City Fron J. J. Mangelinkx,Refining, Lake Charles Ds July 29, 1977 s-jaject Sample Analyses We are sending via the company shuttle two charcoal tubes for Benzene Content, data sheets are attached. We request an additional supply of charcoal tubes. sAL 000009095 DATA SHEET AMBIENT AIR SAMPLES (CHARCOAL TUBE ABSORPTION) 1. Plant: Lake.Charles Refinery 2. Sample 15: LC-BZ- S 3______ 3. Sampling Date____T? Elapsed Time___ Lot No. of Tube/ ^ ^ Time Started ^^^A^Time Ended ? tfoon J * P/~% 4. Atm. Press._________^ 5. -Area the Sample Represents_ ___________ fL fir A*______________ mmKg, Temp.3. 0. CC. C~0tlA. t ____________ 6. Name of Person Who Took the Sample SA/l l_____ fz e> s vj&a/ 7. Pump Calibration Date: Atnos. Press . H ^ 3. c* mnHq , Temp. 2. C . / C. Pump Flow Rate^p~cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump v/orn in job performance 10. Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM SAL 000009096 DATA SHEET AMBIENT AIR SAMPLES (CHARCOAL TUBE ABSORPTION) Plant: Lake.Charles Refinery Sample I D ; LC-3Z- _____ Lot No. of lube / OC Sampling Date_ *> A 7 T i me Started LhS Time Ended // 00 1 Elapsed TimeV- 3____________________ WevAS : Atm. Press. . Area the Sample Represents (PAUl t*l jnmHg, Temp. C- o K - yM A M J.X c Name of Person Who Took the Sample _____ O v Hoa* Pump Calibration Data: Atmos. Press. ^13. C mrnHg, Temp. X c,( op. v rPump Flow Rate__ _______ _cc r s/min. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 8*T7A*0S H-Z H&OAS Q&AO Prf-r0A * *> S/Zuic 9. Sample Procedure: Personal Sampling pump v/orn in job performance 10. Sampling and analytical method: Absorption or charcoal Desorption v/ith carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPK SAL 000009097 Interoffice Communication to K. C. Hunt, Refining, Ponca City From J. J. Mangelinkx,Refining, Lake Charles Da July 25, 1977 subject Sample Analyses We are sending via the company shuttle three charcoal tubes for Benzene Content, data sheets are attached. 000009098 SAL DATA SHEET AMBIENT AIR SAMPLES (CHARCOAL TUBE ABSORPTION) 1. Plant: Lake.Charles Refinery 2. Sample ID: LC-3Z- / 3. Sampling Date Elapsed Time Lot No. of lube Tine Started 6 J & t* At Tt me Ended -2 - 4. Atm. Press . ^ *7 3. 0 mmHq , Temp . 5. .Area the Sample Represents C~ek./L - Z. * C-& A/TtLOi* ***** 3^ c- A t- c- \ as0 A , c. 6. Marne of Person Who seek the Sample R\MSy Q H*? 7. Pump Calibration Data: Atno s. Press. n^t.X mmHq, Temp. *<--3 oc. Pun? Flow Rate ^ cc' s/min. 8. Remarks: Include ar.y pertinent information such es spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 3.1. TSL Analysis Data: PPM ** SAL 000009099 DATA SHEET AMBIENT AIR SAMPLES (CHARCOAL TUBE ABSORPTION) 1. Plant : take.Charles Refinery 2. Sample iD: LC-3Z- S' -1. Lot No. of lube Joc 3. Sampling Date "7 Ji.S/7? Time Started C^^^Time Ended Elapsed Time dr, o. Umax 4. Atm. Pres s . ^7 J' 5. Area the Sample Represents & Q U i l* A* PMT mmHq, Temp. c- ? M 0/1 _ C ALt a A- X to C. 6. flame of Person Who Took the Sample 7. Pump Cali braticn Data: Atmos . Press. A K e-A>Af f\SOA> "7 *>/. Z. mmHq, Temp, Pump Flow Rate S cc*s/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, v/hich may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump v/orn In job performance 10. S-ampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL- Analysis Data: PPM ^ 000009100 SAt r' DATA SHEET AMBIENT AIR SAMPLES (CHARCOAL TUBE ABSORPTION) 1. Plant: Lake.Charles Refinery 2. Sample I D : LC-3Z- ~&Lot No. of Tube/ 0 ______________ 3. Sampling Date"> Time Started C * * T j me Ended -3 ^ Elapsed Time0 HmaS 4. Atm. Press.C 3 r &_________________ mmHg, Temp.-3 A ?C. 5. -Area the Sample Represents_________ C QttEA C-AK t A t ____ _________ 0 P & A ____________________________________________________________ 6. Name of Person Who Took the Sample L-0SDE. f & & $ 7 _ 7. Pump Calibration Data: Atmos. Press. 7 /- ^ mmKq , Temp. 2-6.3 C. Pump Flow RateS' 3^cc*s/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph IT. TSL Analysis Data: PP.M SAL 000009101 Interoffice Communication To K. C. Hunt, Refining* Ponca City 0. j. Mangelinkx,Refining, Lake Charles Dat, July 21 , 1977 s-ibject Sample Analyses We are sending via the company shuttle three charcoal tubes for Benzene Content, data sheets are attached. CC: ME0-THM-FILE(2) shU 00000910Z DATA SHEET AMD I E.TT AIR SAMPLES ( CHARCOAL T US E ABSORPTION? 1. Plant: Lake.Charles Refinery 2. Sample I D ; LC-SZ- H 7Lot "o, of Tubetot* 3. Sampling DateH Jn J1 7 Tine Started 6- V ^Am T f me Ended -2 3 S f*M Elapsed Time^ & Hoon s 4. Atm. Press.O 7Z.?rrmHg, Temp.3. t .*Oq* 5. Area the Sample Represents / 0 AO/A/ G- Ooc-MS 6. Name of Person Who Tech the Sample 7. Pump Calibration Data: Atrscs. Press. *1 J e>. c mm.-g, Temp. 3-C.f C. Punp Flow Rate___________ S Occ's/min. 8. Remarks: Include ar.y pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM sal 00009l03 DATA SHEET AMBIENT AIR SAMPLES (CHARCOAL TUBE ABSORPTION) 1. Plant: Lake.Charles Refinery 2. Sample lu: LC-3Z- H $ 3. Sarnpl inq Date ^f31/ Elapsed Time 4. Atm. Press. ^ 5. -Area the Sample Represents Lot No. of i ufce )o Time Started 4. 4,*~A>sTime Ended i p/-\ *"} - & HovAS --- mmHq,Temp. L 0A O/A/6- 3 0.0 Qo<^X*S c. 6. Name of Person Who Took the Sample WilL/am 7. Pump Calibration Data: Atmos. Press. mmHq, Temp. 2.4.,/ c. Pump Flow Rate H2 cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks J sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM 000009^ SM- DATA SHEET A M BI E r.1 T AIR SAVVIES (CHARCOAL T!J5E ABSORPTION) 1 . Plant: Lake.Charias Refinery .2 Sample I D : LC-3Z- H SLot No* of Tube/ & C_____________________________ 3. Sampling Date"7/2. t J~} 7 Tire Started Time Ended 3 Elapsed T ir.eS*_______________________ H&*> R. i 4. At". Press.0 73.7mraHg, Tem,p.___________________________ 3* OC. 5. Area the Sample Represents LOAQ/AJ&- pcc.u^t / /. oaOA 6. Nare of Person Who 7cc< the Sample_____ Ar As O R ______ -J t> H JS^S d//_____ 7. Pump Cal i brat ion Data: At nos. Press. p ramKg , Temp. / C. Purp Flow Rate_& cc1 s/min . 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM SAL 000009105 conoco) Interoffice Communication to K. C. Hunt, Refining, Ponca City From J. J. Mangelinkx, Refining, Lake Charles Date July 18, 1977 Subject Sample Analyses We are sending via the company shuttle three charcoal tubes for Benzene Content, data sheets are attached. We request an additional supply of charcoal tubes. CC: ME0-THM-FILE(2) DATA SHEET AMBIENT AIR SAMPLES (CHARCOAL TUBE ABSORPTION) 1 . Plant: Lake.Charles Refinery .2 SarnDle ID: LC-3Z- H`iLot No. of Tube 3. Sampling Date H // r) i'? T i e Started Elapsed TireH ova, j /O t***AsTime Ended Z ti*~ -- 4. Atm. Press.7 7*9. 3 mmh'g, Temp.* c- ^_____________ _______ C. 5. Area the Sample Represents Ptt.oovt.-r 7~/ >** 6. Name of Person Who i ock the Sample__ t? L L- L. V O As-S 7. Pump Calibration Data: Atmos. Press Q mrnRg , Temp. 27. Qc Purp Flow RateH *)cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lac, etc. if any, which may be cause for abnormal escape cf hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: SAL 00009107 DATA SHEET AMDU 1 ;t air samples (charcoal tube absorption) 1. Plant: Lake .Charles Refinery 2. Sample I D : IC-3Z- H cLot No. of Tube/ o C_ 3. Sampling Date______/* / ~7">Time Started 4 ^^Time Ended 3- r/^i Elapsed T ime& M oojx j 4. Atm. Press. ^ 7 o.2 mmHg, Temp. X*k. V 5. -Area the Sample Represents PRo QVC*r O /s T/I v /MA-AV 6. Name of Person V.'ho Took the Sample tvnt.AAtf_______s u fit tB 7. Pump Calibration Data: Atmos. Press. 7?*~c mmHg, Temp, c. Oq* Pump Flow RateS'3cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM SAL 000009108 DATA SHEET A>TS11IJT AIR SAMPLES (C :-;rcgal TUBE ABSORPTION) 1. Plant: Lake.Charles Refinery 2. Sample ID: LC-3Z- H 3. Sainalinc Oats ^}tth ' Elapsed Time Lot s o. of Tube /C Tire Started **.A^Time Ended Z*4*' r S^r 0 H-0VA. J 4. Atm. Press . ?o. 3 5. -Area the Sample Represents mmHe , Temp. P R O AOt-'T Z c. *7 p A Ac TV 0 . O 6. Marne of Person Who Took the Sample H &A*R'f o K^o'T Pump Calibration Data: Atncs. Press. cinHg, Temp, a. 7.? Qg Pump Flow Pate>T /cc's/min. 8 Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9 Sam*,ole Procedure: Personal Sampling pump worn in job performanc 'j 10 Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11 TSL Analysis Data: PPiT __ __ T-09 0009 sfr^* If (,1*1 DATA SHEET Ai-!51 EilT AIR SAMPLES (CHARCOAL TUSE ABSORPTION) 1. Plant; Lake .Charles Refinery 2. Sample Iu: LC-3Z- t 3. Semolina Date 3 // Elapsed Time Lot No. of Tube /on Tine Started 7 JA*Time Ended 0 1. s //coA3 4. Atm. Press. 7C mmHq, Temp. i'X . 2. c. 5. Area the Sample Represents C AAinry -rA e/- , x rfS'T^A. 6. Name of Person Who Took the Sample Q ooA.& ots 7. Pump Calibration Data: Atmos. Press. *7 c 3 mmKg, Temp. C Pump Flow Rate cc's/min. 8. Remarks: Induce any pertirsent information such as spills, leaks 9 sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .10. Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM OOOOO^OT-1 (conoco) Interoffice Communication To K. C. Hunt, Refining, Ponca City From J. 0. Mangel inkx, Refining, Lake Charles Dais March 14, 1978 Subject Sample Analyses We are sending via the company shuttle five charcoal tubes for Benzene Content, data sheets are attached. These samples were taken to gather Laboratory Air Circulation Data. CC: HEO, THM, FILE(2) SAL 000009018 (D DATA SHEET AMBIENT .-.IS SAMPLES (CHARCOAL TUBE ABSORPTION) 1. Plant Lake.! 2. Sample ID : LC- 3. Sampl i n g Date El 4. Atm. Press. 5. -Are a the Samp! Lot No. of lube y 69 Tims Started 7 3&A*\ Time Ended 3*3' />** 7----- 7----------------- tfooAS 7<rH mmHg, Temp. V APoA r tif ssuae C. 8ath 6. Name of P e rs on 7. Pump Cali b r a t i Ja Atmos. Press-?<, f jnmHg, Temp. 2o.o op Pump FI ow Rate__________ ______ *S" cc's/min. 8. Reemmaarrkkss:: Indcluce any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .10. Sampling and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide 11. TSL Analysis Data: SAL 000009019 DATA SHEET AMBIENT AIR SAMPLES (CHARCOAL TUBE ABSORPTION) 1. Plant: Lake.Charles Refinery 2. Sample I D: LC-3Z- //J Date 3. Sampling 3/if/ir " / r~ Elapsed Time 4. Atm. Pre SS. 5. Area the Sample Represents Lot No. of lube JO*? Time Started *7 - r,,e> //ooAS Time Ended mmHq, Temp. A *7. ^ PA -TA1 -- c. 6. Name of Person Who Took the Sample &/a 7. Pump Calibration Data: Atmos Press. *7 ^ Pump Flow Rate mmHq, Temp. XOmo C. VP cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump v/orn in job performance 10. S-ampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM SAL 000009020 DATA SHEET A 5 (CHARCOAL TUBE ABSORPTION) 1 . Plant: Lake .Conies Refinery .2 Sample ID: LC-3Z- //*V 3. Sampling Date ________Lot No. of Tube/ 6 *7_ Time Started Time Ended 3 * PM Elapsed Ti reffOQA 5 4. Atm. Press.7CV_rcniH9, Temp._________________________ ________ C. 5, -Area the Sar.pl e Represents / 'r&S'f&AJ 3ALAMC 6. Mare of Person VIhe Took the Sample /a 7. Pump C a 1 i b r a t i cr. Data: Atncs . Press. ~? (r f mmHq, Temp. 3.^. O Oq Purp Flow Rate S' / cc's/min. 8. Rem a rfcs : Incl uds any pertinent information such as spills, leaks. sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal `Sampling pump worn in job performance 10. Sampling and analytical method* Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM _____ SAL 000009021 gj emu* DATA SHEET AMBIENT hiR SAMPLES (CHARCOAL TUBE ABSORPTION) 1. Pi ant : Lake.Charles Refinery 2. Sample ID: LC-3Z- f t f* 3. Sair.olinq Date Elapsed Time Lot No. of lube Time Started /*'7 Time Ended 3^ /*A1 ~ fr0' //aoAS -- 4. A ~ m Press . "7 <-Y 5. Area the Sample Represents X. A 0 *7"A mmHg, Temp. C-W^AWJT J 6VTH fiAJT C. 6. N ane of Person Who Took the Sample 7. Pump Calibration Data: Atmos. Press. *7 C / Pump Flow Rate mmHg, Temp. 2^.^ c. H cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks > sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .10. Sampling and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide 17. TSL Analysis Data: PPM _____ SAL 000009022 () DATA SHEET AMD :z:;t a:a samples (charcoal tube ABSORPTION) v 1. Plant: Lake.Charles Refinery 2. Sample ID LC-3I- //C- 3. Samoline Date 7/ Elapsed Time 4. Atm. Pres s. 7 tV 5. Area the Samp!e Represents Lot No. of Tube Time Started SO1*) Time Ended 3o 3* tfooAS mmHq, Temp, *-7. X Mfifccti (Locm f a co oo 6. Name of Person Who Took the Sample "/a 7. Pump Calibration Data: Atmos. Press. -?(, r mmHg, Temp. Zc. o Oq Pump Flow Rate ^ cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks. sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal `Samp 1ing pump worn in job performance .10- S-ampling and analytical method: Absorption or charcoal Desorption v/ith carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM SAL 000009023 (conoco) Interoffice Communication K. C.-Hunt, Refining, Ponca City Ffom J. J. Mangelinkx, Refining, Lake Charles Oate March 10, 1978 subject Sample Analyses ___ We are sending via the company shuttle five charcoal tubes for Benzene Content, data sheets are attached. SAL 000009024 DATA SHEET AMBIENT AIR SAMPLES (CHARCOAL TUBE ABSORPTION) 1. PI an t: Lake.Charles Refinery 2. Sample ID: LC-3Z- / 3. Sair.pl inq Date 3 /*) Elapsed Time Lot No. of lube / on Time Started "7 ^^A^ITime Ended - . fL ffoo A S 4. Atm. Press . *7 ? 5. -Are a the Sample Pvepresen'ts mmHq, Temp. l~ A go a A-TOW 2.3.o oc . 2 MO 'TfJTfA. S-ftAi/irv -rP,8i.B. 6. Name of Person Who Took the Sampl e L OAKMkM 7. Pump Calibration Data: Atmos. Press. 7 C ^ mmHq, Temp. Xi,i Pump Flow Rate $ cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .10. 11. Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph TSL Analysis Data: PPM oo09 <^5 0 DATA SHEET AMBIENT AIR SAMPLES (CHARCOAL TUBE ABSORPTION) 1. Plant: Lake,Charles Refinery 2. Sample ID: LC-3Z- / & f 3. Samplinc Date 3 // Elapsed Time N Lot No. of Tube J* 7 Time Started Time Ended 2 //OOAS no 4. Atm. Press. f 5. Area the Sample Represents mmHq, Temp. 2- ?, O j- a AATaay . x T&jrjp* 'V 1ST / L-L- A'TtOA> 'T'ASt-B 6. Name of Person Who Took the ScHDle 7. Pump Calibration Date: Atmo s. Press. ?C9 Pump Flow Rate C, Oi.S/*AA/ mm.Hq , Temp. 2./, / C. vT" cc' s/min . 8. Remarks: Include any pertir ent information such as spills, leaks sampling for lab, etc. if any, which nay be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .1011. Sampling and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide TSL Analysis Data: PPM SAL 000009026 DATA SHEET AMBIENT AIR SAMPLES (CHARCOAL TUBE ABSORPTION) 1. Plant: Lake,Charles Refinery 2. Semple ID LC-3Z- / 0 9 3. Sampling Da t== "3 /S // El apsed Time V Lot No. of Tube / 09 Time Started "7^AAlTime Ended ,2 -- Z #*0*3 ---------- 4. Atm. Press. C$ mmHq, Temp. 5. Area the Sample Pvepresents L- A 2S. * c. . / i'r_ rf=srA 6. Name of Person Who Took the Sample^ A firm ^ A GUIL-L.0A'/ 7. Pump Calibration Data: Atmos. Press. ""7 C ? mmHg, Temp. Op. Pump Flow Rate-*T O___________________cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump v/orn in dob performance .10. 11. Sampling and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide TSL Analysis Data: sal 0009 02 7 DATA SHEET A IR SAMPLES (CHARCOAL TUBE ABSORPTION) 1 . Plant: Lake.Charles Refinery .2 Sample ID: LC-3-- J / &______ 3. Sampling Pete Elapsed Time____ Lot No. of iube 9' Time Started Time Elided 2. O. % HOUAS 4. Atm. Press.________ 7 6 f nmKg, Temp._3. d? . Oc. 5. Area the Sample Represents A 8O fLJxTOj *JPfClAl- 0 c*rA/s .6 Marne of Person Who Took the Sample A'LL'fc# S & V O R0-AO Y 7. Pump Cal i brati cr. Data: Atmos. Pres s . *7 C 9 _mmHg, Temp. 3.A / c Pump Flow Rate H*> cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal ^Sampling pump v/orn in job performance 10. Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM 000009028 SAL DATA SHEET AMD I EM AIR SAMPLES (C HARCOAL TUBE ABSORPTION) 1. Plant: \ Lake,Charles Refinery 2. Sample ID: LC-3Z- //^ 3... Samp line Date 3/?/7f / /" Elapsed Time Lot.No. of Tube /O Time Started ^^^AAlTime Ended 3 <5C o tfau/is 4. Atm. Press. O? mmHg, Temp. 3 3. O C. 5. Area the Semple Represents C, H G'tWS'T' GrAS C HA.O M A 'TofL4.hr PH / - 6. Marne of Person Whc Took the Ssnpls &AAV 0ACAAS 7. Pump Calibration Data: Atncs. Press._ ^ It ^ mmHg , Temp. 3~b I C. Pump Flow Rate'S'O___________________ cc's/.amM* 8. Remarks: Induce any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .10- Sampling and analytical method: Absorption or charcoal Desorption v/ith carbon Gas chromatograph disulfide 11. TSL Analysis Data: PPM 00009029 S At 0 (conoco) Interoffice Communication to K. C. Hunt, Refining, Ponca City From J. 0. Mangelinkx,Refining, Lake Charles Da:e November 14, 1977 Sublet Sample Analyses We are sending via the company shuttle one charcoal tube for Benzene Content, a data sheet is attached. 00000^030 SM- D at;. she:? A*'E 5 =jCC-.L TJ5E ABSORPTION) 1. Plane: L2k2.C-.-r**^5 Refinery 2. Sample 15: LC-S~- / & O Lot No* of Tube_______/ 0 _______ ** Sanolino Dace if /^/~? 9 Tir.a Started 9^^.A**7ir.a E r, d e d / ^ ---------- / /--------------- *------------------- ^--------- Elapsed Time* S AStffafcS 4. Atrr. Press.______ V.sT_____________ rr.Kg, Ter.p.C_C. 5. -Area the 5a")e Represents ^ ^ A 1 &____ j- a -8 * # A-t o Av f At u/tTH GASOL/Asg______________________ __________________________________ 6. Ware of Perse" I-.'rc ?cc;: the Sample i~A V&Af____________________ 7. P ump Cal i znzizr. Seta: At-cs. Press. Pur; rlcv.* RateH *7 2. mmKc, Ter.p, 2-H-V Qg. cc's/min. 8. Remarks: Include a-y pertinent information such as spills, leaks, sa-plirc f cr lab, etc. if any, which nay be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. Sampling anc* analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPK ___ SAL 000009031 2 ; 2 ; 5a. s;o -^^4 2 5i Ps>EsL %CO 5 --o --m if IgS <_--, 1cSd *20--5n? 5 $ N> C2.-3 WZ 1g5fs5gws 2Z 2 its> w= E. 4R 5i <fi3 <?<22 o5js 3 >>3 3 3 & 3O "3O ffl 5 8 <= I<<<T=. >^x<_-% a- 2. $ cO_r _= aO<o go eO' e2o gP c2 o 8 co wos ato g& go !?1 "6 >1 fS iO 3 s 5 i M < ll 2 25 2 cjs Us aE o2 33 -"" ll 3= ? 23. Q3C.| <2 2. a5i-2 stcoo sO=i' & - p ,5 9 c2 |J !& _< O3 51 1*1. 55a s_ :*I"*s2< 5 C 2 S' a CT >< ?a sl|ciSo-:e t&a? fjS? S' c co ^ $ & 3 &-- o CEO QJ 32 i 3 "* g3 SCL =S ?.= o-- *o <0 =- 0_Q P co o22. _ CO sffi &o CL SJ co 3 saT a" w> 5 fI i> S c. 22. <c 5i ce jc I2 cl s g* cr o o 5D Scc<' co c" ac s; =: S C_ OO' 5c. 2co < ^ =--n3 S<c' p I It ismi w >n^i It3mO^i |g ? s i.s>z Ig S e co - 5<- Mu Sc - x O' I ^ lg g = c Ca 3 cc-*2o. SO cr %6 II . , cc S=. ccc<o -- x 2. E "< xo =<a = >z 9-^ X0'S-< ca 2a. -- ~ T :~ < >s ;n c<. --s <r-< 3 (aXt* * 3 33 RRS"<i V5! et 3 R1 < _ 6: K 3ffi -- -- S' 5r R 5 t* ~ ft 5 R- F ? -- R--;"--;. 7S5^^^ =. 9R5TMft R /s* r' ~~ ^ u <=- -OO3a' gI i-s Stoo< Sf 1 sS3*' "I & liuX3 T3 "I si f ICfl ;s lo' 5! 1 sw 3Q. Cl <o 1 Ifal ^ ss IHgI-Eif3 5S gl <_-> g- o ^ N3gN--o <wc0c0r cr a 5 Q<. 5 foO t3 ooc >3 ffi % 9. -O 3 9*g I co 5 o3 3Q. o2l W O3o O >< si. a 2 E 5' 33 oOCO z o--__ S3 T3 S<' *3< o3o^* Eo -oC.oO. = o< CclL | 5 oc o mo *30 23. o< ^ o^ =a t5o' Q. a 3NCD oa. 3 3o o0 a g: -s a 3o _c S. o' 3 0 2 w o ^ g M cor -oD O3Ors a3--5. <Oo' ^<Q. o5 5 oNo oc* 3 CC a* o- OD a-5a 0-- a3 -i <32ogSoS3 5toaoo--ICc.`o6OSa3_.-doIogm<Q--. QocSczColr 5qcOuc--O3o;3t--wor';' aaaoS_Sw_3--3_Ic. a53ccgas=i.'9-sS=acC--<L' 5a. O*' 2 co Ct U c S-- .x 3 < 3 o -< < = o3 ~F3< a=- Sir^. 2w oo 5 5 rA 3S -- to wo-- 2 o 3 a zs =1 oc. O o --Sc3i c!cC o _ s a^S (6 =-: cor S5 O3* <5 3 -- = <fi 3 C Cl -- Oo C3 li ^_-& 3O O 5S 5" S a_ So' 3 go 5 7 =_ o * 5 CD gS o** N tn = o3a gg OX 3N Jw ao = s ro 33 O 3 0 o 3 Cl 5- O* 2. ^ . oH'ia2 ==L O oo' g. Q. 35 oUo D_ ow2 - a 2og all S oD O*** 3o2 O so- IIS o a-- 3oc_a3< Cl a Cal. O3' g, a S3 ' 3 aoc O o<. =O S<. " O' o if*rr wo ^iS = . X 3 Q> . O CC 3 oZ Ip <0 5 g Sg a s ,w 5- ^3 S. S ZT e. 3 =* 3 2 2o 33 3O 5 o a a o 2a wj oo oc No"ia2_ gOoo '3cg*io5' S c s a S 5=- 2 a gQ. S0: 3-*< cl Q. <y 3 c. O O< m "oc a55' E! 2 0 o o |S 8.3 S g a 2o cr2. g 5 a to a ? 3 3 3 P- 3 O OO 3 a XO c3 |S s li fo 2 2 3i2 3' = *2. a 3 oOO Qt(oi.oo tczN ^ a o cg ~r ^ 3s S'i p O^. Zo o o2 2 2 O c: O 3. io; = P- S S'5 O S' a. =r p < o si -cofir f g | 2O gO C 5 2 3 | 2 2L o2 (S'- 2. S' leg ^ 5a = ag S^ i o -i s| sS CL =r 5 & oo Cl SO 39 5 3g OH* 2 > -d s5<T-2|o 5 <t> "S< a I- 3< 2. 3 f I? O' --o eZW 2 ocr 2 2-2 3a5 33 9 o' 3 oF N 3 S.g 33 Sag. -5o a 3. 3o O3_Og *og3 oa1^ oo1oCX Q. 3. Qoo. _--. O3-t- 3 _ 2 to o 2.03 cr^S' o 8B w aao 28 S' &i a '* 11 a sag. >B O * 5-i >a N co cr o^ < 3 s 3. a5' |S a. a a^ o 5a' o w 3- C CO O H| o^ CO gffi era g*o aa% s p> =5 SAL 000009032 c: 8C LZ SC ec 2E iC OC 62 82 LI 9Z S2 re tz zz 12 02 61 81 4 91 SI n El 21 LL 01 6 8 Z 9 S r E 2 l (conoco) Interoffice Communication to K. C. Hunt, Refining, Ponca City From J. J. Mangelinkx,Refining, Lake Charles Date October 3, 1977 subject Sample Analyses We are sending via the company shuttle three charcoal tubes for Benzene Content, data sheets are attached. Mangel in lb / CC: MEO, THM, FILE(2) SAL 000009034 DATA SHEET am5ie:;t air samples (charcoal tuse absorption) 1. Plant: Lake,Charles Refinery 5. `Area the Sample Represents,*S Be. A TA4 V , i- A 8# A AcyaA'f 6. Kane of Person V.'hc Took the S ar.pl e l~ BJ*r&A________& t O QL______ 7. Pump Calibration Data: Atncs . Press. "7 C mnHq, Temp . 3. S', c . Pump Flo;-.* Rate^_________H 7______ __cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .1011. Sampling and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide TSL Analysis Data: PPM SAL 000009035 DATA SHEET ak5;e:it air samples (charcoal tube absorption) 1. P'ant: Lake.Charles Refinery .2 Sample ID: LC-3Z- ? p' 3. Semolina Date f & /^. 7 *7 Elapsed Time__ 4. Atm. Press._________7^^. 2^ 5. Area the Sample Represents Lot Wo. of lube /& 7^ Time Started 7 /*T1me r, o tfooAs Ended 3y*/>A> *----- mmHq, Temp. X 2. 3 C. C $ fjJTA.UCTI6** 6. Name of Person Who Took the Sample u/AP/'AC/________ gA ft 0/K 7. Pump Calibration Data: Atmos. Press. O *f r <*> mmHg, Temp. 3. Jt c op Pump Flow Rate H Ccc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .10. 11. Sampling and analytical method* Absorption or charcoal Desorption v/ith carbon disulfide Gas chromatograph TSL Analysis Data: SAL 000009036 D A i A 5 K z z. AMBIENT AIR SAMPLES (CHARCOAL T-JSE ABSORPTION; 1. Plant: Lake,Charles Refinery .2 Sample ID: LC-3Z- ^ ?Lot No. of Tube 3. Sampling Sa te ; ^/ 7 "7 Tire Started 0 /on Tire Er.ded 3 7* J Elapsed TinefN- ^_________________ //OO A. S --t 4. At". Press.7 6. o. ________________ nr.Hg, Temp. 5. Area the Sanple Represents A4CH AJJ t CA6 2 V. * C. .6 Mare of Person V'r.c ;cok the Sarple_ A . *. tvj 7. Pump Calibration Data: Atmos. Press. ^ *f. C "r: , Ten?. 3. Jt v c Pump P1 cPateS' fc:'s/tnin. 8. Remarks: Induce any pertinent 1 r. f c rna tl on such as spills, leaks, sampling for lab, etc. if any, which ray be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .10. Sampling and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide 11. TSL Analysis Data: PPK SAL 000009037 Interoffice Communication To K. C. Hunt, Refining, Ponca City Fro'n 0. J. Mangelinkx, Refining, Lake Charles Date September 30, 1977 Subject Sample Analyses We are sending via the company shuttle three charcoal tubes for Benzene Content, data sheets are attached. CC: MEO, THM, FIUE(2) SAL 000009038 DATA SHEET AMSIgriT ATR SAMPLES (CHARCOAL TUBE ABSORPTION) 1. Pi an-.: Lake.C'.s rlas Refinery 2. Sample 10: LC-3- - <? ^ 3. Semolina Date 9 /j */-} -> / El a:- s e d Time 4. Atm. Press. 5. -Area the Sample Represents ' Lot fio, of lube / ^ *7 Ti r.e Started ") 3 -^Time Ended 3 3 PM r-* hooas ------- --- 1 oO rrur.Kq , Temp. 3-L> JO/* 6, j:=~e of Person c Took the Sample J Am 7. Pump Calibrati Atnos. Press. C ramKg, lemp. R.c- / Pump Flew RateV 7cc's/min. op. 8. Remarks: Induce any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. S-ampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPK 0009039 SAL 00 A kbie:. DATA SKEE I S A * 'r L E 5 ( C-A. PCGAL absorption' 1. .2 loz No. or lube / 6n 3d 3. Elapsed Time______________f_"_-______ //OUAS 4. At". Press. ______7 f. f rtnHg , Temp 3*. c 5- -Area the Sample represents 3 An o/z a *j Atyj t* C. 6. N a - = of Parser. c Trek the $ a m p * e Sz, 0. fZ 6 G A. t Qo 7. Pu.-p C a 1 i b " a t i c r Zizi: At":s . Press. CH. t rrmHc, Temp. 2. C. t c. Pur; :lcr RateV ^cc's/min. 8. Remarks : Include ary pertinent irformation such as spills, leaks, sampling fzr lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10- S-ampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM SAL 000009040 DATA SHE" amsi,e:;t a:3, samples fc-asccal t-jbe absorption) 1 ? ; arc: Lake.C*c**'r5 Refinery 2 -pie I u: LC-E-- ? L._________ Lot No. of lube______ f O O 3 S r.plinc D Tire S tar ted 7 3 0 Am Ii re Ended Elapsed * Hours PM\ 4 Atm. Press.7 & ft Trr.rr.Kr, isrp.J OC. 5 Area the Sample R = p r e s e r. i sP A- A _______________________________ 0 f Person Whc ; C C < til? Sanp It1 z S'/ L c, o v <-H Cal i b r a t i - - ;Cz : r, ^t. ; :s. Press 7 rrca Tens. H./ oc Pur:: Flo; " 3 w C ( cc* !s/min. frv, a .. Ire* s am? u^ 1 - am ^ -y ar-y pertinent fer lab. etc. i; r. f o TT rrati = r.y, on wh i sU:ch as c h na y spills. be cause leaks, for abno r r a 1 escape o:f hydrsca rbons into th e air. 9. Sample Procedure: Personal Sampling pump worn in Job performance 10- Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM SAL 000009041 (conoco) Interoffice Communication To K. C. Hunt, Refining, Ponca City From j# j. Mangelinkx, Refining, Lake Charles Date September 23, 1977 subject Sample Analyses We are sending via the company shuttle three charcoal tubes for Benzene Content, data sheets are attached. SAL 000009042 * r\-'< n- DATA SHEET 3 5 -1' - LES ( Cr ARC0AL TU3E ABSORPTION) 1. Plant: Lake.C'"as Refinery 2. Sample ID: LC-TI- *7 iLot No. of Tube/ C > 3. Sampling Data ^ /x n Tins Started 7 A^Time Ended 3 * ^ Elapsed T i r.e______________ ^ 0 tf>Q A J 4. Atm. Press. ^^ ".He , Tenp.Z __________________________ c. 5. -Area the Semple "epresents______r Aj/tAL * 6. N are of Person 7. Pump Calibratio: 8. Remarks: Ir. clu: s amp 1: 2 bn or: ck the Sarole H-eAT6tf : Atnos . Press. ~?(*<r.o ir^Hg, Temp, o. JT c c. Pu-r.p Flow Fate ' _______ W $C c1 S /mi n . pertinent information such as spills, leaks, r lab, etc. If any, which nay be cause for cape of hydrocarbons Into the air. 9. Sample Procedure: Personal Sampling pump v/orn in job performance 10. S-ampling and analytical method: Absorption or charcoal Desorption, with carbon disulfide Gas chromatcgraph 11. TSL Analysis Data: PPM SAL 000009043 DATA SHEET ambient air samples (charcoal tube absorption) 1. Plant: Late .Carles Refinery 2. Sample ID: LC-SZ- ^ ______ 3. S s " d 1 inq Date 9 --7 7-- El apsed Time Lot No. of lube_______ / O C_________ Time Started / AM~ime Ended 3 S''-0 //ao/>5 s3*! 4. At". Press.^ %_____ mmHg , Temp.__________ ^ ^_________ op. 5. -Area the Sample Represents3 h 3 ^ v fi 3A t/i So A. 6. Name of Person V'hc Took the Sample^_____J O H K>________ U M A \ n 7. Pump Cal i brail c r. Data: Atmos. Press. ~~7 r o mnRq , Temp. x 3- c o c_ Pump Flow RateH V____________________ cc's/min, 8. Remarks: Include any pertinent information such es spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump v/orn in job performance 10. S-amplinc and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM 0000090V* SM- DATA SHEET >:'.0 LS (CHARCO TUBE absorption:) 1 . Plant: take.Carles Refinery 2. Sanpls I v: LC-iZ- 9 3 Lot No. of Tube / & C>______ ______ ____ 3* Sampling Pats ** T i r.e Started *?'* A**Tiiae Ended 3 * p+\ Elapsed Ti me________ ^ ff&O A J 4. At". Press ."7 <- 4. ^mm'Hg, Temp. 5. Area the Sample represents~2->JJ -3. f". S ______________ 6. f'are of Person V-'nc Took the Sample ~UA i- S&M. T 7. Pump C a i i b - a t i cn Tata: Atncs. Press. Vcl o mir.Kg, Temp. 3--C- Oq Pump Flow Rate ^**2* ccrs/min. 8. Rema r k s : I r. c 1 ode ary pertinent information such as spills, leaks, sampling for lab, etc. if any, which' may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM SAL 000009045 (conoco) Interoffice Communication to K. C. Hunt, Refining, Ponca City From J, J, Mangelinkx. Refining, Lake Charles Date September 22, 1977 subject Sample Analyses We are sending via the company shuttle three charcoal tubes for Benzene Content, data sheets are attached. SAL 000009046 DATA SHEET AMBIEilT AIR SAMPLES (CHARCOAL TUBE ABSORPTION) 1 . Plant: Lake,Charles Refinery 2. Sample I D ; LC-3.1- f*' 3. Sampling Date 9 ---- 7-----7----- Elapsed Time_ 4. Pres s. 7 <rC. 5. Area the Sample Represents Lot No. of Tube______ / & (r Tine Started 4*Tirne Ended 3 /*ai //ooas mmHg, Temp.2 PLAA>AfgR 3_____________ c. 6. riara of Person Who Took the Sample *3.8. J 7. Pump Calibration Data: Atncs. Press. "? 5. V mmHg, Temp. ^3.^ Qc. Pump Flow RateS' Ccc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in Job performance .10. 11. Sampling and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide TSL Analysis Data: PPK SAL 000009047 DATA SHEET M!*! P0 *i "r.*.J 7i ;a;r SAMPLES (C-ARCCAL TiiSE ABSORPTION) 1. Plant: lake,Carles Refinery 2. Sample ID: IC-iZ- ^ 9Lot No. of Tube // /OL Jo 3. Sampling Data 5" /Z i/n 7 Tine Started 'J^4<**Time Ended *3 //-t _y----------------- ------------------------ --:----------- Elapsed Time. fT,0 Moo A 5 4. Atm. Press. cc.f r.nHg, Temp. z r. 3 c. 5. Area the Sample Represents 6. Mane of Person Whc Took the Sample A'o A. ^Q 0 _________ _____ 7. Pump Calibration Cats: Atmos. Press. 7 oS.H mmKg , Temp. 3-3.S op. Pump r 1 ov.' RateVec's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10- S-ampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM _________ SAL 000009048 DATA SHEET AMBIENT AIR SAMPLES (CHARCOAL TUBE ABSORPTION) 1. Plant: Lake.Charles Refinery 2. Sample ID: LC-3Z- 9 O______ 3. Samo1ina Da te ^ / zi/-> - // Elapsed T i me 4. Atm. Press. ~? 5. -Area the Sample Reoresents Lot No. of lube_______ ________________ _ Time Started *7 ^ *>Ti me Ended 3 * tfouAS --- ~ mmHg, Temp.________ ________ ^ 3_________Oc. C. O AS X -r & O C-T-to fiJ ?6A,m aas 6. Name of Person Who Took the Sample iasaluac QAhLf{ 7. Pump Calibration Data: Atmos. Press. V mmHg, Temp. c. Pump Flow Rate_________^^________ cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10. Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: ppm SAL 000009049 DATA SHEET AMSIEKT A1R SAMPLES (CHARCOAL TUSE ABSORPTION) 1. Plant: Lake.Charles Refinery 2. Sample I D : LC-3Z-_____ lr S** 3. Sampling Pats // Elapsed Time___ 4. Atm. Press. _____________ C ~7________ 5. -Area the Sample Represents^ Lot No. of Tube/ v ^ Time Started QJ^4*tTime Ended 3 r0 Moors nmHg, Temp.3. c. fOc. j- Asa**-t**/ , 4s>r **r_________ C-HlfF c~ tf IJ*f 6. flare of Person Who Took the Sample_______ At A// C ji 7. Pump Calibratic.' Data: Atncs. Press. *76-9 mmHq, Temp. 2-./ Qc. Pump Flow Rate\f /cc's/min. 8. Remarks: Include any pertinent i n fo rma t i on such as spills, leaks, sampling for lab, etc. if any, which-may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .10. 11. Sampling and analytical methodAbsorption or charcoal Desorption v/ith carbon Gas chromatograph disulfide TSL Analysis Data: PPM 00000905 SM- DATA SHEET AMBIENT AIR SAMPLES (CHARCOAL TUBE ABSORPTION) 1. Plant: Lake .Charles Refinery 2. Sample ID : IC-3Z- ^CLot No. of Tube / 0 C_____________________________ 3. Sampling Date Time Started "> ^Time Ended Elapsed Timejf- O ffOU A J ------ 4. Atm. Press . *7 C __________mmHg, Temp. 3. C. /__________ Qg. 5. -Area the Sample Represents-A $6 c-H-Emwt 6. Name of Person Who Took the Sample ______ At r 7. Pump Calibration Data: Atmos. Press. *> mmHq, Temp. Z C./ op. Pump Flow RateSj_cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .10. 11. Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph TSL Analysis Data: PPM SAL 000009051 DATA SHEET AMBItST AIR SAMPLES (CHARCOAL TUSE ABSORPTION) 1. Plant: Lake.Charles Refinery 2. Sample ID: LC-3d- ^"7 3. Semolina Date ^ f/ Elapsed Time Lot No. of Tube f& Time Started '>**U*iTime Ended 3 `V/*, J~ //ouAS 4. Atm. Press. 7^ 5. Area the Sample Represents mmHq , Temp. "2. 6. / l. a go a p, *ra n-f , c. 7" ei're* 6. Name of Parson *hc ieok the Sample___ /f AAA y 7. Pump Calibration Data: Atmos. Press. "7 6*^ mmHg, Temp. 2 (./ o^. Pump Flow Rate cc's/min. .8 Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which nay be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .10. 11. S-ampling and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide TSL Analysis Data: COCOON SM- A'similar procedure is followed for the backup sections, ifi P-.j the desorption efficiency from the appropriate curve for tlio amounts found <n either the sront or \:r. -.1.; 'cc 'ions. Divide the tel;-! -weight of the a!:r.e ty the cc."orp'.:^r efficiency to ob'ain the corrected mg 'Jsrr.p'.e. corrected ing sample * total weight desorption efficiency W-CUHA, j 1C:---L !-AFttV < ; i, ,' . H fiE^Ol'Tv !' fd? Add the corrected weights of the pentanes. hexanes, heptanes, and octanes present in the front and backup sec tions of the same sample tube to the tola) weight of the Mrianes in the sample <e> The Concentrations of a:*:ur..-s m f; c air rumpled can be expressed in mg cu m. mg cu in * corri-cKd mg x 1 OuO - liter cj mi air volume sample liters) bfo WEST COMPANY APPLICATION FOR VARIANCE AND INTERIM ORDER; GRANT OF INTERIM ORDER [42 FR 33316, July 1, 1977] WEST CO. Application AGENCY: Otvojj.U iconl SiTeiy m-d Health AcmmNtrrtirm. rcp.ir;:::ei.t of Labor. ACTION'S: `I- ir.-i:; e of r-pr.-Lc-K'.-'j" for tcri.-mte rod ii.ierbn -M-er; '2' G.'.'nt of G.uer. SUh'MAF.Y: :.o`U t f-r.itvtmvcs the n,-pir.." 1: /. c-1 The c-s-t Ccmpriiy for a \ i-rd o:cer ;>t'..cl:y.s; & derision .!' the upyht'fiorj fur ?. '-vri- u:i.fc from '.he ~i procu N ed :n C9 CTH ti if-.f !"ic <3.' ' - e > tcoarr.- 3::? mor.tvnt I; s.irc .-'"f u';ccf the tramline Cf an Interim order ur;i' ? cT-cNicr: Is re.-dered cr the r-.pphtaijor; for v.-rifcrce. DATiS: The erTectite cute of the in terim crc er is July 1977. The lest cate for interested peiscrj to submit umr.er.ts is Aui-ust !. :9T7. The last cate for afTv.teb employer? and employees to re quest hearing on the application is Aur-ts; i. :st;. ADDF.ZtSiS: Sene ccm-nte:u$ or re quests for a hearing to: Office of Variance Dsif.m.insf.on. Oc cupation?.! Safety {.no Health Admin istration. US. Department of Da tor. 300 Constitution A-.eivje 2C\v.. r.com N3CCE. A*;;.r.:rt*or., DC. 20310. 70?. HUr.THZ?. INTC ~ MATIC'N CON TACT: Mr. James J. Cm'.rar.: or Direvx-r Of- US. r>-p:-.rvr.cnt cf ! :-.W. O.rv.j--.- :rd H<ahh AJuv thMrritlc?*. 519 vvc?;:S HjCK -iCS. C.s-.wcn, New j,r-*y s;o:. C.S. C-pr.:* :>r.t of Labor. O'm.p.ii'.i'cral Ss-.fc;y H-aleh .AiurinStration. vll vr--.'.: ut ?t rr-; --".t'Cm ?1 r. StI06. 0. K:,::.as City, U.S. r-t*::t ol LaVr. C< r'ir.>.'Jo!;?.j S:.ft ,v r.-.i Krhth AC:r.:r.lstr;ttlon. 113 Vs; C r. CfJOi. .Wrt:-. F!:n;e. Nc-b.v.-Xa V.S Do; S'Ntv ^..c ft 3--br:. O;r-Y-uVi r.sl A(!.r.;:.`*--rr non. 13`.5 NE--Su;-i- i&T. A-;-:".a vilie. ?s. r.aj rmtue appLcMior. rur- jusr.tti* jectirr. fit! of ir.e C:-u::xl;;-n?.] Sftfeiv ;-r.d Hf.-Ut:- Ac i c-: 1&70 34 S:at. 15?6: -? U.S C. 055- urc 3? CTF. '-OOS.il for a variance, and ir.terrm crc'er r-er.d- a cccisicr. on the srpli;n::on for a variance, frem the stancard.' pre.-uribed ii: 21- cf?. if 10 237*c1 -3 -i <c mec-hani- tal g-c'-tr yrv?>es. pc-int of operation. T:*. p-fb-r-'cs c; the places of cr..p!oy- 1''c '.'O'.'.S: a he Com.;. ny. I.tc c r: c vrhed. cu reyrev.i\e. ar.d by ro'-lir.^ a t; .:y at r.11 plr-ccs h.Lie notices to in- >Toyivj a:e rorir.vily Fv-s have iNo b:c-n infc mc-d of thc-ir ri.ltt tr. p^Utivn the A;-it Secretary for a '.tr. !',n?. Kv^-.'.rcinc the i-.-i-rits of the r:r :-heq- lion. the livrr.t `ends that it is > ?. plat* cf c.'.y'.cy-.-.vtnt as i?fe ss that risyuh-od by ? 3 Sr I P.217*'c> i3; *i 'e/ vhich requires that .prNc.*;ico of b:-ih of the eperaters ?.?:.$ \o 'nr-t'-.:::e c. i-r.'.'ir.j convcls :-nd h..a:;',g su-.]i cr,t-'ci; such z s: ft:y ch:r.ce he r, L'f.vs the dj-1 r.vj.vd irate! cr s'oys ; cfere the cperr.'.or : ?n retch hf.o tpc-int of epevation viih his hares. T: '.yy::-:;.r.t sia'.es ti'.r.t it use. 0 3.1. c-x*tc pr:-=cs v.::h 1 :Zl revciu: nr. c-lutuhes. They are um-c in the r.:-.r.u*f.-i r..r.::r c-f its h.'.e of rrt 'ued rut her t ir;-; c ;rh : .-.from to CSHA. :i.v,;:r.j. T; esf c ;;.trn-ls are of a ;: c hand, s.rpie strehe. r.cr.-rfycat type. - :. :c.< 1 r.i U- i;' are reru- or the fo'.icv ir.r "rrvmr.: and Area Siferr tzit Health A ration G..*- tt.iT s-.v.-.e uiuo ?.:,-.r-.:: Stree*.. P>::ace;?i-.:i. Fa 2S104. U-S. of Labor. Occupational Safetv ar.q Health Ad=i=iacrarsoa, William J. Grteo. Jr.. Ftocrat Btilttfiag, 600 Ateh Streev Boom <J5, Fhr.adelphia. Pa. 19106. U.5. Deparistent oi Labor, Occupfttlccal Safety and Health Administration. 1515 Broadway <1 Astor P:aza)--Rooin 3445. New 1'ork. Ne* York J0036. North Ceichna 2S501. Tne V.'es; Company. Lncorporated. 5111 Ptrit Street. N.. St. Petersburg. Florida 33709. The applicant certifies that employees who would be affected by the variance have been notified of the application by giving a copy of it to their authorized cm- li'-. sc safet; births are ar. :r.icrrr.i r - 0.' tne operation c-: all of t:t - opeiv.tc-d ir. the Cc-T.tsny's plants It funner f orvards that the s:-fet:v clntar ; -DM - ra-rulatec using the formula fti.- wir.ec ir. the above referenced OSH A Peculations yields a figure of 35.3 for the presses in Question. If the vari ance sought were to be granted the re sulting distance would be reduced to Oecupoiionol Sofety & Health Reoorter SAL 000008988 We are sending via the company shuttle four charcoal tubes for Benzene, Alkanes and Toluene Content, data sheets are attached. * s> DATA SHEET a me samples (charcoal tube absorption) N v. 1. Plant: Lake, Ct arles Refinery 2. S a ro1e ID: LC-3 Z- i 3. Samoline Date 3 /v=>/-7g // Ela osed Time 4. At". Press. -7 7J. V 5. -Area the Sample R e o r e s e n t s Lot No. of lube J& Time Started r. o tfooAs mmHg, Temp. PA TA L Time Ended 0 C. 6. Tiara of Person Who Took the Sample______ /A. 7. Pump Calibration Data: Atmos. Press. mmHg, Temp. -2<3.l 0 c. Pump Flow Rate___ ___ cc's/min. 8. Remarks: I r. c 1 u i a any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal `Sampling pump worn in job performance .10. 11. S-aiTiplinc and analytical methodAbsorption or charcoal Desorption with carbon Gas chromatograph disulfide TSL Analysis Data: PPM SAL 000008989 X 2.2.^ / DATA SHEET AMS I ENT AIR SAMPLES (CHARCOAL TUBE ABSORPTION) 1. PI an u: Lake,Charles Refinery 2. Sample ID: LC-3Z- J 3Lot No. of Tube i ^ 3. Senolinq Date Tine Started 3 i Time Ended 3^7VS ---------- 7----- 7----------------- ------------------- --- ---------- Elapsed Tim e_______ " ~ S'* O - OA5 4. At". Press._________^ 3* L.mmng, Temp.2. SI C-Oq. 5. -Area the Sample Represents V P 3 A ~r74__ 6. Name of Person Who Took the Sample___ A 7. Pump Calibration Data: Atncs. Press. c rnmHg3 Temp. 3. <* o^. Pump Flow RateS' ____________________ cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sarnpling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump v/orn in job performance .10. 11. S-amplinc and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide TSL Analysis Data: PPM S4L 0oooe99o 62 rvZ DATA SHEET Ar-:S'EM ;:r S.-VPLES (CHARCOAL TUBE ABSORPTION) 1 . Plant: Lake.Carles Refinery 2. Sample l D: LC-3Z- / ^ HLot N;o. of Tube) 3. Scr.Dline Date 3 fa/-* % Time Started *7 ^ Ti me Ended 3 3</Vi Elapsed ;ime_________;-____T__'_O___- tfooAS 4. Press .________ ^73^1-mm.Hg , Temp . 5. Area the Sample Represents S A M fil- S U.O/* <S t ASK C .6 Kars of Person V'r.c ook the Sample_____ /a 7. Pump C a 1 i b r a t i c r. Data: Atncs. Press "7 C___ mmHg, Temp. ?-0'C Q(;t Pump Flow Rate H *1 __ cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure; Personal Sampling pump worn in job performance .10. 11. S-amplinc and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide TSL Analysis Data: P Pi', SAL 000008991 9 2- 1 2.1^ DATA SHEET AMD ' e :;t ;:r samples (charcoal tube ABSORPTION) 1. Plant: Lake.C':ar1es Refinery 2. Sample ID : LC-z:2_ j TlS~ 3. S a r. d 1 i n g Da ts 3 /'zi/y $ /> El a psed T i me 4. Atm. Pres s "7 7 3.x 5. Area the S amp 1s Represents Lot No. of i ube J O ^____ Tims S t a r. t e d ^ aA *1 T i me Ended 3 ~~ ^ O //OOAS mmHg, Temp /^ ^^ C c. & f\L-*uc. 6. Mane of Person V,' r. c Took the Sample A' /A 7. Pump C a 1ib r a ti or. Data: Atnos Press . nun.Hq, Temp. Oq Pump Flow Rate S/ cc's/min. 8. Rema rks: In c1 ube any pertinent information such as spills, leaks. sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: ?ers onal *Sampl i ng pump worn in job performance .10. 11. S-ampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph TSL Analysis Data: PPM SAL 000008992 6) DATA SHEET AMBIENT .-.".a SAMPLES (CHARCOAL TUBE ABSORPTION) 1. Plant: Lake ,C'*-rl-s Refinery 2. Sample ID: LC-3I- 1 3. Sampling D is 3 /z>/? i // Elapsed Time 4. Atm. Pre ss. -7 7 3.x 5. Area the Sample Represents Lot No. of lube 7 t> n Time Started ~D ^ ^ T i me Ended 3 rc o tfooAS mmHg, Temp, z^ ^ C. J s"~ S'AAA Vo. 6. Name of Person V.'hc Took the Sample N /A 7. Pump Cali bra tic n uata : Atmos. Press. ">'7-2^6- mmHq, Temp. Pump Flov/ Rate S' / cc's/min. 8. Remarks: In c 1 u :e any pertinent information such as spills, leaks. sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9- Sample Procedure: Personal Sampling pump worn in job performance .10. Sampling and analytical methodAbsorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM A SAL 000008993 -i 3 o t /3 r\ 0 A A SHEET "TIES (C-APCO-t TUBE ABSORPTION) ]. Plant: Lake.C'* = f"les Refinery 2. Sample : p: LC-EI- } ^ HLet No. of Tube J _________ 3. s = -?lir. r Date J /=>/l% Tir.e Started *? 3 <" n me Ended 3 3a/Af Eh:s = : Tiref' & tfOUAS 4. Atm. Press._______ T T 3 , V,______ nHc, Temp.zl S. ^_______________________ 5. -Area tn e Sample Tepee sents________ A A Ai l--.of*vf / /VX OQt i; a i. 2 o i k t'ns S /a 7 . P u n p C a 1 ' : r a t i c t Z a t a : Atrcs. Press. mmHq, tenp. 'XQ-C o^^ Pur.: 'lOr.' PateH *7cc's/min. 8. Remarks: 20 pertinent 1 r.formation such as spills, leaks, lab, etc. if any, which may he cause for ape of hydrocarbons into the air. 9 Sample Procedure: Personal Sampling pump worn in job performance 10. S-amplinc and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11 TSL Analysis Data: PP, w5 -C <' ?. -A v/ ^ O'c^- * f?'" SAL 000008994- DATA SHEET T AIR SAMPLES fC - AR CG-.L Tu'SE ABSORPTION) Lake.Charles Refinery bar: .2 LC-3Z- / 2- 3 Lot of lube J on Sardine Date 3 /i v? t 7 7---------- Tire Started ^ ^4 ri Time Ended 3 ^ 7V*i Elapsed Tire__________ tr.o #6oas Atm. ? r e s $ ._________ ^ V,mm H g , Temp. 2>r, c c. Area the Sample Represents A VP B A Ttf are or arson co e Sample. S'/A 7. Pump Ca 1* bra tier. Tate: Atrcs. Press. 7Z, c nimHq , Temp. ^ C- Oq ^ Pur; PI ow Pate,___________ ^ ________ cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal 'Sampling pump v/orn in job performance .10- S-amplinc and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide *v; avt:e:.t DATA SHEET samples (charcoal ttse absorption 1. P'icn;: Lake.C-.iNes Refinery 2. Sample I j ; LC-ET- i 2. K _______ Lot' No. of Tube J & *7 3. S a rr: 3 1 t r. c Data O -f- y-- EU:=e: Tine Tine Started ^ a/i Tine Ended --- --- :--------- O //OQAS 4. Atm. Press. "7 ~? 3. "2^. nn H g , T e n p . 2. JZ C* oq 5. -Area the Sample represents______ P A ~7~ A 13 L 6. flare of Person N't .to1; the Sample______M /A________________________ 7. Pump Calibration Tata: Atnos. Press. "? 7A. <- rararc , Temp. Z> o. C op. P j r p Flow Fats_______ V ^c c * s /m i n . 8. Remarks : I r. c 1 - T s ary pertinent information such as spills, leaks, sampling ~zr lab, etc. if any, which nay be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .1011. S-arapling and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide TSL Analysis Data: PPM 6^^^ A or /a i ? rr-- SAL 000008996 / l # V~- DATA SHEET IR SAMPLES (CHARCOAL TUBE ABSORPTION) 1. Plant : Lake.Charles Refinery 2. S a-p 1 e I D: LC-3I- /A I 3. Sar.o line Date 3 /**/->$ // Elapsed Time 4. Atm. Pre S3. 7C.V Lot No. of Tube / on Time Started A* Time Ended - -?.r /souas mmKq, Temp. L'l-.t. Oc. 5. -Are a the Samp!e Represents X r&S'T^A. S AAv 1-r-/ -T A G i- , 6. ?! a me of Person Who Took the Sample ^^A^AAO 8 c>u/ic 6i j 7. P unp Cal i bra tiers Data: Atmos. Press. 30 mmHq, Temp. 3-6.0 op. Pump rlov.' Rate ^ *"7 cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .10. S*ampling and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide 11. TSL Analysis Data: PPM SAL OOOOO8997 V DATA SHEET ame:e;;t ;:p samples (charcoal tuse absorption) 1. Plar, Lake.Charie5 Refinery 2. S a r p le I : LC-3I- U. O 3: Samp 11 n 5 3 /*&/?$ --7----- 7 Elapsed ;ime_ 4. Atm. Pre *7 Ct H 5. -Are a the Lot No. of lube J6 Tine Started 9 ^.4*1 Ti me Ended 3**0eJ*f** 7- <T //&OA5 2.x, Z. c. , UAge/iA'raA'i 6. "Jarre 0 f Person tlho :oofc the Sample ______J ^ 7. Pump Cal Pump FI ov.' P>ate Ht c c' s / m i n . 8. Rera rks : W M. ` W v t M W y V. V \# I WHJ ) Ml) I Vll Wv abnormal escape of hydrocarbons into the air 9. Sample Procedure: Personal Sampling pump worn in job performance 10- Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM O. ? fp- $4(. 0000*99a A`*E 'ENT ;:r samples (c HAP.COAL TUBE absopptio;*; \ / 1. 2. Sarcle 13: LC-EI- / / n Se.Tslir.o Dste 3. 3 />s/~> f // classed Time 4. Atm. Press. 7tV 5. Area the Sample Represents Lot No. of Tube / on Time Start ed *) I#am Time Ended 3*" # #*, 1 So Hours mrnHo, Temp Or L C ft 6 OMi 2- 2.. *2^ C. 6 f;am = of Parser. 7 Pun? C a 1 ' b r a t i the Sample */a_____ = . Press. 3 mnKg, Temp. 0 c Pump Flow RateS o cc1 s/min . 8 Remarks: Ir. c`; any pertinent information such as spills, leaks, . in.V r for lab, etc. if any, which may be cause for 1 escape of hydrocarbons into the air. 9. Sample Procedyr Personal Sampling pump worn in job performance .10. Sampling and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide 11 TSL Analysis Data: P??i CL-"*.' d, / A />/> SAL 000008999 9 DATA SHEET ancient air samples (charcoal tube absorption) 1. Plant: Lake,Charles Refinery 2. Sample ID: LC-3!- 9 f S' x Lot No. of lube J6 1 3. Samolir. c Date ---------- 7 7~ Elapsed Time Time Started -- - r~e- //auAS Ended 4. At-. Prass. 7 t, H 5. -Area the Sample Represents AJl&A mmKg, Temp K X> >-K R. p> *-*--*. , CA c. 6. Mare of Person *r.o Took the Sample 7. Pump Calibration Data: Atnos. Press. y 13 mmHg, Temp. 2o.o Pump Flov/ Rate f cc's/min. 8. Remarks: Include any pertin ent information such as spills, leaks, sampling tot lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .10. Sampling and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide 11. TSL Analysis Data: PPM p DATA SHEET a:r samples (charcoal tube absorption-) X 1. Plane: Lake.Chari as Refinery *V 2. Sample ID: LC-zZ- f f Samolina Date 3. 3/ // Elapsed Time Lot No. of Tube /O? Tima Started ? " r. o //co/>5 Ti me Ended 3r 4. At-. Press . "7 4 V 5. Area the Sample Represents mm.Hg, Temp. 3. M 2-t. ^ vf A M fit. c. 10 * -w/i 6- Mane of Person "he Took the S ample 7. Pump Calibraticn Data: Atmos . Pr a s s . Pump Flow Pvate CZ mmHg , Temo. 2 r. S' / cc?s/min. 8. Remarks: Induce any pertinent Information such as spills, leaks, sampling for lab, etc. If any, which may be cause for abnormal escape of hydrocarbons Into the air. 9. Sample Procedure: Personal Sampling pump worn In job performance .10. 11. Sampling and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide TSL Analysis Data: SAL 000009001 fw ams:e:;t DATA SHEET samples (charcoal tube absorption) 1. Plant: Lake. Che rles Refinery 2. Samole ID: LC-B' - J / ^ 3: Ssme 1 i rq Da te 3 /'*/?? // El ap sed Time 4. Atm. P r e s s. V 5. -A rea the Sample Represents Lot fio. of Tube S O *7 Time Started 9 ^**4 A* Time Ended p/* ~:r //0t>AS mm Hg, Temp. 2.^7. X C- M N ocK Roe** , cl c O TAfi.fi Name of ^^ r ^^ y ^; * i#* ho Took the Sample^ A/A 7, P unp C a 1 icr. Data: Atncs. Press. 7 C ( cur.Hg, Temp .3.^-0 Pump Flow Rate^ cc's/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 10- Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11- TSL Analysis Data: PPK 0,3 7 pf^ SAL 000009002 DATA SHEET amp:e;;t ;.:r samples (charcoal tube absorption) 1. Plant : Lake.Charles Refinery 2. Sampl e ID: L C - B l - f 3. Samp lino Data 3/<*H/ // Elapsed Time Lot ?io. of i ube /6<7 Tine Start ed Time Ended 3^ r, //oo/iS 4. Atm. Press . ~7 mmKq, Temp 10.2^ c. 5. Area the Sample Represents AA B *TA 6. iN a me of Person Ur.o Took the Sample 7. Pump Cal i brati cr. Data : Atmos. Press. Pump Flov/ Rate sS 0AJT "/a *7 C r mmKg, Temp. V cc's/min. 8. Remar ks : Include any pertinent information such as spills, leaks , sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal*Sampling pump worn in Job performance .10- Sampling and analytical method: Absorption or charcoal Desorption v/ith carbon Gas chromatograph disulfide 71- T5L Analysis Data; PPM JL*^~ <9, ^-0 -h If SAL 000009003 2> ; tib70U n* . DA ^S A '*? Li S (C~` -L TUBE ABSORPTION) 1. Plant: lake. C *.a'*'e s As finery 2. Sample ID: LC-SZ- //W _______Lot No. of Tube________i 6 *7 3: Samolinc Date 3 ?? Tims Started Time Ended 3* PM --:---------- Elapsed Tine________ -- #>OA$ 4. Atm. Press.__________________ 7(, V r.r.K g , Temp._______ 2-7. ^ ______ OC. 5. -Area the Sample Pep resents ^ ^ trfJ'fAS ALAMC liars or era or. 7. Pump Cali brati cr. 8 Rer s the Ssnole /VA : Atmos. Press. f ram Kg, Temp. 3.^* & c Pure -low ".ate^ / cc's/min. pertinent information such as spills, leaks, r lab, etc. if any, which may be cause for cape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .10. 11. 5-amp! inc and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide T5L Analysis Data: PPM SAL 000009004 O' DATA SHEET AMD I ENT AIR SAMPLES ( CHARCOAL TUB E ABSORPTION) 1. Plant: Lake.;Charles Refinery 2. Samo T e ID: LC -EZ- <" ^ 3. Samolinc Date 3 /iv/7f s/ El apsed Time X Lot No. of lube y ^ ry ' Time Started 7 A* Time Ended ^ /** tfdOAS --- 4. Atm. Press. 7<rH mjiiHq, Temp. 4. 7. o^_ 5. Area the Sanpi e Represents vapoa r p. -ss u a bath 6. Name of Person Who Took the Sample /A 7. Pump Cal ibrsticn Data: Atmos. Press. Q t mmKq, Temo. Z o. o o r Pump Flow Rate ^ cc's/min- 8. Rems r.ks : Inciu-e any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .10. 11. Sampling and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide TSL Analysis Data: PPM -JL. <?i. 3 G pfTM -Aj. c^c- r SAL 000009005 DATA SHEET AMSIE.'iT SAMPLES (ch ARCGAL TUBE ABSORPTION) 1. Plan t: Lake.C'* = r]es Refinery 2. S arp 7 e ID: LC-Rd- ! t 3 3: Sanolino Date ^ // Elapsed Time 4. Atm. Press. 5. Area the Sample Represents s\ Lot : i 0. Of Tube ' n Tine 5tarted Time Ended 3^* AAf T.o //auAS --. mmHq, Temp i-*- z. C. PA TA 6. M are of Person Who Took the 5 ample */a 7. Punp Calibration Data: Atnos . Pres s. *7 ( Pun p Flow Rate mrnHq, Temp, o r. V? cc's/min. 8. Re n a rks: Include any pertine r. t information such as spills, leaks > abnormal escape of hydrocarbons into the air 9. Sample Procedure: Personal Sampling pump worn in job performance ,10. 11. S-ampling and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide iSL Analysis Data: PPM (conoco) Interoffice Communication to K. C. Hunt, Refining, Ponca City From 0. 0. Mangelinkx, Refining, Lake Charles Date March 15, 1973 Subject Sample Analyses We are sending via the company shuttle five charcoal tubes for Benzene Content, data sheets are attached. These samples were taken to gather Laboratory Air Circulation Data. DATA SHEET AMD IE:; 7 AIR SAMPLES (CHARCOAL TUBE ABSORPTION) 1. Plant: Lake,Charles Refinery 2. Sample ID: LC-3Z- J 3.' Samolina Date 3 / / Jf // Elapsed Time Lot No. of Tube S Time Started "?^*AAlTime Ended xhSpm tfooAS - - --. 4. Atm. Press . *7 C- $ 5. Area the Sample Represents mmHq, Temp. u a 5#AT<5y 2.3.0 C. . 5 MO -r&srfA -*.Avi-ry -rp,$t.. 6. Name of Person V/ho Took the Sample ^A^L O /\ H. Af A A/ 7. Pump Calibration Data: Atmos. Press.__2AJ?. _jnmHg, Temp._ op. Pump Flow Rate__________ *4 $_______ cc's/mln. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump v/orn in job performance .10. 11. Sampling and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide TSL Analysis Data: PPM bv ' ;-4-^W' -- / SAL 000009008 DATA SHEET AMS I EM AIR SAMPLES (C-A.RCOA.L TUBE ABSORPTION) 1. Plant: Lake.Charlas Refinery 2. Sample Iu: LC-5Z- t & $Lot No. of Tube __________________________ 3^ Sampling Data 3 /7f yy Time Started "^^AXTime Ended 2**>/k . ------------------------. Elapsed Time____ HouAS 4. Atm. Press. ^f 5. -Area the Sample Represents rmHq, Temp. *3. 3, 0 /- A &0 Q.firT0A't . z pc TAJ>rjex c. V 1ST / C-LA'T/ofJ T-*BLE 6. Mare of Person V.'hc Took the Sample //M/V C. AA/ 7. Pump Calibration Data: Atmos. Press. 7(5 Pur.p Flow Rate imr.Hg, Temp. / C vT *i ccr s/min _ 8. Rema rks: Indues any pertinent information such as spills, leaks > sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .10. 11. S-ampling and analytical method Absorption or charcoal Desorption with carbon disulfide Gas chromatograph TSL Analysis Data: PP /. A. a*6 <? <f SAL 000009009 DATA SHEET ams:e;;t air samples (charcoal tube absorption) 1. Plant: Lake.Charles Refinery s.NN.. 2. Samole ID: LC-3Z- Lot No. of Tube / O9 3. Sampling Date *3 /'J // Elapsed Time Time Started "?tf^AAlTime Ended 2. - -------- 4. mmHq, Temp. "2 3. c. 5. Area the Sample Represents 2- A'BofLPrrofi'i. / ^ TfJTZA. 6. i'iara of Person V.'ho Took the Sample^ A ATH v A Go i ul.o/1y 7. Pump Calibration Data: Atmos. Press._ mg*? __mrnHg, Temp. op Pump Flow Rate___ SQ ___ cc's/rain. 8. Remarks': Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .10- Sampling and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide 11. TSL Analysis Data: PPK r, s_Z-^} ^ c ' /. A. ^ a. ?-/yi 000009010 SAL J DATA SHEET ? S A " ? L E S (CHARCOAL TUSE ABSORPTION;) Plant: Lake,Charles Refinery Sample I D : LC-S3- f f 0Lot No. of Tube I C~? Sampling gate 3 Time Started 7^g^HTime Ended 2. Elapsed Tine____ r?. % tfQOAS Atm. Press. 7C7 mmKg, Temp. 3.3.0 Area the Sample Represents^ Z- A 1?0 R.frTQfl'f j JP^ciaL C. & c-rAxsfL N a rr e of Person V.'r.c Took the Semple A'Ll'&P 8 & U D fij^AU X______ Pump Calibration Tate: Atmos. Press. "7 9 mrcHg 3 Temp. 2.A / op. Pump Flow Rate*j f cc*s/min . Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in Job performance .10. 11. Sampling and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide TSL Analysis Data: PPM (S>. 5- S', SAL 000009011 DATA SHEET ANCIENT AIR SAMPLES (CHARCOAL TUBE ABSORPTION? N, 'S. 1. Plant: Lake .Charles Refinery 2 Samp 1e ID: LC-3Z- Iff Lot No. of Tube /& 3. Sampling Date 3/l/~?t _Time Started "? ^ ^AiTime Ended 3 ^ Elapsed Time ~ fr O' #60 AS t 4 Atm. Press. OP mmHg, Temp. 2 3. D C. 5 Area the Sample Represents G-AJ c HA.OM MT0&A.UAHY (2 H__________________ 6 Name of Person Vi he Took the Sample &AAV 0ACA/V 7 Pump Calibration Data: Atncs. Press. *7 (, ? mmHq , Temp. iM__ c. Pump Flov: Rate_________ JTO cc Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance 70. Sampling and analytical method-* Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM y lax*^l t a--(J '' SAL 000009012 0 a>;e:e:;t DATA SHEET samples (charcoal tuse absorption) ]. Plant: \ Lake.Ctarles Refinery 2. Sarple ID; LC-3Z- J i ________Lot No. of Tube J O ~) 3. Sar.olino Date 3 ^y Elapsed Time Time Started & //0OA5 Time Ended 3^ ; 4. Atm, Press."7 C H mmH g , Temp. __________________________ C. 5. -Area the Sample Represents________ Gr L C________R 6 o/A______ Pat - .6 Mare of Person Who Took the Sample_____ s'/a 7. Pump Cali brati n Data: Atmos. Press.__ n cj Pump Flow Rate mmKg, Temp. a op. S' o cc1s/min. 8. Remarks: Include any pertinent information such as spills, leaks, sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal `Sampling pump worn in job performance .10. 11. Sampling and analytical method: Absorption or charcoal Desorption v/ith carbon disulfide Gas chromatograph TSL Analysis Data: PPM SAL 000009013 DATA SHEET amb:e:;t a: =. SAMPLES fC HARCOAL TUBE ABSORPTIO iil v\ 1. Plant: Lake.Cte rles Refinery 2. Sample ID: LC-E- -nr Lot ?i0 . of Tube 3, Semolina Date 3 /s/>% 7/ El ap set Time Tine Started "?^^^Time Ended 3 T- 0 tfOUAS 4. Atm. Press. 7CV mmHq, Temp 5. Area the Sample Represents M A/ec-H g L f Wj V & AJL&A 6. Name of Person * r.z Took the Sample /4 7. Pump Cal i brati or Data: Atmos. Press. 7t 3 Pump Flow Rate 2-1--V C. mrr.Kq, Temp. 2-o.o c ^ t cc's/min. 8. Remarks: Irclui = any Per tin ent information such as spills, leaks > sampli 5 for lab, etc. if any, which may be cause for a b n o r r a 1 as cepe of hydrocarbons into the air. 9. Sample Procedure: Personal `Sampling pump worn in job performance .10. 11. Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph T5L Analysis Data: PPM 00000901* sM- 9I DATA 5KEET ame:s:;t a:r samples (charcoal tube absorption) N. 1. Plant: Lake.Charles Refinery 2. Sample I u : LC-5Z- ! t 5 ______ j_ot No. of TubeJ _______________________ _ 3. Samolino Date // 3/'S/Of 77 Tine Started ^ A Time Ended 3 Pm 7--------- Elapsed Time________ -- S'- 6 //OOAS 4. Atm. Press . 7 4V 5. Area the Sample Represents *> IJ P*SAL * A>K mmHcj, Temp. 7" 'T'jT0tLS SA C. 6. Mane of Person ho Took the Sample 7, Pump Cal i brati cr. Data: Atmos. Press. 7 C 3 mmHg , Temp. o.o C Pump Flow Rate t cc's/min. a. Remarks: In cluc s any pertin ent information such as spills, leaks > sampling for lab, etc. if any, which may be cause for abnor-al escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn In job performance 10. Sampling and analytical method: Absorption or charcoal Desorption with carbon disulfide Gas chromatograph 11. TSL Analysis Data: PPM SAL 000009015 (g) 6 9 of31 DATA SHEET AKSIE.'.'T .-:T SAMPLES (CHARCOAL TUBE ABSORPTION) 1. P i a n z : Lake,Charles Re finery 2. Sample I D: LC-3I- /i 0 3: S amoline Date 3 /*/> f r/ Elapsed Ti me 4. Atm. P r e ss. ?< H 5. Area the Sample Represents Lot No. of lube )6 Time Started ~)^0AH Time Ended tfooAS mmHq, Temp. 2-K Z- C. * r'r T&ST&A , j-a$0Aa~toa y 6. 'Jams of Person Who Too k the Sample HA AAV J ** 7. Pump Calibration Data: Atmos. Press. C 3 mmH g, Temp. C. Pump FIow Rate t cc's/min. 8. Rena rfcs: Include any pertinent information such as spills, leaks > sampling for lab, etc. if any, which may be cause for abnormal escape of hydrocarbons into the air. 9. Sample Procedure: Personal Sampling pump worn in job performance .10. 11. S-ampling and analytical method: Absorption or charcoal Desorption with carbon Gas chromatograph disulfide TSL Analysis Data: PPM 000009016 sM-